ES2090982T3 - Purificacion de 6-aminocapronitrilo. - Google Patents

Purificacion de 6-aminocapronitrilo.

Info

Publication number
ES2090982T3
ES2090982T3 ES93906065T ES93906065T ES2090982T3 ES 2090982 T3 ES2090982 T3 ES 2090982T3 ES 93906065 T ES93906065 T ES 93906065T ES 93906065 T ES93906065 T ES 93906065T ES 2090982 T3 ES2090982 T3 ES 2090982T3
Authority
ES
Spain
Prior art keywords
tha
aminocapronitrile
purification
heating
distilling
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES93906065T
Other languages
English (en)
Inventor
James Bernard Sieja
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Application granted granted Critical
Publication of ES2090982T3 publication Critical patent/ES2090982T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00Preparation of carboxylic acid nitriles
    • C07C253/32Separation; Purification; Stabilisation; Use of additives
    • C07C253/34Separation; Purification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

SE PRESENTA UN METODO DE PURIFICACION DEL 6-AMINOCAPRONITRILO CALENTANDO UNA MEZCLA QUE CONTENGA EL MISMO Y THA Y CONVIRTIENDO EL THA EN COMPUESTOS DE MAYOR EBULLICION, Y DESTILANDO ENTONCES EL 6AMINOCAPRONITRILO. EL TIEMPO REQUERIDO PARA CONVERTIR EL THA SE REDUCE SI EN LA MEZCLA ESTA PRESENTE UN COMPUESTO DE CARBONIL ORGANICO DURANTE EL CALENTAMIENTO.
ES93906065T 1992-02-27 1993-02-24 Purificacion de 6-aminocapronitrilo. Expired - Lifetime ES2090982T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US07/841,351 US5162567A (en) 1992-02-27 1992-02-27 Purification of 6-aminocapronitrile

Publications (1)

Publication Number Publication Date
ES2090982T3 true ES2090982T3 (es) 1996-10-16

Family

ID=25284651

Family Applications (1)

Application Number Title Priority Date Filing Date
ES93906065T Expired - Lifetime ES2090982T3 (es) 1992-02-27 1993-02-24 Purificacion de 6-aminocapronitrilo.

Country Status (10)

Country Link
US (1) US5162567A (es)
EP (1) EP0628025B1 (es)
JP (1) JP3289903B2 (es)
KR (1) KR100268689B1 (es)
BR (1) BR9305994A (es)
CA (1) CA2130915C (es)
DE (1) DE69304514T2 (es)
ES (1) ES2090982T3 (es)
MX (1) MX9301069A (es)
WO (1) WO1993016984A1 (es)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5312959A (en) * 1993-07-12 1994-05-17 E. I. Du Pont De Nemours And Company Purification of 2-methylglutaronitrile or adiponitrile
DE19517823A1 (de) * 1995-05-18 1996-11-21 Basf Ag Verfahren zur Herstellung von Caprolactam
FR2735471B1 (fr) * 1995-06-16 1997-08-22 Rhone Poulenc Chimie Procede de preparation de lactames
DE19704613A1 (de) 1997-02-07 1998-08-13 Basf Ag Verfahren zur Abtrennung von 6-Aminocapronsäurenitril aus Mischungen, die 6-Aminocapronsäurenitril und ein Imin enthalten
DE19704620A1 (de) 1997-02-07 1998-08-13 Basf Ag Verfahren zur Abtrennung von 6-Aminocapronitril aus Mischungen, die 6-Aminocapronitril und ein Imin enthalten
DE19704614A1 (de) * 1997-02-07 1998-08-13 Basf Ag Verfahren zur Abtrennnung eines Imins aus einer Mischung enthaltend ein Amin und ein Imin
DE19812427A1 (de) 1998-03-20 1999-09-23 Basf Ag Verfahren zur Abtrennung eines Azepin-Derivats aus einer Mischung enthaltend ein Amin und ein Azepin-Derivat
US5961788A (en) * 1998-10-09 1999-10-05 E. I. Du Pont De Nemours And Company Sequential distillation process for removing tetrahydroazepine from aminocapronitrile and/or hexamethylenediamine
DE10059716A1 (de) 2000-11-30 2002-06-06 Basf Ag Verfahren zur Reduzierung des Gehalts an einem ungesättigten Amin in einer Mischung enthaltend ein Amin und ein Nitril
DE10223827A1 (de) 2002-05-28 2003-12-11 Basf Ag Verfahren zur Reduzierung des Gehalts an einem ungesättigten Amin in einer Mischung enthaltend ein Aminonitril, ein Diamin, ein Dinitril oder deren Gemische
US6858728B2 (en) * 2003-06-17 2005-02-22 Invista North America S.A.R.L. Method for making caprolactam from impure ACN in which THA is not removed until after caprolactam is produced

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA601619A (en) * 1960-07-12 H. Ottenheym Johannes PROCESS FOR THE RECOVERY OF .omega.-AMINOCAPRONITRILE FROM MIXTURES OF .omega.-AMINOCAPRONITRILE,.omega.-CAPRONITRILE AND WATER
US2242309A (en) * 1938-03-23 1941-05-20 Du Pont Process for purifying nitriles
US3004059A (en) * 1958-02-11 1961-10-10 Degussa Process for the recovery of omega-aminonitriles
NL258960A (es) * 1959-12-15
US4601859A (en) * 1984-05-04 1986-07-22 Allied Corporation Selective hydrogenation of aliphatic dinitriles to omega-aminonitriles in ammonia with supported, finely dispersed rhodium-containing catalyst

Also Published As

Publication number Publication date
DE69304514T2 (de) 1997-03-27
WO1993016984A1 (en) 1993-09-02
DE69304514D1 (de) 1996-10-10
KR100268689B1 (ko) 2000-10-16
KR950700238A (ko) 1995-01-16
EP0628025B1 (en) 1996-09-04
BR9305994A (pt) 1997-10-21
CA2130915A1 (en) 1993-09-02
EP0628025A1 (en) 1994-12-14
JP3289903B2 (ja) 2002-06-10
US5162567A (en) 1992-11-10
JPH07504415A (ja) 1995-05-18
CA2130915C (en) 2004-05-18
MX9301069A (es) 1993-08-01

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