ES2142650T3 - Procedimiento para la obtencion de 4-amino-2,2,6,6-tetrametilpiperidina (tad) a traves del producto intermedio 2,2,6,6-tetrametil-4-((2,2,6,6-tetrametil-4-piperidiliden)amino)-piperidina. - Google Patents
Procedimiento para la obtencion de 4-amino-2,2,6,6-tetrametilpiperidina (tad) a traves del producto intermedio 2,2,6,6-tetrametil-4-((2,2,6,6-tetrametil-4-piperidiliden)amino)-piperidina.Info
- Publication number
- ES2142650T3 ES2142650T3 ES97118719T ES97118719T ES2142650T3 ES 2142650 T3 ES2142650 T3 ES 2142650T3 ES 97118719 T ES97118719 T ES 97118719T ES 97118719 T ES97118719 T ES 97118719T ES 2142650 T3 ES2142650 T3 ES 2142650T3
- Authority
- ES
- Spain
- Prior art keywords
- tetrametil
- amino
- tad
- piperidine
- procedure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title abstract 3
- -1 AMINO Chemical class 0.000 title 1
- 239000013067 intermediate product Substances 0.000 title 1
- 150000002466 imines Chemical class 0.000 abstract 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- NQRYJNQNLNOLGT-UHFFFAOYSA-N tetrahydropyridine hydrochloride Natural products C1CCNCC1 NQRYJNQNLNOLGT-UHFFFAOYSA-N 0.000 abstract 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical class [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 238000005984 hydrogenation reaction Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D211/00—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings
- C07D211/04—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D211/68—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member
- C07D211/72—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member with hetero atoms or with carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, directly attached to ring carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D211/00—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings
- C07D211/04—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D211/06—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members
- C07D211/36—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D211/56—Nitrogen atoms
- C07D211/58—Nitrogen atoms attached in position 4
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Hydrogenated Pyridines (AREA)
Abstract
COMO ALTERNATIVA A PROCEDIMIENTOS CONOCIDOS SE DESCRIBE UN PROCEDIMIENTO PARA LA PRODUCCION DE 4 - AMINO - 2,2,6,6 TETRAMETIL - PIPERIDINA (TAD) DE FORMULA I, QUE COMPRENDE UNA SERIE DE FASES. EN UNA PRIMERA FASE SE HACE REACCIONAR 2,2,6,6 - TETRAMETIL - PIPERIDIN - 4 - ONA (TAA) DE FORMULA II, CON TAD HASTA OBTENER 2,2,6,6 - TETRAMETIL - 4 - [(2,2,6,6 TETRAMETIL - 4 - PIPERIDILIDENO) AMINO] - PIPERIDINA (IMINA III) SEGUN LA FORMULA III SIGUIENTE, Y DEJANDO QUE LA IMINA (III) REACCIONE, EN OTRA FASE, EN PRESENCIA DE UN CATALIZADOR DE HIDROGENACION CON AMONIACO E HIDROGENO HASTA OBTENER 2 EQUIVALENTES MOLARES TAD.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19644770A DE19644770A1 (de) | 1996-10-28 | 1996-10-28 | Verfahren zur Herstellung von 4-Amino-2,2,6,6-tetramethylpiperidin (TAD) über das Zwischenprodukt 2,2,6,6-Tetramethyl-4-[(2,2,6,6-tetramethyl-4-piperidyliden)-amino]-piperidin |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2142650T3 true ES2142650T3 (es) | 2000-04-16 |
Family
ID=7810219
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES97118719T Expired - Lifetime ES2142650T3 (es) | 1996-10-28 | 1997-10-28 | Procedimiento para la obtencion de 4-amino-2,2,6,6-tetrametilpiperidina (tad) a traves del producto intermedio 2,2,6,6-tetrametil-4-((2,2,6,6-tetrametil-4-piperidiliden)amino)-piperidina. |
Country Status (5)
Country | Link |
---|---|
US (1) | US5859250A (es) |
EP (1) | EP0838456B1 (es) |
JP (1) | JPH10130237A (es) |
DE (2) | DE19644770A1 (es) |
ES (1) | ES2142650T3 (es) |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3003843A1 (de) * | 1980-02-02 | 1981-08-13 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur herstellung von 4-amino-2,2,6,6-tetramethylpiperidin |
CH664361A5 (de) * | 1985-06-13 | 1988-02-29 | Ni Institutkhimikatov Dlya Pol | Verfahren zur herstellung von 4-amino-2,2,6,6-tetramethylpiperidin. |
IT1216560B (it) * | 1988-04-07 | 1990-03-08 | Ciba Geigy Spa | Procedimento per la preparazione di bis(2,2,6,6_tetrametil_4_piperidil)ammina. |
DE4442990A1 (de) * | 1994-12-02 | 1996-06-05 | Huels Chemische Werke Ag | Verfahren zur Herstellung von 4-Amino-2,2,6,6-tetramethylpiperidin |
-
1996
- 1996-10-28 DE DE19644770A patent/DE19644770A1/de not_active Withdrawn
-
1997
- 1997-10-28 ES ES97118719T patent/ES2142650T3/es not_active Expired - Lifetime
- 1997-10-28 JP JP9295441A patent/JPH10130237A/ja not_active Withdrawn
- 1997-10-28 EP EP97118719A patent/EP0838456B1/de not_active Expired - Lifetime
- 1997-10-28 US US08/959,165 patent/US5859250A/en not_active Expired - Fee Related
- 1997-10-28 DE DE59700961T patent/DE59700961D1/de not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
EP0838456B1 (de) | 2000-01-05 |
DE59700961D1 (de) | 2000-02-10 |
JPH10130237A (ja) | 1998-05-19 |
DE19644770A1 (de) | 1998-04-30 |
EP0838456A1 (de) | 1998-04-29 |
US5859250A (en) | 1999-01-12 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FG2A | Definitive protection |
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