ES2090982T3 - Purificacion de 6-aminocapronitrilo. - Google Patents
Purificacion de 6-aminocapronitrilo.Info
- Publication number
- ES2090982T3 ES2090982T3 ES93906065T ES93906065T ES2090982T3 ES 2090982 T3 ES2090982 T3 ES 2090982T3 ES 93906065 T ES93906065 T ES 93906065T ES 93906065 T ES93906065 T ES 93906065T ES 2090982 T3 ES2090982 T3 ES 2090982T3
- Authority
- ES
- Spain
- Prior art keywords
- tha
- aminocapronitrile
- purification
- heating
- distilling
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/32—Separation; Purification; Stabilisation; Use of additives
- C07C253/34—Separation; Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
SE PRESENTA UN METODO DE PURIFICACION DEL 6-AMINOCAPRONITRILO CALENTANDO UNA MEZCLA QUE CONTENGA EL MISMO Y THA Y CONVIRTIENDO EL THA EN COMPUESTOS DE MAYOR EBULLICION, Y DESTILANDO ENTONCES EL 6AMINOCAPRONITRILO. EL TIEMPO REQUERIDO PARA CONVERTIR EL THA SE REDUCE SI EN LA MEZCLA ESTA PRESENTE UN COMPUESTO DE CARBONIL ORGANICO DURANTE EL CALENTAMIENTO.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/841,351 US5162567A (en) | 1992-02-27 | 1992-02-27 | Purification of 6-aminocapronitrile |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2090982T3 true ES2090982T3 (es) | 1996-10-16 |
Family
ID=25284651
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES93906065T Expired - Lifetime ES2090982T3 (es) | 1992-02-27 | 1993-02-24 | Purificacion de 6-aminocapronitrilo. |
Country Status (10)
Country | Link |
---|---|
US (1) | US5162567A (es) |
EP (1) | EP0628025B1 (es) |
JP (1) | JP3289903B2 (es) |
KR (1) | KR100268689B1 (es) |
BR (1) | BR9305994A (es) |
CA (1) | CA2130915C (es) |
DE (1) | DE69304514T2 (es) |
ES (1) | ES2090982T3 (es) |
MX (1) | MX9301069A (es) |
WO (1) | WO1993016984A1 (es) |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5312959A (en) * | 1993-07-12 | 1994-05-17 | E. I. Du Pont De Nemours And Company | Purification of 2-methylglutaronitrile or adiponitrile |
DE19517823A1 (de) * | 1995-05-18 | 1996-11-21 | Basf Ag | Verfahren zur Herstellung von Caprolactam |
FR2735471B1 (fr) * | 1995-06-16 | 1997-08-22 | Rhone Poulenc Chimie | Procede de preparation de lactames |
DE19704613A1 (de) | 1997-02-07 | 1998-08-13 | Basf Ag | Verfahren zur Abtrennung von 6-Aminocapronsäurenitril aus Mischungen, die 6-Aminocapronsäurenitril und ein Imin enthalten |
DE19704620A1 (de) | 1997-02-07 | 1998-08-13 | Basf Ag | Verfahren zur Abtrennung von 6-Aminocapronitril aus Mischungen, die 6-Aminocapronitril und ein Imin enthalten |
DE19704614A1 (de) * | 1997-02-07 | 1998-08-13 | Basf Ag | Verfahren zur Abtrennnung eines Imins aus einer Mischung enthaltend ein Amin und ein Imin |
DE19812427A1 (de) | 1998-03-20 | 1999-09-23 | Basf Ag | Verfahren zur Abtrennung eines Azepin-Derivats aus einer Mischung enthaltend ein Amin und ein Azepin-Derivat |
US5961788A (en) * | 1998-10-09 | 1999-10-05 | E. I. Du Pont De Nemours And Company | Sequential distillation process for removing tetrahydroazepine from aminocapronitrile and/or hexamethylenediamine |
DE10059716A1 (de) | 2000-11-30 | 2002-06-06 | Basf Ag | Verfahren zur Reduzierung des Gehalts an einem ungesättigten Amin in einer Mischung enthaltend ein Amin und ein Nitril |
DE10223827A1 (de) | 2002-05-28 | 2003-12-11 | Basf Ag | Verfahren zur Reduzierung des Gehalts an einem ungesättigten Amin in einer Mischung enthaltend ein Aminonitril, ein Diamin, ein Dinitril oder deren Gemische |
US6858728B2 (en) * | 2003-06-17 | 2005-02-22 | Invista North America S.A.R.L. | Method for making caprolactam from impure ACN in which THA is not removed until after caprolactam is produced |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA601619A (en) * | 1960-07-12 | H. Ottenheym Johannes | PROCESS FOR THE RECOVERY OF .omega.-AMINOCAPRONITRILE FROM MIXTURES OF .omega.-AMINOCAPRONITRILE,.omega.-CAPRONITRILE AND WATER | |
US2242309A (en) * | 1938-03-23 | 1941-05-20 | Du Pont | Process for purifying nitriles |
US3004059A (en) * | 1958-02-11 | 1961-10-10 | Degussa | Process for the recovery of omega-aminonitriles |
NL258960A (es) * | 1959-12-15 | |||
US4601859A (en) * | 1984-05-04 | 1986-07-22 | Allied Corporation | Selective hydrogenation of aliphatic dinitriles to omega-aminonitriles in ammonia with supported, finely dispersed rhodium-containing catalyst |
-
1992
- 1992-02-27 US US07/841,351 patent/US5162567A/en not_active Expired - Lifetime
-
1993
- 1993-02-24 JP JP51495693A patent/JP3289903B2/ja not_active Expired - Fee Related
- 1993-02-24 KR KR1019940702986A patent/KR100268689B1/ko not_active IP Right Cessation
- 1993-02-24 EP EP93906065A patent/EP0628025B1/en not_active Expired - Lifetime
- 1993-02-24 BR BR9305994A patent/BR9305994A/pt not_active IP Right Cessation
- 1993-02-24 CA CA002130915A patent/CA2130915C/en not_active Expired - Fee Related
- 1993-02-24 DE DE69304514T patent/DE69304514T2/de not_active Expired - Fee Related
- 1993-02-24 ES ES93906065T patent/ES2090982T3/es not_active Expired - Lifetime
- 1993-02-24 WO PCT/US1993/001460 patent/WO1993016984A1/en active IP Right Grant
- 1993-02-26 MX MX9301069A patent/MX9301069A/es not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
DE69304514T2 (de) | 1997-03-27 |
WO1993016984A1 (en) | 1993-09-02 |
DE69304514D1 (de) | 1996-10-10 |
KR100268689B1 (ko) | 2000-10-16 |
KR950700238A (ko) | 1995-01-16 |
EP0628025B1 (en) | 1996-09-04 |
BR9305994A (pt) | 1997-10-21 |
CA2130915A1 (en) | 1993-09-02 |
EP0628025A1 (en) | 1994-12-14 |
JP3289903B2 (ja) | 2002-06-10 |
US5162567A (en) | 1992-11-10 |
JPH07504415A (ja) | 1995-05-18 |
CA2130915C (en) | 2004-05-18 |
MX9301069A (es) | 1993-08-01 |
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