ES402312A1 - A procedure for the production of 1-rent (alkenil) 6,7-oxocinolin-3-carbonitrilos and its intermediate products. (Machine-translation by Google Translate, not legally binding) - Google Patents
A procedure for the production of 1-rent (alkenil) 6,7-oxocinolin-3-carbonitrilos and its intermediate products. (Machine-translation by Google Translate, not legally binding)Info
- Publication number
- ES402312A1 ES402312A1 ES402312A ES402312A ES402312A1 ES 402312 A1 ES402312 A1 ES 402312A1 ES 402312 A ES402312 A ES 402312A ES 402312 A ES402312 A ES 402312A ES 402312 A1 ES402312 A1 ES 402312A1
- Authority
- ES
- Spain
- Prior art keywords
- methylenedioxyquinolin
- oxocinolin
- translation
- production
- machine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fodder In General (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
Abstract
A process for the production of 1-alkyl (or alkenyl) 6,7-oxocinolin-3-carbonitriles and their intermediates of the following formula: ** (see formula) ** Where r is a member of the group consisting of methyl, ethyl, N-propyl, isopropyl, N-butyl, β -hiroxyethyl and allyl, which process consists of: (a) catalytically reducing 2'-nitro-4'-5'-methylenedioxy-acetophenone to 2'-amino-4', 5'-methylenedioxyacetophenone; (b) diazotizing the 2-amino-4'5'-methylenedioxyacetophenone with nitrous acid and cyclizing to form 6,7-methylenedioxyquinolin-4-ol; (c) treating with bromine 6,7-methylenedioxycinolin-4-ol to produce 3-bromo-6,7-methylenedioxyquinolin-4-ol; (d) treating cuprous cyanide with 3-bromo-6,7-methylenedioxyquinolin-4-ol to form 6,7-methylenedioxyquinolin-4-ol-3-carbonitrile; y (e) alkylating 6,7-methylenedioxyquinolin-4-ol-3-carbonitrile with alkyl, alkenyl or β-hydroxyethyl bromide, chloride, iodide or sulfate to form the carbonitrile which corresponds to the above formula. (Machine-translation by Google Translate, not legally binding)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US79654669A | 1969-02-04 | 1969-02-04 | |
US88888069A | 1969-12-29 | 1969-12-29 |
Publications (1)
Publication Number | Publication Date |
---|---|
ES402312A1 true ES402312A1 (en) | 1976-04-01 |
Family
ID=27121747
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES376173A Expired ES376173A1 (en) | 1969-02-04 | 1970-02-03 | A method for the preparation of 6,7-metilendioxi 4 (ih) -oxocinmolin-3-carboxilic acids. (Machine-translation by Google Translate, not legally binding) |
ES402312A Expired ES402312A1 (en) | 1969-02-04 | 1972-05-02 | A procedure for the production of 1-rent (alkenil) 6,7-oxocinolin-3-carbonitrilos and its intermediate products. (Machine-translation by Google Translate, not legally binding) |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES376173A Expired ES376173A1 (en) | 1969-02-04 | 1970-02-03 | A method for the preparation of 6,7-metilendioxi 4 (ih) -oxocinmolin-3-carboxilic acids. (Machine-translation by Google Translate, not legally binding) |
Country Status (2)
Country | Link |
---|---|
JP (1) | JPS4914240B1 (en) |
ES (2) | ES376173A1 (en) |
-
1970
- 1970-02-03 ES ES376173A patent/ES376173A1/en not_active Expired
- 1970-02-04 JP JP45009373A patent/JPS4914240B1/ja active Pending
-
1972
- 1972-05-02 ES ES402312A patent/ES402312A1/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
JPS4914240B1 (en) | 1974-04-05 |
ES376173A1 (en) | 1972-09-01 |
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