ES402121A1 - Procedimiento para la purificacion de esteres de alto pun-to de abullicion. - Google Patents
Procedimiento para la purificacion de esteres de alto pun-to de abullicion.Info
- Publication number
- ES402121A1 ES402121A1 ES72402121A ES402121A ES402121A1 ES 402121 A1 ES402121 A1 ES 402121A1 ES 72402121 A ES72402121 A ES 72402121A ES 402121 A ES402121 A ES 402121A ES 402121 A1 ES402121 A1 ES 402121A1
- Authority
- ES
- Spain
- Prior art keywords
- purification
- high boiling
- decantation
- mixture
- esterification
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/58—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/60—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
- C07C69/80—Phthalic acid esters
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Procedimiento para la purificación de ésteres de alto punto de ebullición , producidos por esterificación de un ácido orgánico carboxílico o de su anhídrido por un alcohol, más particularmente al menos en C8, o un poliol, en presencia de un catalizador de esterificación, tal como el ácido sulfúrico, y a continuación neutralización del producto de reacción, calentamiento a 130-190º, de la mezcla neutralizada, y decantación de esta mezcla para separar una fase orgánica y una fase acuosa, caracterizado porque se efectúa la decantación a una temperatura 120 a 200º, más particularmente de 150 a 190º , y bajo presión más particularmente bajo una presión de 3 a 20 bares efectivos.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7115732A FR2135863A5 (es) | 1971-04-26 | 1971-04-26 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES402121A1 true ES402121A1 (es) | 1975-10-16 |
Family
ID=9076275
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES72402121A Expired ES402121A1 (es) | 1971-04-26 | 1972-04-26 | Procedimiento para la purificacion de esteres de alto pun-to de abullicion. |
Country Status (22)
| Country | Link |
|---|---|
| US (1) | US3849475A (es) |
| JP (1) | JPS5620301B1 (es) |
| AT (1) | AT317872B (es) |
| AU (1) | AU458281B2 (es) |
| BE (1) | BE782634A (es) |
| BR (1) | BR7201933D0 (es) |
| CA (1) | CA956644A (es) |
| CH (1) | CH552554A (es) |
| CS (1) | CS157143B2 (es) |
| DD (1) | DD108072A5 (es) |
| DK (1) | DK136711B (es) |
| ES (1) | ES402121A1 (es) |
| FR (1) | FR2135863A5 (es) |
| GB (1) | GB1329534A (es) |
| HU (1) | HU163592B (es) |
| IT (1) | IT947653B (es) |
| NL (1) | NL7202400A (es) |
| NO (1) | NO136887C (es) |
| PL (1) | PL82681B1 (es) |
| RO (1) | RO58907A (es) |
| SE (1) | SE379191B (es) |
| SU (1) | SU552022A3 (es) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4066835A (en) * | 1974-05-31 | 1978-01-03 | Ruhrchemie Ag | Process for purifying the waste water produced in the process of producing ester plasticizers |
-
1971
- 1971-04-26 FR FR7115732A patent/FR2135863A5/fr not_active Expired
-
1972
- 1972-01-27 AU AU38388/72A patent/AU458281B2/en not_active Expired
- 1972-01-31 RO RO69611A patent/RO58907A/ro unknown
- 1972-02-15 NO NO440/72A patent/NO136887C/no unknown
- 1972-02-17 IT IT20688/72A patent/IT947653B/it active
- 1972-02-23 NL NL7202400A patent/NL7202400A/xx unknown
- 1972-03-02 JP JP2193272A patent/JPS5620301B1/ja active Pending
- 1972-04-04 CS CS223872A patent/CS157143B2/cs unknown
- 1972-04-04 BR BR721933A patent/BR7201933D0/pt unknown
- 1972-04-11 CA CA139,428A patent/CA956644A/en not_active Expired
- 1972-04-11 AT AT311372A patent/AT317872B/de not_active IP Right Cessation
- 1972-04-20 SU SU1773557A patent/SU552022A3/ru active
- 1972-04-21 HU HUME1490A patent/HU163592B/hu unknown
- 1972-04-24 PL PL1972154943A patent/PL82681B1/pl unknown
- 1972-04-25 GB GB1921572A patent/GB1329534A/en not_active Expired
- 1972-04-25 BE BE782634A patent/BE782634A/xx not_active IP Right Cessation
- 1972-04-25 DK DK203672AA patent/DK136711B/da unknown
- 1972-04-25 DD DD162562A patent/DD108072A5/xx unknown
- 1972-04-26 CH CH620172A patent/CH552554A/fr not_active IP Right Cessation
- 1972-04-26 US US00247592A patent/US3849475A/en not_active Expired - Lifetime
- 1972-04-26 ES ES72402121A patent/ES402121A1/es not_active Expired
- 1972-04-26 SE SE7205518A patent/SE379191B/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| PL82681B1 (es) | 1975-10-31 |
| CS157143B2 (es) | 1974-08-23 |
| DK136711C (es) | 1978-05-01 |
| FR2135863A5 (es) | 1972-12-22 |
| BR7201933D0 (pt) | 1973-06-14 |
| GB1329534A (en) | 1973-09-12 |
| HU163592B (es) | 1973-09-27 |
| JPS5620301B1 (es) | 1981-05-13 |
| CA956644A (en) | 1974-10-22 |
| DD108072A5 (es) | 1974-09-05 |
| NL7202400A (es) | 1972-10-30 |
| US3849475A (en) | 1974-11-19 |
| NO136887B (no) | 1977-08-15 |
| IT947653B (it) | 1973-05-30 |
| DE2215902A1 (es) | 1972-11-09 |
| AT317872B (de) | 1974-09-25 |
| SU552022A3 (ru) | 1977-03-25 |
| DE2215902B2 (de) | 1976-04-15 |
| DK136711B (da) | 1977-11-14 |
| CH552554A (fr) | 1974-08-15 |
| AU458281B2 (en) | 1975-01-31 |
| BE782634A (fr) | 1972-10-25 |
| NO136887C (no) | 1977-11-23 |
| AU3838872A (en) | 1973-08-02 |
| SE379191B (es) | 1975-09-29 |
| RO58907A (es) | 1976-01-15 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| ES414004A1 (es) | Procedimiento de esterificacion. | |
| ES368127A1 (es) | Procedimiento continuo para la fabricacion de esteres. | |
| GB903613A (en) | Improvements in or relating to the production of acetoacetic acid esters | |
| ES402121A1 (es) | Procedimiento para la purificacion de esteres de alto pun-to de abullicion. | |
| GB1173089A (en) | Production of Esters | |
| GB925812A (en) | Novel ester of hydroxymethylfurfural and process for its preparation | |
| ES329474A1 (es) | Un procedimiento para la fabricacion de acido tereftalico a partir de productos oxidados. | |
| GB1216926A (en) | Process for purifying high boiling esters | |
| GB1003007A (en) | Improvements in or relating to the production of ethyl acrylate | |
| ES390387A3 (es) | Un procedimiento para la esterificacion del acido terefta- lico. | |
| ES301028A1 (es) | Procedimiento para la obtencion de un poliester. | |
| ES437932A1 (es) | Procedimiento para la depuracion del agua residual que se produce en la fabricacion de los plastificantes de esteres. | |
| ES409540A3 (es) | Un procedimiento para la preparacion de esteres dialcohili-cos del acido tereftalico. | |
| ES271069A3 (es) | Procedimiento para la preparación de poliésteres lineales | |
| GB1166636A (en) | Process for the production of Cycloacetal Esters and Cycloketal Esters | |
| GB1317342A (en) | Preparation of alkali metal benzoates | |
| ES245855A1 (es) | Procedimiento continuo de preparaciën de anhidrido maleico incoloro muy puro por deshidrataciën del acido maleico | |
| ES372341A1 (es) | Un procedimiento para el tratamiento de acidos carboxilicosorganicos contenidos en solucion acuosa. | |
| GB844237A (en) | Esters of aromatic dicarboxylic acids | |
| GB1205180A (en) | Process for the catalytic preparation of epoxyalkyl esters | |
| ES367087A3 (es) | Procedimiento para la fabricacion de acetato de isopropilo. | |
| ES269458A1 (es) | Procedimiento para la purificacion de tereftalato de dimetilo | |
| GB1087259A (en) | Process for producing furan | |
| ES404214A1 (es) | Procedimiento para la obtencion de esteres plastificantes altamente puros. | |
| ES342497A1 (es) | Procedimiento para la produccion de un ester isopropilico. |