EP3234095A1 - Verfahren zur herstellung von hygienisch sauberem textil - Google Patents
Verfahren zur herstellung von hygienisch sauberem textilInfo
- Publication number
- EP3234095A1 EP3234095A1 EP15813674.7A EP15813674A EP3234095A1 EP 3234095 A1 EP3234095 A1 EP 3234095A1 EP 15813674 A EP15813674 A EP 15813674A EP 3234095 A1 EP3234095 A1 EP 3234095A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- textiles
- temperature
- less
- zone
- textile
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000004753 textile Substances 0.000 title claims abstract description 58
- 238000000034 method Methods 0.000 title claims description 30
- 238000005406 washing Methods 0.000 claims abstract description 13
- 238000004061 bleaching Methods 0.000 claims abstract description 11
- 239000007844 bleaching agent Substances 0.000 claims description 22
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 9
- 239000000460 chlorine Substances 0.000 claims description 9
- 229910052801 chlorine Inorganic materials 0.000 claims description 9
- WQYVRQLZKVEZGA-UHFFFAOYSA-N hypochlorite Chemical compound Cl[O-] WQYVRQLZKVEZGA-UHFFFAOYSA-N 0.000 claims description 8
- 239000005708 Sodium hypochlorite Substances 0.000 claims description 7
- 238000004900 laundering Methods 0.000 claims description 7
- SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical group [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 claims description 7
- 239000003599 detergent Substances 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 2
- 230000006378 damage Effects 0.000 abstract description 5
- 238000004659 sterilization and disinfection Methods 0.000 abstract description 5
- 241000588724 Escherichia coli Species 0.000 description 14
- 241000293869 Salmonella enterica subsp. enterica serovar Typhimurium Species 0.000 description 12
- 244000052769 pathogen Species 0.000 description 8
- GHXZTYHSJHQHIJ-UHFFFAOYSA-N Chlorhexidine Chemical compound C=1C=C(Cl)C=CC=1NC(N)=NC(N)=NCCCCCCN=C(N)N=C(N)NC1=CC=C(Cl)C=C1 GHXZTYHSJHQHIJ-UHFFFAOYSA-N 0.000 description 7
- 229960003260 chlorhexidine Drugs 0.000 description 7
- 229920000742 Cotton Polymers 0.000 description 6
- 239000002054 inoculum Substances 0.000 description 6
- 239000000645 desinfectant Substances 0.000 description 5
- 241000191967 Staphylococcus aureus Species 0.000 description 4
- 244000005700 microbiome Species 0.000 description 4
- 229920000728 polyester Polymers 0.000 description 4
- 239000000725 suspension Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 241000589517 Pseudomonas aeruginosa Species 0.000 description 3
- 241001138501 Salmonella enterica Species 0.000 description 3
- YZIYKJHYYHPJIB-UUPCJSQJSA-N chlorhexidine gluconate Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O.C1=CC(Cl)=CC=C1NC(=N)NC(=N)NCCCCCCNC(=N)NC(=N)NC1=CC=C(Cl)C=C1 YZIYKJHYYHPJIB-UUPCJSQJSA-N 0.000 description 3
- 229940098803 hibiclens Drugs 0.000 description 3
- 238000011282 treatment Methods 0.000 description 3
- 230000037303 wrinkles Effects 0.000 description 3
- 241000894006 Bacteria Species 0.000 description 2
- 238000002835 absorbance Methods 0.000 description 2
- 239000012190 activator Substances 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 238000011534 incubation Methods 0.000 description 2
- 238000011081 inoculation Methods 0.000 description 2
- 238000005374 membrane filtration Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000001717 pathogenic effect Effects 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000001974 tryptic soy broth Substances 0.000 description 2
- 108010050327 trypticase-soy broth Proteins 0.000 description 2
- YRIZYWQGELRKNT-UHFFFAOYSA-N 1,3,5-trichloro-1,3,5-triazinane-2,4,6-trione Chemical compound ClN1C(=O)N(Cl)C(=O)N(Cl)C1=O YRIZYWQGELRKNT-UHFFFAOYSA-N 0.000 description 1
- 241000588626 Acinetobacter baumannii Species 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 241000224466 Giardia Species 0.000 description 1
- 201000008225 Klebsiella pneumonia Diseases 0.000 description 1
- 241000588747 Klebsiella pneumoniae Species 0.000 description 1
- 241000589248 Legionella Species 0.000 description 1
- 208000007764 Legionnaires' Disease Diseases 0.000 description 1
- 241000186779 Listeria monocytogenes Species 0.000 description 1
- RJQXTJLFIWVMTO-TYNCELHUSA-N Methicillin Chemical compound COC1=CC=CC(OC)=C1C(=O)N[C@@H]1C(=O)N2[C@@H](C(O)=O)C(C)(C)S[C@@H]21 RJQXTJLFIWVMTO-TYNCELHUSA-N 0.000 description 1
- 206010035717 Pneumonia klebsiella Diseases 0.000 description 1
- SSBRSHIQIANGKS-UHFFFAOYSA-N [amino(hydroxy)methylidene]azanium;hydrogen sulfate Chemical compound NC(N)=O.OS(O)(=O)=O SSBRSHIQIANGKS-UHFFFAOYSA-N 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 239000004599 antimicrobial Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000003749 cleanliness Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000001351 cycling effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- QWPPOHNGKGFGJK-UHFFFAOYSA-N hypochlorous acid Chemical compound ClO QWPPOHNGKGFGJK-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- LWXVCCOAQYNXNX-UHFFFAOYSA-N lithium hypochlorite Chemical compound [Li+].Cl[O-] LWXVCCOAQYNXNX-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229960003085 meticillin Drugs 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 230000004763 spore germination Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229950009390 symclosene Drugs 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
- D06L4/70—Multi-step processes
- D06L4/75—Multi-step processes combined with cleaning or washing
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/395—Bleaching agents
- C11D3/3956—Liquid compositions
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
- D06L4/20—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which contain halogen
- D06L4/22—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which contain halogen using inorganic agents
- D06L4/24—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which contain halogen using inorganic agents using chlorites or chlorine dioxide
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
- C11D2111/10—Objects to be cleaned
- C11D2111/12—Soft surfaces, e.g. textile
Definitions
- Thermal disinfection has been shown to be insufficient in killing spore forming bacteria, such as C. diff. C. diff. can survive extended heating at 160°F. Temperatures of 145-160°F may actually enhance spore germination of some aged spores.
- EPA registered sanitizers/disinfectants are sometimes used in healthcare laundries. When used properly, these sanitizers/disinfectants have kill claims on certain organisms. The deficiency in using these sanitizers/disinfectants is that they do not have kill claims on many organisms present in the healthcare environment.
- One such sanitizer/disinfectant has kill claims for Staphylococcus aureus, Klebsiella pneumonia, Pseudomonas aeruginosa, methicillin resistant Staphylococcus aureus (M SA), Acinetobacter baumannii, Listeria monocytogenes, Ecsherichia coli, and Salmonella enterica.
- Certain textiles require a bleaching step. This is particularly required for white textiles such as white linen.
- Chlorine-based bleaches such as sodium hypochlorite, are typically used. Generally the commercial laundries bleach such textiles at temperatures about 150°F, similar to the laundering temperature, and at relatively high pHs, around 10.2 to 10.8. If the chlorine bleaches are used at lower pHs, the textiles are damaged by the bleach.
- the present invention is premised on the realization that one can effectively launder and bleach textiles by initially washing the textile at a low temperature, generally 140°F or lower, and subsequently bleaching the textiles, again at a low temperature of less than 140°F, at a pH less than 9.5, generally from about 7 to 9. This effectively launders and bleaches the textile without causing any damage to the textile, which typically would be expected when bleaching at such a low pH.
- the linens are cleaned in a four zone process, the first zone designed to remove chlorhexidine also referred to as Hibiclens, wherein a concentrated high-performance detergent is used, along with a Hibiclens remover, such as Hibiclear, to remove any chlorhexidine from the fabric, preventing it from setting in subsequent zones.
- the linens are washed, again at a low temperature, generally 140°F or less, such as 100°F, down to 85°F.
- a high performance laundry detergent along with a concentrated alkali, is added. This zone helps to reduce microorganism contamination.
- the textiles become hygienically clean by treating the textiles with sodium hypochlorite, a bleach activator, at a pH of less than 9.5, generally 7 to 9, more particularly 7-8, again at a temperature less than 140°F, generally 100°F or less.
- the linens are rinsed and the pH adjusted to about 7.
- softeners can be added if required.
- FIG. 1 is a graph showing tensile strength of a cotton fabric after repeated washes.
- FIG. 2 is a graph showing tensile strength of a 65/35 polyester/cotton blend after repeated washes.
- textiles are laundered in a manner that ensures destruction of bacteria and other pathogens to provide hygienically clean textiles.
- the washing process will be conducted in typical commercial laundry facilities.
- any commercial laundry equipment can be used in the process of the present invention.
- One such typical apparatus is a tunnel washing apparatus, generally one having at least four zones.
- the textiles are initially subjected to a low temperature, low pH laundering.
- the textiles are treated in a manner, well-known to remove chlorhexidine, an antimicrobial agent typically used in hospitals, also referred us to as Hibiclens.
- the textiles are subjected to a wash at an acid pH to prevent the chlorhexidine from setting.
- the wash washing solution can include Hibiclear, a commercially available product which is designed to facilitate removal of chlorhexidine.
- This initial zone washing is conducted generally at a lower temperature, preferably at 140°F or less, such as 130, 120, 110 and generally about 100°F.
- the initial wash is conducted for a time effective to remove any chlorhexidine present and generally from about 2 to about 8 minutes and generally about 8 minutes. This step is unnecessary for textiles that do not include chlorhexidine.
- the textiles are treated in the initial zone, they pass to a wash zone, where they are washed using a high-performance, low temperature laundry detergent, generally a nonionic surfactant- based detergent at an alkaline pH.
- This washing step is conducted at a temperature of 140° to 85°F , generally 130°F to 95°F, 120°F or less, 110°F or less and preferably at about 100°F.
- the time during which the textiles are treated in the wash zone may vary, depending upon the materials being laundered. In most applications, the time is from 6 to about 15 and generally about 12.
- the washing liquid is separated from the textiles.
- the textiles are then passed to a third zone, which is a pathogen removal zone or a bleaching zone.
- a bleach solution typically sodium hypochlorite at a pH of 6.5 to 9.5, generally 8 to 6.5 and, in particular, a pH of 7.
- the pH is adjusted as needed by the addition of an appropriate water soluble buffer, such as urea sulfate.
- the concentration of the bleach will be about 5 ounces to 30 ounces per hundred weight textile or 25 to 500 ppm.
- a bleach activator is added, such as Pathfree. This will effectively established the pH within the desired range.
- the temperature in this zone will be maintained at 140°F or less, generally 130°F or less, 120°F or less, 1 10°F or less and typically at about 100°F.
- other suitable bleaches include powdered bleaches such as lithium hypochlorite, trichloroisocyanuric acid and hypochlorous acid.
- the washing solution in zone three should have a minimum oxygen reduction potential of 665MV, which is achieved by establishing sufficient sodium hypochlorite and an effective pH.
- the clothing is subjected to the hypochlorite solution for about 4 to about 30 minutes, which is more than adequate to destroy potential pathogens on the textile.
- the textile is rinsed in a fourth zone or a finishing zone. In this zone, which is optional, any remaining wash chemicals are removed from the textiles and the pH is adjusted to a proper finish pH of 6-7. Softener may be added as required by the end-user.
- the present invention has many different advantages.
- all the zones are operated at lower temperatures, generally around 100°F. This eliminates the need for either adding or removing energy from the textiles during the laundry procedure.
- they are disinfected, destroying pathogens utilizing the third zone which effectively kills the pathogens with the hypochlorite at a relatively low pH and low temperature. Again, the low
- the present invention reduces the damage to the textiles, as compared to current bleach parameters which operate at a higher temperature and higher pHs.
- the tensile strength of cotton is measured after repeated washes, either under current bleach parameters or the low temperature bleach parameters as discussed above for zone three.
- the tensile strengths of the textiles bleached with the bleach parameters of the present invention are substantially higher than those bleached using current bleach parameters (i.e. higher temperatures and pHs).
- current bleach parameters i.e. higher temperatures and pHs.
- test Parameters The objective was to evaluate the effectiveness of the present invention as a means of reducing known amounts of microorganisms. Test Parameters:
- the effect of the present invention on known quantities of microbes was tested to examine how the different wash parameters affect the different organisms.
- One by one inch square swatches of linen were inoculated. After inoculation the swatches were allowed to dry for thirty minutes in a sterile petri dish. Upon completion of the dry time, the swatches were pinned to a mesh net and subjected to the differing wash parameters.
- Each organism was grown in trypitic soy broth for approximately 24 hours at 32.5°C in a sterile baffled flask, while shaking on a Thermo Scientific multipurpose orbital shaker. After the incubation period the suspension was diluted with tryptic soy broth, to yield a specific absorbance with the Hach D 2700 spectrophotometer. The adjusted suspension contains approximately 5.0 x 10 8 CFU/mL.
- the objective was to evaluate the effectiveness of resource conservation wash parameters as a means of reducing known amounts of microorganisms.
- Each organism was grown in trypitic soy broth for approximately 24 hours at 32.5°C in a sterile baffled flask, while shaking on a Thermo Scientific multipurpose orbital shaker. After the incubation period the suspension was diluted with tryptic soy broth, to yield a specific absorbance with the Hach D 2700 spectrophotometer. The adjusted suspension contains approximately 5.0 x 10 8 CFU/mL.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Apparatus For Disinfection Or Sterilisation (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US14/571,394 US20160168780A1 (en) | 2014-12-16 | 2014-12-16 | Process to produce hygienically clean textile |
PCT/US2015/064884 WO2016100062A1 (en) | 2014-12-16 | 2015-12-10 | Process to produce hygienically clean textile |
Publications (1)
Publication Number | Publication Date |
---|---|
EP3234095A1 true EP3234095A1 (de) | 2017-10-25 |
Family
ID=54937399
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP15813674.7A Withdrawn EP3234095A1 (de) | 2014-12-16 | 2015-12-10 | Verfahren zur herstellung von hygienisch sauberem textil |
Country Status (4)
Country | Link |
---|---|
US (1) | US20160168780A1 (de) |
EP (1) | EP3234095A1 (de) |
CA (1) | CA2974047A1 (de) |
WO (1) | WO2016100062A1 (de) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20180094226A1 (en) * | 2016-10-03 | 2018-04-05 | The Procter & Gamble Company | Laundry detergent composition |
PL3301152T3 (pl) | 2016-10-03 | 2022-06-13 | The Procter & Gamble Company | Suszona rozpyłowo cząstka detergentu nadająca niskie ph w kąpieli piorącej |
US11884899B2 (en) * | 2018-06-01 | 2024-01-30 | Amtex Innovations Llc | Methods of laundering stitchbonded nonwoven towels using a soil release polymer |
US10822578B2 (en) * | 2018-06-01 | 2020-11-03 | Amtex Innovations Llc | Methods of washing stitchbonded nonwoven towels using a soil release polymer |
Family Cites Families (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2938764A (en) * | 1957-02-25 | 1960-05-31 | Wyandotte Chemicals Corp | Highly alkaline dichlorodimethylhydantoin bleaching solutions and methods |
US3650667A (en) * | 1969-02-26 | 1972-03-21 | Steiner American Corp | Laundry process for producing fabrics that are substantially free from bacteria and bacterial spores |
US4120650A (en) * | 1977-12-05 | 1978-10-17 | Basf Wyandotte Corporation | Laundering process for dual bleaching stained fabrics |
US4600406A (en) * | 1985-03-22 | 1986-07-15 | Diversey Wyandotte Corporation | Method of low temperature bleaching with reduced amounts of chlorine requiring reduced bleaching intervals |
ES2158878T3 (es) * | 1994-06-10 | 2001-09-16 | Procter & Gamble | Emulsiones acuosas con abrillantadores. |
US5707483A (en) * | 1996-07-05 | 1998-01-13 | Minnesota Mining And Manufacturing Company | Rotary acoustic horn |
DE19700799C2 (de) * | 1997-01-13 | 1999-02-04 | Henkel Kgaa | Wäßrige Textilbleichmittel |
DE69736927D1 (de) * | 1997-09-19 | 2006-12-21 | Procter & Gamble | Verfahren zum Bleichen von Gewebe |
CA2280259C (en) * | 1998-08-26 | 2009-10-27 | The Clorox Company | Method for increasing brightness retention of laundered fabrics |
TR200200043T2 (tr) * | 1999-07-14 | 2002-04-22 | Unilever N.V. | Bir deterjan bileşimi ve çamaşır yıkama yöntemi |
US6534462B1 (en) * | 2000-07-10 | 2003-03-18 | Access Business Group International Llc | Liquid laundry detergent and pretreatment composition |
GB0216173D0 (en) * | 2002-07-12 | 2002-08-21 | Fabric Care Res Ass Ltd | A laundry preparation |
US7285522B2 (en) * | 2004-08-25 | 2007-10-23 | The Clorox Company | Bleaching with improved whitening |
GB0428202D0 (en) * | 2004-12-23 | 2005-01-26 | Fabric Care Res Ass Ltd | A method of disinfecting textile articles during laundering and a laundry preparation for use in said method |
DE102005041436A1 (de) * | 2005-08-31 | 2007-03-01 | Henkel Kgaa | Flüssiges hypohalogenithaltiges Bleichmittel |
WO2007107898A2 (en) * | 2006-03-17 | 2007-09-27 | The Procter & Gamble Company | Process of bleaching fabric |
US8449626B2 (en) * | 2009-11-11 | 2013-05-28 | The Procter & Gamble Company | Cleaning method |
MY171527A (en) * | 2010-02-03 | 2019-10-16 | Cleary Dolcetti Joseph | An exoskeleton system |
GB201015277D0 (en) * | 2010-09-14 | 2010-10-27 | Xeros Ltd | Novel cleaning method |
WO2012166768A1 (en) * | 2011-06-03 | 2012-12-06 | The Procter & Gamble Company | Laundry care compositions containing dyes |
WO2014124927A2 (en) * | 2013-02-14 | 2014-08-21 | Novozymes A/S | Industrial and institutional laundering using multi-enzyme compositions |
-
2014
- 2014-12-16 US US14/571,394 patent/US20160168780A1/en not_active Abandoned
-
2015
- 2015-12-10 CA CA2974047A patent/CA2974047A1/en not_active Abandoned
- 2015-12-10 EP EP15813674.7A patent/EP3234095A1/de not_active Withdrawn
- 2015-12-10 WO PCT/US2015/064884 patent/WO2016100062A1/en active Application Filing
Non-Patent Citations (2)
Title |
---|
None * |
See also references of WO2016100062A1 * |
Also Published As
Publication number | Publication date |
---|---|
US20160168780A1 (en) | 2016-06-16 |
CA2974047A1 (en) | 2016-06-23 |
WO2016100062A1 (en) | 2016-06-23 |
WO2016100062A4 (en) | 2016-07-28 |
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