EP3866749A1 - Cosmetic foam which is suitable for jar products and production of such cosmetic foam - Google Patents
Cosmetic foam which is suitable for jar products and production of such cosmetic foamInfo
- Publication number
- EP3866749A1 EP3866749A1 EP19773072.4A EP19773072A EP3866749A1 EP 3866749 A1 EP3866749 A1 EP 3866749A1 EP 19773072 A EP19773072 A EP 19773072A EP 3866749 A1 EP3866749 A1 EP 3866749A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- emulsion
- oil
- wax
- foam according
- cosmetic foam
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000008260 cosmetic foam Substances 0.000 title claims abstract description 30
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 10
- 239000000839 emulsion Substances 0.000 claims abstract description 62
- 239000001993 wax Substances 0.000 claims abstract description 47
- 238000002844 melting Methods 0.000 claims abstract description 25
- 230000008018 melting Effects 0.000 claims abstract description 24
- 239000003921 oil Substances 0.000 claims abstract description 24
- 239000007789 gas Substances 0.000 claims abstract description 16
- 239000003380 propellant Substances 0.000 claims abstract description 14
- 239000007788 liquid Substances 0.000 claims abstract description 13
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 13
- 150000002148 esters Chemical class 0.000 claims abstract description 12
- 239000004094 surface-active agent Substances 0.000 claims abstract description 11
- 150000002170 ethers Chemical class 0.000 claims abstract description 10
- 229920001451 polypropylene glycol Polymers 0.000 claims abstract description 10
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 7
- 239000002480 mineral oil Substances 0.000 claims abstract description 6
- 108090000623 proteins and genes Proteins 0.000 claims abstract description 6
- 102000004169 proteins and genes Human genes 0.000 claims abstract description 6
- 229920002545 silicone oil Polymers 0.000 claims abstract description 6
- VUWCWMOCWKCZTA-UHFFFAOYSA-N 1,2-thiazol-4-one Chemical class O=C1CSN=C1 VUWCWMOCWKCZTA-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000007764 o/w emulsion Substances 0.000 claims abstract description 5
- 239000012184 mineral wax Substances 0.000 claims abstract description 4
- 239000006260 foam Substances 0.000 claims description 23
- 235000019198 oils Nutrition 0.000 claims description 23
- -1 parabens Chemical class 0.000 claims description 20
- 150000001875 compounds Chemical class 0.000 claims description 16
- 238000002360 preparation method Methods 0.000 claims description 15
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims description 9
- 238000003860 storage Methods 0.000 claims description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 6
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 6
- 239000008346 aqueous phase Substances 0.000 claims description 6
- NOPFSRXAKWQILS-UHFFFAOYSA-N docosan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCCCCO NOPFSRXAKWQILS-UHFFFAOYSA-N 0.000 claims description 6
- 238000011049 filling Methods 0.000 claims description 6
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 claims description 6
- VVOAZFWZEDHOOU-UHFFFAOYSA-N magnolol Chemical compound OC1=CC=C(CC=C)C=C1C1=CC(CC=C)=CC=C1O VVOAZFWZEDHOOU-UHFFFAOYSA-N 0.000 claims description 6
- HLZKNKRTKFSKGZ-UHFFFAOYSA-N tetradecan-1-ol Chemical compound CCCCCCCCCCCCCCO HLZKNKRTKFSKGZ-UHFFFAOYSA-N 0.000 claims description 6
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- YBJHBAHKTGYVGT-ZKWXMUAHSA-N (+)-Biotin Chemical compound N1C(=O)N[C@@H]2[C@H](CCCCC(=O)O)SC[C@@H]21 YBJHBAHKTGYVGT-ZKWXMUAHSA-N 0.000 claims description 4
- YVLPJIGOMTXXLP-UHFFFAOYSA-N 15-cis-phytoene Chemical compound CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=CC=CC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)C YVLPJIGOMTXXLP-UHFFFAOYSA-N 0.000 claims description 4
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 4
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 claims description 4
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- DDRJAANPRJIHGJ-UHFFFAOYSA-N creatinine Chemical compound CN1CC(=O)NC1=N DDRJAANPRJIHGJ-UHFFFAOYSA-N 0.000 claims description 4
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 4
- 239000000194 fatty acid Substances 0.000 claims description 4
- 229930195729 fatty acid Natural products 0.000 claims description 4
- 150000004665 fatty acids Chemical class 0.000 claims description 4
- OVBPIULPVIDEAO-LBPRGKRZSA-N folic acid Chemical compound C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)N[C@@H](CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-LBPRGKRZSA-N 0.000 claims description 4
- AGBQKNBQESQNJD-UHFFFAOYSA-N lipoic acid Chemical compound OC(=O)CCCCC1CCSS1 AGBQKNBQESQNJD-UHFFFAOYSA-N 0.000 claims description 4
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- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 claims description 4
- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 claims description 4
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- LEACJMVNYZDSKR-UHFFFAOYSA-N 2-octyldodecan-1-ol Chemical compound CCCCCCCCCCC(CO)CCCCCCCC LEACJMVNYZDSKR-UHFFFAOYSA-N 0.000 claims description 3
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 3
- ANZUDYZHSVGBRF-UHFFFAOYSA-N 3-ethylnonane-1,2,3-triol Chemical compound CCCCCCC(O)(CC)C(O)CO ANZUDYZHSVGBRF-UHFFFAOYSA-N 0.000 claims description 3
- 235000019489 Almond oil Nutrition 0.000 claims description 3
- 241000196324 Embryophyta Species 0.000 claims description 3
- 239000008168 almond oil Substances 0.000 claims description 3
- BTFJIXJJCSYFAL-UHFFFAOYSA-N arachidyl alcohol Natural products CCCCCCCCCCCCCCCCCCCCO BTFJIXJJCSYFAL-UHFFFAOYSA-N 0.000 claims description 3
- 229940116224 behenate Drugs 0.000 claims description 3
- UKMSUNONTOPOIO-UHFFFAOYSA-M behenate Chemical compound CCCCCCCCCCCCCCCCCCCCCC([O-])=O UKMSUNONTOPOIO-UHFFFAOYSA-M 0.000 claims description 3
- 229940081733 cetearyl alcohol Drugs 0.000 claims description 3
- 229960000541 cetyl alcohol Drugs 0.000 claims description 3
- 229940074979 cetyl palmitate Drugs 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 239000003240 coconut oil Substances 0.000 claims description 3
- 235000019864 coconut oil Nutrition 0.000 claims description 3
- 229960000735 docosanol Drugs 0.000 claims description 3
- 239000000975 dye Substances 0.000 claims description 3
- 125000005456 glyceride group Chemical group 0.000 claims description 3
- PXDJXZJSCPSGGI-UHFFFAOYSA-N hexadecanoic acid hexadecyl ester Natural products CCCCCCCCCCCCCCCCOC(=O)CCCCCCCCCCCCCCC PXDJXZJSCPSGGI-UHFFFAOYSA-N 0.000 claims description 3
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- 238000005259 measurement Methods 0.000 claims description 3
- 229940043348 myristyl alcohol Drugs 0.000 claims description 3
- GOQYKNQRPGWPLP-UHFFFAOYSA-N n-heptadecyl alcohol Natural products CCCCCCCCCCCCCCCCCO GOQYKNQRPGWPLP-UHFFFAOYSA-N 0.000 claims description 3
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- 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 3
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- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 2
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 claims description 2
- PHIQHXFUZVPYII-ZCFIWIBFSA-O (R)-carnitinium Chemical compound C[N+](C)(C)C[C@H](O)CC(O)=O PHIQHXFUZVPYII-ZCFIWIBFSA-O 0.000 claims description 2
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- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 2
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- WNLRTRBMVRJNCN-UHFFFAOYSA-N hexanedioic acid Natural products OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- WPFVBOQKRVRMJB-UHFFFAOYSA-N hydroxycitronellal Chemical compound O=CCC(C)CCCC(C)(C)O WPFVBOQKRVRMJB-UHFFFAOYSA-N 0.000 description 1
- 235000015243 ice cream Nutrition 0.000 description 1
- 239000012182 japan wax Substances 0.000 description 1
- SVURIXNDRWRAFU-UHFFFAOYSA-N juniperanol Natural products C1C23C(C)CCC3C(C)(C)C1C(O)(C)CC2 SVURIXNDRWRAFU-UHFFFAOYSA-N 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000000171 lavandula angustifolia l. flower oil Substances 0.000 description 1
- 235000001510 limonene Nutrition 0.000 description 1
- 229940087305 limonene Drugs 0.000 description 1
- 229930007744 linalool Natural products 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- JPTOCTSNXXKSSN-UHFFFAOYSA-N methylheptenone Chemical compound CCCC=CC(=O)CC JPTOCTSNXXKSSN-UHFFFAOYSA-N 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 235000010446 mineral oil Nutrition 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 235000011929 mousse Nutrition 0.000 description 1
- 239000001627 myristica fragrans houtt. fruit oil Substances 0.000 description 1
- 125000000740 n-pentyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 238000010943 off-gassing Methods 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000010816 packaging waste Substances 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 244000045947 parasite Species 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 244000052769 pathogen Species 0.000 description 1
- 235000019271 petrolatum Nutrition 0.000 description 1
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 description 1
- 230000002028 premature Effects 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000010668 rosemary oil Substances 0.000 description 1
- 229940058206 rosemary oil Drugs 0.000 description 1
- 239000002453 shampoo Substances 0.000 description 1
- 230000036556 skin irritation Effects 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- RYYKJJJTJZKILX-UHFFFAOYSA-M sodium octadecanoate Chemical class [Na+].CCCCCCCCCCCCCCCCCC([O-])=O RYYKJJJTJZKILX-UHFFFAOYSA-M 0.000 description 1
- KDHFCTLPQJQDQI-BDQAORGHSA-M sodium;(4s)-4-amino-5-octadecanoyloxy-5-oxopentanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC(=O)OC(=O)[C@@H](N)CCC([O-])=O KDHFCTLPQJQDQI-BDQAORGHSA-M 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 229940116411 terpineol Drugs 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 229960000790 thymol Drugs 0.000 description 1
- CRDAMVZIKSXKFV-UHFFFAOYSA-N trans-Farnesol Natural products CC(C)=CCCC(C)=CCCC(C)=CCO CRDAMVZIKSXKFV-UHFFFAOYSA-N 0.000 description 1
- 239000001069 triethyl citrate Substances 0.000 description 1
- 235000013769 triethyl citrate Nutrition 0.000 description 1
- VMYFZRTXGLUXMZ-UHFFFAOYSA-N triethyl citrate Natural products CCOC(=O)C(O)(C(=O)OCC)C(=O)OCC VMYFZRTXGLUXMZ-UHFFFAOYSA-N 0.000 description 1
- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 description 1
- FGQOOHJZONJGDT-UHFFFAOYSA-N vanillin Natural products COC1=CC(O)=CC(C=O)=C1 FGQOOHJZONJGDT-UHFFFAOYSA-N 0.000 description 1
- 235000012141 vanillin Nutrition 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000007762 w/o emulsion Substances 0.000 description 1
- 239000008256 whipped cream Substances 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/062—Oil-in-water emulsions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/463—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/33—Free of surfactant
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/34—Free of silicones
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/87—Application Devices; Containers; Packaging
Definitions
- the present invention relates to a cosmetic foam containing
- O / W emulsion being free from polyethylene glycols and their ethers or esters, polypropylene glycols and their ethers and esters, surfactants, proteins, mineral oils and waxes, silicone oils and waxes, parabens, isothiazolinones and 3-iodopropargyl-A / butylcarbamate (IPBC),
- Emulsions are generally understood to be heterogeneous systems which consist of two immiscible or only to a limited extent miscible liquids, which are usually referred to as phases and in which one of the two liquids is dispersed in the form of very fine droplets in the other liquid. When viewed externally and with the naked eye, emulsions appear homogeneous.
- the two liquids are water and oil and oil droplets are finely distributed in water, then it is an oil-in-water emulsion (O / W emulsion, e.g. milk).
- O / W emulsion e.g. milk
- the basic character of an O / W emulsion is characterized by the water.
- a water-in-oil emulsion (W / O emulsion, e.g. butter) is the opposite principle, whereby the basic character is determined by the oil.
- foamed emulsions have a special feeling on the skin due to their foam consistency, which users perceive as being easier to distribute on the skin. It is a "lighter” and less sticky skin feeling.
- Foamed cosmetic preparations are usually presented in the form of aerosol cans. Such products are relatively undemanding when compared to "permanent foams" because the foam only has to be stable for a relatively short time. However, they have the disadvantage that certain safety aspects must be taken into account during storage and manufacture, since they are a due to the excess pressure of the propellant gas
- the large-scale production of preparations foamed in the crucible is anything but trivial, since the propellant gas must be incorporated into the recipe in a stable manner during the manufacturing process. As a rule, this requires the highest possible consistency so that the propellant gas does not escape again.
- the preparation must be so low-viscous that it is stirrable, flowable and fillable. The bottling is usually carried out in
- Polypropylene glycols and derivatives are used.
- PEG derivatives or PPG derivatives and / or surfactants i.e. surface-active compounds with an HLB value greater than 10.
- Polyethylene glycols and polyethylene glycol derivatives are compounds with an alcohol or acid function that are wholly or partially etherified or esterified with polyethylene glycols. The same applies to the polypropylene glycols. These PEG derivatives or PPG derivatives are increasingly undesirable for consumers, as they are used by some
- a foamed emulsion which is free of polyethylene glycols, Polypropylene glycols and their derivatives (PEG derivatives, PPG derivatives) and free of surfactants (whereby sodium cetearyl sulfate is by definition not counted among the surfactants).
- the composition of the oil phase of an emulsion also influences the stability of a cosmetic foam.
- the oil phase usually contains mineral oils (e.g. petroleum jelly, paraffin oils and waxes) and / or silicone oils to protect the foam from outgassing.
- Proportion of propellant gas (up to about 10% by volume), which are usually referred to as "mousse” or whipped cream. With such a low gas content, the foam bubbles are practically barely noticeable. In terms of their sensory properties, these products clearly lag behind foams with a higher gas content (greater than or equal to 20% by volume).
- a cosmetic foam containing a) an oil-in-water emulsion (O / W emulsion) containing aa) a wax combination of at least two waxes, the first wax having a melting point of 40-50 ° C. 1.013 bar and the second wax has a melting point of over 50 ° C. at 1.013 bar, the wax having a melting point of 40-50 ° C. in a concentration of 4 to 10% by weight and the wax having a Melting point of over 50 ° C is contained in a concentration of 1-8 wt.% Each based on the total weight of the O / W emulsion
- O / W emulsion being free from polyethylene glycols and their ethers or esters, polypropylene glycols and their ethers and esters, surfactants, proteins, mineral oils and waxes, silicone oils and waxes, parabens, isothiazolinones and 3-iodopropargyl-A / butylcarbamate (IPBC),
- the emulsion has a solid fat content at 40 ° C. of at least 40%, measured by means of DSC measurement.
- the emulsion has a solid fat content at 50 ° C. of at least 15%, measured by means of DSC measurement. It is also advantageous according to the invention if the density of the foam is 0.5 to 0.8 g / ml. This information refers to the condition at 20 ° C and 1,013 bar ambient pressure.
- the waxes with a melting point of over 50 ° C. at 1,013 bar are selected from the group of the compounds candellila wax, carnauba wax, cetearyl behenate,
- Cetearyl alcohol behenyl alcohol, stearyl alcohol, C18-38 alkyl hydroxystearoyl stearate, beeswax, lanolin alcohol, C18-36 fatty acid triglyceride, C20-40 alkyl stearate, Japan wax, glyceryl stearate, sunflower wax, myristic acid, hydrogenated vegetable oils, jojoba ester, hydrogenated olive oil.
- the preferred use concentration according to the invention of the waxes with a melting point of over 50 ° C. at 1,013 bar is 2 to 5% by weight, based on the total weight of the O / W emulsion.
- waxes with a melting point of 40-50 ° C. at 1,013 bar are selected from the group of the compounds cetyl palmitate, cetyl alcohol, hydrogenated plant glyceride,
- Myristyl alcohol hydrogenated coconut glyeride, shea butter, hydrogenated rapeseed oil.
- the preferred use concentration of the waxes according to the invention with a melting point of 40-50 ° C. at 1,013 bar is 5 to 7% by weight, based on the total weight of the O / W emulsion.
- the preferred use concentration according to the invention for the sum of both waxes i.e.
- the total wax combination is: 8 to 12% by weight, based on the total weight of the O / W emulsion.
- the oils which are liquid at 20 ° C. and 1,013 bar are selected from the group of the compounds rapeseed oil, almond oil, jojoba oil, Olus oil, vegetable oil, decyl oleate, macadamia oil, argan oil, coconut oil, avocado oil, peach kernel oil, sunflower oil, shea butter ethyl ester, caprylic / capric triglycerides, squalane, octyldodecanol, propylheptyl caprylate olive oil, grape seed oil, coco-caprylylate / coco-caprylate-ethoxylate / coco-caprylate-ethoxylate Stearates, dicaprylyl ether, octyl cocoate.
- oils which are liquid at 20 ° C. and 1,013 bar: jojoba oil, olus oil, vegetable oil, decyl oleates, rapeseed oil, almond oil, coconut oil, caprylic / capric triglycerides, octyldodecanol, Octyl cocoate.
- the preferred use concentration according to the invention for these oils is 3-6% by weight, based on the total weight of the O / W emulsion.
- oils and waxes used are of vegetable origin.
- the lipophilic phase can contain the usual components of an emulsion oil phase.
- emulsifiers are selected from the group of the compounds sodium stearoyl glutamate, sodium cetearyl sulfate, potassium cetyl sulfate, glyceryl stearate SE, glyceryl stearate citrate,
- the aqueous phase of the emulsion also contains 3 to 20% by weight, based on the total weight of the emulsion, of glycerol in addition to water.
- the aqueous phase can also contain a water-soluble dye.
- Embodiments of the present invention which are advantageous according to the invention are characterized in that the propellant gas is selected from the group of air and nitrogen.
- the preparation selects one or more active substances from the group of compounds of UV filters, glycyrrhetinic acid, urea, arctiin, alpha-lipoic acid, folic acid, phytoene, D-biotin, coenzyme Q10, hyaluronic acid, alpha-glucosyl rutin , Carnitine, carnosine, natural and / or synthetic isoflavonoids, flavonoids, creatine, creatinine, taurine, b-alanine, panthenol, magnolol, honokiol, polydocanol, Contains glyceryl glycose, tocopherol, tocopherol acetate, ascorbic acid, ascorbyl palmitate, sodium hyaluronate, caffeine and / or licochalcone A.
- the cosmetic foam is phenoxyethanol, propylene glycol, butylene glycol, 2-methylpropane-1,3-diol, ethylhexylglycerol, 1,2-pentanediol, 1,2-hexanediol, 1,2-octanediol and / or contains 1,2-decanediol.
- the cosmetic foam is phenoxyethanol, propylene glycol, butylene glycol, 2-methylpropane-1,3-diol, ethylhexylglycerol, 1,2-pentanediol, 1,2-hexanediol, 1,2-octanediol and / or contains 1,2-decanediol.
- a combination of is preferred according to the invention
- the foam is free from fatty acids, their ethers or esters and ethanol and does not use propane, butane, dimethyl ether or fluorine / chlorine hydrocarbons as the propellant. Also on cationic surfactants like
- the O / W emulsion contains at least two consistency agents selected from the group of the compounds sodium polyacrylate, C10-30 alkyl acrylate crosspolymer, carbomer, carragenan, xantham rubber, gelatin rubber, ammonium acryloyldimethyl taurate / VP copolymer, tapioca starch.
- the embodiments which are advantageous according to the invention are characterized in that the consistency adjusters are contained in a total amount of 0.5 to 4% by weight, based on the total weight of the O / W emulsion.
- the aqueous phase of the O / W emulsion contains EDTA and / or its sodium salts and / or dyes.
- Advantageous embodiments of the present invention are characterized in that the preparation one or more perfume substances selected from the group of the compounds compounds limonene, citral, linalool, alpha-isomethylionone, geraniol, citronellol, 2-isobutyl-4-hydroxy-4-methyltetrahydropyran, 2 -tet-pentylcyclohexyl acetate, 3-methyl-5-phenyl-1-pentanol, 7-acetyl-1, 1, 3,4,4,6-hexamethyltetralin, adipic acid diester, alpha-amylcinnamaldehyde, alpha-methylionone, amyl C, butylphenylmethyl propionalcinnamal, amyl salicylate, Amylcinnamylalkohol, anisyl alcohol, benzoin, benzyl alcohol, benzyl benzoate, benzyl cinnamate, benzyl salicylate
- crucible containing a cosmetic foam as described in more detail above.
- According to the invention is also a method for producing and filling a cosmetic foam as described above, characterized in that
- the emulsion is transferred from the storage container into a gassing device in which the emulsion is gassed with mixing and under pressure,
- the crucibles are then filled with the aid of a piston stroke system via a metering unit, the pressure equalizing with the ambient pressure being achieved by filling the crucible, the gas in the emulsion expanding as a result of the pressure drop which occurs.
- step i) it is advantageous according to the invention to use a Becomix mixer.
- step ii) it is also preferred according to the invention to stir the emulsion only slightly in step ii) in order to avoid premature introduction of gas.
- gassing in step iii) is preferably carried out with the aid of a dynamic foam generator.
- a rotor-stator system has e.g. from Hansa Mixer or HAAS-Mondomix as advantageous according to the invention.
- a temperature range from 35 ° C. to 50 ° C. is advantageously selected as the foaming temperature according to the invention, so that the heat generated by the friction of the foam generator may have to be dissipated by cooling.
- a back pressure of 1.5 to 3 bar is advantageous.
- the cosmetic preparation is made using a homogenizer such as e.g. Get Becomix 125 CD by following these steps:
- the bulk is mixed using a homogenizer such as e.g. Becomix 125 CD manufactured and possibly transferred to a tempered storage container.
- a homogenizer such as e.g. Becomix 125 CD manufactured and possibly transferred to a tempered storage container.
- the mass is fed to the fumigation unit (e.g. Hansa mixer) with the help of a pump
- the foaming temperature is chosen so that part of the waxes in the
- Formulation are already crystallized, but the formula is still fluid. It has proven to be advantageous if the fumigation unit is cooled if, for example, friction causes the temperature in the fumigation unit to rise, so that the temperature increase in the fumigation unit does not exceed 7 ° C.
- the mass is kept under pressure by means of a back pressure valve installed after the fumigation unit.
- a pressure of 1.4 to 4 bar in the gassing unit is advantageous.
- the bulk and foam are prepared as in Examples A-E.
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Chemical & Material Sciences (AREA)
- Emergency Medicine (AREA)
- Dispersion Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
Description
Claims
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102018217678.7A DE102018217678A1 (en) | 2018-10-16 | 2018-10-16 | Cosmetic foam suitable for crucible products and their manufacture |
PCT/EP2019/075312 WO2020078659A1 (en) | 2018-10-16 | 2019-09-20 | Cosmetic foam which is suitable for jar products and production of such cosmetic foam |
Publications (1)
Publication Number | Publication Date |
---|---|
EP3866749A1 true EP3866749A1 (en) | 2021-08-25 |
Family
ID=67999670
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP19773072.4A Pending EP3866749A1 (en) | 2018-10-16 | 2019-09-20 | Cosmetic foam which is suitable for jar products and production of such cosmetic foam |
Country Status (3)
Country | Link |
---|---|
EP (1) | EP3866749A1 (en) |
DE (1) | DE102018217678A1 (en) |
WO (1) | WO2020078659A1 (en) |
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CN112451406B (en) * | 2020-12-15 | 2022-04-22 | 广州艾卓生物科技股份有限公司 | Plant source multi-effect composition and preparation method and application thereof |
DE102021131466A1 (en) * | 2021-11-30 | 2023-06-01 | Henkel Ag & Co. Kgaa | Hair care products without silicone oil and with natural oils and waxes |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
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DE3231827A1 (en) | 1982-08-24 | 1984-03-01 | Schering AG, 1000 Berlin und 4709 Bergkamen | 11SS-ARYL-17 (ALPHA) -ALKINYL-17SS-HYDROXY-4.9 (10) - ESTRADIEN-3-ON DERIVATIVES, THEIR PRODUCTION AND THEIR PHARMACEUTICAL PREPARATIONS CONTAINING THEM |
WO2002017860A1 (en) | 2000-08-31 | 2002-03-07 | Shiseido Co., Ltd. | Whipped o/w emulsion cosmetic and processes for producing the same |
DE10058384B4 (en) * | 2000-11-24 | 2004-12-16 | Wella Aktiengesellschaft | Cosmetic or dermatological agent in the form of a creamy permanent foam or a stably foamed cream, its use and method for producing the agent |
DE10063342A1 (en) | 2000-12-19 | 2002-06-20 | Beiersdorf Ag | Cosmetic or dermatological composition contains three-part emulsifier system and gas |
DE10113048A1 (en) | 2001-03-15 | 2002-09-19 | Beiersdorf Ag | Self-foaming or foamed cosmetic or dermatological composition comprises a specified emulsifier system, a lipid phase, a gas and a particulate hydrophobic and/or oil-absorbing solid |
US20020192245A1 (en) * | 2001-04-17 | 2002-12-19 | Jensen Claude Jarkae | Morinda Citrifolia (Noni) enhanced protective night cream moisturizer |
DE10333710A1 (en) | 2003-07-23 | 2005-02-24 | Beiersdorf Ag | Cosmetic, dermatological or pharmaceutical preparations based on gas-containing lipid / wax mixtures |
US20090017079A1 (en) | 2005-04-01 | 2009-01-15 | Christina Zech | Foam-like preparation and process for the production thereof |
DE102007028026A1 (en) * | 2007-06-14 | 2008-12-18 | Beiersdorf Ag | Slowly oxygen-releasing cosmetic preparations |
US9193852B2 (en) | 2013-12-27 | 2015-11-24 | L'oreal | Stable aerated compositions |
DE102015221566A1 (en) * | 2015-11-04 | 2017-05-04 | Beiersdorf Ag | Cosmetic foam of an emulsion containing sodium cetearyl sulfate and glyceryl monostearate |
DE102015221567A1 (en) * | 2015-11-04 | 2017-05-04 | Beiersdorf Ag | Cosmetic foam from an emulsion containing betaine |
DE102015221568A1 (en) * | 2015-11-04 | 2017-05-04 | Beiersdorf Ag | Cosmetic foam of an emulsion containing glycerol and alcohol |
-
2018
- 2018-10-16 DE DE102018217678.7A patent/DE102018217678A1/en not_active Withdrawn
-
2019
- 2019-09-20 WO PCT/EP2019/075312 patent/WO2020078659A1/en unknown
- 2019-09-20 EP EP19773072.4A patent/EP3866749A1/en active Pending
Also Published As
Publication number | Publication date |
---|---|
WO2020078659A1 (en) | 2020-04-23 |
DE102018217678A1 (en) | 2020-04-16 |
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