ES427627A1 - Un procedimiento para la recuperacion de eta-caprolactama ycristales de sulfato de amonio a partir de una mezcla de reaccion que contiene la lactama y acido sulfurico. - Google Patents
Un procedimiento para la recuperacion de eta-caprolactama ycristales de sulfato de amonio a partir de una mezcla de reaccion que contiene la lactama y acido sulfurico.Info
- Publication number
- ES427627A1 ES427627A1 ES427627A ES427627A ES427627A1 ES 427627 A1 ES427627 A1 ES 427627A1 ES 427627 A ES427627 A ES 427627A ES 427627 A ES427627 A ES 427627A ES 427627 A1 ES427627 A1 ES 427627A1
- Authority
- ES
- Spain
- Prior art keywords
- caprolactam
- recovery
- reaction mixture
- sulphuric acid
- lactam
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 title abstract 3
- 238000000034 method Methods 0.000 title 1
- 239000011541 reaction mixture Substances 0.000 title 1
- 238000011084 recovery Methods 0.000 title 1
- 235000011149 sulphuric acid Nutrition 0.000 title 1
- 239000001117 sulphuric acid Substances 0.000 title 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 abstract 2
- 150000003951 lactams Chemical class 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 238000006237 Beckmann rearrangement reaction Methods 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 abstract 1
- 229910052921 ammonium sulfate Inorganic materials 0.000 abstract 1
- 235000011130 ammonium sulphate Nutrition 0.000 abstract 1
- 238000001704 evaporation Methods 0.000 abstract 1
- 230000007062 hydrolysis Effects 0.000 abstract 1
- 238000006460 hydrolysis reaction Methods 0.000 abstract 1
- 238000006386 neutralization reaction Methods 0.000 abstract 1
- 230000003472 neutralizing effect Effects 0.000 abstract 1
- 230000008707 rearrangement Effects 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/16—Separation or purification
-
- E—FIXED CONSTRUCTIONS
- E05—LOCKS; KEYS; WINDOW OR DOOR FITTINGS; SAFES
- E05Y—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES E05D AND E05F, RELATING TO CONSTRUCTION ELEMENTS, ELECTRIC CONTROL, POWER SUPPLY, POWER SIGNAL OR TRANSMISSION, USER INTERFACES, MOUNTING OR COUPLING, DETAILS, ACCESSORIES, AUXILIARY OPERATIONS NOT OTHERWISE PROVIDED FOR, APPLICATION THEREOF
- E05Y2900/00—Application of doors, windows, wings or fittings thereof
- E05Y2900/10—Application of doors, windows, wings or fittings thereof for buildings or parts thereof
- E05Y2900/104—Application of doors, windows, wings or fittings thereof for buildings or parts thereof for elevators
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Other In-Based Heterocyclic Compounds (AREA)
- Fertilizers (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL7308834A NL7308834A (es) | 1973-06-26 | 1973-06-26 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES427627A1 true ES427627A1 (es) | 1976-10-16 |
Family
ID=19819146
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES427627A Expired ES427627A1 (es) | 1973-06-26 | 1974-06-25 | Un procedimiento para la recuperacion de eta-caprolactama ycristales de sulfato de amonio a partir de una mezcla de reaccion que contiene la lactama y acido sulfurico. |
Country Status (19)
| Country | Link |
|---|---|
| US (1) | US3907781A (es) |
| JP (1) | JPS5036483A (es) |
| AR (1) | AR199442A1 (es) |
| AT (1) | AT334382B (es) |
| AU (1) | AU476555B2 (es) |
| BE (1) | BE816872A (es) |
| BR (1) | BR7405226D0 (es) |
| CS (1) | CS168478B2 (es) |
| DD (1) | DD114078A5 (es) |
| DE (1) | DE2430757A1 (es) |
| ES (1) | ES427627A1 (es) |
| FR (1) | FR2235121B1 (es) |
| GB (1) | GB1434687A (es) |
| IN (1) | IN139743B (es) |
| IT (1) | IT1016162B (es) |
| NL (1) | NL7308834A (es) |
| SU (1) | SU552019A3 (es) |
| TR (1) | TR18106A (es) |
| ZA (1) | ZA744054B (es) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL7410450A (nl) * | 1974-08-05 | 1976-02-09 | Stamicarbon | Werkwijze voor het winnen van epsilon-capro- lactam uit een epsilon-caprolactamzwavelzuur reactiemengsel. |
| NL7505130A (nl) * | 1975-05-01 | 1976-11-03 | Stamicarbon | Werkwijze voor de winning van zuiver epsilon- -caprolactam uit een waterige oplossing hiervan. |
| US4138472A (en) * | 1976-11-10 | 1979-02-06 | Basf Aktiengesellschaft | Process for obtaining coarsely crystalline pure ammonium sulfate |
| DE2651195C3 (de) * | 1976-11-10 | 1985-01-31 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Gewinnung von grobkristallinem reinem Ammonsulfat |
| DE2845019A1 (de) * | 1978-10-16 | 1980-04-30 | Basf Ag | Verfahren zur kontinuierlichen herstellung von epsilon -caprolactam durch beckmann'sche umlagerung |
| FR2786180B1 (fr) * | 1998-11-19 | 2001-11-23 | Rhone Poulenc Fibres | Procede de traitement de lactames et procede de purification d'un lactame |
| EP1092681A1 (de) * | 1999-10-13 | 2001-04-18 | Va Tech Wabag AG | Verfahren zum Neutralisieren einer Abfallsäure und gleichzeitigem Gewinnen von Salzkristallen |
| EA022192B1 (ru) | 2010-07-02 | 2015-11-30 | ДСМ АйПи АССЕТС Б.В. | Высокотемпературная нейтрализация лактама |
| WO2013053377A1 (en) | 2011-10-10 | 2013-04-18 | Dsm Ip Assets B.V. | High temperature lactam neutralisation |
| CN103012273A (zh) * | 2012-11-26 | 2013-04-03 | 中国化学赛鼎宁波工程有限公司 | 一种己内酰胺重排液制备己内酰胺的中和结晶系统及其方法 |
| CN103145618B (zh) * | 2013-03-15 | 2014-06-18 | 东明天军化工有限公司 | 一种己内酰胺和硫酸铵联产的方法 |
| CN104356039B (zh) * | 2014-11-10 | 2017-02-15 | 河北美邦工程科技有限公司 | 一种己内酰胺制备工艺 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2993889A (en) * | 1961-07-25 | Separation of a lactam from an acid | ||
| NL144600B (nl) * | 1964-03-07 | 1975-01-15 | Stamicarbon | Afscheiding van lactamen uit een sterk zwavelzuur milieu. |
| GB1123472A (en) * | 1965-01-21 | 1968-08-14 | Snia Viscosa | Improvements in or relating to the neutralization of acid solutions of caprolactam |
| US3852273A (en) * | 1971-05-07 | 1974-12-03 | Stamicarbon | Process for preparing and recovering lactams |
| NL164028C (nl) * | 1971-05-07 | 1980-11-17 | Stamicarbon | Werkwijze voor de afscheiding van lactamen. |
-
1973
- 1973-06-26 NL NL7308834A patent/NL7308834A/xx unknown
-
1974
- 1974-06-18 AT AT503874A patent/AT334382B/de active
- 1974-06-24 DD DD179427A patent/DD114078A5/xx unknown
- 1974-06-24 IT IT51708/74A patent/IT1016162B/it active
- 1974-06-24 SU SU2040365A patent/SU552019A3/ru active
- 1974-06-24 ZA ZA00744054A patent/ZA744054B/xx unknown
- 1974-06-24 US US482601A patent/US3907781A/en not_active Expired - Lifetime
- 1974-06-25 TR TR18106A patent/TR18106A/xx unknown
- 1974-06-25 ES ES427627A patent/ES427627A1/es not_active Expired
- 1974-06-25 FR FR7422071A patent/FR2235121B1/fr not_active Expired
- 1974-06-26 CS CS4506A patent/CS168478B2/cs unknown
- 1974-06-26 BR BR5226/74A patent/BR7405226D0/pt unknown
- 1974-06-26 AR AR254412A patent/AR199442A1/es active
- 1974-06-26 GB GB2839274A patent/GB1434687A/en not_active Expired
- 1974-06-26 DE DE2430757A patent/DE2430757A1/de active Pending
- 1974-06-26 BE BE145892A patent/BE816872A/xx unknown
- 1974-06-26 JP JP49073141A patent/JPS5036483A/ja active Pending
- 1974-07-02 AU AU70727/74A patent/AU476555B2/en not_active Expired
- 1974-07-26 IN IN1671/CAL/74A patent/IN139743B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| BE816872A (fr) | 1974-12-27 |
| US3907781A (en) | 1975-09-23 |
| BR7405226D0 (pt) | 1975-01-21 |
| SU552019A3 (ru) | 1977-03-25 |
| DD114078A5 (es) | 1975-07-12 |
| AU476555B2 (en) | 1976-09-30 |
| GB1434687A (en) | 1976-05-05 |
| ZA744054B (en) | 1975-10-29 |
| FR2235121A1 (es) | 1975-01-24 |
| JPS5036483A (es) | 1975-04-05 |
| CS168478B2 (es) | 1976-06-29 |
| NL7308834A (es) | 1974-12-30 |
| AR199442A1 (es) | 1974-08-30 |
| TR18106A (tr) | 1976-09-30 |
| IT1016162B (it) | 1977-05-30 |
| DE2430757A1 (de) | 1975-01-23 |
| FR2235121B1 (es) | 1978-01-13 |
| AU7072774A (en) | 1976-01-08 |
| IN139743B (es) | 1976-07-24 |
| ATA503874A (de) | 1976-05-15 |
| AT334382B (de) | 1976-01-10 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| ES427627A1 (es) | Un procedimiento para la recuperacion de eta-caprolactama ycristales de sulfato de amonio a partir de una mezcla de reaccion que contiene la lactama y acido sulfurico. | |
| MY123175A (en) | Method for producing an aqueous solution of free hydroxylamine | |
| ES402472A1 (es) | Procedimiento para la preparacion de lactamas. | |
| GB1353866A (en) | Process for removing lactams | |
| GB1399000A (en) | Process for the recovery of pure epsilon-caprolactam | |
| GB1508942A (en) | Process for producing lactams | |
| ES417501A2 (es) | Procedimiento para la recuperacion de lactamas de una mezclaobtenida por conversion de las oximas correspondientes. | |
| GB1462740A (en) | Process for the recovery of epsilon-caprolactam from reaction mixture of epsilon-caprolactam and sulphuric acid | |
| GB1259747A (en) | Process for the preparation of aliphatic tertiary amides | |
| GB1500084A (en) | Process for preparing lactams | |
| ES443998A1 (es) | Procedimiento para el tratamiento de vapor de agua generado al concentrar una solucion acuosa de urea. | |
| GB1256587A (es) | ||
| GB1506139A (en) | Process for the recovery of epsilon-caprolactam from a reaction mixture of epsilon-caprolactam and sulphuric acid | |
| US2737511A (en) | Extraction of lactam | |
| GB1284138A (en) | Methionine purification | |
| US4140685A (en) | Process for recovering ε-caprolactam from an ε-caprolactam/sulfuric acid reaction mixture | |
| GB1370951A (en) | Process for the manufacture of a lactam | |
| GB1397289A (en) | Process for the recovery of lactam | |
| GB920625A (en) | Improvements in the production of aminocaproic acid | |
| GB1129354A (en) | Process for the separation of ammonia and nitriles | |
| ES466424A1 (es) | Un procedimiento para la recuperacion de epsilon-caprolacta-ma de una mezcla de reaccion de epsilon-caprolactama y acidosulfurico. | |
| GB1286427A (en) | Process of purifying lactams | |
| GB1001547A (en) | Process for the separation of ªÏ-dodecalactam | |
| FR2291195A1 (fr) | Procede de production d'e-caprolactame par transposition de l'oxime de cyclohexanone et nouveau produit ainsi obtenu | |
| GB1143847A (es) |