ES2199683B1 - Procedimiento de separacion o extraccion con fluidos supercriticos asistidos por ultrasonidos de alta intensidad. - Google Patents

Procedimiento de separacion o extraccion con fluidos supercriticos asistidos por ultrasonidos de alta intensidad.

Info

Publication number
ES2199683B1
ES2199683B1 ES200201822A ES200201822A ES2199683B1 ES 2199683 B1 ES2199683 B1 ES 2199683B1 ES 200201822 A ES200201822 A ES 200201822A ES 200201822 A ES200201822 A ES 200201822A ES 2199683 B1 ES2199683 B1 ES 2199683B1
Authority
ES
Spain
Prior art keywords
separation
supercritical fluids
assisted
high intensity
relates
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
ES200201822A
Other languages
English (en)
Other versions
ES2199683A1 (es
Inventor
Enrique F. Riera Franco De Sarabia
Juan Antonio Gallego Juarez
Fausto Montoya Vitini
Alfonso Blanco Blanco
Antonio Mulet Pons
Jose J. Benedito Fort
Ramon Peña Cervero
Yolanda Golas Sanchez
Angel Berna Prats
Sebastian Subirats Huerta
Miguel Blasco Piquer
Jose Garcia Reverter
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ASOCIACION DE INVESTIGACION de la INDUSTRIA AGROAL
Original Assignee
Consejo Superior de Investigaciones Cientificas CSIC
Universidad Politecnica de Valencia
Asociacion de Investigacion de la Industria Agroalimentaria AINIA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Consejo Superior de Investigaciones Cientificas CSIC, Universidad Politecnica de Valencia, Asociacion de Investigacion de la Industria Agroalimentaria AINIA filed Critical Consejo Superior de Investigaciones Cientificas CSIC
Priority to ES200201822A priority Critical patent/ES2199683B1/es
Priority to AT03766422T priority patent/ATE510616T1/de
Priority to EP03766422A priority patent/EP1547679B1/en
Priority to AU2003254516A priority patent/AU2003254516A1/en
Priority to PCT/ES2003/000398 priority patent/WO2004012859A1/es
Publication of ES2199683A1 publication Critical patent/ES2199683A1/es
Application granted granted Critical
Publication of ES2199683B1 publication Critical patent/ES2199683B1/es
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/10—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing sonic or ultrasonic vibrations
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0203—Solvent extraction of solids with a supercritical fluid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0261—Solvent extraction of solids comprising vibrating mechanisms, e.g. mechanical, acoustical
    • B01D11/0265—Applying ultrasound
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/008—Processes carried out under supercritical conditions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/10—Production of fats or fatty oils from raw materials by extracting
    • C11B1/104—Production of fats or fatty oils from raw materials by extracting using super critical gases or vapours
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/10—Production of fats or fatty oils from raw materials by extracting
    • C11B1/106—Production of fats or fatty oils from raw materials by extracting using ultra-sounds
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

Abstract

Procedimiento para procesos de separación o extracción con fluidos supercríticos asistidos por ultrasonidos de alta intensidad. El procedimiento de la presente invención propone la aplicación de los ultrasonidos de alta intensidad para acelerar y mejorar la eficiencia del proceso de transferencia de materia en fluidos supercríticos, basado en el proceso de separación por contacto de una sustancia que contiene los componentes extraibles con un solvente en condiciones supercríticas o cercanas al punto crítico. Para la aplicación de este procedimiento se ha desarrollado un dispositivo basado en la generación de un campo ultrasónico estacionario intenso en el interior de un recipiente a presión convencional para fluidos supercríticos, y que forma parte de la presente invención. Finalmente, forma parte de la presente invención el uso del procedimiento descrito para la separación ó extracción de productos naturales de utilidad en campos, entre otros, como el agroalimentario, químico, cosmético yfarmacéutico.
ES200201822A 2002-08-01 2002-08-01 Procedimiento de separacion o extraccion con fluidos supercriticos asistidos por ultrasonidos de alta intensidad. Expired - Fee Related ES2199683B1 (es)

Priority Applications (5)

Application Number Priority Date Filing Date Title
ES200201822A ES2199683B1 (es) 2002-08-01 2002-08-01 Procedimiento de separacion o extraccion con fluidos supercriticos asistidos por ultrasonidos de alta intensidad.
AT03766422T ATE510616T1 (de) 2002-08-01 2003-07-31 Trenn- oder extraktionsverfahren unter verwendung von superkritischen fluiden mit unterst tzung durch hochintensitutsultraschall
EP03766422A EP1547679B1 (en) 2002-08-01 2003-07-31 Separation or extraction method using supercritical fluids assisted by high-intensity ultrasound
AU2003254516A AU2003254516A1 (en) 2002-08-01 2003-07-31 Separation or extraction method using supercritical fluids assisted by high-intensity ultrasound
PCT/ES2003/000398 WO2004012859A1 (es) 2002-08-01 2003-07-31 Procedimiento de separación o extracción con fluidos supercríticos asistidos por ultrasonidos de alta intensidad

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
ES200201822A ES2199683B1 (es) 2002-08-01 2002-08-01 Procedimiento de separacion o extraccion con fluidos supercriticos asistidos por ultrasonidos de alta intensidad.

Publications (2)

Publication Number Publication Date
ES2199683A1 ES2199683A1 (es) 2004-02-16
ES2199683B1 true ES2199683B1 (es) 2005-06-01

Family

ID=31198115

Family Applications (1)

Application Number Title Priority Date Filing Date
ES200201822A Expired - Fee Related ES2199683B1 (es) 2002-08-01 2002-08-01 Procedimiento de separacion o extraccion con fluidos supercriticos asistidos por ultrasonidos de alta intensidad.

Country Status (5)

Country Link
EP (1) EP1547679B1 (es)
AT (1) ATE510616T1 (es)
AU (1) AU2003254516A1 (es)
ES (1) ES2199683B1 (es)
WO (1) WO2004012859A1 (es)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7846341B2 (en) 2006-12-04 2010-12-07 Bacoustics, Llc Method of ultrasonically treating a continuous flow of fluid
ES2395819B1 (es) * 2011-06-29 2014-06-06 Universidad Politécnica De Valencia Procedimiento de inactivación de microorganismos mediante la combinación de fluidos supercríticos y ultrasonidos
GB201317864D0 (en) * 2013-10-09 2013-11-20 Univ Birmingham Inhibition of microbial and cellular growth in substances
FR3025115B1 (fr) * 2014-09-03 2018-12-07 Commissariat A L'energie Atomique Et Aux Energies Alternatives Procede d'extraction selectif de platinoides, a partir d'un support les contenant, avec un milieu d'extraction comprenant un fluide supercritique et un ligand organique.
IT201900020630A1 (it) * 2019-11-08 2021-05-08 Univ Degli Studi Genova Processo e sistema per l’estrazione di molecole da matrici solide particellari
CN115430176A (zh) * 2022-10-14 2022-12-06 江苏黎明食品集团有限公司 一种黑蒜口服液生产用提取装置及其提取方法

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AT389235B (de) * 1987-05-19 1989-11-10 Stuckart Wolfgang Verfahren zur reinigung von fluessigkeiten mittels ultraschall und vorrichtungen zur durchfuehrung dieses verfahrens
DE19539533A1 (de) * 1995-10-24 1997-04-30 Basf Ag Apparat zur Schallbehandlung von Produkten
US6620351B2 (en) * 2000-05-24 2003-09-16 Auburn University Method of forming nanoparticles and microparticles of controllable size using supercritical fluids with enhanced mass transfer
FR2832703B1 (fr) * 2001-11-29 2005-01-14 Electricite De France Dispositif sono-electrochimique et procede sono-electrochimique de degradation de molecules organiques
FR2833618B1 (fr) * 2001-12-17 2005-02-11 Shamy Sayed El Reacteur electrochimique-filtre a cartouche de construction polygene combinable
US7128840B2 (en) * 2002-03-26 2006-10-31 Idaho Research Foundation, Inc. Ultrasound enhanced process for extracting metal species in supercritical fluids

Also Published As

Publication number Publication date
ATE510616T1 (de) 2011-06-15
AU2003254516A8 (en) 2004-02-23
EP1547679B1 (en) 2011-05-25
AU2003254516A1 (en) 2004-02-23
EP1547679A1 (en) 2005-06-29
ES2199683A1 (es) 2004-02-16
WO2004012859A1 (es) 2004-02-12

Similar Documents

Publication Publication Date Title
DE50112925D1 (de) Vorrichtung und Verfahren zur Aufnahme und/oder Abgabe von Flüssigkeitsproben
DE60011253D1 (de) Vorrichtung und verfahren zur ultraschall-lyse biologischer zellen
AU2002359620A1 (en) Consolidated body fluid testing device and method
DE50100406D1 (de) Vorrichtung zur Aufnahme und Abgabe von Flüssigkeitsproben
NO20025611D0 (no) Fremgangsmåte og anordning til steking av produkter
MXPA03008316A (es) Metodo y sistema para remover gas disuelto de una solucion.
ES2199683B1 (es) Procedimiento de separacion o extraccion con fluidos supercriticos asistidos por ultrasonidos de alta intensidad.
AU2002311798A1 (en) Granulation method and device using focused acoustic energy
ES2040004T3 (es) Procedimiento y dispositivo para la evacuacion de medios liquidos con residuos de produccion.
FR2760533B1 (fr) Appareil et procede de caracterisation de liquides
WO2004020078A8 (en) Method and apparatus for mixing liquid samples using a sinusoidal mixing action
DE69726828D1 (de) Verfahren und Vorrichtung zum Testen einer mit einem Arbeitsfluidum und einem Treibmittel gefüllten Verpackung
EE05101B1 (et) Seade ja meetod vedelike t””tlemiseks ultraheliga
Luo et al. An experimental study on the coalescence process of binary droplets in oil under ultrasonic standing waves
NO20076470L (no) Fremgangsmate og anordning for a registrere en temperaturokning i en kjoler
WO2003057310A3 (en) Liquid sample processing apparatus and method
ATE343964T1 (de) Verfahren und vorrichtung zur blutdruckmessung
FR2829404B1 (fr) Appareil automatique pour la synthese de petites molecules organiques et procede de synthese mettant en oeuvre cet appareil
KR100819779B1 (ko) 순간고온스팀법을 이용한 잠재지문 채취방법
DE60004006D1 (de) Verfahren und vorrichtung zum öffnen eines beutels
BR8108937A (pt) Metodo e dispositivo para marcar o tempo em processos de sedimentacao
AU2003246512A1 (en) Method and device for soil analysis
Hadi et al. The development of interactive multimedia learning pyramid and prism for junior high school using macromedia authorware
Agani Quizizz as Media of Formative Assessment in EFL Learning: Its Effect on Vocabulary, Grammar, and Reading Comprehension
Rotondi et al. A new underwater laser cleaning tool for large bronze artefacts

Legal Events

Date Code Title Description
EC2A Search report published

Date of ref document: 20040216

Kind code of ref document: A1

GC2A Exploitation certificate registered application with search report

Effective date: 20130709

PC2A Transfer of patent

Owner name: ASOCIACION DE INVESTIGACION DE LA INDUSTRIA AGROAL

Effective date: 20130712

FD2A Announcement of lapse in spain

Effective date: 20220826