ES351495A1 - Chemical processing apparatus - Google Patents

Chemical processing apparatus

Info

Publication number
ES351495A1
ES351495A1 ES351495A ES351495A ES351495A1 ES 351495 A1 ES351495 A1 ES 351495A1 ES 351495 A ES351495 A ES 351495A ES 351495 A ES351495 A ES 351495A ES 351495 A1 ES351495 A1 ES 351495A1
Authority
ES
Spain
Prior art keywords
acid
chambers
chamber
phosphoric acid
phosphate rock
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES351495A
Other languages
Spanish (es)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CB&I Technology Inc
Original Assignee
Lummus Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Lummus Co filed Critical Lummus Co
Publication of ES351495A1 publication Critical patent/ES351495A1/en
Expired legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • B01J19/1862Stationary reactors having moving elements inside placed in series
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00Phosphorus; Compounds thereof
    • C01B25/16Oxyacids of phosphorus; Salts thereof
    • C01B25/18Phosphoric acid
    • C01B25/22Preparation by reacting phosphate-containing material with an acid, e.g. wet process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00117Controlling the temperature by indirect heating or cooling employing heat exchange fluids with two or more reactions in heat exchange with each other, such as an endothermic reaction in heat exchange with an exothermic reaction
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00159Controlling the temperature controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)

Abstract

Phosphoric acid is produced from phosphate rock, phosphoric acid and sulphuric acid in apparatus in which the reaction slurry flows from one chamber to the next alternately via over flow and underflow baffles which define the chambers and which may be heat conductive. Foam formed on the surface may be sucked in through slots 54 in draft tubes 52 and broken by agitators 50. The apparatus also comprises a steel or concrete shell 60, acid impervious neoprene layer 58 and abrasion and acid resistent carbon brick 59. In the embodiment of Fig. 3, phosphate rock and phosphoric acid are reacted in chamber 78 in heat exchange with chambers 70, 72 and 74 through which chambers the product from chamber 78 flows while it is reacted with sulphuric acid added in each chamber. In the embodiment of Figs. 5 and 6 (not shown), phosphate rock/phosphoric acid is introduced into a digester (83) via a channel (92) so that it is heated to reaction temperature by heat exchange with the walls of chambers (86 and 88) in which sulphuric acid and already formed monocalcium phosphate are reacting.
ES351495A 1967-03-20 1968-03-12 Chemical processing apparatus Expired ES351495A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US62433567A 1967-03-20 1967-03-20

Publications (1)

Publication Number Publication Date
ES351495A1 true ES351495A1 (en) 1969-06-01

Family

ID=24501593

Family Applications (1)

Application Number Title Priority Date Filing Date
ES351495A Expired ES351495A1 (en) 1967-03-20 1968-03-12 Chemical processing apparatus

Country Status (6)

Country Link
BE (1) BE712517A (en)
DE (1) DE1667162A1 (en)
ES (1) ES351495A1 (en)
FR (1) FR1556829A (en)
GB (1) GB1203364A (en)
NL (1) NL6803873A (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3047505A1 (en) * 1980-12-17 1982-07-22 Hoechst Ag, 6000 Frankfurt PLANT FOR THE PRODUCTION OF PHOSPHORPENTASULFID
FI20145759A (en) * 2014-09-02 2016-03-03 Outotec Finland Oy Autoclave and heat transfer element
CN111774023A (en) * 2020-06-23 2020-10-16 刘岩 Reation kettle with heat preservation function
CN113842864B (en) * 2021-10-19 2023-12-15 沛县宗赢工程机械制造有限公司 Quinone natural product extraction equipment capable of crystallizing and extracting waste liquid

Also Published As

Publication number Publication date
FR1556829A (en) 1969-02-07
NL6803873A (en) 1968-09-23
GB1203364A (en) 1970-08-26
BE712517A (en) 1968-07-31
DE1667162A1 (en) 1971-06-09

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