ES282091A1 - Procedure for the purification of sucrose esters (Machine-translation by Google Translate, not legally binding) - Google Patents

Procedure for the purification of sucrose esters (Machine-translation by Google Translate, not legally binding)

Info

Publication number
ES282091A1
ES282091A1 ES282091A ES282091A ES282091A1 ES 282091 A1 ES282091 A1 ES 282091A1 ES 282091 A ES282091 A ES 282091A ES 282091 A ES282091 A ES 282091A ES 282091 A1 ES282091 A1 ES 282091A1
Authority
ES
Spain
Prior art keywords
sucrose
solution
diesters
translation
purification
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES282091A
Other languages
Spanish (es)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ledoga SpA
Original Assignee
Ledoga SpA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ledoga SpA filed Critical Ledoga SpA
Publication of ES282091A1 publication Critical patent/ES282091A1/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/005Splitting up mixtures of fatty acids into their constituents
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07HSUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/04Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
    • C07H13/06Fatty acids
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B7/00Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
    • C11B7/0008Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents
    • C11B7/0025Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents in solvents containing oxygen in their molecule

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biochemistry (AREA)
  • Molecular Biology (AREA)
  • Genetics & Genomics (AREA)
  • Microbiology (AREA)
  • General Chemical & Material Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Biotechnology (AREA)
  • Health & Medical Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Saccharide Compounds (AREA)
  • Cosmetics (AREA)

Abstract

Process for the purification of sucrose esters, especially process for the separation of sucrose monoesters and diesters of fatty acids, characterized by dissolving a mixture of such esters in a low aliphatic alcohol, at a temperature of about 40º c, at a temperature of about reflux, cooling the solution thus obtained to temperatures ranging from 0ºC to about 35º c, separating the sucrose diesters from the saturated acids with at least 16 carbon atoms, which precipitate, evaporating the alcohol solution, dissolving the residue in ethyl acetate. Ethyl, cooling the solution thus obtained to around 5-20º c, collecting the monoesters of sucrose, which precipitate, evaporating the solution to dryness, and recovering as residue the sucrose diesters of saturated fatty acids, having a maximum of 14 carbon atoms and the sucrose diesters with unsaturated fatty acids. (Machine-translation by Google Translate, not legally binding)
ES282091A 1961-10-31 1962-10-31 Procedure for the purification of sucrose esters (Machine-translation by Google Translate, not legally binding) Expired ES282091A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
IT1968261 1961-10-31

Publications (1)

Publication Number Publication Date
ES282091A1 true ES282091A1 (en) 1963-02-01

Family

ID=11160353

Family Applications (1)

Application Number Title Priority Date Filing Date
ES282091A Expired ES282091A1 (en) 1961-10-31 1962-10-31 Procedure for the purification of sucrose esters (Machine-translation by Google Translate, not legally binding)

Country Status (7)

Country Link
AT (1) AT246175B (en)
BE (1) BE624273A (en)
CH (1) CH417559A (en)
DE (1) DE1205511B (en)
ES (1) ES282091A1 (en)
FR (1) FR1338709A (en)
GB (1) GB1018554A (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0065390A1 (en) * 1981-05-11 1982-11-24 TATE & LYLE PUBLIC LIMITED COMPANY Purification of sucrose esters

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL111638C (en) * 1955-12-12

Also Published As

Publication number Publication date
CH417559A (en) 1966-07-31
FR1338709A (en) 1963-09-27
AT246175B (en) 1966-04-12
GB1018554A (en) 1966-01-26
DE1205511B (en) 1965-11-25
BE624273A (en) 1963-02-15

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