ES2196041T3 - Procedimiento de purificacion de polieterpolioles mediante catalizadores de cianuro de doble metal. - Google Patents
Procedimiento de purificacion de polieterpolioles mediante catalizadores de cianuro de doble metal.Info
- Publication number
- ES2196041T3 ES2196041T3 ES95300349T ES95300349T ES2196041T3 ES 2196041 T3 ES2196041 T3 ES 2196041T3 ES 95300349 T ES95300349 T ES 95300349T ES 95300349 T ES95300349 T ES 95300349T ES 2196041 T3 ES2196041 T3 ES 2196041T3
- Authority
- ES
- Spain
- Prior art keywords
- polyol
- metal cyanide
- double metal
- mixt
- polyeterpoliols
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000003054 catalyst Substances 0.000 title abstract 4
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 title abstract 2
- 229910052751 metal Inorganic materials 0.000 title abstract 2
- 239000002184 metal Substances 0.000 title abstract 2
- 238000000034 method Methods 0.000 title 1
- 238000000746 purification Methods 0.000 title 1
- 229920005862 polyol Polymers 0.000 abstract 6
- 150000003077 polyols Chemical class 0.000 abstract 5
- -1 poly(oxypropylene) Polymers 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- HCWCAKKEBCNQJP-UHFFFAOYSA-N magnesium orthosilicate Chemical compound [Mg+2].[Mg+2].[O-][Si]([O-])([O-])[O-] HCWCAKKEBCNQJP-UHFFFAOYSA-N 0.000 abstract 1
- 229910052919 magnesium silicate Inorganic materials 0.000 abstract 1
- 235000019792 magnesium silicate Nutrition 0.000 abstract 1
- 239000000391 magnesium silicate Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2645—Metals or compounds thereof, e.g. salts
- C08G65/2663—Metal cyanide catalysts, i.e. DMC's
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/30—Post-polymerisation treatment, e.g. recovery, purification, drying
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Toxicology (AREA)
- Polyethers (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/187,955 US5416241A (en) | 1994-01-27 | 1994-01-27 | Method for purifying polyether polyols made with double metal cyanide catalysts |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2196041T3 true ES2196041T3 (es) | 2003-12-16 |
Family
ID=22691183
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES95300349T Expired - Lifetime ES2196041T3 (es) | 1994-01-27 | 1995-01-20 | Procedimiento de purificacion de polieterpolioles mediante catalizadores de cianuro de doble metal. |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US5416241A (OSRAM) |
| EP (1) | EP0665254B1 (OSRAM) |
| JP (1) | JP3281500B2 (OSRAM) |
| AT (1) | ATE237652T1 (OSRAM) |
| CA (1) | CA2140499C (OSRAM) |
| DE (1) | DE69530331T2 (OSRAM) |
| DK (1) | DK0665254T3 (OSRAM) |
| ES (1) | ES2196041T3 (OSRAM) |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5844070A (en) * | 1997-05-16 | 1998-12-01 | Arco Chemical Technology, L.P. | Process for rapid activation of double metal cyanide catalysts |
| DE19903274A1 (de) | 1999-01-28 | 2000-08-03 | Basf Ag | Verfahren zur Herstellung von Polyetherpolyolen |
| US6613714B2 (en) | 1999-06-02 | 2003-09-02 | Basf Aktiengesellschaft | Multimetal cyanide compounds, their preparation and their use |
| US6800583B2 (en) | 1999-06-02 | 2004-10-05 | Basf Aktiengesellschaft | Suspension of multimetal cyanide compounds, their preparation and their use |
| EP1370600B1 (de) * | 2000-11-22 | 2004-10-13 | Basf Aktiengesellschaft | Verfahren zur aufarbeitung von polyetheralkoholen |
| DE10137628A1 (de) * | 2001-08-03 | 2003-02-27 | Basf Ag | Verfahren zur Herstellung von Polyurethan-Weichschaumstoffen |
| ES2199666B1 (es) * | 2002-02-25 | 2005-06-01 | Repsol Quimica, S.A. | Procedimiento de produccion de polioleteres. |
| EP1493769B1 (en) * | 2003-06-30 | 2007-11-21 | Repsol Quimica S.A. | Process to purify polyether polyols |
| CN102574977B (zh) * | 2009-09-30 | 2013-12-11 | 旭硝子株式会社 | 异氰酸酯基末端预聚物的制造方法以及由此获得的预聚物及聚氨酯树脂 |
| US20110319669A1 (en) | 2010-06-29 | 2011-12-29 | Wanglin Yu | Branched secondary alcohol alkoxylate surfactants and process to make them |
| US20130231508A1 (en) | 2010-11-23 | 2013-09-05 | Dow Global Technologies Llc | Branched secondary alcohol alkoxylate surfactants and process to make them |
| US9527958B2 (en) * | 2014-05-02 | 2016-12-27 | Covestro Llc | Process for purification of polyether carbonate polyols |
| KR101867721B1 (ko) | 2016-12-16 | 2018-06-14 | 주식회사 포스코 | 폴리에테르 카보네이트 폴리올 제조공정에서의 프로필렌 카보네이트의 분리방법 |
| US20190119444A1 (en) | 2017-10-25 | 2019-04-25 | Covestro Llc | Process to remove dmc catalysts from polyether carbonate polyols |
| EP3567067A1 (de) | 2018-05-08 | 2019-11-13 | Covestro Deutschland AG | Abtrennung von doppelmetallcyanid-katalysator |
| EP3927791A1 (en) | 2019-02-19 | 2021-12-29 | Dow Global Technologies LLC | Enhanced crude oil recovery from subterranean crude oil-bearing sandstone reservoirs |
| WO2022015638A1 (en) | 2020-07-17 | 2022-01-20 | Dow Global Technologies Llc | Polyurethanes with reduced cobalt extractables |
| KR102682351B1 (ko) | 2022-05-30 | 2024-07-08 | 고등기술연구원연구조합 | 역유동 장치 및 이를 이용한 폴리에테르 카보네이트 폴리올의 정제 방법 |
| US12515212B2 (en) | 2022-10-12 | 2026-01-06 | Covestro Llc | Processes for purifying polyether polyols using ion exchange resins |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3278457A (en) * | 1963-02-14 | 1966-10-11 | Gen Tire & Rubber Co | Method of making a polyether using a double metal cyanide complex compound |
| US3829505A (en) * | 1970-02-24 | 1974-08-13 | Gen Tire & Rubber Co | Polyethers and method for making the same |
| US4029879A (en) * | 1975-11-17 | 1977-06-14 | Basf Wyandotte Corporation | Process for the removal of catalysts from polyether polyols employing water and adsorbent |
| CA1155871A (en) * | 1980-10-16 | 1983-10-25 | Gencorp Inc. | Method for treating polypropylene ether and poly-1,2- butylene ether polyols |
| US4721818A (en) * | 1987-03-20 | 1988-01-26 | Atlantic Richfield Company | Purification of polyols prepared using double metal cyanide complex catalysts |
| US4877906A (en) * | 1988-11-25 | 1989-10-31 | Arco Chemical Technology, Inc. | Purification of polyols prepared using double metal cyanide complex catalysts |
| US4987271A (en) * | 1989-02-17 | 1991-01-22 | Asahi Glass Company, Ltd. | Method for purifying a polyoxyalkylene alcohol |
| US5010047A (en) * | 1989-02-27 | 1991-04-23 | Arco Chemical Technology, Inc. | Recovery of double metal cyanide complex catalyst from a polymer |
| JP2745664B2 (ja) * | 1989-04-07 | 1998-04-28 | 旭硝子株式会社 | ポリエーテル類の製造方法 |
| DE3913937A1 (de) * | 1989-04-27 | 1990-10-31 | Hoechst Ag | Verfahren zur reinigung von alkylenoxid-addukten |
| US4994627A (en) * | 1990-03-16 | 1991-02-19 | Texaco Chemical Company | Purification of polyoxyalkylene glycols |
| US5099075A (en) * | 1990-11-02 | 1992-03-24 | Olin Corporation | Process for removing double metal cyanide catalyst residues from a polyol |
| JPH04214722A (ja) * | 1990-12-14 | 1992-08-05 | Asahi Glass Co Ltd | ポリエーテル類の製造方法 |
| US5144093A (en) * | 1991-04-29 | 1992-09-01 | Olin Corporation | Process for purifying and end-capping polyols made using double metal cyanide catalysts |
| US5235114A (en) * | 1991-04-29 | 1993-08-10 | Olin Corporation | Process for purifying and end-capping polyols made using double metal cyanide catalysts |
| US5248883A (en) * | 1991-05-30 | 1993-09-28 | International Business Machines Corporation | Ion traps of mono- or multi-planar geometry and planar ion trap devices |
| US5266681A (en) * | 1992-08-03 | 1993-11-30 | Olin Corporation | Process and composition for providing double metal cyanide catalyzed polyols having enhanced reactivity |
-
1994
- 1994-01-27 US US08/187,955 patent/US5416241A/en not_active Expired - Fee Related
-
1995
- 1995-01-18 CA CA002140499A patent/CA2140499C/en not_active Expired - Fee Related
- 1995-01-20 DE DE69530331T patent/DE69530331T2/de not_active Expired - Fee Related
- 1995-01-20 AT AT95300349T patent/ATE237652T1/de not_active IP Right Cessation
- 1995-01-20 ES ES95300349T patent/ES2196041T3/es not_active Expired - Lifetime
- 1995-01-20 DK DK95300349T patent/DK0665254T3/da active
- 1995-01-20 EP EP95300349A patent/EP0665254B1/en not_active Expired - Lifetime
- 1995-01-25 JP JP02772395A patent/JP3281500B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| EP0665254A3 (en) | 1996-02-28 |
| JPS352492B1 (OSRAM) | 1960-03-18 |
| DE69530331T2 (de) | 2003-10-23 |
| JPH07238161A (ja) | 1995-09-12 |
| JP3281500B2 (ja) | 2002-05-13 |
| EP0665254B1 (en) | 2003-04-16 |
| DE69530331D1 (de) | 2003-05-22 |
| DK0665254T3 (da) | 2003-07-28 |
| US5416241A (en) | 1995-05-16 |
| EP0665254A2 (en) | 1995-08-02 |
| CA2140499A1 (en) | 1995-07-28 |
| CA2140499C (en) | 2005-09-06 |
| ATE237652T1 (de) | 2003-05-15 |
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