ES2623898T3 - Composición de resina de reacción así como su uso - Google Patents
Composición de resina de reacción así como su uso Download PDFInfo
- Publication number
- ES2623898T3 ES2623898T3 ES14718608.4T ES14718608T ES2623898T3 ES 2623898 T3 ES2623898 T3 ES 2623898T3 ES 14718608 T ES14718608 T ES 14718608T ES 2623898 T3 ES2623898 T3 ES 2623898T3
- Authority
- ES
- Spain
- Prior art keywords
- compound
- amine
- component
- resin composition
- well
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000011342 resin composition Substances 0.000 title abstract 2
- 239000011347 resin Substances 0.000 abstract description 5
- 229920005989 resin Polymers 0.000 abstract description 5
- 239000000203 mixture Substances 0.000 abstract description 4
- 229920000642 polymer Polymers 0.000 abstract description 3
- 239000003638 chemical reducing agent Substances 0.000 abstract description 2
- 150000001412 amines Chemical class 0.000 abstract 5
- 150000001875 compounds Chemical class 0.000 abstract 4
- 150000001880 copper compounds Chemical class 0.000 abstract 4
- 150000002978 peroxides Chemical group 0.000 abstract 4
- 239000005749 Copper compound Substances 0.000 abstract 2
- 229910021591 Copper(I) chloride Inorganic materials 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- XHCLAFWTIXFWPH-UHFFFAOYSA-N [O-2].[O-2].[O-2].[O-2].[O-2].[V+5].[V+5] Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[V+5].[V+5] XHCLAFWTIXFWPH-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- OXBLHERUFWYNTN-UHFFFAOYSA-M copper(I) chloride Chemical compound [Cu]Cl OXBLHERUFWYNTN-UHFFFAOYSA-M 0.000 description 2
- IMNIMPAHZVJRPE-UHFFFAOYSA-N triethylenediamine Chemical compound C1CN2CCN1CC2 IMNIMPAHZVJRPE-UHFFFAOYSA-N 0.000 description 2
- IBDVWXAVKPRHCU-UHFFFAOYSA-N 2-(2-methylprop-2-enoyloxy)ethyl 3-oxobutanoate Chemical compound CC(=O)CC(=O)OCCOC(=O)C(C)=C IBDVWXAVKPRHCU-UHFFFAOYSA-N 0.000 description 1
- OMQHDIHZSDEIFH-UHFFFAOYSA-N 3-Acetyldihydro-2(3H)-furanone Chemical compound CC(=O)C1CCOC1=O OMQHDIHZSDEIFH-UHFFFAOYSA-N 0.000 description 1
- 101000801643 Homo sapiens Retinal-specific phospholipid-transporting ATPase ABCA4 Proteins 0.000 description 1
- 102100033617 Retinal-specific phospholipid-transporting ATPase ABCA4 Human genes 0.000 description 1
- 241000779819 Syncarpia glomulifera Species 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000012973 diazabicyclooctane Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 125000005609 naphthenate group Chemical group 0.000 description 1
- 125000005474 octanoate group Chemical group 0.000 description 1
- 239000001739 pinus spp. Substances 0.000 description 1
- 238000010526 radical polymerization reaction Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229940036248 turpentine Drugs 0.000 description 1
- 150000003681 vanadium Chemical class 0.000 description 1
- 229910001935 vanadium oxide Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/02—Macromolecular compounds
- C04B26/04—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C04B26/06—Acrylates
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/02—Macromolecular compounds
- C04B26/04—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/13—Phenols; Phenolates
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
- C09K8/56—Compositions for consolidating loose sand or the like around wells without excessively decreasing the permeability thereof
- C09K8/57—Compositions based on water or polar solvents
- C09K8/575—Compositions based on water or polar solvents containing organic compounds
- C09K8/5751—Macromolecular compounds
- C09K8/5753—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00715—Uses not provided for elsewhere in C04B2111/00 for fixing bolts or the like
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21D—SHAFTS; TUNNELS; GALLERIES; LARGE UNDERGROUND CHAMBERS
- E21D20/00—Setting anchoring-bolts
- E21D20/02—Setting anchoring-bolts with provisions for grouting
- E21D20/025—Grouting with organic components, e.g. resin
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Macromonomer-Based Addition Polymer (AREA)
- Mining & Mineral Resources (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Geochemistry & Mineralogy (AREA)
- Geology (AREA)
Abstract
Composición de resina de reacción que comprende un componente (A) de resina, el cual contiene un compuesto (a-1) que puede formar polímeros por radicales, un compuesto (a-2) que puede reaccionar con una amina, y un compuesto (a-3) que forma puente con por lo menos dos funcionalidades reactivas, de las que una puede formar (co)polímeros por radicales y una puede reaccionar con una amina, y un componente (H) de curado que contiene por lo menos un peróxido (h-1) de dialquilo y por lo menos una amina (h-2), en la que el componente (A) de resina y el componente (H) de curado o el componente (A) de resina y el por lo menos un peróxido (h-1) de dialquilo y la por lo menos una amina (h-2) del componente (H) de curado están separados espacialmente uno de otro, para impedir una reacción antes de la mezcla de estos componentes, caracterizada porque el componente (H) de curado contiene además una mezcla (B) de acelerador, que comprende un compuesto (b-1) de cobre y un compuesto (b-2) de 1,3-dicarbonilo, con la condición de que el componente (A) de resina contenga además un agente (R) reductor, cuando el compuesto (b-1) de cobre es di o polivalente
Description
Ejemplos de comparación
Como comparación se omitieron en la composición el acelerador y el agente reductor correspondientes a los ejemplos 1 a 7. Al respecto, se observó que los tiempos de formación de gel (25 →80°C) aumentaron claramente por encima de 90 minutos y las temperaturas máximas cayeron claramente por debajo de 100°C. Esto conduce a propiedades mecánicas insuficientes ("polímeros blandos") y sugiere que aquí sólo curó la fracción epoxi-amina, mientras la polimerización por radicales tuvo lugar sólo de manera insuficiente o no ocurrió.
Tabla 1: composición de la mezcla de acelerador, tiempo de formación de gel y temperaturas máximas
- Ejemplo
- 1 2 3 4 5 6 7
- Resina
- 100
- Acelerador 1 (b-1)
- Octoato de Cu(II) 1,00 1,00 2,50 1,00 1,00
- TIB-KAT808 1)
- 1,00
- CuCl·DABCO 2)
- 1,00
- Acelerador 2 (b-2)
- AAEMA 3) 5,00 5,00 5,00 5,00 5,00 5,00
- ABL 4)
- 5,00 5,00
- Acelerador 3 (b-3)
- VP0132 5) 1,00 1,00 1,00 2,50 1,00
- AB106355 6)
- 1,00
- t (25 • 80°C)
- min 33 25 34 38 49 78 75
- t (25 • T(máx))
- min 38 29 36 41 56 85 80
- T (máx)
- °C 175 155 170 160 151 114 135
- 1) Solución de naftenato de Cu(II) en aguarrás (Compañía TIB Chemicals AG) 2) CuCl·1,4-diazabiciclo[2.2.2]octano (Compañía Sigma Aldrich) 3) 2-(Acetoacetoxi)etilmetacrilato 4) α-acetilbutirolactona 5) sal de vanadio (V) de un éster ha sido de ácido fosfórico, en solución (Compañía OMG Borchers GmbH) 6) óxido de vanadio (IV) -bis(2,4-pentanodionato) (Compañía ABCR GmbH & Co. KG)
13
Claims (1)
-
imagen1 imagen2
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP13164652 | 2013-04-22 | ||
| EP13164652.3A EP2796433A1 (de) | 2013-04-22 | 2013-04-22 | Reaktionsharz-Zusammensetzung sowie deren Verwendung |
| PCT/EP2014/058065 WO2014173864A1 (de) | 2013-04-22 | 2014-04-22 | Reaktionsharz-zusammensetzung sowie deren verwendung |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2623898T3 true ES2623898T3 (es) | 2017-07-12 |
Family
ID=48143150
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES14718608.4T Active ES2623898T3 (es) | 2013-04-22 | 2014-04-22 | Composición de resina de reacción así como su uso |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US20160039960A1 (es) |
| EP (2) | EP2796433A1 (es) |
| CA (1) | CA2910230C (es) |
| ES (1) | ES2623898T3 (es) |
| WO (1) | WO2014173864A1 (es) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2829524A1 (de) * | 2013-07-24 | 2015-01-28 | HILTI Aktiengesellschaft | Harzmischung, Reaktionsharz-Mörtel, Mehrkomponenten-Mörtelsystem und deren Verwendung |
| DE102016124075A1 (de) | 2016-12-12 | 2018-06-14 | Fischerwerke Gmbh & Co. Kg | Hybridbindemittel sowie dessen Verwendung |
| EP3424971A1 (de) | 2017-07-03 | 2019-01-09 | HILTI Aktiengesellschaft | Urethanmethacrylat-verbindungen enthaltende reaktivharze, reaktivharzkomponenten sowie reaktivharz-systeme und deren verwendung |
| CN116410717A (zh) * | 2021-12-29 | 2023-07-11 | 中国石油天然气股份有限公司 | 一种调驱剂及其制备方法和应用 |
Family Cites Families (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2391920A (en) | 1942-11-16 | 1946-01-01 | Du Pont | Polymerization catalysts |
| US3297745A (en) | 1962-04-05 | 1967-01-10 | Robertson Co H H | Ethylenically unsaturated di-and tetra-urethane monomers |
| GB1352063A (en) | 1971-01-08 | 1974-05-15 | Ici Ltd | Polymerisable compositions and resins derived thererom |
| US4618658A (en) | 1985-05-16 | 1986-10-21 | The Dow Chemical Company | Polymer modified epoxy resin compositions |
| DE3744390A1 (de) | 1987-12-29 | 1989-07-13 | Basf Ag | Faserverbundwerkstoffe auf basis von modifizierten vinylesterurethanharzen |
| GB8810299D0 (en) | 1988-04-29 | 1988-06-02 | Scott Bader Co | Vinyl terminated urethane containing resins |
| DE3940309A1 (de) | 1989-12-06 | 1991-06-13 | Hilti Ag | Moertelmasse |
| DE4131457A1 (de) | 1991-09-21 | 1993-03-25 | Basf Ag | Patrone oder kartusche fuer die chemische befestigungstechnik |
| DE19531649A1 (de) | 1995-08-29 | 1997-03-06 | Basf Ag | Dübelmasse für die chemische Befestigungstechnik |
| DE69811729T2 (de) | 1997-12-08 | 2003-08-14 | Vantico Gmbh & Co Kg | Novolacke als wasserunempfindliche beschleuniger für epoxyharz-härter |
| DE19956509A1 (de) | 1999-11-24 | 2001-01-18 | Basf Ag | Inhibitorkomposition zur Stabilisierung von ethylenisch ungesättigten Verbindungen gegen vorzeitige radikalische Polymerisation |
| EP1221452A1 (en) | 2000-12-22 | 2002-07-10 | Dsm N.V. | Vinyl ether resins for structural applications |
| DE10115587B4 (de) | 2001-03-29 | 2017-06-14 | Fischerwerke Gmbh & Co. Kg | Verwendung eines Harzes mit bestimmten härtbaren Harnstoffderivaten zur Befestigung mit Hilfe von Verankerungsmitteln |
| DE10115591A1 (de) | 2001-03-29 | 2002-10-02 | Fischer Artur Werke Gmbh | Mehrkomponentenkits und Kombinationen, ihre Verwendung und erhältliche Kunstmörtel |
| DE10226613B4 (de) * | 2002-06-14 | 2007-05-16 | Hilti Ag | Härterkomponente für eine mindestens zweikomponentige Mörtelmasse und Verfahren zu ihrer Herstellung |
| EP1674495A1 (en) | 2004-12-22 | 2006-06-28 | Huntsman Advanced Materials (Switzerland) GmbH | Coating system |
| CA2614050C (en) * | 2006-12-21 | 2015-04-21 | Hilti Aktiengesellschaft | Two-component reaction resin and method of fastening using the resin |
| JP5598934B2 (ja) | 2009-03-25 | 2014-10-01 | ディーエスエム アイピー アセッツ ビー．ブイ． | ビニルエステル樹脂組成物 |
| ES2382766T3 (es) * | 2009-11-30 | 2012-06-13 | Hilti Aktiengesellschaft | Composición de mortero de dos componentes adecuada para fines de construcción, su uso y objetos estructurales curados obtenidos mediante la misma |
| EP2357162B1 (en) | 2010-02-11 | 2012-09-05 | HILTI Aktiengesellschaft | Resin mortar suitable for construction purposes, especially for chemical anchoring |
| GB201006368D0 (en) | 2010-04-15 | 2010-06-02 | Phosphonics Ltd | Functionalised materials and uses thereof |
| DE102010051818B3 (de) * | 2010-11-18 | 2012-02-16 | Hilti Aktiengesellschaft | Zweikomponenten-Mörtelmasse und ihre Verwendung |
| DE102011077254B3 (de) * | 2011-06-09 | 2012-09-20 | Hilti Aktiengesellschaft | Verwendung einer Inhibitorkombination, Harzmischung, Reaktionsharzmörtel, Zweikomponenten - Mörtelsystem und dessen Verwendung sowie Patrone, Kartusche oder Folienbeutel enthaltend ein Zweikomponenten - Mörtelsystem |
| DE102011077248B3 (de) | 2011-06-09 | 2012-09-27 | Hilti Aktiengesellschaft | Verwendung eines Inhibitors, Harzmischung, Reaktionsharzmörtel, Zweikomponenten - Mörtelsystem und dessen Verwendung sowie Patrone, Kartusche oder Folienbeutel enthaltend ein Zweikomponenten - Mörtelsystem |
-
2013
- 2013-04-22 EP EP13164652.3A patent/EP2796433A1/de not_active Withdrawn
-
2014
- 2014-04-22 ES ES14718608.4T patent/ES2623898T3/es active Active
- 2014-04-22 WO PCT/EP2014/058065 patent/WO2014173864A1/de active Application Filing
- 2014-04-22 EP EP14718608.4A patent/EP2989061B1/de active Active
- 2014-04-22 CA CA2910230A patent/CA2910230C/en active Active
-
2015
- 2015-10-22 US US14/920,595 patent/US20160039960A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| EP2989061A1 (de) | 2016-03-02 |
| WO2014173864A1 (de) | 2014-10-30 |
| EP2989061B1 (de) | 2017-02-01 |
| CA2910230A1 (en) | 2014-10-30 |
| EP2796433A1 (de) | 2014-10-29 |
| CA2910230C (en) | 2016-08-16 |
| US20160039960A1 (en) | 2016-02-11 |
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