EP4064881A1 - Article de génération d'aérosol avec papier épais - Google Patents

Article de génération d'aérosol avec papier épais

Info

Publication number
EP4064881A1
EP4064881A1 EP20815946.7A EP20815946A EP4064881A1 EP 4064881 A1 EP4064881 A1 EP 4064881A1 EP 20815946 A EP20815946 A EP 20815946A EP 4064881 A1 EP4064881 A1 EP 4064881A1
Authority
EP
European Patent Office
Prior art keywords
aerosol generating
paper wrapper
micrometers
generating substrate
aerosol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
EP20815946.7A
Other languages
German (de)
English (en)
Inventor
Ivan Prestia
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Philip Morris Products SA
Original Assignee
Philip Morris Products SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Philip Morris Products SA filed Critical Philip Morris Products SA
Publication of EP4064881A1 publication Critical patent/EP4064881A1/fr
Pending legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00—Cigars; Cigarettes
    • A24D1/02—Cigars; Cigarettes with special covers
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • A24B15/14—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco made of tobacco and a binding agent not derived from tobacco
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00—Cigars; Cigarettes
    • A24D1/04—Cigars; Cigarettes with mouthpieces or filter-tips
    • A24D1/045—Cigars; Cigarettes with mouthpieces or filter-tips with smoke filter means
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00—Cigars; Cigarettes
    • A24D1/20—Cigarettes specially adapted for simulated smoking devices
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/40—Constructional details, e.g. connection of cartridges and battery parts
    • A24F40/46—Shape or structure of electric heating means
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/40—Constructional details, e.g. connection of cartridges and battery parts
    • A24F40/46—Shape or structure of electric heating means
    • A24F40/465—Shape or structure of electric heating means specially adapted for induction heating

Definitions

  • the present disclosure relates an aerosol generating article having a thick wrapper.
  • the thick wrapper and a second wrapper circumscribe an aerosol generating substrate joining the aerosol generating substrate to a filter element and forming an aerosol generating article.
  • Aerosol generating articles in which an aerosol generating substrate, such as a tobacco containing substrate, is heated rather than combusted, are known in the art.
  • an aerosol is generated by the transfer of heat from a heat source to a physically separate aerosol generating substrate or material, which may be located in contact with, within, around, or downstream of the heat source.
  • volatile compounds are released from the aerosol generating substrate by heat transfer from the heat source and are entrained in air drawn through the aerosol generating article. As the released compounds cool, they condense to form an aerosol.
  • Paper that is used to wrap the aerosol generating substrate and form the aerosol generating substrate element can absorb aerosol former, water and other liquid compounds found in the mainstream smoke or aerosol passing through the aerosol generating article, or humidity or moisture surrounding the paper.
  • the absorbed liquid may stain or weaken the paper and negatively affects the appearance and structural integrity of the aerosol generating article.
  • Heated aerosol generating articles are particularly susceptible to wetting and breakage due to the high levels of aerosol former in the aerosol generating substrate of these heated aerosol generating articles.
  • Heated aerosol generating articles are particularly susceptible to swelling as aerosol components are absorbed by the wrapper, leading to difficult removal from the heating device.
  • a resistive heating blade may be inserted into the aerosol generating substrate to heat the aerosol generating substrate and release volatile compounds from the aerosol generating substrate.
  • the resistive heating blade may provide a localized heat source within the aerosol generating substrate that may be located along a central axis of the aerosol generating substrate.
  • the aerosol generating substrate located about the periphery or interface with the paper wrapper may not be sufficiently heated by the centrally located resistive heating blade, resulting in unused aerosol generating substrate within the aerosol generating substrate.
  • an aerosol generating article including an aerosol generating substrate, a filter element, and a first paper wrapper and a second paper wrapper circumscribing the aerosol forming substrate.
  • the first paper wrapper having a thickness in a range from about 60 micrometers to about 160 micrometers.
  • the first paper wrapper or the second paper wrapper joining the aerosol forming substrate to a filter element.
  • an aerosol generating article including an aerosol generating substrate, a filter element, and a first paper wrapper and a second paper wrapper circumscribing the aerosol forming substrate.
  • the first paper wrapper having a thickness in a range from about 90 micrometers to about 160 micrometers.
  • the second paper wrapper joining the aerosol forming substrate to a filter element.
  • the first paper wrapper may separate the second paper wrapper from the aerosol generating substrate.
  • the first paper wrapper may not extend beyond the aerosol generating substrate.
  • the first wrapper extends an entire length of the aerosol generating substrate.
  • the second paper wrapper may join the aerosol generating substrate to the filter element.
  • the first paper wrapper may extend an entire length of the generating substrate.
  • the second paper wrapper may extend less than about 50% of the length of the generating substrate.
  • the second paper wrapper may separate the first paper wrapper from the aerosol generating substrate.
  • the second paper wrapper may not extend beyond the aerosol generating substrate.
  • the first paper wrapper may join the aerosol generating substrate to the filter element.
  • the first paper wrapper may extend an entire length of the generating substrate.
  • the first paper wrapper may have a paper thickness in a range from about 78 micrometers to about 160 micrometers.
  • the first paper wrapper may have a paper thickness in a range from about 78 micrometers to about 140 micrometers.
  • the first paper wrapper may have a paper thickness in a range from about 90 micrometers to about 140 micrometers.
  • the first paper wrapper may have a paper thickness in a range from about 100 micrometers to about 140 micrometers.
  • the first paper wrapper may have a paper thickness in a range from about 110 micrometers to about 140 micrometers.
  • the first paper wrapper may have a paper thickness in a range from about 125 micrometers to about 140 micrometers.
  • the first paper wrapper may have a paper thickness in a range from about 130 micrometers to about 140 micrometers.
  • the second paper wrapper may have a paper thickness that is less than the paper thickness of the first paper wrapper.
  • the second paper wrapper may have a paper thickness in a range from about 10 micrometers to about 50 micrometers.
  • the second paper wrapper may have a paper thickness in a range from about 10 micrometers to about 35 micrometers.
  • the second paper wrapper may have a paper thickness in a range from about 15 micrometers to about 30 micrometers.
  • the second paper wrapper may have a paper thickness in a range from about 20 micrometers to about 25 micrometers.
  • the aerosol generating substrate may define a substantially cylindrical shape having a diameter in a range from about 6.8 mm to about 7.1 mm, or from about 6.8 mm to about 7.0 mm.
  • the first paper wrapper may have a ratio of paper thickness to tobacco substrate diameter in a range from about 1:120 to about 1:40.
  • the first paper wrapper may have a ratio of paper thickness to tobacco substrate diameter in a range from about 1:100 to about 1:50.
  • the first paper wrapper may have a ratio of paper thickness to tobacco substrate diameter in a range from about 1:70 to about 1:50.
  • the first paper wrapper may have a ratio of paper thickness to tobacco substrate diameter in a range from about 1:60 to about 1:50.
  • the aerosol generating substrate may include homogenized tobacco material.
  • the homogenized tobacco material may include tobacco material, from about 1 percent to about 5 percent of a binder, and from about 5 percent to about 30 percent of an aerosol-former, in dry weight basis.
  • the aerosol generating substrate may include a gathered sheet of homogenized tobacco material that is preferably crimped.
  • the aerosol generating substrate may include a metallic induction heating element.
  • the aerosol generating substrate may include a plurality of metallic induction heating elements. According to this disclosure, there is provided an aerosol generating system comprising, the aerosol generating article, described herein, and an aerosol generating device comprising a heating element configured to heat the aerosol generating substrate.
  • the heating element may be a resistive heating blade element configured to be inserted into the aerosol generating substrate.
  • the heating element may be an inductive heating element configured to inductively heat metallic induction heating elements embedded within the aerosol generating substrate.
  • aerosol generating articles that include a thick wrapper about the aerosol generating substrate may provide a visually and mechanically stable aerosol generating article, particularly for heat-not-burn aerosol generating articles that contain a high level of liquids or aerosol formers.
  • swelling, visible staining and physical weakening of the wrapper portion of the aerosol generating article may be reduced even when a high level of humectant is included in the aerosol generating substrate.
  • aerosol generating substrate elements that include a thick wrapper may be formed on conventional aerosol generating article forming manufacturing equipment. This may improve the processability of the aerosol generating substrate elements and reduce manufacturing costs.
  • aerosol generating substrate elements that include a thick wrapper may increase the amount of aerosol generating substrate that is uniformly heated and consumed, thus reducing unused or wasted aerosol generating substrate material.
  • aerosol generating substrate elements that include a thick wrapper may utilize internal heating of the aerosol generating substrate via induction or resistive heating elements embedded or inserted into the aerosol generating substrate, and the thick paper wrapping the aerosol generating substrate may not negatively affect the heating of the heat-not- burn aerosol generating substrate.
  • a conventional cigarette is lit when a user applies a flame to one end of the cigarette and draws air through the other end.
  • the localised heat provided by the flame and the oxygen in the air drawn through the cigarette causes the end of the cigarette to ignite, and the resulting combustion generates an inhalable smoke.
  • an aerosol is generated by heating a flavour generating substrate, such as tobacco.
  • Known heated aerosol generating articles include, for example, electrically heated aerosol generating articles and aerosol generating articles in which an aerosol is generated by the transfer of heat from a combustible fuel element or heat source to a physically separate aerosol forming substrate.
  • aerosol generating articles according to the disclosure find particular application in aerosol generating systems comprising an electrically heated aerosol generating device having an internal heater blade which is adapted to be inserted into the rod of aerosol generating substrate.
  • Aerosol generating articles of this type are described in the prior art, for example, in EP 0822670.
  • aerosol generating device refers to a device comprising a heater element that interacts with the aerosol generating substrate of the aerosol generating article to generate an aerosol.
  • aerosol generating system refers to a combination of an aerosol generating device and an aerosol generating article.
  • aerosol generating article refers to an article including an aerosol generating substrate that is heated to produce and deliver inhalable aerosol to a consumer.
  • aerosol generating substrate element is used herein to denote an aerosol generating substrate wrapped with a paper layer to form a portion of an aerosol generating article.
  • aerosol generating substrate refers to substance capable of generating or releasing an aerosol.
  • the aerosol generating substrate may be a solid, paste, gel, slurry, liquid, or comprise any combination of solid, paste, gel, slurry, and liquid compounds.
  • the aerosol generating substrate is a solid, or a gel composition.
  • the aerosol generating substrate may preferably include nicotine.
  • mouthpiece is used herein to indicate the portion of the aerosol generating article that is designed to be contacted with the mouth of the consumer.
  • the mouthpiece can be the portion of the aerosol generating article that may include a filter, or in some cases the mouthpiece can be defined by the extent of the tipping wrapper.
  • An aerosol generating article includes an aerosol generating substrate, a filter element, and a first paper wrapper and a second paper wrapper circumscribing the aerosol forming substrate.
  • the first paper wrapper having a thickness in a range from about 60 micrometres to about 160 micrometres.
  • the first paper wrapper or the second paper wrapper joining the aerosol forming substrate to a filter element.
  • the first paper wrapper may separate the second paper wrapper from the aerosol generating substrate.
  • the first paper wrapper may contact the aerosol generating substrate.
  • the first paper wrapper may contact the second paper wrapper.
  • the second paper wrapper may not contact the aerosol generating substrate.
  • the first paper wrapper may circumscribe the aerosol forming substrate.
  • the second paper wrapper may circumscribe the first paper wrapper.
  • the second paper wrapper may overlap only a portion of the first paper wrapper.
  • the second paper wrapper may overlap less than about 50%, or less than 25% of the downstream length of the generating substrate.
  • the second paper wrapper may join the aerosol generating substrate to the filter element.
  • the second paper wrapper may be referred to as tipping paper.
  • the first paper wrapper may define an upstream outer surface of the aerosol generating article and the second paper may define a downstream outer surface of the aerosol generating article.
  • the first paper wrapper may not extend beyond the ends or length of the aerosol generating substrate.
  • the first paper wrapper may extend an entire length of the generating substrate.
  • the second paper wrapper may separate the first paper wrapper from the aerosol generating substrate.
  • the second paper wrapper may contact the aerosol generating substrate.
  • the second paper wrapper may contact the first paper wrapper.
  • the second paper wrapper may circumscribe the aerosol forming substrate.
  • the first paper wrapper may circumscribe the second paper wrapper.
  • the first paper wrapper may overlap the entire length of the second paper wrapper.
  • the first paper wrapper may overlap the entire length of the second paper wrapper and be coextensive with the second paper wrapper.
  • the first paper wrapper may join the aerosol generating substrate to the filter element.
  • the first paper wrapper may define an entire outer surface of the aerosol generating article.
  • the second paper wrapper may not extend beyond the ends or length of the aerosol generating substrate.
  • the second paper wrapper may extend an entire length of the generating substrate. At least about 80%, or at least about 90%, or at least about 95% of the aerosol generating substrate circumference may be circumscribed by less than three paper layers. Preferably the less than three paper layers do not extend beyond a length of the aerosol generating substrate. Preferably at least about 80%, or at least about 90%, or at least about 95% of the aerosol generating substrate circumference is circumscribed by less than three paper layers which circumscribe the aerosol generating substrate along substantially a length of the aerosol generating substrate.
  • the first paper wrapper and the second paper wrapper circumscribe the entire circumference of the aerosol generating substrate with very little overlap of each paper wrapper onto itself.
  • An overlap region forms more than one paper layer, such as two layers for example. The overlap region extends along the longitudinal length of the paper wrapper.
  • the overlap of the first paper wrapper and the overlap of the second paper wrapper are preferably offset from each other.
  • the overlap of the first paper wrapper and the overlap of the second paper wrapper are preferably offset from each other by at least about 45 degrees about the circumference of the aerosol generating substrate.
  • the overlap of the first paper wrapper and the overlap of the second paper wrapper are preferably offset from each other by at least about 90 degrees about the circumference of the aerosol generating substrate.
  • the overlap of the first paper wrapper and the overlap of the second paper wrapper are preferably offset from each other by about 180 degrees about the circumference of the aerosol generating substrate.
  • each paper wrapper onto itself may be about 20% or less of the circumference of the aerosol generating substrate. This overlap may be about 15% or less of the circumference of the aerosol generating substrate. This overlap may be about 10% or less of the circumference of the aerosol generating substrate. Reducing an overlay or overlap of the paper may help to prevent or minimize void spaces or air pockets defined between the paper layers in an overlap region.
  • the first paper wrapper may have a paper thickness in a range from about 60 micrometers to about 160 micrometers.
  • the first paper wrapper may have a paper thickness in a range from about 78 micrometers to about 160 micrometers.
  • the first paper wrapper may have a paper thickness in a range from about 78 micrometers to about 140 micrometers.
  • the first paper wrapper may have a paper thickness in a range from about 90 micrometers to about 160 micrometers.
  • the first paper wrapper may have a paper thickness in a range from about 100 micrometers to about 140 micrometers.
  • the first paper wrapper may have a paper thickness in a range from about 110 micrometers to about 160 micrometers.
  • the first paper wrapper may have a paper thickness in a range from about 125 micrometers to about 140 micrometers.
  • the first paper wrapper may have a paper thickness in a range from about 130 micrometers to about 160 micrometers.
  • the second paper wrapper may have a paper thickness in a range from about 10 micrometers to about 50 micrometers.
  • the second paper wrapper may have a paper thickness in a range from about 10 micrometers to about 35 micrometers.
  • the second paper wrapper may have a paper thickness in a range from about 15 micrometers to about 30 micrometers.
  • the second paper wrapper may have a paper thickness in a range from about 20 micrometers to about 25 micrometers.
  • the aerosol generating substrate may define a substantially cylindrical shape having a diameter in a range from about 6.8 mm to about 7.1 mm.
  • the aerosol generating substrate may define a substantially cylindrical shape having a diameter in a range from about 6.8 mm to about 7.0 mm.
  • the first paper wrapper may have a ratio of paper thickness to tobacco substrate diameter in a range from about 1:120 to about 1:40.
  • the first paper wrapper may have a ratio of paper thickness to tobacco substrate diameter in a range from about 1 : 100 to about 1 :50.
  • the first paper wrapper may have a ratio of paper thickness to tobacco substrate diameter in a range from about 1:75 to about 1:50.
  • the first paper wrapper may have a ratio of paper thickness to tobacco substrate diameter in a range from about 1 :60 to about 1 :50.
  • Conventionally wrapped tobacco substrates may have a ratio of paper wrapper thickness to tobacco substrate diameter of about 1:300.
  • the first paper wrapper may have a ratio of paper thickness to tobacco substrate element diameter in a range from about 1 : 100 to about 1 :40, or about 1 :75 to about 1 :50, or about 1 :65 to about 1 :50, or about 1 :60 to about 1 :50.
  • Conventionally wrapped tobacco substrates may have a ratio of paper thickness to tobacco substrate element diameter of about 1:300.
  • the first paper wrapper and the second paper wrapper may circumscribe the aerosol generating substrate to define the aerosol generating substrate with a substantially cylindrical shape.
  • the aerosol generating substrate may define a substantially cylindrical shape having a diameter in a range from about 6.8 mm to about 7.1 mm.
  • the aerosol generating substrate element wrapped by the first paper wrapper and the second paper wrapper may define a substantially cylindrical shape having a diameter in a range from about 7.1 mm to about 7.3 mm.
  • the aerosol generating article preferably includes an aerosol generating substrate, a filter element, and a first paper wrapper circumscribing the aerosol forming substrate and a second paper wrapper circumscribing the first paper wrapper.
  • the first paper wrapper having a thickness in a range from about 60 micrometres to about 160 micrometres.
  • the second paper wrapper joining the aerosol forming substrate to a filter element and having a thickness in a range from about 20 micrometres to about 40 micrometres.
  • the first paper wrapper does not extend beyond the ends of the aerosol generating substrate.
  • the first paper wrapper circumscribes an entire length of the aerosol generating substrate.
  • the first paper wrapper and the second paper wrapper each have an overlap of less than 20% of the circumference of the aerosol generating substrate.
  • the aerosol generating substrate has a diameter in a range from about 6.8 mm to about 7.0 mm.
  • the second paper wrapper circumscribes less than about 25% of the downstream length of the aerosol generating substrate.
  • the aerosol generating substrate element preferably includes an aerosol generating substrate having a diameter and a first paper wrapper having a thickness circumscribing the aerosol generating substrate and at least 80%, or at least 90% of the aerosol generating substrate circumference is circumscribed by less than three paper layers.
  • the first paper wrapper does not extend beyond the ends of the aerosol generating substrate.
  • the first paper wrapper circumscribes an entire length of the aerosol generating substrate.
  • the ratio of first paper wrapper thickness to tobacco substrate diameter is in a range from about 1:120 to about 1:40, or about 1:100 to about 1:50, or about 1:75.
  • the second paper wrapper circumscribes less than about 25% of the downstream length of the aerosol generating substrate.
  • the aerosol generating article includes the aerosol generating substrate and a mouthpiece.
  • the mouthpiece may comprise a filter.
  • a tipping wrapper (being either the first paper wrapper or preferably the second paper wrapper) may join the filter to the aerosol generating substrate.
  • One or more intermediate sections may separate the aerosol generating substrate and a mouthpiece.
  • the aerosol generating substrate may be a solid composition. This composition may include plant-based material.
  • the aerosol generating substrate may include tobacco, and preferably the tobacco contains volatile tobacco flavour compounds, which are released from the aerosol generating substrate upon heating.
  • the aerosol generating substrate may comprise homogenized tobacco material, aerosol former and a binder.
  • the aerosol generating substrate may include homogenized tobacco material.
  • the homogenized tobacco material may include tobacco material, from about 1 percent to about 5 percent of a binder, and from about 5 percent to about 30 percent of an aerosol-former, in dry weight basis.
  • the aerosol generating substrate may include a gathered sheet of homogenized tobacco material that is preferably crimped.
  • Nicotine may be present in the aerosol generating substrate in a range from about 0.5 to about 10% wt, nicotine, or about 0.5 to about 5% wt. nicotine.
  • the aerosol generating substrate may include about 1 to about 3% wt, nicotine, or about 1.5 to about 2.5% wt. nicotine, or about 2% wt nicotine.
  • the aerosol generating substrate may comprise any suitable type or types of tobacco material or tobacco substitute, in any suitable form.
  • the aerosol generating substrate may include flue-cured tobacco, Burley tobacco, Maryland tobacco, Oriental tobacco, specialty tobacco, homogenized or reconstituted tobacco, or any combination thereof.
  • the aerosol generating substrate may be provided in the form of tobacco cut filler, tobacco lamina, processed tobacco materials, such as volume expanded or puffed tobacco, processed tobacco stems, such as cut- rolled or cut-puffed stems, homogenized tobacco, reconstituted tobacco, cast leaf tobacco, or blends thereof, and the like.
  • tobacco cut filler is used herein to indicate tobacco material that is predominately formed from the lamina portion of the tobacco leaf.
  • tobacco cut filler is used herein to indicate both a single species of Nicotiana and two or more species of Nicotiana forming a tobacco cut filler blend.
  • homogenised tobacco denotes a material formed by agglomerating particulate tobacco. Homogenized tobacco may include reconstituted tobacco or cast leaf tobacco, or a mixture of both.
  • reconstituted tobacco refers to paper-like material that can be made from tobacco by-products, such as tobacco fines, tobacco dusts, tobacco stems, or a mixture of the foregoing. Reconstituted tobacco can be made by extracting the soluble chemicals in the tobacco by-products, processing the leftover tobacco fibers into a sheet, and then reapplying the extracted materials in concentrated form onto the sheet.
  • the term “cast leaf tobacco” is used herein to refer to a product resulting from a process well known in the art, which is based on casting a slurry comprising ground tobacco particles and a binder (for example, guar) onto a supportive surface, such as a belt conveyor, drying the slurry and removing the dried sheet from the supportive surface.
  • a supportive surface such as a belt conveyor
  • Exemplary methods for producing these types of aerosol generating substrates are described in US 5,724,998; US 5,584,306; US 4,341 ,228; US 5,584,306 and US 6,216,706.
  • the homogenised tobacco may be formed into a sheet which is crimped, convoluted, folded, or otherwise compressed, before being wrapped to form a rod.
  • sheets of homogenised tobacco material for use in the invention may be crimped using a crimping unit of the type described in CH-A-691156, which comprises a pair of rotatable crimping rollers.
  • sheets of homogenised tobacco material for use in the invention may be textured using other suitable machinery and processes that deform or perforate the sheets of homogenised tobacco material.
  • the aerosol generating substrate used in aerosol generating articles generally includes a higher level of aerosol former(s) than combusted smoking articles, such as cigarettes.
  • Humectants can also be referred to as an “aerosol former”.
  • An aerosol former is used to describe any suitable known compound or mixture of compounds that, in use, facilitates formation of an aerosol and that is substantially resistant to thermal degradation at the operating temperature of the aerosol generating substrate.
  • Suitable aerosol-formers are known in the art and include, but are not limited to: polyhydric alcohols, such as propylene glycol, triethylene glycol, 1,3-butanediol and glycerine; esters of polyhydric alcohols, such as glycerine mono-, di- or triacetate; and aliphatic esters of mono-, di- or polycarboxylic acids, such as dimethyl dodecanedioate and dimethyl tetradecanedioate.
  • Preferred aerosol formers are polyhydric alcohols or mixtures thereof, such as propylene glycol, triethylene glycol, 1,3-butanediol and, most preferred, glycerine or glycerine.
  • the aerosol generating substrate may comprise a single aerosol former. Alternatively, the aerosol generating substrate may comprise a combination of two or more aerosol formers.
  • the aerosol generating substrate may have a high level of aerosol former.
  • a high level of aerosol former means aerosol former content that is greater than about 10% or preferably greater than about 15% or more preferably greater than about 20%, by weight.
  • the aerosol generating substrate can also have an aerosol former content of between about 10% and about 30%, from about 15% and about 30%, or from about 20% and about 30%, by weight.
  • the aerosol generating substrate can also have a glycerine content of between about 10% and about 30%, from about 15% and about 30%, or from about 20% and about 30%, by weight.
  • the aerosol generating substrate may comprise at least about 1%, or at least about 2%, or at least about 5%, or at least about 7%, or at least about 10%, or at least about 12%, or at least about 15%, or at least about 18% aerosol former, by weight.
  • the aerosol generating substrate may comprise aerosol former in a range from about 1 to about 20%, or about 5 to about 20%, or about 10 to about 20%, by weight.
  • the aerosol generating substrate may comprise at least about 1%, or at least about 2%, or at least about 5%, or at least about 7%, or at least about 10%, or at least about 12%, or at least about 15%, or at least about 18% glycerine, by weight.
  • the aerosol generating substrate may comprise glycerine in a range from about 1 to about 20%, or about 5 to about 20%, or about 10 to about 20%, by weight.
  • the aerosol generating article may be generally cylindrical. This enables a smooth flow of the aerosol.
  • the aerosol generating article may have an outer diameter, for example, between 7.1 millimetres and 7.3 millimetres, or between 7.15 millimetres and 7.25 millimetres.
  • the aerosol generating article may have a length, for example, between 10 millimetres and 60 millimetres, between 15 millimetres to 50 millimetres, or between 20 millimetres and 45 millimetres.
  • the aerosol generating substrate may include a flavourant. Botanical materials provide flavourantthat may impart a flavour to the taste of the aerosol generated by the aerosol generating article.
  • a flavourant is any natural or artificial compound that affects the organoleptic quality of the aerosol.
  • sources of flavourants include mints such as peppermint and spearmint, coffee, tea, cinnamon, clove, cocoa, vanilla, eucalyptus, geranium, agave, and juniper; and combinations thereof.
  • the aerosol generating substrate may include an essential oil.
  • Essential oils may provide flavourantthat may impart a flavour to the taste of the aerosol generated by the aerosol generating article. Suitable essential oils include, but are not limited to, eugenol, peppermint oil and spearmint oil. A preferred essential oil is eugenol.
  • Essential oil may be present in the aerosol generating substrate in an amount of at least about 0.1% by weight, or at least about 0.5% by weight, or at least about 1% by weight.
  • Essential oil may be present in the aerosol generating substrate in a range from about 0.1% by weight to about 10% by weight, or from about 0.1 % by weight to about 5% by weight, or from about 0.5% by weight to about 2%.
  • the aerosol generating substrate may include homogenized tobacco material.
  • the homogenized tobacco material may include tobacco material, from about 1 percent to about 5 percent of a binder, and from about 5 percent to about 30 percent of an aerosol-former, on a dry weight basis.
  • Sheets of homogenized tobacco for use in the aerosol-generating article of the present invention may be made by methods known in the art, for example the methods disclosed in International patent application WO-A-201 2/1 64009 A2.
  • sheets of homogenized tobacco material for use in the aerosol-generating article are formed from a slurry comprising particulate tobacco, guar gum, cellulose fibres and glycerine by a casting process.
  • the aerosol generating substrate may include a gathered sheet of homogenized tobacco material that is preferably crimped.
  • crimped denotes a sheet having a plurality of substantially parallel ridges or corrugations.
  • the substantially parallel ridges or corrugations extend along or parallel to the longitudinal axis of the aerosol-generating article.
  • An aerosol generating system may comprise: a heat source; an aerosol generating substrate; at least one air inlet downstream of the aerosol generating substrate; and an airflow pathway extending between the at least one air inlet and the mouth-end of the article.
  • the heat source may be integral with an aerosol generating device and a consumable aerosol generating article may be releasably received within the aerosol generating device.
  • the heat source may be a combustible heat source, a chemical heat source, an electrical heat source, a heat sink or any combination thereof.
  • the heat source may be an electrical heat source, preferably shaped in the form of a blade that can be inserted into the aerosol generating substrate.
  • the heat source may be configured to surround the aerosol generating substrate, and as such may be in the form of a hollow cylinder, or any other such suitable form.
  • the heat source is configured to heat the aerosol generating substrate directly without transmitting heat to the aerosol generating substrate through the at least one paper layer.
  • the aerosol generating substrate may include an induction heating element or susceptor or a plurality of induction heating elements or susceptors. Induction heating elements or susceptors heat up in the presence of an alternating or fluctuating electromagnetic field. When heating is by induction heating, a fluctuating electromagnetic field is transmitted through the aerosol generating article to the induction heating element or susceptor such that the susceptor or inducting heating element changes the fluctuating field into thermal energy thus heating the aerosol generating substrate.
  • the induction heating element or susceptor may be formed from any material that can be inductively heated to a temperature sufficient to generate an aerosol from the aerosol generating substrate.
  • the induction heating element or susceptor may comprises a metal or carbon.
  • a preferred induction heating element or susceptor may comprise a ferromagnetic material, for example ferritic iron, or a ferromagnetic steel or stainless steel.
  • the induction heating element or susceptor may comprise aluminium.
  • Induction heating element or susceptors may be formed from 400 series stainless steels, for example grade 410, or grade 420, or grade 430 stainless 20 steel. Different materials will dissipate different amounts of energy when positioned within electromagnetic fields having similar values of frequency and field strength.
  • the induction heating element or susceptors are heated to a temperature in excess of 250 degrees Celsius. However, preferably the induction heating element or susceptors are heated less than 350 degrees Celsius to prevent burning of material in contact with the susceptor.
  • the aerosol generating substrate may comprise a metallic induction heating element.
  • the metallic induction heating element may comprise plurality of metallic induction heating elements.
  • the metallic induction heating element may comprise a metallic induction heating ring element.
  • the first paper wrapper may exhibit a range of permeability including not being permeable. Permeability of cigarette paper is determined by utilizing the International Standard test method ISO 2965:2009 and the result is presented as cubic centimetres per minute per square centimetre and referred to as “CORESTA units”.
  • the permeability of the wrapper described herein may be in a range from about 1 to about 10 CORESTA units, about 5 to about 20 CORESTA units, or about 1 to about 5 CORESTA units.
  • the first paper wrapper and the second paper wrapper may each be independently formed of any cellulosic material such as paper, wood, textile, natural as well as artificial fibers.
  • the first paper wrapper may comprise a laminate of a paper layer and a metal layer.
  • the first paper wrapper may comprise a laminate of a paper layer and an aluminium layer.
  • the laminate of a paper layer and an aluminium layer may have a uniform thickness in a range from about 78 micrometers to about 160 micrometers, or from about 78 micrometers to about 140 micrometers, or from about 100 micrometers to about 140 micrometers, or from about 125 micrometers to about 140 micrometers.
  • the laminate of a paper layer and a metal layer may not extend beyond ends of the aerosol generating substrate.
  • the resistance to draw (RTD) of the aerosol-generating article after insertion into the aerosol generating device is preferably between about 80 mm WG and about 140 mm WG, more preferably between about 100 mm WG and about 120 mm WG.
  • resistance to draw is expressed with the units of pressure 'mm WG' or 'mm of water gauge' and is measured in accordance with ISO 6565:2002.
  • the resistance to draw (RTD) of the rod of aerosol-generating substrate is preferably between about 50 mm WG and about 80 mm WG.
  • the RTD of the rod of aerosol-generating substrate is between about 5 mm WG and about 8 mm WG per millimetre length of the rod.
  • FIG. 1 A is a schematic cross-sectional diagram of an aerosol generating article.
  • FIG. 1 B is a schematic cross-sectional diagram of another aerosol generating article.
  • FIG. 2 is a schematic cross-sectional diagram of the aerosol generating substrate element along line 2-2 in FIG. 1A.
  • FIG. 3 is a schematic cross-sectional diagram of the aerosol generating substrate element along line 3-3 in FIG. 2.
  • FIG. 4 is a schematic cross-sectional diagram of an aerosol generating system.
  • FIG. 5 is a schematic cross-sectional diagram a heating blade inserted into the aerosol generating substrate element.
  • FIGS. 1-5 illustrate one or more examples of aerosol generating articles, components of aerosol generating articles, or aerosol generating systems described above.
  • the schematic drawings are not necessarily to scale and are presented for purposes of illustration and not limitation.
  • the drawings depict one or more aspects described in this disclosure. However, it will be understood that other aspects not depicted in the drawings fall within the scope and spirit of this disclosure.
  • the aerosol generating article includes an aerosol generating substrate 20, a filter element 22, and a first paper wrapper 30 and a second paper wrapper 40 circumscribing the aerosol forming substrate 20.
  • the first paper wrapper 30 has a thickness in a range from about 60 micrometers to about 160 micrometers.
  • the first paper wrapper 30 or the second paper wrapper 40 joins the aerosol forming substrate 20 to a filter element 22.
  • the aerosol generating article includes an aerosol generating substrate 20, a filter element 22, and a first paper wrapper 30 and a second paper wrapper 40 circumscribing the aerosol forming substrate 20.
  • the first paper wrapper 30 has a thickness in a range from about 90 micrometers to about 160 micrometers.
  • the second paper wrapper 40 joins the aerosol forming substrate 20 to a filter element 22.
  • FIG. 1A illustrates the first paper wrapper 30 circumscribing the aerosol generating substrate 20 and the second paper wrapper 40 circumscribing the first paper wrapper 30 and the filter element 22.
  • the first paper wrapper 30 extends along the entire length of the aerosol generating substrate 20.
  • the second paper wrapper 40 joins the aerosol generating substrate 20 to the filter element 22.
  • the second paper wrapper 40 extends onto only a downstream portion of the first paper wrapper 30.
  • FIG. 1B illustrates the second paper wrapper 40 circumscribing the aerosol generating substrate 20 and the first paper wrapper 30 circumscribing the second paper wrapper 40 and the filter element 22.
  • the first paper wrapper 30 joins the aerosol generating substrate 20 to the filter element 22.
  • the first paper wrapper 30 is coextensive with the second paper wrapper 40 along the entire length of the aerosol generating substrate 20 from the distal end 13 to a proximal end 11.
  • An intermediate section 24 separates a filter element 22 from the aerosol generating substrate element 12.
  • the aerosol generating substrate 12, intermediate section 24, and a filter element 22 are aligned from a distal end 13 to a proximal end 11 in serial order and form a cylinder.
  • the second paper wrapper 40 or the first paper wrapper 30 circumscribes the aerosol generating article 10 to join the aerosol generating substrate element 12 to the intermediate section 24, and a filter element 22.
  • the intermediate section 24 may comprise on or more of, a hollow cellulose acetate tube or a polylactic acid filter segment.
  • the filter element 22 may define a mouthpiece segment and be formed of cellulose acetate material.
  • the aerosol generating substrate element 12, the intermediate section 24, and a filter element 22 may be individually wrapped with a paper layer and then joined to each other with the second paper wrapper 40 or the first paper wrapper 30.
  • the aerosol-generating substrate element 12 is wrapped with the second paper wrapper 40 or the first paper wrapper 30, as described herein.
  • the aerosol generating article 10 has a mouth end or proximal end 11 and an upstream, distal end 13 located at the opposite end of the article to the mouth end 11.
  • the aerosol generating article 10 shown in FIG. 1A and FIG. 1B are particularly suitable for use with an electrically operated aerosol generating device comprising a heater for heating the aerosol generating substrate element 12.
  • FIG. 2 is a schematic cross-sectional diagram of the aerosol generating substrate element
  • FIG. 3 is a schematic cross-sectional diagram of the aerosol generating substrate element 12 along line 3-3 in FIG. 2.
  • the first paper wrapper 30 circumscribes the aerosol generating substrate 20 to define the aerosol generating substrate element 12 with a substantially cylindrical shape.
  • the second paper wrapper circumscribes the first paper wrapper 30 to define a substantially cylindrical shape
  • the aerosol generating substrate 20 defines a substantially cylindrical shape having a diameter 23 in a range from about 6.8 mm to about 7.1 mm.
  • the aerosol generating substrate element 12 defines a substantially cylindrical shape having a diameter 33 in a range from about 7.1 mm to about 7.3 mm or from about 7.15 mm to about 7.25 mm.
  • the first paper wrapper 30 has a thickness T in a range from about 60 micrometers to about 160 micrometers.
  • the first paper wrapper 30 may preferably have a thickness in a range from about 78 micrometers to about 160 micrometers, or about 78 micrometers to about 140 micrometers, or from about 100 micrometers to about 140 micrometers, or from about 125 micrometers to about 140 micrometers.
  • the first paper wrapper 30 has a ratio of paper thickness T to tobacco substrate diameter
  • the first paper wrapper 30 circumscribes the entire circumference of the aerosol generating substrate 20 with very little first overlap 100 of the first paper wrapper 30 onto itself.
  • the first overlap 100 region forms more than one paper layer. In FIG. 2, the first overlap 100 forms two layers of paper.
  • the first overlap 100 may be about 20% or less of the circumference of the aerosol generating substrate 20.
  • the first overlap 100 may be about 10% or less of the circumference of the aerosol generating substrate 20.
  • the first overlap 100 may be about 5% or less of the circumference of the aerosol generating substrate 20.
  • the first paper wrapper 30 may not extend beyond the ends 25, 26 of the aerosol generating substrate 20.
  • the first paper wrapper 30 circumscribes an entire length of the aerosol generating substrate 20 between the ends 25, 26 of the aerosol generating substrate 20.
  • the second paper wrapper 40 circumscribes the entire circumference of the first paper wrapper 30 with very little second overlap 101 of the second paper wrapper 40 onto itself.
  • the second overlap 101 region forms more than one paper layer. In FIG. 2, the second overlap 101 forms two layers of paper.
  • the second overlap 101 may be about 20% or less of the circumference of the aerosol generating substrate 20.
  • the second overlap 101 may be about 10% or less of the circumference of the aerosol generating substrate 20.
  • the second overlap 101 may be about 5% or less of the circumference of the aerosol generating substrate 20.
  • the second paper wrapper 40 may extend beyond the downstream end 26 of the aerosol generating substrate 20.
  • the second paper wrapper 40 circumscribes only a downstream about 25% of the entire length of the aerosol generating substrate 20 between the ends 25, 26 of the aerosol generating substrate 20.
  • the first overlap 100 region is offset from the second overlap 101 region by at least about 45 degrees about the circumference of the aerosol generating substrate 20.
  • FIG. 2 illustrates that where the second paper wrapper 40 overlays the first paper wrapper 30, each paper wrapper forms substantially single turn or single layer around the circumference of the aerosol generating substrate 20. At least about 80%, or at least about 90%, or at least about 95% of the aerosol generating substrate 20 circumference is circumscribed by less than three paper layers or wrappers 30, 40. At least about 80%, or at least about 90%, or at least about 95% of the aerosol generating substrate 20 circumference is circumscribed by less than two paper layers or wrappers that do not extend beyond a length or the ends 25, 26 of the aerosol generating substrate 20.
  • FIG. 4 is a schematic cross-sectional diagram of an aerosol generating system 201.
  • FIG. 5 is a schematic cross-sectional diagram a heating blade 230 inserted into the aerosol generating substrate element 12.
  • the aerosol generating article 10 may be used with the aerosol generating device 200 as illustrated in FIG. 4 and FIG. 5.
  • the aerosol generating device 200 includes a housing 210 defining the receptacle 220, which is configured to receive the aerosol generating article 10.
  • the aerosol generating device 200 also includes a heating blade element 230 configured to pierce the aerosol generating substrate element 12 of the aerosol generating article 10.
  • the heating blade element 230 may comprise an electrically resistive heating component.
  • the device 200 includes a power supply 240 and control electronics 250 that cooperate to control heating of heating blade element 230.
  • the aerosol generating article 10 illustrates an aerosol-generating substrate element 12, an intermediate section 24, and a filter element 22 aligned from a distal end 13 to a proximal end 11 in serial order and form a cylinder.
  • the aerosol generating substrate 12 has a length of about 12 millimetres.
  • the aerosol generating substrate 12 is cylindrical in shape and has a substantially circular cross-section.
  • the aerosol generating substrate 12 may comprise a gathered sheet of homogenised tobacco material.
  • the sheet of homogenised tobacco material may comprise about 10 percent by weight on a dry basis of glycerine.
  • the intermediate section 24 may be a hollow cellulose acetate tube having a length of about 8 millimetres and a thickness of 1 millimetre.
  • the mouthpiece segment or filter element 22 may comprises a plug of cellulose acetate tow of 8 denier per filament and has a length of about 7 millimetres.
  • FIG. 5 illustrates the heating blade element 230 disposed within the aerosol generating substrate 12, 20.
  • the heating blade element 230 may heat the aerosol generating substrate 12 of the aerosol generating article 10. Heating of the aerosol generating substrate 12 causes the aerosol generating substrate 12 to generate an aerosol containing the nicotine which can transfer out of the aerosol generating article 10 at the proximal end 11.
  • the heating blade element 230 may have a width 233 of about 5 mm.
  • the aerosol generating substrate 20 defines a substantially cylindrical shape having a diameter 23 in a range from about 6.8 mm to about 7.1 mm, or about 6.9 mm to about 7.0 mm.
  • the aerosol generating substrate element 12 defines a substantially cylindrical shape having a diameter 33 in a range from about 7.1 mm to about 7.3 mm, or about 7.15 mm to about 7.25 mm.
  • the heating blade element 230 may lie within about 1 mm from the first paper wrapper 30.
  • the heating mechanism may be by induction where the heating element emits radio-magnetic radiation which is absorbed by one or more metallic induction heating elements when the aerosol generating article 10 is positioned in the receptacle 220 of the aerosol generating device 200.
  • the volatile compounds evolved from the aerosol generating substrate 12 are drawn downstream through the aerosol generating article 10 and condense to form an aerosol that is drawn through the mouthpiece 11 of the aerosol generating article 10 into the user’s mouth.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)
  • Nozzles (AREA)
  • Containers And Packaging Bodies Having A Special Means To Remove Contents (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Paper (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
  • Disinfection, Sterilisation Or Deodorisation Of Air (AREA)

Abstract

Un article de génération d'aérosol (10) comprend un substrat de génération d'aérosol (20), un élément de filtre (22), et une première enveloppe de papier (30) et une seconde enveloppe de papier (40) entourant le substrat de formation d'aérosol. La première enveloppe de papier a une épaisseur dans une plage d'environ 90 micromètres à environ 160 micromètres. La seconde enveloppe de papier relie le substrat de formation d'aérosol à un élément de filtre.
EP20815946.7A 2019-11-29 2020-11-23 Article de génération d'aérosol avec papier épais Pending EP4064881A1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP19212668 2019-11-29
PCT/IB2020/061050 WO2021105855A1 (fr) 2019-11-29 2020-11-23 Article de génération d'aérosol avec papier épais

Publications (1)

Publication Number Publication Date
EP4064881A1 true EP4064881A1 (fr) 2022-10-05

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US (1) US20220408799A1 (fr)
EP (1) EP4064881A1 (fr)
JP (1) JP2023503560A (fr)
KR (1) KR20220109399A (fr)
CN (1) CN114650738A (fr)
BR (1) BR112022009053A2 (fr)
MX (1) MX2022006449A (fr)
WO (1) WO2021105855A1 (fr)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2024017787A1 (fr) * 2022-07-20 2024-01-25 Philip Morris Products S.A. Article de génération d'aérosol avec enveloppe épaisse et légère
WO2024017792A1 (fr) * 2022-07-20 2024-01-25 Philip Morris Products S.A. Article de génération d'aérosol avec enveloppe épaisse et substrat dense

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4341228A (en) 1981-01-07 1982-07-27 Philip Morris Incorporated Method for employing tobacco dust in a paper-making type preparation of reconstituted tobacco and the smoking material produced thereby
IE63936B1 (en) * 1989-06-23 1995-06-28 British American Tobacco Co Improvements relating to smoking articles
JP3681410B2 (ja) 1992-04-09 2005-08-10 フィリップ・モーリス・プロダクツ・インコーポレイテッド 再構成タバコシート及びその製造法及び使用法
US5584306A (en) 1994-11-09 1996-12-17 Beauman; Emory Reconstituted tobacco material and method of its production
US5774493A (en) 1996-08-02 1998-06-30 General Electric Company Sequence constructions for delay-and-correlate transmitted reference signaling
CH691156A5 (fr) 1998-05-19 2001-05-15 Philip Morris Prod Ligne d'alimentation d'une machine de production de filtres de cigarettes.
US6216706B1 (en) 1999-05-27 2001-04-17 Philip Morris Incorporated Method and apparatus for producing reconstituted tobacco sheets
EP3033950B1 (fr) 2011-05-31 2018-07-04 Philip Morris Products S.a.s. Tiges pour une utilisation dans des articles à fumer
WO2016042101A1 (fr) * 2014-09-19 2016-03-24 Philip Morris Products S.A. Procédé et appareil de stockage intermédiaire de produits semi-finis à double longueur
RU2750012C2 (ru) * 2016-09-01 2021-06-21 Филип Моррис Продактс С.А. Узел сусцептора и изделие для генерирования аэрозоля, содержащее его

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BR112022009053A2 (pt) 2022-08-09
KR20220109399A (ko) 2022-08-04
WO2021105855A1 (fr) 2021-06-03
JP2023503560A (ja) 2023-01-31
MX2022006449A (es) 2022-06-22
CN114650738A (zh) 2022-06-21
US20220408799A1 (en) 2022-12-29

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