ES8301904A1 - Procedimiento para la preparacion de derivados de urea. - Google Patents
Procedimiento para la preparacion de derivados de urea.Info
- Publication number
- ES8301904A1 ES8301904A1 ES507324A ES507324A ES8301904A1 ES 8301904 A1 ES8301904 A1 ES 8301904A1 ES 507324 A ES507324 A ES 507324A ES 507324 A ES507324 A ES 507324A ES 8301904 A1 ES8301904 A1 ES 8301904A1
- Authority
- ES
- Spain
- Prior art keywords
- preparation
- urea derivatives
- chlorine
- fluorine
- compounds
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000003672 ureas Chemical class 0.000 title 1
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical group FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 abstract 2
- 239000000460 chlorine Substances 0.000 abstract 2
- 229910052801 chlorine Inorganic materials 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- 229910052731 fluorine Chemical group 0.000 abstract 2
- 239000011737 fluorine Chemical group 0.000 abstract 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical group [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract 1
- 241000607479 Yersinia pestis Species 0.000 abstract 1
- 239000004480 active ingredient Substances 0.000 abstract 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical group [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 125000001309 chloro group Chemical group Cl* 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 150000002431 hydrogen Chemical class 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 230000000361 pesticidal effect Effects 0.000 abstract 1
- 229910052717 sulfur Chemical group 0.000 abstract 1
- 239000011593 sulfur Chemical group 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C265/00—Derivatives of isocyanic acid
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/34—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the groups, e.g. biuret; Thio analogues thereof; Urea-aldehyde condensation products
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
- C07C205/07—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by halogen atoms
- C07C205/11—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by halogen atoms having nitro groups bound to carbon atoms of six-membered aromatic rings
- C07C205/12—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by halogen atoms having nitro groups bound to carbon atoms of six-membered aromatic rings the six-membered aromatic ring or a condensed ring system containing that ring being substituted by halogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C265/00—Derivatives of isocyanic acid
- C07C265/12—Derivatives of isocyanic acid having isocyanate groups bound to carbon atoms of six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C275/00—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C275/46—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups containing any of the groups, X being a hetero atom, Y being any atom, e.g. acylureas
- C07C275/48—Y being a hydrogen or a carbon atom
- C07C275/54—Y being a carbon atom of a six-membered aromatic ring, e.g. benzoylureas
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C335/00—Thioureas, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C335/04—Derivatives of thiourea
- C07C335/24—Derivatives of thiourea containing any of the groups, X being a hetero atom, Y being any atom
- C07C335/26—Y being a hydrogen or a carbon atom, e.g. benzoylthioureas
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PROCEDIMIENTO PARA LA PREPARACION DE DERIVADOS DE UREA DE FORMULA GENERAL (I), EN DONDE Q REPRESENTA UN GRUPO DE FORMULA (II); X REPRESENTA OXIGENO O AZUFRE; Y REPRESENTA CLORO O FLUOR; Y Z REPRESENTA HIDROGENO, CLORO O FLUOR. CONSISTE EN HACER REACCIONAR UN ISOCIANATO O ISOTIOCIANATO DE FORMULA: Q<024>NCX, CON UNA BENZAMIDA DE FORMULA (III). LA REACCION SE LLEVA A EFECTO ENTRE LA TEMPERATURA AMBIENTE Y LA TEMPERATURA DE EBULLICION DE LA MEZCLA DE REACCION. COMO MEDIO DE REACCION SE UTILIZA UN DISOLVENTE INERTE, TAL COMO TOLUENO, XILENO, CLOROBENCENO, PIRIDINA, O UN ETER TAL COMO DIOXANO O TETRAHIDROFURANO, EN PRESENCIA DE UNA BASE ORGANICA TERCIARIA. DE APLICACION EN LA PREPARACION DE SUSTANCIAS ACTIVAS EMPLEADAS COMO INSECTICIDAS Y ACARICIDAS.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19803044055 DE3044055A1 (de) | 1980-11-22 | 1980-11-22 | Harnstoffderivate, ihre herstellung und verwendung |
DE19813123720 DE3123720A1 (de) | 1981-06-15 | 1981-06-15 | Harnstoffderivate, ihre herstellung und verwendung |
Publications (2)
Publication Number | Publication Date |
---|---|
ES507324A0 ES507324A0 (es) | 1983-01-01 |
ES8301904A1 true ES8301904A1 (es) | 1983-01-01 |
Family
ID=25789258
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES507324A Expired ES8301904A1 (es) | 1980-11-22 | 1981-11-20 | Procedimiento para la preparacion de derivados de urea. |
ES507310A Granted ES507310A0 (es) | 1980-11-22 | 1981-11-20 | Procedimiento para la preparacion de derivados de urea. |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES507310A Granted ES507310A0 (es) | 1980-11-22 | 1981-11-20 | Procedimiento para la preparacion de derivados de urea. |
Country Status (14)
Country | Link |
---|---|
US (2) | US4457943A (es) |
EP (1) | EP0052833B1 (es) |
AU (1) | AU537096B2 (es) |
BR (1) | BR8202968A (es) |
CA (1) | CA1177852A (es) |
DD (1) | DD202007A5 (es) |
DE (1) | DE3161657D1 (es) |
ES (2) | ES8301904A1 (es) |
HU (1) | HU185066B (es) |
IL (1) | IL64317A (es) |
MX (1) | MX154685A (es) |
NZ (1) | NZ199011A (es) |
PL (1) | PL129912B1 (es) |
YU (1) | YU41998B (es) |
Families Citing this family (33)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5245071A (en) * | 1970-05-15 | 1993-09-14 | Duphar International Research B.V. | Organic compounds derived from urea or thiourea |
US5342958A (en) * | 1970-05-15 | 1994-08-30 | Solvay Duphar International Research B.V. | Organic compounds derived from urea or thiourea |
CA1238650A (en) * | 1982-03-01 | 1988-06-28 | Hiroshi Nagase | Urea derivatives, their production and use |
US4665097A (en) * | 1983-03-31 | 1987-05-12 | Union Carbide Corporation | Novel bicyclooxyaryl thioureas and process for preparation |
EP0176868B1 (de) * | 1984-09-29 | 1989-04-12 | Shell Internationale Researchmaatschappij B.V. | Neue insektizid wirksame Benzoylharnstoffe |
JPS61148157A (ja) * | 1984-12-21 | 1986-07-05 | Nippon Kayaku Co Ltd | ベンゾイルフエニル尿素誘導体およびそれを含有する害虫防除剤 |
DE3508429A1 (de) * | 1985-03-09 | 1986-09-11 | Bayer Ag, 5090 Leverkusen | Benzoylharnstoffe |
DE3626503A1 (de) * | 1986-08-05 | 1988-02-11 | Celamerck Gmbh & Co Kg | Verfahren zur herstellung von benzoylharnstoffen |
DE3640175A1 (de) * | 1986-11-25 | 1988-06-01 | Bayer Ag | Benzoyl(thio)harnstoffe |
DE3642332A1 (de) * | 1986-12-11 | 1988-06-23 | Bayer Ag | Verfahren zur herstellung von substituierten 3,5-dichlor-2,4-difluor-benzolen |
DE3642333A1 (de) * | 1986-12-11 | 1988-06-23 | Bayer Ag | Verfahren zur herstellung von 3,5-dichlor-2,4-difluornitrobenzol |
AU595417B2 (en) * | 1987-02-04 | 1990-03-29 | Sumitomo Chemical Company, Limited | A benzoylurea derivative and its production and use |
US5157155A (en) * | 1987-02-04 | 1992-10-20 | Sumitomo Chemical Company, Limited | Benzoylurea derivative and its production and use |
US4925876A (en) * | 1987-05-08 | 1990-05-15 | Ciba-Geigy Corporation | N-benzolyl-N'-trihalo-haloalkoxyphenylureas and pesticidal compositions containing them |
US4910018A (en) * | 1987-09-25 | 1990-03-20 | Ciba-Geigy Corp. | N-benzoyl-N'-2,4-difluoro-3,5-dihalophenylureas, their preparation and use in pest control |
JP2661709B2 (ja) * | 1988-07-08 | 1997-10-08 | ダウ・ケミカル日本株式会社 | 高活性な農薬水和剤の製法 |
GB8829817D0 (en) * | 1988-12-21 | 1989-02-15 | Shell Int Research | Benzamide compounds,their preparation and their use as pesticides |
GB8905741D0 (en) * | 1989-03-13 | 1989-04-26 | Shell Int Research | Process for preparing carbamates,and intermediates therin |
US5874615A (en) * | 1998-03-17 | 1999-02-23 | American Cyanamid Co | Method for the preparation of insecticidal benzoylurea compounds |
DE19953775A1 (de) | 1999-11-09 | 2001-05-10 | Bayer Ag | Wirkstoffkombinationen mit insektiziden und akariziden Eigenschaften |
DE10043610A1 (de) * | 2000-09-05 | 2002-03-14 | Bayer Ag | Wirkstoffkombinationen mit insektiziden und akariziden Eigenschaften |
DE102006031978A1 (de) * | 2006-07-11 | 2008-01-17 | Bayer Cropscience Ag | Wirkstoffkombinationen mit insektiziden und akariziden Eigenschaften |
CN100564355C (zh) * | 2006-08-02 | 2009-12-02 | 浙江工业大学 | 一种苯甲酰脲类衍生物的制备方法 |
EP2039248A1 (de) * | 2007-09-21 | 2009-03-25 | Bayer CropScience AG | Wirkstoffkombinationen mit insektiziden und akariziden Eigenschaften |
DE102007045957A1 (de) | 2007-09-26 | 2009-04-09 | Bayer Cropscience Ag | Wirkstoffkombinationen mit insektiziden und akarziden Eigenschaften |
AU2009243775B2 (en) * | 2008-05-07 | 2015-05-14 | Bayer Intellectual Property Gmbh | Synergistic active ingredient combinations |
EP2127522A1 (de) | 2008-05-29 | 2009-12-02 | Bayer CropScience AG | Wirkstoffkombinationen mit insektiziden und akariziden Eigenschaften |
CN102448305B (zh) | 2009-03-25 | 2015-04-01 | 拜尔农作物科学股份公司 | 具有杀昆虫和杀螨虫特性的活性成分结合物 |
EP2382865A1 (de) | 2010-04-28 | 2011-11-02 | Bayer CropScience AG | Synergistische Wirkstoffkombinationen |
CN102617360B (zh) * | 2012-03-01 | 2013-11-06 | 江西吉翔医药化工有限公司 | 3,5-二氯-2,4-二氟苯胺的合成方法 |
CN105801429B (zh) * | 2014-12-31 | 2019-09-24 | 安徽新北卡化学有限公司 | 一种3,5-二氯-2,4-二氟苯胺的制备方法 |
CN105265460B (zh) * | 2015-02-12 | 2017-12-26 | 四川利尔作物科学有限公司 | 杀虫杀螨组合物及其应用 |
CN104926694A (zh) * | 2015-05-15 | 2015-09-23 | 重庆大学 | 一种n-酰基脲衍生物的合成方法 |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL160809C (nl) * | 1970-05-15 | 1979-12-17 | Duphar Int Res | Werkwijze ter bereiding van benzoylureumverbindingen, alsmede werkwijze ter bereiding van insekticide prepara- ten op basis van benzoylureumverbindingen. |
DE2837086A1 (de) * | 1978-08-24 | 1980-03-06 | Bayer Ag | Substituierte n-phenyl-n'-benzoyl- thioharnstoffe, verfahren zu ihrer herstellung und ihre verwendung als schaedlingsbekaempfungsmittel |
US4310548A (en) * | 1979-02-01 | 1982-01-12 | Ciba-Geigy Corporation | Pesticidal N-tetrafluorophenyl-N'-benzoyl ureas |
US4399152A (en) * | 1980-04-03 | 1983-08-16 | Duphar International B.V. | Substituted benzoyl ureas as insecticides |
-
1981
- 1981-11-11 DE DE8181109618T patent/DE3161657D1/de not_active Expired
- 1981-11-11 EP EP81109618A patent/EP0052833B1/de not_active Expired
- 1981-11-16 US US06/321,446 patent/US4457943A/en not_active Expired - Lifetime
- 1981-11-19 IL IL64317A patent/IL64317A/xx not_active IP Right Cessation
- 1981-11-20 YU YU2738/81A patent/YU41998B/xx unknown
- 1981-11-20 PL PL1981233920A patent/PL129912B1/pl unknown
- 1981-11-20 CA CA000390554A patent/CA1177852A/en not_active Expired
- 1981-11-20 AU AU77725/81A patent/AU537096B2/en not_active Expired
- 1981-11-20 HU HU813477A patent/HU185066B/hu unknown
- 1981-11-20 NZ NZ199011A patent/NZ199011A/en unknown
- 1981-11-20 ES ES507324A patent/ES8301904A1/es not_active Expired
- 1981-11-20 DD DD81235011A patent/DD202007A5/de unknown
- 1981-11-20 ES ES507310A patent/ES507310A0/es active Granted
-
1982
- 1982-04-30 MX MX6352A patent/MX154685A/es unknown
- 1982-05-21 BR BR8202968A patent/BR8202968A/pt not_active IP Right Cessation
-
1984
- 1984-04-26 US US06/604,371 patent/US4622340A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
DD202007A5 (de) | 1983-08-24 |
CA1177852A (en) | 1984-11-13 |
ES8301903A1 (es) | 1982-12-16 |
IL64317A0 (en) | 1982-02-28 |
ES507324A0 (es) | 1983-01-01 |
US4622340A (en) | 1986-11-11 |
NZ199011A (en) | 1984-11-09 |
PL129912B1 (en) | 1984-06-30 |
MX154685A (es) | 1987-11-25 |
US4457943A (en) | 1984-07-03 |
AU7772581A (en) | 1982-06-03 |
YU273881A (en) | 1983-12-31 |
IL64317A (en) | 1985-07-31 |
YU41998B (en) | 1988-04-30 |
PL233920A1 (es) | 1982-07-19 |
DE3161657D1 (en) | 1984-01-19 |
HU185066B (en) | 1984-11-28 |
ES507310A0 (es) | 1982-12-16 |
EP0052833A1 (de) | 1982-06-02 |
EP0052833B1 (de) | 1983-12-14 |
AU537096B2 (en) | 1984-06-07 |
BR8202968A (pt) | 1983-12-27 |
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