FI19991985A - Chromatographic fractionation of plant material - Google Patents

Chromatographic fractionation of plant material

Info

Publication number
FI19991985A
FI19991985A FI991985A FI19991985A FI19991985A FI 19991985 A FI19991985 A FI 19991985A FI 991985 A FI991985 A FI 991985A FI 19991985 A FI19991985 A FI 19991985A FI 19991985 A FI19991985 A FI 19991985A
Authority
FI
Finland
Prior art keywords
pectin
chromatographic fractionation
fraction
plant material
sugar
Prior art date
Application number
FI991985A
Other languages
Finnish (fi)
Swedish (sv)
Other versions
FI113453B (en
Inventor
Tapio Juhani Antila
Timo Vaekevaeinen
Irma Christina Lindqvist
Hannu Koivikko
Matti Tylli
Juho Jumppanen
Original Assignee
Sohkar Oy
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FI991985A priority Critical patent/FI113453B/en
Application filed by Sohkar Oy filed Critical Sohkar Oy
Priority to CZ2002948A priority patent/CZ295865B6/en
Priority to CA002385109A priority patent/CA2385109C/en
Priority to HU0202872A priority patent/HUP0202872A3/en
Priority to CZ2002799A priority patent/CZ295265B6/en
Priority to AU72910/00A priority patent/AU7291000A/en
Priority to HU0203963A priority patent/HUP0203963A3/en
Priority to PL356680A priority patent/PL196962B1/en
Priority to AT00960708T priority patent/ATE448848T1/en
Priority to EP00960709A priority patent/EP1227866A1/en
Priority to JP2001524693A priority patent/JP2003509576A/en
Priority to EP00960708A priority patent/EP1218079B8/en
Priority to AU72909/00A priority patent/AU7290900A/en
Priority to PCT/FI2000/000780 priority patent/WO2001021272A1/en
Priority to JP2001524692A priority patent/JP2003509575A/en
Priority to DE60043347T priority patent/DE60043347D1/en
Priority to CA002384874A priority patent/CA2384874C/en
Priority to PCT/FI2000/000779 priority patent/WO2001021271A1/en
Priority to PL353991A priority patent/PL196961B1/en
Publication of FI19991985A publication Critical patent/FI19991985A/en
Priority to US10/091,892 priority patent/US6663717B2/en
Priority to US10/091,891 priority patent/US6660099B2/en
Publication of FI113453B publication Critical patent/FI113453B/en
Application granted granted Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
    • C08B37/0006—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid
    • C08B37/0045—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid alpha-D-Galacturonans, e.g. methyl ester of (alpha-1,4)-linked D-galacturonic acid units, i.e. pectin, or hydrolysis product of methyl ester of alpha-1,4-linked D-galacturonic acid units, i.e. pectinic acid; Derivatives thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction
    • B01D15/361—Ion-exchange
    • B01D15/362—Cation-exchange
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
    • C08B37/0003—General processes for their isolation or fractionation, e.g. purification or extraction from biomass

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Sustainable Development (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Jellies, Jams, And Syrups (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Saccharide Compounds (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Abstract

The invention relates to chromatographic fractionation of pectin-containing vegetable material, such as sugar beet pulp. In the method of the invention, a pectin-containing hydrolysate is chromatographically separated into a pectin fraction, a salt fraction and a sugar fraction. The method is carried out by using a cation exchange resin, which is preferably in the form of a multivalent metal.
FI991985A 1999-09-17 1999-09-17 Chromatographic fractionation of plant material FI113453B (en)

Priority Applications (21)

Application Number Priority Date Filing Date Title
FI991985A FI113453B (en) 1999-09-17 1999-09-17 Chromatographic fractionation of plant material
PCT/FI2000/000779 WO2001021271A1 (en) 1999-09-17 2000-09-15 Chromatographic fractionation of vegetable material
EP00960708A EP1218079B8 (en) 1999-09-17 2000-09-15 Recovery of pectin by cation exchange chromatography of a vegetable material
CZ2002799A CZ295265B6 (en) 1999-09-17 2000-09-15 Chromatographic fractionation of vegetable material
AU72910/00A AU7291000A (en) 1999-09-17 2000-09-15 Process for the fractionation of sugar beet pulp
HU0203963A HUP0203963A3 (en) 1999-09-17 2000-09-15 Process for the fractionation of sugar beet pulp
PL356680A PL196962B1 (en) 1999-09-17 2000-09-15 Chromatographic fractionation of vegetable material
AT00960708T ATE448848T1 (en) 1999-09-17 2000-09-15 CHROMATOGRAPHIC FRACTIONATION OF VEGETAIVE MATERIAL
EP00960709A EP1227866A1 (en) 1999-09-17 2000-09-15 Process for the fractionation of sugar beet pulp
PCT/FI2000/000780 WO2001021272A1 (en) 1999-09-17 2000-09-15 Process for the fractionation of sugar beet pulp
CZ2002948A CZ295865B6 (en) 1999-09-17 2000-09-15 Method of simultaneous purification and separation of pectin and pectic sugars or oligomers from sugar beet pulp
HU0202872A HUP0202872A3 (en) 1999-09-17 2000-09-15 Chomatographic fractionation of vegetable material
JP2001524693A JP2003509576A (en) 1999-09-17 2000-09-15 Fractionation method of sugar beet pulp
JP2001524692A JP2003509575A (en) 1999-09-17 2000-09-15 Chromatographic fractionation of plant material
DE60043347T DE60043347D1 (en) 1999-09-17 2000-09-15 CHROMATOGRAPHIC FRACTIONATION OF VEGETATIVE MATERIAL
CA002384874A CA2384874C (en) 1999-09-17 2000-09-15 Process for the fractionation of sugar beet pulp
CA002385109A CA2385109C (en) 1999-09-17 2000-09-15 Chromatographic fractionation of vegetable material
PL353991A PL196961B1 (en) 1999-09-17 2000-09-15 Process for the fractionation of sugar beet pulp
AU72909/00A AU7290900A (en) 1999-09-17 2000-09-15 Chromatographic fractionation of vegetable material
US10/091,892 US6663717B2 (en) 1999-09-17 2002-03-06 Process for the fractionation of sugar beet pulp
US10/091,891 US6660099B2 (en) 1999-09-17 2002-03-06 Chromatographic fractionation of vegetable material

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FI991985 1999-09-17
FI991985A FI113453B (en) 1999-09-17 1999-09-17 Chromatographic fractionation of plant material

Publications (2)

Publication Number Publication Date
FI19991985A true FI19991985A (en) 2001-03-17
FI113453B FI113453B (en) 2004-04-30

Family

ID=8555306

Family Applications (1)

Application Number Title Priority Date Filing Date
FI991985A FI113453B (en) 1999-09-17 1999-09-17 Chromatographic fractionation of plant material

Country Status (12)

Country Link
US (2) US6660099B2 (en)
EP (2) EP1227866A1 (en)
JP (2) JP2003509576A (en)
AT (1) ATE448848T1 (en)
AU (2) AU7291000A (en)
CA (2) CA2384874C (en)
CZ (2) CZ295265B6 (en)
DE (1) DE60043347D1 (en)
FI (1) FI113453B (en)
HU (2) HUP0202872A3 (en)
PL (2) PL196961B1 (en)
WO (2) WO2001021272A1 (en)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FI113453B (en) * 1999-09-17 2004-04-30 Sohkar Oy Chromatographic fractionation of plant material
US7037378B2 (en) * 2003-09-24 2006-05-02 Danisco Sweetners Oy Separation of sugars
US20050096464A1 (en) 2003-10-30 2005-05-05 Heikki Heikkila Separation process
GB2407573A (en) * 2003-10-30 2005-05-04 Danisco Sweeteners Oy Production of arabinose
EP1765874A1 (en) 2004-03-26 2007-03-28 Glycogenesys, Inc. Modified pectins, compositions and methods related thereto
JP5112859B2 (en) 2004-06-04 2013-01-09 ホリズン サイエンス ピーティーワイ リミテッド Natural sweetener
EP1714562A1 (en) * 2005-04-22 2006-10-25 N.V. Nutricia Process for drying uronic acid oligosaccharides
CA2608865C (en) * 2005-06-03 2015-08-25 Horizon Science Pty Ltd Molasses extract having body mass redistribution properties
CN101325884A (en) * 2005-12-09 2008-12-17 丹尼斯科糖业有限公司 Stabilised emulsion
WO2007066234A2 (en) * 2005-12-09 2007-06-14 Danisco Sugar A/S Beverage emulsion
EP2064352B1 (en) * 2006-09-19 2019-12-04 The Product Makers (Australia) Pty Ltd Extracts derived from sugar cane and a process for their manufacture
FR2916447B1 (en) * 2007-05-25 2012-09-21 Univ Picardie PROCESS FOR THE PRODUCTION AND USE OF OLIGOMERIC FAMILIES OF GALACTURONIC ACID
RU2541037C2 (en) * 2009-08-11 2015-02-10 ЭфПиИННОВЕЙШНЗ Fractionation of waste liquid stream from nanocrystalline cellulose production
EP2672832B1 (en) 2011-02-08 2020-03-25 The Product Makers (Australia) Pty Ltd Sugar extracts
WO2013063251A1 (en) * 2011-10-26 2013-05-02 Frito-Lay North America, Inc. Sustainable conversion of citrus peel waste
EP3569298B1 (en) 2012-08-28 2021-08-11 The Product Makers (Australia) Pty Ltd Sugar cane derived extract
AU2014306366B9 (en) 2013-08-16 2020-03-26 Poly Gain Pte Ltd Sugar cane derived extracts and methods of treatment
EP3152334A4 (en) 2014-06-03 2018-02-28 Putsch&Company, Inc. Process for producing pulp from sugar beets
CN104744525B (en) * 2015-03-24 2017-03-01 浙江大学 A kind of technique that preparation high-purity L arabinose is extracted for raw material with arabic gum
EP3356563B1 (en) * 2015-10-02 2019-08-28 Coöperatie Koninklijke Cosun U.A. Methods of enriching arabinose fractions

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS50148399A (en) * 1974-05-17 1975-11-27
JPS5611903A (en) * 1979-06-11 1981-02-05 Chisso Corp Preparation of powdery pectin
US5008254A (en) 1982-09-03 1991-04-16 Weibel Michael K Sugar beet pectins and their use in comestibles
SE453511B (en) * 1986-06-10 1988-02-08 Nils Monten Pectin-type consistency indicator prodn.
DE3702653A1 (en) * 1987-01-29 1988-08-11 Sueddeutsche Zucker Ag METHOD FOR PRODUCING CRYSTALLINE L-ARABINOSE
EP0446291B1 (en) 1988-12-05 1995-08-02 British Sugar Plc Debranched araban and its use as a fat substitute
JPH03149201A (en) * 1989-11-02 1991-06-25 Atsushi Imai Production of pectin
US5952308A (en) 1991-07-29 1999-09-14 Pola Chemical Industries Inc. Mineral absorption promoting agent
DE69325189T2 (en) 1992-01-20 1999-11-25 Japan Tobacco Inc New pectinase
BE1006377A3 (en) * 1992-11-24 1994-08-09 Raffinerie Tirlemontoise Sa SEPARATION METHOD OF polydispersed composition SACCHARIDES, PRODUCTS OBTAINED BY THE METHOD AND USE OF PRODUCTS OBTAINED IN FOOD COMPOSITIONS.
US5472952A (en) 1993-03-18 1995-12-05 Bristol-Myers Squibb Company Partially hydrolyzed pectin in nutritional compositions
DE4313549C1 (en) * 1993-04-26 1994-10-13 Herbstreith & Fox Kg Pektin Fa Process for obtaining pectin extract from sugar beet and the use thereof
FI104500B (en) * 1997-08-26 2000-02-15 Cultor Oyj Process for preparing L-arabinose from sugar beet cut
FI105691B (en) * 1997-08-26 2000-09-29 Sohkar Oy Raw material useful in the preparation of pectin and related compounds, and process for its preparation
KR100252194B1 (en) * 1997-10-10 2000-04-15 박호군 Novel pectin type polysaccharide from Angelica gigas Nakai, purification process thereof
FI113453B (en) * 1999-09-17 2004-04-30 Sohkar Oy Chromatographic fractionation of plant material

Also Published As

Publication number Publication date
DE60043347D1 (en) 2009-12-31
AU7291000A (en) 2001-04-24
ATE448848T1 (en) 2009-12-15
AU7290900A (en) 2001-04-24
PL353991A1 (en) 2003-12-15
WO2001021271A1 (en) 2001-03-29
US20020189606A1 (en) 2002-12-19
HUP0202872A3 (en) 2004-03-01
HUP0203963A2 (en) 2003-04-28
CA2384874A1 (en) 2001-03-29
US6660099B2 (en) 2003-12-09
PL196961B1 (en) 2008-02-29
EP1227866A1 (en) 2002-08-07
JP2003509575A (en) 2003-03-11
JP2003509576A (en) 2003-03-11
EP1218079B8 (en) 2010-01-06
CZ2002799A3 (en) 2002-08-14
PL356680A1 (en) 2004-06-28
HUP0202872A2 (en) 2002-12-28
EP1218079B1 (en) 2009-11-18
CZ295265B6 (en) 2005-06-15
HUP0203963A3 (en) 2004-03-01
CA2385109C (en) 2008-12-23
CA2384874C (en) 2008-12-23
PL196962B1 (en) 2008-02-29
FI113453B (en) 2004-04-30
CZ2002948A3 (en) 2002-09-11
US6663717B2 (en) 2003-12-16
EP1218079A1 (en) 2002-07-03
CA2385109A1 (en) 2001-03-29
CZ295865B6 (en) 2005-11-16
US20020150652A1 (en) 2002-10-17
WO2001021272A1 (en) 2001-03-29

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