ES2115167T3 - Un procedimiento para la produccion de zeolitas. - Google Patents
Un procedimiento para la produccion de zeolitas.Info
- Publication number
- ES2115167T3 ES2115167T3 ES94309545T ES94309545T ES2115167T3 ES 2115167 T3 ES2115167 T3 ES 2115167T3 ES 94309545 T ES94309545 T ES 94309545T ES 94309545 T ES94309545 T ES 94309545T ES 2115167 T3 ES2115167 T3 ES 2115167T3
- Authority
- ES
- Spain
- Prior art keywords
- reaction mixture
- templating agent
- zeolites
- mixture
- zeolite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000010457 zeolite Substances 0.000 title abstract 6
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 title abstract 5
- 239000011541 reaction mixture Substances 0.000 abstract 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 4
- 239000003795 chemical substances by application Substances 0.000 abstract 4
- 229910021536 Zeolite Inorganic materials 0.000 abstract 3
- 239000000203 mixture Substances 0.000 abstract 3
- 239000000377 silicon dioxide Substances 0.000 abstract 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract 1
- 229910052782 aluminium Inorganic materials 0.000 abstract 1
- 239000004411 aluminium Substances 0.000 abstract 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 1
- 238000001354 calcination Methods 0.000 abstract 1
- 229910052681 coesite Inorganic materials 0.000 abstract 1
- 229910052593 corundum Inorganic materials 0.000 abstract 1
- 229910052906 cristobalite Inorganic materials 0.000 abstract 1
- 239000013078 crystal Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 150000007529 inorganic bases Chemical class 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 235000012239 silicon dioxide Nutrition 0.000 abstract 1
- 229910052682 stishovite Inorganic materials 0.000 abstract 1
- 229910052905 tridymite Inorganic materials 0.000 abstract 1
- 229910001845 yogo sapphire Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/04—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof using at least one organic template directing agent, e.g. an ionic quaternary ammonium compound or an aminated compound
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/36—Pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
- C01B39/38—Type ZSM-5
- C01B39/40—Type ZSM-5 using at least one organic template directing agent
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S423/00—Chemistry of inorganic compounds
- Y10S423/22—MFI, e.g. ZSM-5. silicalite, LZ-241
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
ZEOLITAS QUE TIENEN UNA RELACION DE SIO2 A AL2O3 MAYOR DE 10, PARTICULARMENTE ZEOLITAS ZSM-5, SE PRODUCEN POR: (A) LA FORMACION DE UNA MEZCLA DE REACCION (1) QUE CONSTA DE UNA FUENTE DE SILICE, UNA FUENTE DE ALUMINIO UNA BASE INORGANICA Y UN AGENTE TEMPLADOR, Y EL AJUSTADOR DEL PH ENTRE 10,7-11,7; (B) CALENTAMIENTO DE LA MEZCLA DE REACCION A TRAVES DE LA CUAL SE FORMAN LOS CRISTALES (2) DE ZEOLITA; (C) SEPARACION DE LA ZEOLITA CRISTALIZADA (2) DESDE LA MEZCLA DE REACCION DEJANDO ATRAS UNA MEZCLA RESIDUAL (3) Y CALCINANDO LA ZEOLITA PARA DESCOMPONER EL COMPONENTE ORGANICO; (D) ADICION A LA MEZCLA RESIDUAL DE UN AGENTE TEMPLADOR EN UNA CANTIDAD DE MODO QUE SE FORME UNA MEZCLA DE REACCION (4) EN DONDE EL NIVEL DEL AGENTE TEMPLADOR ESTE COMO EN LA MEZCLA DE REACCION DEL PASO (A); Y (E) REPETIR LOS PASOS (A)-(D), CON LA MEZCLA DE REACCION (4) OBTENIDA EN EL PASO (D) SIRVIENDO COMO FUENTE PARA EL AGENTE TEMPLADOR DEL PASO (A) Y CADA UNO O MAS CICLOS, TRATANDO LA MEZCLA RESIDUAL DEL PASO (C) PARAREMOVER LA SALES DE ALLI.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IL108272A IL108272A (en) | 1994-01-05 | 1994-01-05 | Process for production of zeolites |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2115167T3 true ES2115167T3 (es) | 1998-06-16 |
Family
ID=11065672
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES94309545T Expired - Lifetime ES2115167T3 (es) | 1994-01-05 | 1994-12-20 | Un procedimiento para la produccion de zeolitas. |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US5624658A (es) |
| EP (1) | EP0662450B1 (es) |
| AT (1) | ATE164147T1 (es) |
| DE (1) | DE69409085T2 (es) |
| DK (1) | DK0662450T3 (es) |
| ES (1) | ES2115167T3 (es) |
| IL (1) | IL108272A (es) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB9600082D0 (en) * | 1996-01-04 | 1996-03-06 | Exxon Chemical Patents Inc | Molecular sieves and processes for their manufacture |
| US5637287A (en) * | 1996-02-02 | 1997-06-10 | Exxon Research & Engineering Company | Synthesis process for faujasite family zeolites using mother liquor recycle |
| KR0165014B1 (ko) * | 1996-03-11 | 1999-01-15 | 선우현범 | 섬유상 제올라이트 zsm-5 및 그 제조 방법 |
| US6132618A (en) * | 1998-04-16 | 2000-10-17 | Pq Corporation | System and method for waking a computer having a plurality of power resources from a system state using a data structure |
| TW526172B (en) * | 1999-06-30 | 2003-04-01 | Sumitomo Chemical Co | A process for producing pentacyl-type crystalline zeolites and a process for producing ε-caprolactam using the same |
| DE19939416A1 (de) * | 1999-08-20 | 2001-02-22 | Basf Ag | Verfahren zur Herstellung eines kristallinen, zeolithischen Feststoffs |
| DE19951781A1 (de) | 1999-10-27 | 2001-05-03 | Sued Chemie Ag | Verfahren zur Herstellung von synthetischen Zeolithen mit MFI-Struktur |
| US7098161B2 (en) * | 2000-10-20 | 2006-08-29 | Abb Lummus Global Inc. | Method of treating zeolite |
| US7585490B2 (en) | 2005-04-15 | 2009-09-08 | University Of Iowa Research Foundation | Synthesis and use of nanocrystalline zeolites |
| WO2008097481A1 (en) * | 2007-02-06 | 2008-08-14 | Exxonmobil Research And Engineering Company | Method of manufacturing m41s family molecular sieve |
| CN112939010B (zh) * | 2013-10-31 | 2024-01-09 | 庄信万丰股份有限公司 | Aei沸石合成 |
| WO2022076839A1 (en) * | 2020-10-08 | 2022-04-14 | Phillips 66 Company | Modified zsm-5 catalyst for converting light hydrocarbons to liquid fuels |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3228969A (en) * | 1962-04-30 | 1966-01-11 | Socony Mobil Oil Co Inc | Process for synthesizing a methylammonium crystalline zeolite |
| FR2398698A1 (fr) * | 1977-07-29 | 1979-02-23 | Ugine Kuhlmann | Procede industriel de fabrication en continu de zeolithe a |
| IT1165442B (it) * | 1979-01-26 | 1987-04-22 | Montedison Spa | Zeoliti di tipo a,ad elevato grado di cristallinita' e a granulometria fine e processo per la loro produzione |
| NZ193927A (en) * | 1979-06-11 | 1982-09-07 | Mobil Oil Corp | Continuous stream method of preparing crystalline zeolite |
| US4385042A (en) * | 1979-08-06 | 1983-05-24 | Mobil Oil Corporation | Continuous reaction/separation method for nucleated growth reactions |
| DE3325515A1 (de) * | 1983-07-15 | 1985-01-24 | Hoechst Ag, 6230 Frankfurt | Verfahren zur herstellung von aluminiumsilikaten mit zeolithstrukturen |
| US5143879A (en) * | 1991-07-18 | 1992-09-01 | Mobil Oil Corporation | Method to recover organic templates from freshly synthesized molecular sieves |
| US5194410A (en) * | 1991-11-15 | 1993-03-16 | Mobil Oil Corporation | Crystalline molecular sieve synthesis using quaternary ammonium-functionalized organosiliconate |
| US5227151A (en) * | 1991-11-15 | 1993-07-13 | Mobil Oil Corporation | Method of preparing silicoaluminophosphate compositions using a reagent containing both quaternary ammonium and silicon reactive sites in the same molecule |
-
1994
- 1994-01-05 IL IL108272A patent/IL108272A/en not_active IP Right Cessation
- 1994-12-20 DE DE69409085T patent/DE69409085T2/de not_active Expired - Fee Related
- 1994-12-20 ES ES94309545T patent/ES2115167T3/es not_active Expired - Lifetime
- 1994-12-20 DK DK94309545T patent/DK0662450T3/da active
- 1994-12-20 EP EP94309545A patent/EP0662450B1/en not_active Expired - Lifetime
- 1994-12-20 AT AT94309545T patent/ATE164147T1/de not_active IP Right Cessation
- 1994-12-28 US US08/365,613 patent/US5624658A/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| EP0662450B1 (en) | 1998-03-18 |
| DK0662450T3 (da) | 1999-01-11 |
| DE69409085D1 (de) | 1998-04-23 |
| EP0662450A1 (en) | 1995-07-12 |
| DE69409085T2 (de) | 1998-08-20 |
| ATE164147T1 (de) | 1998-04-15 |
| US5624658A (en) | 1997-04-29 |
| IL108272A0 (en) | 1994-04-12 |
| IL108272A (en) | 1998-02-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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