EP4357575A1 - Déformation in situ de structures de support pour unités de verre isolant sous vide - Google Patents

Déformation in situ de structures de support pour unités de verre isolant sous vide Download PDF

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Publication number
EP4357575A1
EP4357575A1 EP22202420.0A EP22202420A EP4357575A1 EP 4357575 A1 EP4357575 A1 EP 4357575A1 EP 22202420 A EP22202420 A EP 22202420A EP 4357575 A1 EP4357575 A1 EP 4357575A1
Authority
EP
European Patent Office
Prior art keywords
support structures
gap
support structure
glass sheet
present disclosure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
EP22202420.0A
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German (de)
English (en)
Inventor
Simon Johnsen
Annette Johncock KRISKO
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
VKR Holding AS
Original Assignee
VKR Holding AS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by VKR Holding AS filed Critical VKR Holding AS
Priority to EP22202420.0A priority Critical patent/EP4357575A1/fr
Priority to PCT/EP2023/077727 priority patent/WO2024083528A1/fr
Priority to PCT/EP2023/077733 priority patent/WO2024083530A1/fr
Priority to PCT/EP2023/077728 priority patent/WO2024083529A1/fr
Priority to PCT/EP2023/077719 priority patent/WO2024083526A1/fr
Publication of EP4357575A1 publication Critical patent/EP4357575A1/fr
Pending legal-status Critical Current

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Classifications

    • E—FIXED CONSTRUCTIONS
    • E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
    • E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
    • E06B3/00—Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
    • E06B3/66—Units comprising two or more parallel glass or like panes permanently secured together
    • E06B3/6612—Evacuated glazing units
    • E—FIXED CONSTRUCTIONS
    • E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
    • E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
    • E06B3/00—Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
    • E06B3/66—Units comprising two or more parallel glass or like panes permanently secured together
    • E06B3/663—Elements for spacing panes
    • E06B3/66304—Discrete spacing elements, e.g. for evacuated glazing units
    • E—FIXED CONSTRUCTIONS
    • E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
    • E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
    • E06B3/00—Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
    • E06B3/66—Units comprising two or more parallel glass or like panes permanently secured together
    • E06B3/673—Assembling the units
    • E06B3/67326—Assembling spacer elements with the panes
    • E06B3/6733—Assembling spacer elements with the panes by applying, e.g. extruding, a ribbon of hardenable material on or between the panes
    • E—FIXED CONSTRUCTIONS
    • E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
    • E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
    • E06B3/00—Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
    • E06B3/66—Units comprising two or more parallel glass or like panes permanently secured together
    • E06B3/673—Assembling the units
    • E06B3/67326—Assembling spacer elements with the panes
    • E06B3/67334—Assembling spacer elements with the panes by soldering; Preparing the panes therefor
    • E—FIXED CONSTRUCTIONS
    • E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
    • E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
    • E06B3/00—Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
    • E06B3/66—Units comprising two or more parallel glass or like panes permanently secured together
    • E06B3/673—Assembling the units
    • E06B3/67365—Transporting or handling panes, spacer frames or units during assembly
    • E06B3/67369—Layout of the assembly streets
    • E—FIXED CONSTRUCTIONS
    • E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
    • E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
    • E06B3/00—Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
    • E06B3/66—Units comprising two or more parallel glass or like panes permanently secured together
    • E06B3/673—Assembling the units
    • E06B3/67365—Transporting or handling panes, spacer frames or units during assembly
    • E06B3/67386—Presses; Clamping means holding the panes during assembly
    • E—FIXED CONSTRUCTIONS
    • E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
    • E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
    • E06B3/00—Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
    • E06B3/66—Units comprising two or more parallel glass or like panes permanently secured together
    • E06B3/677—Evacuating or filling the gap between the panes ; Equilibration of inside and outside pressure; Preventing condensation in the gap between the panes; Cleaning the gap between the panes
    • E06B3/6775—Evacuating or filling the gap during assembly
    • E—FIXED CONSTRUCTIONS
    • E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
    • E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
    • E06B3/00—Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
    • E06B3/66—Units comprising two or more parallel glass or like panes permanently secured together
    • E06B3/663—Elements for spacing panes
    • E06B3/66309—Section members positioned at the edges of the glazing unit
    • E06B3/66333—Section members positioned at the edges of the glazing unit of unusual substances, e.g. wood or other fibrous materials, glass or other transparent materials
    • E06B2003/66338—Section members positioned at the edges of the glazing unit of unusual substances, e.g. wood or other fibrous materials, glass or other transparent materials of glass

Definitions

  • the present disclosure relates to a method of producing a vacuum insulated glass unit, and to a vacuum insulated glass unit.
  • VIG units may provide superior heat insulation properties when compared to weight and material use of the unit.
  • a pump evacuates the gap before sealing the gap.
  • support structures also known as pillars or spacers, are distributed in the evacuated gap, often in a predefined pattern.
  • US 6, 689, 241 B1 discloses a solution where stainless steel balls are used as support structures/spacers in an evacuated gap of a VIG unit, where the balls are rolled over a glass sheet surface and adheres to adhesive dots.
  • US 6,261,652 discloses a solution where ceramic spacers/support structures are used in an evacuated gap.
  • Other patent documents discloses different support structures/spacers for evacuated gap of a VIG unit, where these comprises predefined contact surfaces.
  • the present disclosure may e.g. improve cost efficiency of VIG units with good heat insulating properties.
  • the present disclosure may additionally provide advantages in relation to obtaining an advantageous VIG unit manufacturing solution.
  • the present disclosure relates to a method of producing a vacuum insulated glass (VIG) unit.
  • the method comprises:
  • a plastic deformation of the provided support structures is provided by means of said major surfaces so that the initial height of a plurality of the support structures is reduced by at least 10%, such as at least 20%, such as at least 40% to a reduced support structure height.
  • the plastic deformation may provide a flattening and enlarging of opposing contact surfaces of the support structures in contact with the first and second major surfaces respectively.
  • the provided support structures arranged at the first major surface comprises solid, spherical balls.
  • Modern VIG units may be produced with a reduced pressure in the evacuated gap below 0.005 millibar such as substantially 0.001 millibar or below. This provides superior heat insulating capabilities.
  • the atmosphere may exhibit a pressure of 10 tons per square meter evacuated VIG.
  • Manufacturing such VIG units often comprises use of support structures having predefined, plane contact surfaces.
  • the inventor has realized that handing support structures having predefined, plane contact surfaces prior to arranging these at the glass sheet may be complex and/or time consuming and may increase the risk of jamming or inducing other issues at support structure placement/handling equipment.
  • the solution of the present disclosure provides advantages with regards to handing of the support structures during VIG unit manufacturing prior to the deformation, e.g. in embodiments where the support structures comprises spherical balls. Spherical balls may be less likely to jam or in other ways provide issues when handling the balls prior to arranging and during arranging the balls at the first major surface, when compared to support structures/spacers having predefined, such as flat, contact surfaces.
  • Tempered glass sheets such as thermally tempered glass sheets, provides improved glass sheet strength, thereby enabling providing a larger mutual distance between adjacent support structures, which may e.g. help to reduce the visibility of the support structures to the human eye, or reduce the risk that the human eye will notice the support structures. This is a feature that is often considered relevant in order to compete with the visual impression of gas filled, conventional insulating glass units where no support structures are used in the gas filled gap.
  • solid spherical balls for example solid spherical steel balls
  • Such balls are often even available with tight tolerances and are cost efficient.
  • the present inventor has surprisingly found that utilization of solid, spherical balls between glass sheet where these are arranged with a rather large mutual distance of 30 mm or above and providing the desired vacuum of below 0.005 millibar, may provide a plastic deformation of the solid balls by means of the atmosphere so that the balls adapt to the surface topology of the glass sheets.
  • the plastic deformation provides an individual shaping and adaption of contact surfaces of the solid support structures, such as spherical, solid balls, at the individual location by means of the glass sheets compressing the balls in the gap due to the atmospheric pressure gradually increasing as the gap is gradually evacuated.
  • the present inventor found that deformation of spherical, solid balls, even though the initial contact surface of the balls touching the glass surfaces is small, may not inflict critical damages to the tempered glass sheets at the spots where the support structures was placed when the pressure in the gap was gradually dropped by means of the pump.
  • the plastic deformation may help to increase contact surface area of the support structure(s) and also provide an advantageous adaption to surface variations of the major glass surfaces.
  • intentionally providing plastic deformation of solid, spherical balls in situ by means of providing vacuum during VIG unit production and gap evacuation may provide a solution that is both cost efficient and compatible with obtaining a desired low pressure in the evacuated gap of below 0.005 mbar or below 0.004 mbar, such as to below 0.002 mbar without compromising the vacuum integrity of the VIG unit.
  • the present disclosure provides a solution that enables providing a desirable aesthetic VIG unit appearance due to increased mutual support structure distance when using tempered glass sheets and provides a solution that may reduce manufacturing issues prior to arranging the support structures at the glass sheet surface.
  • the solid spherical balls may comprises or consist of metal such as steel, such as a monolithic steel structure.
  • such balls may have the advantages of being available with rather tight tolerances relating to the deviation form a complete spherical shape.
  • spherical balls such as solid spherical balls, such as solid steel balls are available "off the shelf' which are precisely manufactured and hence may serve as candidates for use as support structures for VIG units. Such balls are also known as "precision balls”. Cost efficient precision balls are available on the market with a nominal diameter less than 1 mm, such as less than 600 um, and even around 400 um or lower nominal diameter.
  • the solid spherical balls may comprise or consist of a polymer.
  • the material of the solid support structures may have a Youngs modulus between 170 Gpa and 280 GPA, such as between 180 GPa and 230 GPa at 20°C.
  • Such support structures such as solid spherical balss balls, may provide desired/acceptable properties that may make them suitable for use in VIG units.
  • the mutual distance between adjacent support structures at the glass sheet surface may be between 30 mm and 60 mm such as between 35 mm and 45 mm, for example between 38 mm and 42 mm.
  • the load subjected at each support structure may vary.
  • smaller mutual support structure distance may provide a load of between 7 and 11 kg at each support structure whereas larger mutual support structure distance may provide a load of between 23 and 28 kg at each support structure.
  • the support structure distance may be adapted so that the load acting at each support structure may be between 7 kg and 30 kg, such as between 12 kg and 20 kg, for example between 14 kg and 18 kg
  • the material of the support structures such as the solid, spherical balls may have a yield stress of less than 600 MPa, such as less than 530 MPa, for example less than 480 MPa at 20°C
  • all solid spherical balls (10) at the major glass sheet surface is of the same diameter ⁇ tolerances.
  • said tolerances may be within ⁇ 200 um, such as within ⁇ 100 um, such as within ⁇ 50 um, for example within ⁇ 20 um.
  • a plurality of said plastically deformed support structures comprises a first convex side surface and a second opposite, convex side surface when seen in a cross section of the plastically deformed support structure, where said convex side surfaces extends between the major glass sheet surfaces.
  • the side surfaces of solid spherical balls may adapt due to the plastic deformation so that the side surface curvature of the convex sides describes smaller circles than before the deformation.
  • the side surfaces changes shape from the initial shape where each side surface was so to say part of the same circle, i.e. the outer surface of the spherical ball.
  • the side surfaces may tend to change surface curvature into substantially circular arcs that may each have a centre between the major surface glass sheets, and where these centres may be non-coinciding. This may be provided in response to increasing the contact area of the contact surfaces of the support structures.
  • the cross section may be provided in a cross sectional plane extending through a centre portion of the contact surfaces and extending substantially perpendicular to a plane defined by the major surfaces of the glass sheets facing the gap.
  • the non-coinciding centres may have a mutual distance of at least 3% of the initial diameter of the spherical ball, such as a mutual distance of at least 10% of the initial diameter of the spherical ball, such as a mutual distance of at least 20% or at last 35 % of the initial diameter of the spherical ball.
  • the convex side surfaces may each describes minor, circular arcs having non-coinciding centres, such as as a result of the plastic deformation.
  • a plurality of said plastically deformed support structures may comprise a first convex side surface and a second opposite, convex side surface when seen in a cross section of the plastically deformed support structure. These convex side surfaces may extend between the major glass sheet surfaces.
  • each of the circles comprising each their convex side surface may be is at least 10%, such as at least 20%, such as at least 30%, smaller than the radius of the initial solid spherical ball before the deformation.
  • the curvature of the side surfaces may change during deformation of the spherical balls and that this may cause a reduction of the radius of a circle comprising the respective convex side surface when compared to the radius of the initial solid spherical ball. This may be a result of an automatic adaption and enlargement of the contact surfaces of the individual support structures when plastically deforming these by reducing the pressure in the gap.
  • the radius of each of said circles comprising each their convex side surface may be between 10% and 70%, such as between 20% and 70%, such as between 30% and 60%, smaller than the radius of the initial solid spherical ball before said deformation by means of the pump.
  • the envisages circles substantially comprising each their convex side surface may each have a diameter that is larger than the reduced support structure height.
  • the maximum width of each of a plurality of the support structures in the gap after the plastic deformation may be larger than the initial diameter of the solid spherical balls before the plastic deformation. In some embodiments of the present disclosure, the maximum width may be at least 10% larger, for example 20 % larger, for example at least 40% larger, than the initial diameter of the solid spherical balls before the plastic deformation.
  • the maximum width of each of a plurality of the support structures in the gap after the plastic deformation is at least 20% larger, such as at least 40% larger, for example at least 60% larger than the initial diameter of the solid spherical balls before the plastic deformation.
  • the maximum width of each of a plurality of the support structures in the gap after the plastic deformation may be between 3% and 120%, such as between 5% and 85%, for example between 20% and 65% larger than the initial diameter of the solid spherical balls before the plastic deformation.
  • the tempered glass sheets are thermally tempered glass sheets.
  • Such glass sheets provides the advantage of being cost efficient and very strong when compared to annealed glass sheets. This provides advantages with regards to providing a cost efficient VIG unit with larger mutual support structure distances.
  • thermally tempered glass sheets may suffer from slightly uneven surface variations due to so-called roller waves originating from the production of the glass sheets and other out of flatness effects.
  • the surface variations may even get above 0.1 mm and in some occasions, also more "global" surface variations may be present when looking at the curvature of the thermally tempered glass sheets.
  • the thermally tempered glass sheets have an out of flatness deflection of at least 0,1mm or more.
  • the present inventor has however found that using spherical balls as support structures may enable advantageous plastic adaption of the balls to the individual characteristic of the thermally tempered glass sheets that are paired to provide a VIG unit. This May reduce need determining surface characteristic of the glass sheets, and may even make such determination superfluous.
  • an evacuation pump provides a part of said reduction of the initial height during evacuation of the gap.
  • an evacuation pump may provide substantially the entire reduction of the initial height of the spherical ball, during evacuation of the gap.
  • a plurality of the support structures are subjected to varying plastic deformation in response to surface unevenness of the thermally tempered glass sheets so as to have different reduced heights.
  • a plurality of the plastically deformed support structures may have difference in reduced height of at least 0.02 mm, such as at least 0.05 mm, for example at least 0.08 mm.
  • the solid spherical balls may be are maintained in position at the first major surface by means of a support structure maintaining arrangement, such as a temporary support structure maintaining arrangement.
  • a support structure maintaining arrangement such as a temporary support structure maintaining arrangement.
  • the support structure maintaining arrangement may be arranged external to the gap.
  • the temporary support structure maintaining arrangement may comprise comprises a magnetic maintaining arrangement, and/or a template.
  • This may e.g. provide a more advantageous manufacturing solution such as a more simple and/or reliable manufacturing solution. Also it may reduce or remove the need for adhesive solutions at the support structure positions for adhering the support structures to the first major surface.
  • the temporary support structure maintaining arrangement is configured to maintain the spherical balls in position at the major glass sheet surface, it is understood that the solid balls may comprise a ferromagnetic material.
  • no adhesive may be placed to adhere the solid, spherical balls to the major surface.
  • the reduced support structure height of a plurality of the support structures in the gap may be between 15% and 95%, such as between 20% and 85%, such as between 30% and 80% of the initial height of the respective solid spherical balls.
  • the reduced support structure height of a plurality of the support structures is between 70% and 98%, such as between 80% and 95% of the initial height of the respective solid spherical balls.
  • the reduced support structure height is the result of/originates from a plastic deformation of the spherical ball. Hence, if the respective support structure was removed from the VIG unit gap, e.g. by equalling the gap pressure to atmospheric pressure, the reduced support structure height due to plastic deformation may be maintained.
  • At least 10%, such as at least 40%, for example at least 70% of the total amount of spherical balls arranged at the first surface may be plastically deformed to said reduced support structure height (H1).
  • At least 40%, for example at least 70% of the total amount of spherical balls arranged at the first surface may be plastically deformed to said reduced support structure height, wherein said reduced support structure height is between 20% and 85%, such as between 30% and 80% of the initial height of the respective solid spherical balls.
  • At least 10%, such as at least 40%, for example at least 70% of the total amount of spherical balls arranged at the first surface may be plastically deformed to a reduced support structure height which is between 15% and 95%, such as between 20% and 85%, such as between 30% and 80% of the initial height of the respective solid spherical balls.
  • the surface area of each of the major surfaces of the first and second sheet is larger than 1 m 2 , such as larger than 1.3 m 2 .
  • one or both of the tempered glass sheets have a thickness between 2 mm and 6 mm, such as between 2 mm and 4 mm, for example between 2.5 mm and 3.5 mm including both end points
  • the solid spherical balls at the major glass sheet surface have a diameter between 0.1 mm and 0.8 mm, such as between 0.2 mm and 0.6 mm, such as between 0.25 mm and 0.45 mm.
  • the evacuation of the VIG unit gap is provided by means of a pump to a gap pressure below 0.005 mbar, such as below 0.003 mbar, such as to below 0.002 mbar.
  • the number of support structures in the evacuated gap is below 1500 support structures per VIG unit m 2 , such as below 900 support structures per VIG unit m 2 , for example below 700 support structures per VIG unit m 2 .
  • the number of support structures in the evacuated gap is between 200 and 1800 support structures per VIG unit m 2 , such as between 300 and 1300 support structures per VIG unit m 2 , for example between 280 and 800 support structures per VIG unit m 2 .
  • At least a part of the plastic deformation, such as substantially the entire plastic deformation, of the support structures, such as solid spherical balls, in the gap by means of said major surfaces may be provided by evacuating the gap in a surrounding pressure such as atmospheric pressure, such as by means of an evacuation pump. This may e.g. provide a fast and efficient adaption of the support structure height.
  • At least a part of the plastic deformation of the support structures, such as solid spherical balls, by means of said major surfaces may be provided by evacuating the gap in a surrounding pressure such as atmospheric pressure, for example by means of an evacuation pump.
  • At least a part of the plastic deformation of the solid spherical balls by means of said major surfaces may be provided by means of an external mechanical pressing arrangement configured to provide a compression force to exterior major surfaces of the glass sheets. This may e.g. provide a good control of the support structure deformation and/or an efficient adaption of the support structure height.
  • At least a part of the plastic deformation, such as substantially the entire plastic deformation, of the support structures, such as spherical balls, by means of said major surfaces is provided by means of an external mechanical pressing arrangement configured to provide a compression force to exterior major surfaces of the VIG unit assembly such as the glass sheets.
  • the external mechanical pressing arrangement comprises pressing bodies and one or more actuators. In one or more embodiments of the present disclosure, the external mechanical pressing arrangement comprises a hardware controller for controlling the one or more actuators.
  • the provided solid support structures may have another shape than spherical and may hence not be spherical balls.
  • the provided support structures may be solid support structures having another shape than spherical.
  • the plastic deformation of the provided solid support structures by means of said major surfaces may hence be provided to solid, such as monolithic, support structures of another shape than spherical balls.
  • the solid support structures of another shape than spherical balls may have a rectangular shape, a conical shape, e.g. the shape of a frustum of a cone or frustum of a pyramid, the shape of a cylinder and/or the like.
  • the present disclosure moreover relates to a vacuum insulated glass (VIG) unit according to a second aspect.
  • the VIG unit according to the second aspect comprises a first thermally tempered glass sheet and a second thermally tempered glass sheet, and a plurality of solid, plastically deformed support structures comprising a first contact surface and a second contact surface are distributed in the evacuated gap between opposing, major surfaces of the thermally tempered glass sheets.
  • the mutual distance between adjacent support structures in the evacuated gap is above 30 mm.
  • the plastically deformed support structures comprises a first convex side surface and a second opposite, convex side surface when seen in a cross section of the plastically deformed support structure, and said convex side surfaces extends between the major glass sheet surfaces, wherein the convex side surfaces each describes minor circular arcs having non-coinciding centres.
  • a VIG unit as defined above may be cost efficient and/or more easy to produce while still obtaining a VIG unit with desired support structure distance.
  • the support structures may be made from solid, cost efficient spherical balls such as steel balls, such as precision balls. Such balls may be gradually plastically deformed by the atmosphere when a pump evacuates the gap, and hence, the deformation may adapt to the surface topology at the respective support structure location.
  • the plastically deformed support structures have different heights, wherein the difference in height is at least 0.02 mm, such as at least 0.05 mm, for example at least 0.08 mm.
  • the vacuum insulated glass unit is made by means of a method according to one or more of the above mentioned embodiments.
  • Such height variations may be provided dependent on the surface variation of the tempered, such as thermally tempered, glass sheets.
  • the plastic deformation of the support structures is caused by atmospheric pressure in response to evacuation of the gap.
  • the present disclosure relates in a third aspect to a method of producing a vacuum insulated glass unit comprising a first tempered glass sheet and a second tempered glass sheet, wherein a plurality of solid, spherical balls are distributed and plastically deformed in a gap by major surfaces of the tempered glass sheets by means of a pump during evacuation of the gap, so that the initial height of the plurality of the solid spherical balls in the gap is reduced with at least 10%, such as at least 20%, such as at least 30%.
  • the present disclosure relates in a fourth aspect to a method of producing a vacuum insulated glass (VIG) unit, wherein said method comprises:
  • a plastic deformation of the support structures is provided by means of said major surfaces so that the initial height of a plurality of the support structures is reduced by at least 10%, such as at least 20%, such as at least 40% to a reduced support structure height.
  • the fourth aspect may be be combined with one or more of the previously described embodiments.
  • Figs. 1a-1c illustrates schematically embodiments of the present disclosure relating to manufacturing a vacuum insulated glass unit.
  • a plurality of support structures 5 are distributed at a major surface first tempered glass sheet 3 so that the support structures 5 supports on a first major surface 3a of the tempered glass sheet 3.
  • the support structures 5, may also be called spacers or pillars.
  • the support structures 5 are placed with a mutual distance DIS1 at the surface 3a.
  • This distance DIS1 may in embodiments of the present disclosure be at least 30 mm, for example it may be between 30 mm and 60 mm.
  • the support structures are solid spherical balls 5.
  • the solid spherical balls 10 may comprise or consist of metal such as steel, such as a monolithic steel structure.
  • the balls may or may not be ferromagnetic.
  • the solid spherical balls 10 may comprise or consist of a polymer.
  • the material of the solid, spherical balls may have a Youngs modulus between 170 Gpa and 280 GPA, such as between 180 GPa and 230 GPa at 20°C. In embodiments of the present disclosure, the material of the solid, spherical balls may have a yield stress of less than 600 MPa, such as less than 530 MPa, for example less than 480 MPa at 20°C.
  • the balls 10 may in embodiments of the present disclosure have a diameter D1 of less than 0.6 mm, such as less than 0.5 mm, for example less than 0.4 mm.
  • the diameter D1 may be between 0.25 mm and 1.5 mm, such as between 0.25 mm and 1 mm, such as between 0.28 mm and 0.42 mm.
  • the balls used may be balls having a diameter of 0.30 mm or 0.40 mm.
  • the balls 10 may in embodiments of the present disclosure have a diameter H2 between 0.1 mm and 0.8 mm, such as between 0.2 mm and 0.6 mm, such as between 0.25 mm and 0.45 mm.
  • At least 80%, such as at least 95% such as substantially all solid spherical balls 10 at the major glass sheet surface 3a may be of the same diameter ⁇ tolerances.
  • said tolerances may be within ⁇ 200 um, such as within ⁇ 100 um, such as within ⁇ 50 um, for example within ⁇ 20 um.
  • Cost efficient precision balls are available on the market with a nominal diameter less than 1 mm, such as less than 600 um, and even around 400 um or lower nominal diameter. At the same time, such precision balls may have good/tight tolerances, for example defined by ISO 3290 relating to features of finished steel balls for roller bearings, and defining different grades of ball bearings.
  • tolerances such as ball diameter variations lower than 1 um, (According to some manufacturers corresponding to "Grade G40") such as lower than 0.4 um, (According to some manufacturers corresponding to “Grade G16”) may be used as the balls for support structures.
  • this support structure maintaining arrangement 80 comprises magnets 81 placed with a mutual distance to provide the mutual support structure 5 distance DIS1 of adjacent support structures 5.
  • the balls are metal balls and magnetic, and the magnets 81 maintain the balls in the desired place with the desired distance DIS1 through the glass sheet 3.
  • the support structure maintaining arrangement 80 may comprise a template.
  • the template may e.g. comprise predefined, distributed openings for receiving said solid spherical balls and temporarily maintain these at the desired respective location. For example until a magnetic 81 arrangement takes over the position maintenance and/or the spherical balls until the gap evacuation has started.
  • the support structure maintaining arrangement 80 may comprise a liquid or the like that may be placed at the desired position(s) of the surface 3a, and may maintain the balls in place thereby.
  • the support structure maintaining arrangement 80 may be considered a temporary support structure maintaining arrangement.
  • an array 100 comprising a plurality of outlets 110 is provided.
  • the outlets 110 are arranged side by side, transverse to a movement direction of the glass sheet 3 (or the array 500) in a direction along the glass sheet surface 3.
  • the outlets 510 are hence arranged e.g. side by side in a dispenser distribution direction DIR1 that may be transverse to the movement direction with which a motor or the like provides a relative displacement between the array and the glass sheet 3 along the glass sheet surface 3a.
  • the outlets 110 of the array 100 are placed with a mutual distance and may dispense a row of support structures 5 at a time, for example simultaneously, onto the glass sheet surface 3a.
  • the mutual outlet 510 distance may substantially correspond to the distance DIS1 to provide that the support structures are placed with the desired distance.
  • the array 50 may in embodiments of the present disclosure comprise between 4 outlets 110 and 80 outlets 110, such as between 4 outlets 110 and 50 outlets 110, such as between 6 outlets 110 and 30 outlets 110.
  • Each outlet 110 may be part of/comprised in an individual support structure 5 dispensing system or be provided at a single dispensing system.
  • One or more guiding pipes or the like may guide the balls 10 from a ball storage 10a containing/storing a plurality of balls 10 to the outlet 110.
  • a movable support structure retainer 120 retains the respective ball 110 until it is desired to be dispensed/dropped towards the surface 3a.
  • the movable retainer 120 may be controlled by means of an actuator such as a linear actuator or a motor (not illustrated).
  • the retainer 120 may comprise a magnetizing unit or the like if the support structure 5 is magnetic, and then the retainer 120 may or may not be movable.
  • the balls 10 are dropped or laid onto the surface 3a and maintained in the desired position by means of the maintaining arrangement 80. Then a second tempered glass sheet 4 is arranged so that the distributed support structures 5 are placed in a gap 6 between the first major surface 3a and a second major surfaces 4a of the second tempered glass sheet 4.
  • An edge seal 7 is provided around the periphery of the glass sheets 3, 4, and the glass sheets are sealed together.
  • the sealing together of the first and second glass sheets 3, 4 may comprise use of an edge seal material 7 such as a solder glass material, e.g. a glass frit material, a solder metal material or the like placed at the glass sheet periphery.
  • the edge sealing material 7 may be omitted.
  • the glass sheets 3, 4 may e.g. be fused together.
  • the sealing together of the glass sheets may comprise locally heating at least at the edge seal location, or heating the entire VIG unit assembly including the support structures to a desired temperature in e.g. a furnace.
  • this furnace temperature may be set to be below a temperature where the glass sheets de-tempers.
  • the sealing together of the glass sheet 3, 4 edges may provide a fused, rigid edge seal.
  • Other airtight edge seal solutions may alternatively be provided.
  • the glass sheets 3, 4 may be thermally tempered glass sheets.
  • One or both glass sheets 3,4 may have a thickness between 2 mm and 6 mm, such as between 2 mm and 4 mm, for example between 2.5 mm and 3.5 mm including both end points.
  • the glass sheets 3, 4 may be of the same or different thickness.
  • the surface area of each of the major surfaces 3a, 4a of the first and second sheet 3, 4 may be larger than 1 m 2 , such as larger than 1.3 m 2 .
  • Thermally tempered glass may have a glass sheet surface 3a with an unevenness of at least 0.1 mm, such as at least 0.2 mm, for example at least 0.3 mm. this may occur due to one or more of glass sheet bowing, glass sheet warp, glass sheet edge lift, roller waves and/or the like that may e.g. occur during tempering of the glass sheet to obtain a thermally tempered glass sheet.
  • the glass sheet 3, 4 surface 3a, 4a unevenness for each glass may even be equal to or larger than the support structure 5 height.
  • the glass sheet surfaces 3a, 4a may comprise one or more low-e coatings and/or the like to e.g. provide advantageous/desired heat regulation and/or other functionalities. It is understood that one or both contact surface(s) 5a, 5b may abut such coatings of the glass sheet. In other embodiments, the glass sheet surface(s) abutting the contact surface of the support structure may be uncoated.
  • a suction cup 9 is in fluid communication with the evacuation pump 11, and the suction cup 9 is placed to cover an evacuation hole in the glass sheet 4, see also fig. 2 .
  • the pump 11 evacuates the gap 6 through the evacuation hole 6a by means of the suction cup 9.
  • a vacuum chamber such as a vacuum chamber with flexible walls, for containing the entire VIG unit during evacuation may be used instead of the suction cup.
  • the atmosphere hence gradually increased the load on the glass sheets and hence compresses the spherical balls.
  • the evacuation outlet/opening 6a is sealed by a sealing 6b, such as at least partly by means of a solder material.
  • the sealing 6b comprises a tube and a solder material arranged round the tube, and when these are heated, these parts soften/melt and seals the gap 6.
  • the evacuation hole 6a in a glass sheet of the VIG unit assembly may in embodiments be omitted, and instead, gap 6 evacuation may be provided through an opening between the glass sheets 3, 4 at the glass sheet edges (not illustrated).
  • Fig. 1c illustrates a cross sectional view of a VIG unit 1 according to embodiments of the present disclosure.
  • the gap 5 has been evacuated to a reduced pressure by the pump 11, see fig. 1b .
  • the pressure in the gap 6 may be below 0.05 mbar, such as below 0.005 mbar, such as 0.003 or 0.001 mbar or below after the evacuation of the gap and sealing of the gap 6.
  • the support structures 2 maintains a distance between the glass sheet surfaces 3a, 4a across the evacuated gap 6 by means of their height when the gap has been evacuated.
  • the distance between the glass sheet surfaces 3a, 4a after gap 6 evacuation may in embodiments of the present disclosure be 0.5 mm or below, such as 0.3 mm or below, for example 0.2mm or below.
  • One square meter VIG unit may often contain more than 500 such as more than 500 or more than 3000, such as between 500-3000 discretely distributed support structures.
  • the number of support structures in the evacuated gap 6 may be below 1500 support structures per VIG unit m 2 , such as below 900 support structures per VIG unit m 2 , for example below 700 support structures per VIG unit m 2 .
  • the number of support structures 5 in the evacuated gap is between 200 and 1800 support structures per VIG unit m 2 , such as between 300 and 1300 support structures per VIG unit m 2 , for example between 280 and 800 support structures per VIG unit m 2 .
  • the glass sheets 3, 4 each comprises major surfaces 3b, 4b facing away from the evacuated gap 6.
  • Fig. 2 illustrates schematically a cross section of a part of a VIG unit assembly during evacuation of the gap 6 by an evacuation pump 11 according to embodiments of the present disclosure.
  • the evacuation of the gap 6 may be provided in a surrounding pressure such as atmospheric pressure.
  • This provides a plastic deformation of the solid spherical balls 10 by means of the major surfaces 3a, 4a of the glass sheets.
  • the initial shape of the spherical ball is illustrated by the dash-dotted circle 91.
  • the evacuation of the gap 6 provides that the initial height H2 of a plurality of the solid spherical balls 10 in the gap is reduced by at least 10%.
  • the initial height H2 which corresponds to the ball diameter, may in embodiments of the present disclosure be reduced by at least 20%, such as at least 40% to a reduced support structure height HI.
  • This flattens and enlarges opposing contact surfaces 5a, 5b of the support structures 5 in contact with the first and second major surfaces 3a, 4a respectively.
  • the ball had substantially no predefined, pre-shaped contact surfaces.
  • the part of the ball(s) 10 in contact with the surface(s) 3a, 4a may be small due to the curvature of the ball surface.
  • the balls are thereby plastically deformed by the surfaces 3a, 4a, and the contact surface area 5a, 5b of the support structures 5 gradually increases as the support structure height decreases from the initial height H2 being the ball diameter to the reduced height HI.
  • the evacuation pump 11 may provide at least a part of the reduction /plastic deformation of the initial height H2 due to the gap evacuation. In some embodiments, the pump 11 may provide substantially the entire reduction /plastic deformation of the initial height H2 due to the evacuation of the gap 6.
  • the reduced support structure height HI of a plurality of the support structures 5 in the gap 6 may be between 15% and 95%, such as between 20% and 85%, such as between 30% and 80% of the initial height H2 of the respective solid spherical balls 10. It is understood that this height H1 may be provided by plastic deformation.
  • At least 10%, such as at least 40%, for example at least 70% or at least 90% of the total amount of spherical balls 10 arranged at the first surface 3a may be plastically deformed to the reduced support structure height HI.
  • At least 40%, for example at least 70% or at least 90% of the total amount of spherical balls 10 arranged at the first surface 3a are plastically deformed to said reduced support structure height H1, where said reduced support structure height H1 is between 20% and 85%, such as between 30% and 80% of the initial height H2 of the respective solid spherical balls 10.
  • the major glass sheet surfaces 3a, 4a may have a surface variation caused due to the tempering process, such as caused by roller waves, warp and/or the like as e.g. previously described.
  • a plurality of the support structures 5 are hence subjected to varying plastic deformation in response to surface 3a, 4a unevenness of the thermally tempered glass sheets so as to have different reduced heights HI. This may e.g.
  • the plastically deformed support structures 5 in the gap have a difference in reduced height HI of at least 0.02 mm, such as at least 0.05 mm, for example at least 0.08 mm or even 0.01 mm or more.
  • This provides that the ball height H2 is changed to automatically fit to the individual surface variations of the selected pair of tempered glass sheets 3, 4.
  • the thermally tempered glass sheets have an out of flatness deflection of at least 0.1mm or more.
  • a plurality of the balls are plastically deformed into support structures comprising a first convex side surface 5c and a second opposite, convex side surface 5d when seen in a cross section (as in e.g. fig. 2 ) of the plastically deformed support structure 5.
  • These convex side surfaces 5a, 5b extends between the major glass sheet surfaces 3a, 4a.
  • the convex side surfaces 5c, 5d now each describes a minor, curved, such as circular 92, arc having non-coinciding centres C1, C2 as a result of the plastic deformation.
  • each minor circular arc 5c, 5d is substantially coinciding with the circle CI1, CI2 periphery of the respective circle.
  • the non-coinciding centres C1, C2 may have a mutual distance DIS2 of at least 3% of the initial diameter of the spherical ball, such as a mutual distance of at least 10% of the initial diameter of the spherical ball, such as a mutual distance of at least 20% or at last 35 % of the initial diameter of the spherical ball.
  • the weight and/or volume of the respective support structure 5 placed at the first glass sheet substantially corresponds to the weight and/or volume of the initial ball 10 used for the support structure 5 before the deformation.
  • the radius r1, r2 of each of the circles 92 comprising each their convex side surface 5c, 5d is at least 10%, such as at least 20%, such as at least 30%, smaller than the radius r3 of the initial solid spherical ball (10) before the deformation. This may occur to at least 40%, such as at last 70% or at least 90% of all support structures in the evacuated gap 6 of the VIG unit.
  • the radius r1, r2 of each of said circles CI1, CI2 comprising each their convex side surface may be between 10% and 70%, such as between 20% and 70%, such as between 30% and 60%, smaller than the radius (r3) of the initial solid spherical ball before the ball deformation provided by means of evacuating the gap 6.
  • the envisaged circles CI1, CI2 substantially comprising each their convex side surface 5c, 5d may each have a diameter that is larger than the reduced support structure height HI.
  • Fig. 3 illustrates schematically a cross sectional view of an embodiment of the present disclosure, where it is indicated that the contact surfaces 5a, 5b of the support structure 5 that have been provided and shaped by the glass sheets 3, 4, extends partly into the respective glass sheet surface 3a, 4a.
  • the initial glass sheet surface before gap 6 evacuation is illustrated by the dashed lines GSL.
  • the glass sheets 3, 4 may be tempered, such as thermally tempered.
  • Thermally tempered glass sheets comprises exterior compressive zones CZ and an interior tensile stress zone TZ.
  • the contact surfaces 5a, 5b of the support structure 5 has been forced into the compressive stress zone CZ of the glass sheet 3, 4, causing a recess in the respective major surface 4a, 3a into the compressive stress zone CZ proximate the gap 6.
  • This the inventor has found that this may be acceptable for a VIG unit 1 with a gap 6 pressure of below 0.005 mbar or below 0.002 mbar, for example substantially 0.001 mbar without compromising the vacuum integrity of the VIG unit.
  • the maximum height H1 of the support structure 5 may in some embodiments be slightly larger than the actual gap distance DIS3 proximate the side surface 5c, 5d of the support structure 5 due to that at least a part of the contact surface 5a, 5b extends into the glass sheet surface as a result of the evacuation of the gap 6.
  • Fig. 4 illustrates schematically a cross sectional view of a support structure 5, according to embodiments of the present disclosure, where the support structure 5 has a maximum width W1.
  • the contour of the initial ball 10 that was used for the support structure is also illustrated by the dash-dotted circle 91.
  • the glass sheets of the VIG unit, the evacuated gap and the like are not illustrated in fig. 4 in order to improve figure understanding.
  • the maximum support structure width W1 increases when compared to the initial width, i.e. the ball diameter corresponding to the height H2, when the ball is plastically deformed in the gap 6.
  • the maximum width W1 of each of a plurality of the support structures 5 in the gap 6 after the plastic deformation is at least 10% larger, for example 20 % larger, for example at least 40% larger, than the initial ball diameter H2 of the respective, solid spherical ball 10 before the plastic deformation.
  • the maximum width W1 of each of a plurality of the support structures 5 in the gap 6 after the plastic deformation may be at least 20% larger, such as at least 40% larger, for example at least 60% larger than the initial diameter H2 of the solid spherical balls 10 before the plastic deformation.
  • the maximum width W1 of each of a plurality of the support structures 5 in the gap 6 after the plastic deformation may be between 3% and 120%, such as between 5% and 85%, for example between 20% and 65% larger than the initial height H2 of the solid spherical balls 10 before the plastic deformation.
  • Fig. 5 illustrates schematically an embodiment of the present disclosure wherein the support structures 5 in the evacuated gap 6 of a VIG unit 1 have different heights due to different magnitudes of plastic support structure deformation provided during the gap 6 evacuation.
  • the support structures are placed with the mutual distance DIS1.
  • the magnitude of the plastic deformation of the spherical balls 10 may vary.
  • the plastically deformed support structures 56 of a VIG unit 1 may have difference in reduced height HI of at least 0.02 mm, such as at least 0.05 mm, for example at least 0.08 mm. This may occur to a plurality of the support structures at the VIG unit. This may be caused by one or more of glass sheet bowing, glass sheet warp, glass sheet edge lift, roller waves and/or the like. Thermally tempered glass sheets may suffer for one or more of such surface unevenness. In fig.
  • the plastic deformation subjected to the spherical ball used for providing the support structure 5 to the right is larger than the plastic deformation subjected to the spherical ball used for providing the support structure 5 to the left. This is due to the surface unevenness of the glass sheets 3a, 3b.
  • the varying support structure deformation is indicated as occurring to adjacent support structures in the gap 6, but it is understood that the difference in reduced support structure height HI within the above mentioned ranges may not necessarily be occurring to neighbouring/adjacent support structures.
  • the difference in reduced height H1 within the above mentioned range may occur between the support structure a of the final VIG unit that has been subjected to the largest plastic deformation due to the gap evacuation, and the support structure of the final VIG unit that has been subjected to the smallest plastic deformation due to the gap 6 evacuation.
  • Figs. 6a-6c illustrates microscopic images of a support structure 5 according to various embodiments of the present disclosure where a spherical, solid steel ball has been deformed into a support structure having a height HI.
  • the initial steel ball was here a precision steel ball having a diameter of 0.4 mm, but other ball diameters may be used in other embodiments of the present disclosure, as e.g. described previously in this document.
  • the compression/deformation of the steel ball was provided by means of coining the solid steel ball, to provide the contact surfaces 5a, 5b.
  • the microscope used for the image may be a stereo microscope or a dyno light microscope.
  • the solid spherical balls 10 may be metal precision balls such as steel precision balls. Such precision balls may have good/tight tolerances, for example defined by ISO 3290 relating to features of finished steel balls for roller bearings, and defining different grades of ball bearings. In embodiments of the present disclosure, tolerances such as ball diameter variations lower than 1 um, (According to some manufacturers corresponding to "Grade G40") such as lower than 0.4 um, (According to some manufacturers corresponding to "Grade G16”) may be used as the support structure workpieces. In other embodiments of the present disclosure, balls with larger overall diameter variations/lower tolerance than mentioned above may be used.
  • the side surface 9c extends between the opposing contact surfaces 5a, 5b, and extends in the present example convexly, such as bulging, between the surfaces 5a, 5b.
  • the side surface 5c is bulging, and in a cross sectional view (see e.g. fig. 4 ), the side surface 5c describes an arc, such as substantially a circular arc, between the surfaces 5a, 5b at both sides of a support structure cross section. See fig. 6c where the cross section can be imagined as the silhouette of the support structure 5 seen from the side towards the side surface 9c.
  • the side surface 9c arc described by the surface 5c between the contact surfaces 5a, 5b may substantially be an arc of/comprised in a circle CI1, CI2, and these circles have non-coinciding centres C1, C2, see also fig. 4 .
  • a similar situation may be caused by the plastic deformation during gap evacuation by as pump.
  • the side surface 5c arc extending between the contact surfaces 5a, 5b may have a length that is larger than the height HI (or H2), such as at least 1.1 or at least 1.3 times the height HI.
  • the support structure 5 has a width W1.
  • the support structure 5 in embodiments of the present disclosure as illustrated in figs. 6a-6c may have an outer circular side periphery described by the side surface/side edge surface 9c extending between the contact surfaces 5a, 5b, the width W1 may be a maximum diameter.
  • the maximum width W1, such as the maximum diameter, of the support structure 5 may be larger than the height H1 provided after the deformation of the spacer/support structure 5, such as at least 1.3, times, such as at least 1.5 times or at least 1.8 times larger than the height HI of the support structure 5.
  • the maximum width W1, such as the maximum diameter, of the support structure 5 may be between 1.3 and 6 times, such as between 1.5 and 6 times, for example between 2 times and 4 times larger than the height HI of the spacer 2.
  • the maximum width W1, such as the maximum diameter, of the support structure 5 may be at least 2 times, such as at least 2.4 times or at least 2.8 times larger than the height H1 of the support structure 5. This may be provided for a plurality of the support structures in the evacuated gap, naturally accounting for potentially present glass sheet surface variations.
  • the increased maximum width W1 when compared to the support structure height H1 obtained by means of the deformation of the spherical ball is provided due to the deformation of the ball during VIG gap evacuation so that the plastic deformation of the ball due to the deformation provides a "flow" of the ball material that result in a support structure width W1 that is larger than the initial ball width/diameter.
  • the width W2 (such as diameter) of the contact surfaces 5a, 5b is less than the maximum width W1 (such as diameter) of the support structure , as the maximum width W1 is determined between the bulging side surfaces.
  • the width W2 (such as diameter) of the contact surfaces 5a, 5b may be between 0.6 and 0.96 times the maximum width W1 (such as diameter) of the support structure, such as between 0.7 and 0.9 times the maximum width W1 (such as diameter) of the support structure.
  • the width (such as diameter) W2 of the contact surfaces 5a, 5b may be less than 0.95 times, such as less than 0.8 times, for example less than 0.6 times the maximum width W1 (such as diameter) of the support structure 5.
  • the width W2 (such as diameter) of the contact surfaces 5a, 5b may be larger than 0.4 times, such as larger than 0.5 times , for example larger than 0.6 times the maximum width W1 (such as diameter) of the support structure 5.
  • the contact surface 5a, 5b area after ball deformation may make up 50% or more of the support structure 5 silhouette when seen perpendicular to the respective contact surface 5a, 5b.
  • the support structures 5 may have a support structure height HI after the deformation by the deformation unit of less than 0.6 mm, such as less than 0.5 mm such as less than 0.3 mm, such as less than 0.25 mm.
  • the support structure/spacer height HI may be 0.2 mm or less.
  • the compressive load on at least 80% or 90%, such as substantially all support structures of the VIG unit may be between 0.5 GPa and 2 GPa, such as between 0.6 and 1.3 GPa.
  • Outgassing from the support structure 5 should be minimized. Particularly outgassing of non-getterable species should be avoided for example argon.
  • the maximum width W1 of the support structure 5 after the deformation of the balls in the evacuated gap is larger, such as at least 3% larger, for example 20 % larger, such as at least 35% larger or at least 100% larger than the initial width D1 of the ball before the ball deformation.
  • This may be the case for a plurality of the support structures in the VIG unit, for example for at least 50%, such as at least 80%, such as at least 95% of the support structures in the evacuated gap.
  • the maximum width W1 of the support structure 5 after the ball deformation due to the gap evacuation is at least 40% larger, for example at least 50% larger, such as at least 80% larger than the initial width D1 of the ball before the ball deformation.
  • the maximum width W1 of the support structure 5 after the ball deformation due to the VIG gap evacuation is between 10% and 85% larger, for example between 20% and 70% larger than the initial width D1 of the ball before the ball deformation.
  • Fig. 7 illustrates an image of a support structure 5 according to embodiments of the present disclosure, where the support structure 5 was made from a spherical, solid metal ball of a diameter of 0.4 mm.
  • the support structures After deformation by means of a deformation unit such as a press or stamp, the support structures has a height of 298 microns, i.e. approximately 0.3 mm.
  • the maximum support structure width W1 is here 555 microns, corresponding to about 0.6 mm.
  • the contact surface area 5a, 5b width W2, such as the diameter of the contact surfaces is about 391 and 392 microns respectively, corresponding to about 0.4 mm.
  • Fig. 8 illustrates an image of a support structure 5 according to embodiments of the present disclosure, where the support structure 5 is made from a spherical, solid metal ball of a diameter of 0.4 mm.
  • the support structure 5 After deformation by means of a deformation unit, the support structure 5 has a height of 204 microns, i.e. approximately 0.2 mm.
  • the maximum width W1 is here 668 microns, corresponding to about 0.7 mm.
  • the contact surface width W2, such as the diameter of the contact surfaces 5a, 5b is about 578 and 561 microns respectively, corresponding to 0.6 mm.
  • the deformations illustrated in figs. 6a-8 indicates the behaviour of a solid steel ball when the steel ball is deformed during VIG unit evacuation.
  • the resulting contact surfaces 5a, 5b after plastic deformation of the steel ball during VIG evacuation may be less plane than indicated in the images.
  • Fig. 9a illustrates an initial special, massive steel ball for use as a VIG unit support structure workpiece 10 according to embodiments of the present disclosure.
  • the spherical ball 10 has a diameter D1 of for example 0.4 mm.
  • Figs. 9b-9e illustrates the silhouette/contour of the ball of the type of fig. 9a , and are the contour silhouette/contour of the ball which are drawn up based on microscopic images of spherical, solid steel balls that have been plastically deformed by different loads.
  • the deformation load/force provided by e.g. the deformation unit 20 increases from 5 kg to 20 kg, the contact surface 5a, 5b area increases, the support structure height HI decreases, and also the maximum support structure width W1 increases.
  • Fig. 10 illustrates a square support structure grid arranged at a major surface 3a according to embodiments of the present disclosure.
  • the support structures 5 are arranged with a mutual distance DIS1.
  • the distance DIS1 may as previously described be at least 30 mm, for example it may be between 30 mm and 60 mm.
  • the distance DIS1 may be between 30 mm and 60 mm, such as between 35 mm and 45 mm, for example between 38 mm and 42 mm.
  • the mutual distance DIS1 between at last 80%, of adjacent support structures, such as at least 90% of adjacenet support structures of the final VIG unit may be at least 30 mm such as between 30 mm and 60 mm such as between 35 mm and 45 mm, for example between 38 mm and 42 mm.
  • the mutual distance DIS1 between substantially all adjacent support structures of the final VIG unit may be at least 30 mm such as between 30 mm and 60 mm such as between 35 mm and 45 mm, for example between 38 mm and 42 mm.
  • Fig. 11 illustrates schematically a manufacturing line 200 for a VIG unit according to various embodiments of the present disclosure.
  • the first glass sheet 3 first enters a first station 200 where edge seal material 7 such as solder glass edge seal material or metal solder edge seal material is provided to the upwardly facing major glass sheet surface 3a.
  • edge seal material 7 such as solder glass edge seal material or metal solder edge seal material is provided to the upwardly facing major glass sheet surface 3a.
  • the glass sheet 3a is moved to a support structure placement station 240 where one or more support structure dispensers, such as a dispenser system array 100 as previously described, dispenses solid spherical balls onto the major surface 3a.
  • a support structure placement station 240 where one or more support structure dispensers, such as a dispenser system array 100 as previously described, dispenses solid spherical balls onto the major surface 3a.
  • a relative movement MOV1 may be provided by means of a motor to provide a relative movement between the one or more support structure dispensers and the glass sheet in a direction along the glass sheet surface 3a.
  • the movement MOV1 and the direction DIR1 may be perpendicular to each other.
  • the glass sheets 4 and 3 are paired by placing the second glass sheet 4 on top of the first glass sheet 3 to cover the support structures 5.
  • the glass sheet 4 may e.g. rest on the edge seal material 7.
  • the glass pairing station 250 may comprise automation systems such as one or more of a robotic arm, one or more linear displacement members, one or more rails and/or the like for transporting the glass sheet 4 to the position opposite the surface 3a and lowering the glass sheet towards the surface 3a.
  • the edge seal material 7 of the VIG unit assembly 150 may be heated and the gap is evacuated to a reduced pressure as e.g. previously described (not illustrated in fig. 13 in order to deform the spherical balls placed at the station 240. It is understood that the edge seal material 7, if even needed, may be placed/applied subsequent to placing the support structures at station 240 instead. It may even in some embodiments be omitted if the glass sheets 3, 4 are fused directly together by a glass sheet 3, 4 edge melting operation.
  • the solid spherical balls at the major glass sheet surface 3a may be maintained in position at the first major surface 3a by means of a temporary support structure maintaining arrangement 80 (not illustrated in fig. 11 ) as previously described.
  • the support structure placement station 240 and the glass pairing station 250 may be placed at the same physical location so that moving of the glass sheet 3a with the balls thereon is reduced.
  • the support structure placement station 240 and the glass pairing station 250 may be placed at different locations at the manufacturing line as illustrated.
  • the support structure maintaining arrangement 80 may be movable together with the glass sheet in order to maintain the ball position(s) at the surface 3a.
  • Fig. 12 illustrates a support structure 5 deformation according to embodiments of the present disclosure.
  • the support structure deformation to obtain the support structure height HI is provided by means of the evacuation pump which evacuates the gap.
  • an external mechanical pressing arrangement 300 comprising pressing bodies 310, 320 such as pressing plates, and actuators 330 instead provides the second support structure deformation to obtain the support structure height HI.
  • the bodies 310, 320 may e.g. comprise metal bodies or bodies of another material.
  • the pressing bodies 310, 320 comprises pressing surfaces 310a, 320a, and one or both pressing bodies is/are configured to move towards and away from the other body so as to increase or reduce the distance between the pressing surfaces 310a, 320a. This movement is provided by means of the one or more actuators 330.
  • a VIG unit assembly 50 comprising the glass sheets 3, 4 (that may e.g. be annealed glass sheets or thermally tempered glass sheets) and the support structures 5 distributed between the glass sheets is placed between the pressing plate 310, 320 surface 310a, 320a.
  • the support structures 5 of the VIG unit assembly 50 when the assembly is placed in the gap, has the initial support structure height HI.
  • One or more actuators 330 are controlled by a hardware controller (340) so that the distance between pressing surfaces 310a, 320a of the pressing bodies 310, 320 is reduced.
  • This provides a compression force F towards the major exterior surfaces of the glass sheets of the VIG unit assembly 50 that faces away from the gap 6.
  • This compression force F provides that the major glass sheet surfaces 3a, 4a facing the gap 6 provides a plastic deformation of the support structures 5 in the gap 6 so that the height H2 of the support structures (in this case spherical balls) is reduced to a second, reduced height HI.
  • This provides an individual adaption of the spacer height to the surface 3a, 4a topography of the glass sheets 3a, 4a.
  • the magnitude of the plastic deformation from the height H2 into the height H1 may in embodiments of the present disclosure be as described in relation to one or more embodiments described above, e.g. in relation to fig. 7 and/or 7a.
  • the actuator(s) 330 is/are controlled so that the top press plate 210 moves towards the lower plate 320.
  • the actuator(s) 330 may be directly or indirectly connected to the lower pressing plate 320 instead, and the lower plate 320 may hence be moved, together with the VIG unit assembly 50 supporting thereon, towards the upper pressing plate 310.
  • one or more actuators 330 may be provided and configured to move one or both bodies 310, 320, and both pressing bodies 310, 320 may be movable towards and/or away from each other.
  • the external mechanical pressing arrangement 300 may provide some of the plastic deformation to obtain the height H1, or most, such as substantially all of the deformation to obtain the height HI.
  • the deformation such as plastic deformation, may be provided partly by means of an evacuation pump evacuating the gap (e.g. as described above in relation to the description of fig. 2 ) and partly by the external mechanical pressing arrangement 300.
  • the actuator(s) 330 may in embodiments of the present disclosure be or comprise a pneumatic actuator, a hydraulic actuator, an electric actuator, e.g. comprising an electric motor and/or the like. It may or may not comprise a gearing.
  • the support structure to be deformed by the surfaced 3a, 4a is a spherical ball. It is understood that in other embodiments, the support structure may have a different shape than spherical, e.g. as described further below.
  • a hardware controller 340 controls the actuator(s) 330, e.g. based on a software program code stored in a data storage (not illustrated).
  • one or more load sensors may be configured to directly or indirectly detect the amount of force F provided to the assembly 50.
  • the one or more load sensors may comprise a processing unit receiving/retrieving electric current consumption information obtained from the actuator(s), it may comprise one or more strain gauges and/or the like.
  • load sensor(s) may provide feedback to a closed control loop system of a controller 340 controlling the actuator(s) 330.
  • the compression force F such as a maximum compression force, applied by means of the actuator(s) 330 may in embodiments of the present disclosure be a predetermined compression force.
  • the predetermined compression force may be based on one or more parameters stored in a data storage such as the above mentioned data storage.
  • the one or more parameters may e.g. be related to the distance between adjacent spacers/support structures 5 in the gap, the support structure material, support structure size and/or the like.
  • the hardware controller may control the actuator(s) to gradually increase the force F to the predetermined compression force such as a predetermined maximum compression force. This may e.g. be provided by ramping up the force applied from an initial lower force.
  • a resilient sheet (not illustrated) may be placed between the respective pressing surface 310a, 320a and the respective major exterior glass sheet 3, 4, surface facing away from the gap 6. This my e.g. help to distribute forces and/or protect glass sheet surfaces.
  • the embodiments described above in relation to one or more of the figures 1-12 are generally illustrated and described in relation to using solid, spherical balls such as metal balls as the support structures to be deformed in the gap 6 by means of, the major surfaces 3a, 4a of the glass sheets.
  • the provided solid support structures may have another shape than spherical.
  • the plastic deformation of the provided solid support structures by means of said major surfaces 3a, 4a may hence be provided to solid, such as monolithic, support structures of another shape than spherical balls.
  • such solid support structures of another shape than spherical balls may comprise or consist of solid metal support structures.
  • the solid support structures of another shape than spherical balls may have a rectangular shape, a conical shape, e.g. the shape of a frustum of a cone or frustum of a pyramid, the shape of a cylinder and/or the like.
  • the solid support structures of another shape than spherical balls may be support structures cut from a wire, e.g. at the manufacturing line for manufacturing VIG unit assemblies.
  • the VIG unit may e.g. be transparent to at least visible light.
  • the manufactured VIG unit may be for use in a building window.
  • the building window may be a roof window.
  • the building window may be a vertical window such as a façade window.
  • the VIG unit when used in a building window may be laminated at one or both sides of the VIG unit by means of an interlayer and a further glass sheet.
  • the VIG unit may be used for e.g. cooling furniture such as in a door of a refrigerator or freezer and/or for heating furniture such as in a door of an oven. The VIG unit to enable a view through the VIG unit towards the goods stored in the interior of the cooling or heating furniture.

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  • Engineering & Computer Science (AREA)
  • Civil Engineering (AREA)
  • Structural Engineering (AREA)
  • Joining Of Glass To Other Materials (AREA)
EP22202420.0A 2022-10-19 2022-10-19 Déformation in situ de structures de support pour unités de verre isolant sous vide Pending EP4357575A1 (fr)

Priority Applications (5)

Application Number Priority Date Filing Date Title
EP22202420.0A EP4357575A1 (fr) 2022-10-19 2022-10-19 Déformation in situ de structures de support pour unités de verre isolant sous vide
PCT/EP2023/077727 WO2024083528A1 (fr) 2022-10-19 2023-10-06 Déformation in situ de structures de support pour des unités de vitrage isolant sous vide
PCT/EP2023/077733 WO2024083530A1 (fr) 2022-10-19 2023-10-06 Commande de distance de sortie d'intercalaire lors de la fabrication d'une unité de vig au moyen d'un dispositif de commande de distance
PCT/EP2023/077728 WO2024083529A1 (fr) 2022-10-19 2023-10-06 Production d'unité de vig comprenant l'utilisation d'un distributeur comprenant une feuille de collecte
PCT/EP2023/077719 WO2024083526A1 (fr) 2022-10-19 2023-10-06 Pré-déformation de pièces de structure de support pour structures de support d'unités de vitrage isolant sous vide

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP22202420.0A EP4357575A1 (fr) 2022-10-19 2022-10-19 Déformation in situ de structures de support pour unités de verre isolant sous vide

Publications (1)

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EP4357575A1 true EP4357575A1 (fr) 2024-04-24

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EP22202420.0A Pending EP4357575A1 (fr) 2022-10-19 2022-10-19 Déformation in situ de structures de support pour unités de verre isolant sous vide

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EP (1) EP4357575A1 (fr)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6261652B1 (en) 1996-07-31 2001-07-17 Saint-Gobain Vitrage Method for producing a vacuum between two glass sheets and insulating glazing
US6689241B1 (en) 1998-12-10 2004-02-10 Saint-Gobain Glass France Sealed vacuum double glazing and method for making
DE102010021127A1 (de) * 2010-05-21 2011-11-24 Grenzebach Maschinenbau Gmbh Verfahren und Vorrichtung zum Herstellen von Mehrscheiben-Isolierglas mit einer Hochvakuum-Isolierung
US20190106931A1 (en) * 2017-10-06 2019-04-11 Vkr Holding A/S Vacuum insulated glazing unit

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6261652B1 (en) 1996-07-31 2001-07-17 Saint-Gobain Vitrage Method for producing a vacuum between two glass sheets and insulating glazing
US6689241B1 (en) 1998-12-10 2004-02-10 Saint-Gobain Glass France Sealed vacuum double glazing and method for making
DE102010021127A1 (de) * 2010-05-21 2011-11-24 Grenzebach Maschinenbau Gmbh Verfahren und Vorrichtung zum Herstellen von Mehrscheiben-Isolierglas mit einer Hochvakuum-Isolierung
US20190106931A1 (en) * 2017-10-06 2019-04-11 Vkr Holding A/S Vacuum insulated glazing unit

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