EP3625321A1 - Method for producing gel-like preparations - Google Patents

Method for producing gel-like preparations

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Publication number
EP3625321A1
EP3625321A1 EP18720246.0A EP18720246A EP3625321A1 EP 3625321 A1 EP3625321 A1 EP 3625321A1 EP 18720246 A EP18720246 A EP 18720246A EP 3625321 A1 EP3625321 A1 EP 3625321A1
Authority
EP
European Patent Office
Prior art keywords
premix
production line
batch production
line
filling
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP18720246.0A
Other languages
German (de)
French (fr)
Other versions
EP3625321B1 (en
EP3625321B2 (en
Inventor
Uwe Trebbe
Harald Müller
Thomas Holderbaum
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel AG and Co KGaA
Original Assignee
Henkel AG and Co KGaA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA
Priority to PL18720246T priority Critical patent/PL3625321T3/en
Publication of EP3625321A1 publication Critical patent/EP3625321A1/en
Publication of EP3625321B1 publication Critical patent/EP3625321B1/en
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/0094—Process for making liquid detergent compositions, e.g. slurries, pastes or gels
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0008—Detergent materials or soaps characterised by their shape or physical properties aqueous liquid non soap compositions
    • C11D17/003—Colloidal solutions, e.g. gels; Thixotropic solutions or pastes
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2003—Alcohols; Phenols
    • C11D3/2065—Polyhydric alcohols

Definitions

  • the present invention relates to a process for the preparation of gel substances, in particular gel detergents or cleaners.
  • the process should be suitable for the preparation of gelled detergents and cleaners.
  • a process for preparing gelatinous substances comprises providing a premix on a batch production line, wherein the premix contains at least water, glycerol and surfactants.
  • the method further comprises admixing replenishers for premix, wherein the replenishers comprise at least perfumes, on a bottling line following the batch production line.
  • supplements in particular fragrances
  • a filling line is understood here and below to mean that part of a production line from which the filling of the finished product takes place, for example, in single-quantity containers.
  • Upstream of the filling line is the batch production line, in which the mixing of all ingredients apart from the Supplements takes place and on which the nearly finished product is optionally kept in a collecting container to be fed to the filling line.
  • Starting mixture containing water, glycerol and liquid nonionic surfactants and a second starting mixture containing at least fatty alcohol ethoxylates (FAEO) provided.
  • the two starting mixtures are mixed in a mixer of the batch production line. This may in particular be a static mixer.
  • the premix is particularly easy to process and blistering is minimized.
  • the premix is provided at a temperature of at least 60 ° C, more preferably at least 75 ° C, on the batch production line.
  • a temperature of at least 60 ° C, more preferably at least 75 ° C on the batch production line.
  • Such high temperatures on the batch production line have the advantage that the premix has a relatively low viscosity and the individual components can be mixed well.
  • the supplements are admixed with temperatures of at most 40 ° C on the filling line.
  • the supplements can be admixed with room temperature on the filling line.
  • At least one dye can be added to the filling line.
  • the premix is divided into at least two parts which are further treated on different filling lines, with a first part of the premix being mixed with other additives than with a second part.
  • This approach has the advantage that different branches of filling lines provide different end products. The production can thus still be varied in the last section of the bottling in some parameters in which different supplements are added. This has the advantage that the production is particularly economical and flexible. In particular, the cleaning effort and waste is reduced by allowing the same premix to be used on the batch production line for different end products on different filling lines.
  • FIG. 1 shows schematically a production line for gel-like substances according to FIG.
  • FIG. 2 shows a flowchart of a method according to an embodiment of the
  • FIG. 1 shows a production line 1 for producing gel-like substances, in particular for producing gel-type detergents or cleaners.
  • the production line 1 is divided into a batch production line 2 and a subsequent filling line 3.
  • the batch production line 2 the production of a batch, i. a large amount of the substance by mixing different starting substances.
  • the filling line 3 the filling of the finished substance takes place for example in a number of single-quantity containers. According to the invention, the addition of supplements also takes place on the filling line 3.
  • the gelatinous substance is not finished yet, but a premix is provided which still needs to be supplemented by the replenishers to obtain the final gelatinous substance.
  • the first starting mixture 4 contains at least water, glycerol and liquid nonionic surfactants. This first source mixture 4 is typically provided at a temperature of about 80 ° C. Mixing the ingredients of the first
  • Starting mixture can be static or dynamic, for example by means of a planetary mixer. After mixing, the first starting mixture 4 can be kept in a collecting container 5 for further steps.
  • the second starting mixture 6 is also typically at a temperature provided by 80 ° C.
  • the first starting mixture 4 and the second starting mixture 6 are mixed in a mixer 7, in particular a static mixer, to provide the premix.
  • the finished premix with a temperature of 80 ° C is ready at the output of the batch production line 2 ready.
  • the premix can be divided into different branches.
  • the premix is divided into a first branch 8 and a second branch 9 of the filling line 3.
  • a first supplement 10 is metered into the premix and mixed with it in a mixer 11, in particular a static mixer.
  • the first supplement 10 contains, in particular, at least one first fragrance.
  • the first supplement 10 includes a first dye.
  • the gel-form substance is obtained. It can be kept ready for filling in a collecting container 12 and, if appropriate, fed into a circuit until it is filled.
  • Supplements 10 a second supplement 13 added.
  • a second supplement 13 which has at least a second perfume and a second dye.
  • the second supplement 13 is added at a temperature of 25 ° C to the premix to obtain the final gelatinous substance having a second fragrance and a second color.
  • a collecting container 15 can also be provided in the second branch 9, in which the finished gel-form substance is kept ready for filling and optionally circulated.
  • FIG. 2 shows a flowchart of the method described with reference to FIG.
  • a first starting mixture 4 and a second starting mixture 6 are provided at temperatures of about 80 ° C. on the batch production line 2.
  • a second step 200 the two starting mixtures 4, 6 are mixed together, in particular by means of a static mixer 7.
  • a third step 300 the premix thus obtained is fed to a filling line 3 of the production line 1.
  • a fourth step 400 at least one admixing takes place

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention relates to a method for producing gel-like substances, comprising the provision of a premixture on a batch production line (2), the premixture containing at least water, glycerin and surfactants, and the addition of supplements (10, 13) to the premixture on a filling line (3) which is subsequent to the batch production line (2), the supplements (10, 13) comprising at least fragrances.

Description

VERFAHREN ZUR HERSTELLUNG GELFÖRMIGER ZUBEREITUNGEN  METHOD FOR THE PRODUCTION OF MORELLOUS PREPARATIONS
Die vorliegende Erfindung betrifft ein Verfahren zur Herstellung gelförmiger Substanzen, insbesondere gelförmiger Wasch- oder Reinigungsmittel. The present invention relates to a process for the preparation of gel substances, in particular gel detergents or cleaners.
Aus der DE 10 2010 055 770 A1 ist ein Verfahren zur Herstellung kosmetischer und oder dermatologischer Emulsionen bekannt, bei dem sämtliche Inhaltsstoffe in mehreren Stufen in einer Chargenproduktionslinie vermischt werden. Anschließend wird die fertige Emulsion zu einer Abfülllinie gepumpt und abgefüllt. From DE 10 2010 055 770 A1 a process for the preparation of cosmetic and / or dermatological emulsions is known in which all ingredients are mixed in several stages in a batch production line. Subsequently, the finished emulsion is pumped to a filling line and filled.
Ein derartiges Vorgehen hat den Nachteil, dass die Produktion verhältnismäßig unflexibel ist. Zudem sind verschiedene empfindliche Inhaltsstoffe, insbesondere Duft- und Farbstoffe, für längere Zeit sehr hohen Temperaturen ausgesetzt. Dies führt zu einem teilweisen Verlust dieser Stoffe in der Produktionslinie. Zudem ist es häufig schwierig, wegen der hohen Viskosität zu vermischender Stoffe blasenfrei zu arbeiten. Teilweise wird zur Beseitigung von Blasen unter Vakuum gearbeitet, was jedoch ebenfalls zum Verlust flüchtiger Inhaltsstoffe, insbesondere Duftstoffe, führt. Such a procedure has the disadvantage that the production is relatively inflexible. In addition, various sensitive ingredients, especially fragrances and dyes are exposed to very high temperatures for a long time. This leads to a partial loss of these substances in the production line. In addition, it is often difficult to work bubble-free because of the high viscosity of substances to be mixed. Partial works to eliminate bubbles under vacuum, but this also leads to the loss of volatile ingredients, especially fragrances leads.
Es ist eine Aufgabe der vorliegenden Erfindung, ein verbessertes Verfahren zur Herstellung gelförmiger Substanzen bereitzustellen, bei dem die genannten Nachteile nicht auftreten. It is an object of the present invention to provide an improved process for the preparation of gel substances in which said disadvantages do not occur.
Insbesondere soll das Verfahren zur Herstellung gelförmiger Wasch- und Reinigungsmittel geeignet sein. In particular, the process should be suitable for the preparation of gelled detergents and cleaners.
Diese Aufgabe wird gelöst durch den Gegenstand des unabhängigen Patentanspruchs. Weitere Ausführungsformen sind Gegenstand der Unteransprüche. This object is solved by the subject matter of the independent patent claim. Further embodiments are the subject of the dependent claims.
Gemäß einer Ausführungsform der Erfindung umfasst ein Verfahren zur Herstellung gelförmiger Substanzen das Bereitstellen einer Vormischung auf einer Chargenproduktionslinie, wobei die Vormischung zumindest Wasser, Glycerin und Tenside enthält. Das Verfahren umfasst ferner das Zumischen von Ergänzungsmitteln zur Vormischung, wobei die Ergänzungsmittel zumindest Duftstoffe umfassen, auf einer der Chargenproduktionslinie nachfolgenden Abfülllinie. According to one embodiment of the invention, a process for preparing gelatinous substances comprises providing a premix on a batch production line, wherein the premix contains at least water, glycerol and surfactants. The method further comprises admixing replenishers for premix, wherein the replenishers comprise at least perfumes, on a bottling line following the batch production line.
Erfindungsgemäß werden somit Ergänzungsmittel, insbesondere Duftstoffe, zu einem späten Zeitpunkt in der Produktion zudosiert, und zwar erst auf einer Abfülllinie. Unter einer Abfülllinie wird hier und im Folgenden derjenige Teil einer Produktionslinie verstanden, aus dem die Abfüllung des fertigen Produktes beispielsweise in Einzelmengenbehälter erfolgt. Der Abfülllinie vorgelagert ist die Chargenproduktionslinie, in der die Vermischung sämtlicher Inhaltsstoffe abgesehen von den Ergänzungsmitteln erfolgt und auf der das nahezu fertig gestellte Produkt gegebenenfalls in einem Sammelbehälter vorgehalten wird, um der Abfülllinie zugeführt zu werden. Thus, according to the invention, supplements, in particular fragrances, are added at a later time in the production, namely only on a filling line. A filling line is understood here and below to mean that part of a production line from which the filling of the finished product takes place, for example, in single-quantity containers. Upstream of the filling line is the batch production line, in which the mixing of all ingredients apart from the Supplements takes place and on which the nearly finished product is optionally kept in a collecting container to be fed to the filling line.
Durch das Zumischen von Ergänzungsmitteln erst unmittelbar vor der Abfüllung wird eine kontinuierliche kostengünstige Produktion erreicht, bei der eine Blasenbildung vermindert werden kann und bei der eine sehr schonende Zugabe empfindlicher Duftstoffe ermöglicht ist. Zudem ist das Verfahren besonders flexibel und der Reinigungsaufwand wird minimiert, da eine Variation des fertigen Produktes noch in der Abfülllinie durch eine Variation der dort zugegebenen By adding additives only immediately before bottling, a continuous low-cost production is achieved in which a blistering can be reduced and in which a very gentle addition of sensitive fragrances is possible. In addition, the process is particularly flexible and the cleaning effort is minimized because a variation of the finished product still in the filling line by a variation of the added there
Ergänzungsmittel möglich ist. Supplements is possible.
Gemäß einer Ausführungsform wird zur Bereitstellung der Vormischung eine erste In one embodiment, to provide the premix, a first
Ausgangsmischung enthaltend Wasser, Glycerin und flüssige nichtionische Tenside und eine zweite Ausgangsmischung enthaltend zumindest Fettalkoholethoxylate (FAEO) bereitgestellt. Die beiden Ausgangsmischungen werden in einem Mischer der Chargenproduktionslinie gemischt. Dabei kann es sich insbesondere um einen statischen Mischer handeln. Starting mixture containing water, glycerol and liquid nonionic surfactants and a second starting mixture containing at least fatty alcohol ethoxylates (FAEO) provided. The two starting mixtures are mixed in a mixer of the batch production line. This may in particular be a static mixer.
Auf diese Weise ist die Vormischung besonders leicht zu verarbeiten und eine Blasenbildung wird minimiert. In this way, the premix is particularly easy to process and blistering is minimized.
Gemäß einer Ausführungsform wird die Vormischung mit einer Temperatur von mindestens 60 °C, insbesondere von mindestens 75 °C auf der Chargenproduktionslinie bereitgestellt. Derart hohe Temperaturen auf der Chargenproduktionslinie haben den Vorteil, dass die Vormischung eine verhältnismäßig geringe Viskosität aufweist und sich die einzelnen Bestandteile gut vermischen lassen. In one embodiment, the premix is provided at a temperature of at least 60 ° C, more preferably at least 75 ° C, on the batch production line. Such high temperatures on the batch production line have the advantage that the premix has a relatively low viscosity and the individual components can be mixed well.
Gemäß einer Ausführungsform werden die Ergänzungsmittel mit Temperaturen von höchstens 40 °C auf der Abfülllinie zugemischt. Insbesondere können die Ergänzungsmittel mit Raumtemperatur auf der Abfülllinie zugemischt werden. According to one embodiment, the supplements are admixed with temperatures of at most 40 ° C on the filling line. In particular, the supplements can be admixed with room temperature on the filling line.
Diese verhältnismäßig niedrigen Temperaturen haben den Vorteil, dass temperaturempfindliche Stoffe, insbesondere Duftstoffe, aber auch Farbstoffe, nicht über längere Zeit hohen Temperaturen ausgesetzt werden, die diese zerstören könnten. These relatively low temperatures have the advantage that temperature-sensitive substances, especially fragrances, but also dyes, are not exposed to high temperatures for a long time, which could destroy them.
Neben Duftstoffen kann auf der Abfülllinie auch zumindest ein Farbstoff zugemischt werden. In addition to fragrances, at least one dye can be added to the filling line.
Gemäß einer Ausführungsform wird die Vormischung nach der Chargenproduktionslinie in zumindest zwei Teile geteilt, die auf unterschiedlichen Abfülllinien weiter behandelt werden, wobei einem ersten Teil der Vormischung andere Ergänzungsmittel zugemischt werden als einem zweiten Teil. Dieses Vorgehen hat den Vorteil, dass verschiedene Zweige von Abfülllinien unterschiedliche Endprodukte bereitstellen. Die Produktion kann somit noch in dem letzten Abschnitt der Abfüllung in einigen Parametern variiert werden, in dem unterschiedliche Ergänzungsmittel zugefügt werden. Dies hat den Vorteil, dass die Produktion besonders ökonomisch und flexibel erfolgt. Insbesondere ist der Reinigungsaufwand und der Abfall reduziert dadurch, dass dieselbe Vormischung auf der Chargenproduktionslinie für unterschiedliche Endprodukte auf unterschiedlichen Abfülllinien verwendet werden kann. According to one embodiment, after the batch production line, the premix is divided into at least two parts which are further treated on different filling lines, with a first part of the premix being mixed with other additives than with a second part. This approach has the advantage that different branches of filling lines provide different end products. The production can thus still be varied in the last section of the bottling in some parameters in which different supplements are added. This has the advantage that the production is particularly economical and flexible. In particular, the cleaning effort and waste is reduced by allowing the same premix to be used on the batch production line for different end products on different filling lines.
Ausführungsformen der Erfindung werden im Folgenden anhand von Figuren näher beschrieben. Darin zeigen Embodiments of the invention are described below with reference to figures. Show in it
Figur 1 schematisch eine Produktionslinie für gelförmige Substanzen gemäß 1 shows schematically a production line for gel-like substances according to FIG
einem Verfahren gemäß einer Ausführungsform der Erfindung und  a method according to an embodiment of the invention and
Figur 2 ein Ablaufdiagramm eines Verfahrens gemäß einer Ausführungsform der FIG. 2 shows a flowchart of a method according to an embodiment of the
Erfindung.  Invention.
Figur 1 zeigt eine Produktionslinie 1 zur Herstellung gelförmiger Substanzen, insbesondere zur Herstellung gelförmiger Wasch- oder Reinigungsmittel. Die Produktionslinie 1 gliedert sich in eine Chargenproduktionslinie 2 und eine nachfolgende Abfülllinie 3. In der Chargenproduktionslinie 2 erfolgt die Produktion einer Charge, d.h. einer Großmenge der Substanz durch Vermischen verschiedener Ausgangssubstanzen. In der Abfülllinie 3 erfolgt die Abfüllung der fertigen Substanz beispielsweise in eine Anzahl von Einzelmengenbehältern. Erfindungsgemäß erfolgt auf der Abfülllinie 3 zudem die Zumischung von Ergänzungsmitteln. FIG. 1 shows a production line 1 for producing gel-like substances, in particular for producing gel-type detergents or cleaners. The production line 1 is divided into a batch production line 2 and a subsequent filling line 3. In the batch production line 2, the production of a batch, i. a large amount of the substance by mixing different starting substances. In the filling line 3, the filling of the finished substance takes place for example in a number of single-quantity containers. According to the invention, the addition of supplements also takes place on the filling line 3.
Auf der Chargenproduktionslinie 2 wird demnach die gelförmige Substanz noch nicht fertiggestellt, sondern es wird eine Vormischung bereitgestellt, die noch durch die Ergänzungsmittel ergänzt werden muss, um die fertige gelförmige Substanz zu erhalten. Accordingly, on the batch production line 2, the gelatinous substance is not finished yet, but a premix is provided which still needs to be supplemented by the replenishers to obtain the final gelatinous substance.
Auf der Chargenproduktionslinie 2 erfolgt zunächst die Bereitstellung einer ersten On the batch production line 2, the provision of a first
Ausgangsmischung 4. Die erste Ausgangsmischung 4 enthält zumindest Wasser, Glycerin und flüssige nichtionische Tenside. Diese erste Ausgangsmischung 4 wird typischerweise bei einer Temperatur von etwa 80 °C bereitgestellt. Das Vermischen der Bestandteile der ersten Starting mixture 4. The first starting mixture 4 contains at least water, glycerol and liquid nonionic surfactants. This first source mixture 4 is typically provided at a temperature of about 80 ° C. Mixing the ingredients of the first
Ausgangsmischung kann statisch oder dynamisch beispielsweise mittels eines Planetenmischers erfolgen. Nach dem Vermischen kann die erste Ausgangsmischung 4 in einem Sammelbehälter 5 für weitere Schritte vorgehalten werden. Starting mixture can be static or dynamic, for example by means of a planetary mixer. After mixing, the first starting mixture 4 can be kept in a collecting container 5 for further steps.
Anschließend erfolgt die Zumischung einer zweiten Ausgangsmischung 6 zu der ersten Subsequently, the admixing of a second starting mixture 6 to the first takes place
Ausgangsmischung 4, wobei die zweite Ausgangsmischung 6 insbesondere Fettalkoholethoxylate (FAEO) enthält. Auch die zweite Ausgangsmischung 6 wird typischerweise bei einer Temperatur von 80 °C bereitgestellt. Die erste Ausgangsmischung 4 und die zweite Ausgangsmischung 6 werden in einem Mischer 7, insbesondere einem statischen Mischer, zur Bereitstellung der Vormischung vermischt. Somit steht am Ausgang der Chargenproduktionslinie 2 die fertige Vormischung mit einer Temperatur von 80 °C bereit. Starting mixture 4, wherein the second starting mixture 6 in particular fatty alcohol ethoxylates (FAEO). The second starting mixture 6 is also typically at a temperature provided by 80 ° C. The first starting mixture 4 and the second starting mixture 6 are mixed in a mixer 7, in particular a static mixer, to provide the premix. Thus, the finished premix with a temperature of 80 ° C is ready at the output of the batch production line 2 ready.
Auf der nachfolgenden Abfülllinie 3 kann die Vormischung auf verschiedene Zweige aufgeteilt werden. In der in Figur 1 gezeigten Ausführungsform wird die Vormischung in einen ersten Zweig 8 und einen zweiten Zweig 9 der Abfülllinie 3 aufgeteilt. In dem ersten Zweig 8 der Abfülllinie 3 wird ein erstes Ergänzungsmittel 10 zu der Vormischung zudosiert und mit dieser in einem Mischer 1 1 , insbesondere einem statischen Mischer, vermischt. Das erste Ergänzungsmittel 10 enthält insbesondere zumindest einen ersten Duftstoff. Ferner enthält das erste Ergänzungsmittel 10 in der gezeigten Ausführungsform einen ersten Farbstoff. Damit ist die gelformige Substanz erhalten. Sie kann für die Abfüllung in einem Sammelbehälter 12 vorgehalten und gegebenenfalls bis zur Abfüllung in einem Kreislauf geführt werden. On the subsequent filling line 3, the premix can be divided into different branches. In the embodiment shown in FIG. 1, the premix is divided into a first branch 8 and a second branch 9 of the filling line 3. In the first branch 8 of the filling line 3, a first supplement 10 is metered into the premix and mixed with it in a mixer 11, in particular a static mixer. The first supplement 10 contains, in particular, at least one first fragrance. Further, in the embodiment shown, the first supplement 10 includes a first dye. Thus, the gel-form substance is obtained. It can be kept ready for filling in a collecting container 12 and, if appropriate, fed into a circuit until it is filled.
Im zweiten Zweig 9 der Abfülllinie 3 wird zu der Vormischung anstelle des ersten In the second branch 9 of the filling line 3 is added to the premix instead of the first
Ergänzungsmittels 10 ein zweites Ergänzungsmittel 13 zudosiert. In dem in Figur 1 gezeigten Ausführungsbeispiel wird ein zweites Ergänzungsmittel 13 verwendet, das zumindest einen zweiten Duftstoff und einen zweiten Farbstoff aufweist. Das zweite Ergänzungsmittel 13 wird bei einer Temperatur von 25 °C zu der Vormischung zudosiert, um die fertige gelformige Substanz mit einem zweiten Duft und einer zweiten Färbung zu erhalten. Supplements 10 a second supplement 13 added. In the embodiment shown in FIG. 1, a second supplement 13 is used which has at least a second perfume and a second dye. The second supplement 13 is added at a temperature of 25 ° C to the premix to obtain the final gelatinous substance having a second fragrance and a second color.
Wie im ersten Zweig kann auch im zweiten Zweig 9 ein Sammelbehälter 15 vorgesehen sein, in dem die fertige gelformige Substanz zur Abfüllung bereitgehalten und gegebenenfalls im Kreislauf geführt wird. As in the first branch, a collecting container 15 can also be provided in the second branch 9, in which the finished gel-form substance is kept ready for filling and optionally circulated.
Figur 2 zeigt ein Ablaufdiagramm des anhand von Figur 1 beschriebenen Verfahrens. In einem ersten Schritt 100 werden eine erste Ausgangsmischung 4 und eine zweite Ausgangsmischung 6 bei Temperaturen von etwa 80 °C auf der Chargenproduktionslinie 2 bereitgestellt. FIG. 2 shows a flowchart of the method described with reference to FIG. In a first step 100, a first starting mixture 4 and a second starting mixture 6 are provided at temperatures of about 80 ° C. on the batch production line 2.
In einem zweiten Schritt 200 werden die beiden Ausgangsmischungen 4, 6 miteinander vermischt, insbesondere mithilfe eines statischen Mischers 7. In a second step 200, the two starting mixtures 4, 6 are mixed together, in particular by means of a static mixer 7.
In einem dritten Schritt 300 wird die dadurch erhaltene Vormischung einer Abfülllinie 3 der Produktionslinie 1 zugeführt. In a third step 300, the premix thus obtained is fed to a filling line 3 of the production line 1.
Auf der Abfülllinie 3 erfolgt in einem vierten Schritt 400 das Zumischen zumindest eines On the filling line 3, in a fourth step 400, at least one admixing takes place
Ergänzungsmittels 10, 13 zu der Vormischung. In einem fünften Schritt 500 erfolgt die Abfüllung der fertigen gelförmigen Substanz. Bezugszeichenliste Supplement 10, 13 to the premix. In a fifth step 500, the filling of the finished gel-like substance takes place. LIST OF REFERENCE NUMBERS
1 Produktionslinie 1 production line
2 Chargenproduktionslinie 2 batch production line
3 Abfülllinie 3 filling line
4 erste Ausgangsmischung 4 first starting mixture
5 Sammelbehälter5 collection containers
6 zweite Ausgangsmischung6 second starting mixture
7 Mischer 7 mixers
8 erster Zweig  8 first branch
9 zweiter Zweig  9 second branch
10 erste Ergänzungsmittel 10 first supplements
1 1 Mischer 1 1 mixer
12 Sammelbehälter 12 collection containers
13 zweite Ergänzungsmittel13 second supplements
14 Mischer 14 mixers
15 Sammelbehälter  15 collection containers
100 Schritt 100 steps
200 Schritt  200 step
300 Schritt  300 step
400 Schritt  400 step
500 Schritt  500 step

Claims

Patentansprüche claims
1. Verfahren zur Herstellung gelförmiger Substanzen, wobei das Verfahren folgendes A process for producing gel substances, the process comprising
umfasst:  includes:
- bereitstellen einer Vormischung auf einer Chargenproduktionslinie (2), wobei die  - Provide a premix on a batch production line (2), wherein the
Vormischung zumindest Wasser, Glycerin und Tenside enthält, und  Premix contains at least water, glycerol and surfactants, and
- zumischen von Ergänzungsmitteln (10, 13) zur Vormischung, wobei die Ergänzungsmittel (10, 13) zumindest Duftstoffe umfassen, auf einer der Chargenproduktionslinie (2) nachfolgenden Abfülllinie (3).  mixing of supplementing agents (10, 13) for premixing, wherein the supplementing agents (10, 13) comprise at least perfumes, on a filling line (3) following the batch production line (2).
2. Verfahren nach Anspruch 2, 2. The method according to claim 2,
wobei zur Bereitstellung der Vormischung eine erste Ausgangsmischung (4) enthaltend Wasser, Glycerin und flüssige nichtionische Tenside und eine zweite Ausgangsmischung (6) enthaltend zumindest Fettalkoholethoxylate bereitgestellt und die beiden  wherein for providing the premix a first starting mixture (4) comprising water, glycerol and liquid nonionic surfactants and a second starting mixture (6) containing at least fatty alcohol ethoxylates are provided and the two
Ausgangsmischungen (4, 6) in einem Mischer (7) der Chargenproduktionslinie (2) gemischt werden.  Starting mixtures (4, 6) in a mixer (7) of the batch production line (2) are mixed.
3. Verfahren nach Anspruch 1 oder 2, 3. The method according to claim 1 or 2,
wobei die Vormischung mit einer Temperatur von mindestens 60 °C auf der  the premix having a temperature of at least 60 ° C on the
Chargenproduktionslinie (2) bereitgestellt wird.  Batch production line (2) is provided.
4. Verfahren nach einem der Ansprüche 1 bis 3, 4. The method according to any one of claims 1 to 3,
wobei die Vormischung mit einer Temperatur von mindestens 75 °C auf der  the premix having a temperature of at least 75 ° C on the
Chargenproduktionslinie (2) bereitgestellt wird.  Batch production line (2) is provided.
5. Verfahren nach einem der Ansprüche 1 bis 4, 5. The method according to any one of claims 1 to 4,
wobei die Ergänzungsmittel (10, 13) mit Temperaturen von höchstens 40 °C auf der Abfülllinie (3) zugemischt werden.  wherein the supplementary means (10, 13) are admixed with temperatures of at most 40 ° C on the filling line (3).
6. Verfahren nach einem der Ansprüche 1 bis 5, 6. The method according to any one of claims 1 to 5,
wobei die Ergänzungsmittel (10, 13) mit Raumtemperatur auf der Abfülllinie (3) zugemischt werden.  wherein the supplement (10, 13) are admixed with room temperature on the filling line (3).
7. Verfahren nach einem der Ansprühe 1 bis 6, 7. The method according to any one of claims 1 to 6,
wobei neben Duftstoffen auf der Abfülllinie (3) auch zumindest ein Farbstoff zugemischt wird.  wherein in addition to perfumes on the filling line (3) and at least one dye is added.
8. Verfahren nach einem der Ansprüche 1 bis 7, 8. The method according to any one of claims 1 to 7,
wobei die Vormischung nach der Chargenproduktionslinie (2) in zumindest zwei Teile geteilt wird, die auf unterschiedlichen Abfülllinien (3) weiterbehandelt werden, wobei einem ersten Teil der Vormischung andere Ergänzungsmittel (10, 13) zugemischt werden als einem zweiten Teil.  wherein the premix after the batch production line (2) is divided into at least two parts which are further processed on different filling lines (3), with a first part of the premix being mixed with other additives (10, 13) than with a second part.
EP18720246.0A 2017-05-19 2018-04-26 Method for producing gel-like preparations Active EP3625321B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL18720246T PL3625321T3 (en) 2017-05-19 2018-04-26 Method for producing gel-like preparations

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102017208559.2A DE102017208559A1 (en) 2017-05-19 2017-05-19 Process for the preparation of gel substances
PCT/EP2018/060659 WO2018210542A1 (en) 2017-05-19 2018-04-26 Method for producing gel-like preparations

Publications (3)

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EP3625321A1 true EP3625321A1 (en) 2020-03-25
EP3625321B1 EP3625321B1 (en) 2021-06-09
EP3625321B2 EP3625321B2 (en) 2024-05-01

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EP (1) EP3625321B2 (en)
DE (1) DE102017208559A1 (en)
ES (1) ES2880777T3 (en)
PL (1) PL3625321T3 (en)
WO (1) WO2018210542A1 (en)

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DE102021200796A1 (en) 2021-01-28 2022-07-28 Psa Automobiles Sa Storage system for an electric vehicle charging cable

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2606393B1 (en) † 1986-11-10 1989-03-10 Erca METHOD AND INSTALLATION FOR FILLING CONTAINERS WITH A MIXTURE OF AT LEAST TWO PASTY AND / OR LIQUID PRODUCTS
AU623371B2 (en) 1988-02-04 1992-05-14 Colgate-Palmolive Company, The Thixotropic aqueous automatic dishwashing detergent compositions
US5296157A (en) 1991-03-05 1994-03-22 The Proctor & Gamble Company Liquid soap personal cleanser with critical heat cycle stabilizing system
DE4216453A1 (en) 1992-05-19 1993-11-25 Henkel Kgaa Process for the preparation of pasty detergents
US20040116539A1 (en) 2002-12-16 2004-06-17 Unilever Home & Personal Care Usa, Division Of Conopco, Inc. Late variant addition process for personal care products
US20040247534A1 (en) 2003-06-06 2004-12-09 Sultan Dental Products, Ltd Foamable fluoride gel compositions and methods of treatment using the same
JP2008031115A (en) † 2006-07-31 2008-02-14 Sunstar Inc Method and apparatus for producing liquid composition
CN102224233A (en) 2008-09-25 2011-10-19 荷兰联合利华有限公司 Liquid detergents
MX343424B (en) 2010-11-11 2016-11-04 Unilever Nv Leave-on nonsolid skin conditioning compositions containing 12-hydroxystearic acid.
DE102010055770A1 (en) 2010-12-23 2012-06-28 Beiersdorf Ag Preparing cosmetic and/or dermatological emulsion comprises adding one or more glucosylglycerides to an aqueous phase and/or an oil phase at a specified temperature, and combining the oil and aqueous phases
EP2746379B1 (en) * 2012-12-20 2017-03-29 The Procter & Gamble Company Process for the production of a liquid composition
EP3031891B1 (en) * 2014-12-12 2019-03-20 The Procter and Gamble Company A multi-compartment laundry detergent water-soluble pouch
BR112017018719A2 (en) * 2015-03-02 2018-04-17 Unilever Nv viscous scented cleaning fluid for substrate cleaning and method of manufacturing a viscous fluid cleaning composition for cleaning a substrate with a high flow viscosity

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EP3625321B1 (en) 2021-06-09
EP3625321B2 (en) 2024-05-01
WO2018210542A1 (en) 2018-11-22
DE102017208559A1 (en) 2018-11-22
PL3625321T3 (en) 2021-10-04
ES2880777T3 (en) 2021-11-25

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