EP2655731A1 - A method of controlling a pulping process in a feed-forward manner - Google Patents

A method of controlling a pulping process in a feed-forward manner

Info

Publication number
EP2655731A1
EP2655731A1 EP11851854.7A EP11851854A EP2655731A1 EP 2655731 A1 EP2655731 A1 EP 2655731A1 EP 11851854 A EP11851854 A EP 11851854A EP 2655731 A1 EP2655731 A1 EP 2655731A1
Authority
EP
European Patent Office
Prior art keywords
wood chips
digester
controlling
pulping process
dry
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP11851854.7A
Other languages
German (de)
French (fr)
Other versions
EP2655731A4 (en
EP2655731B1 (en
Inventor
Mats NÄSMAN
Marko Harinen
Olli Timonen
Kimmo Ruohoniemi
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Stora Enso Oyj
Original Assignee
Stora Enso Oyj
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Stora Enso Oyj filed Critical Stora Enso Oyj
Publication of EP2655731A1 publication Critical patent/EP2655731A1/en
Publication of EP2655731A4 publication Critical patent/EP2655731A4/en
Application granted granted Critical
Publication of EP2655731B1 publication Critical patent/EP2655731B1/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C1/00Pretreatment of the finely-divided materials before digesting
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00Pulping cellulose-containing materials
    • D21C3/22Other features of pulping processes
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00Pulping cellulose-containing materials
    • D21C3/22Other features of pulping processes
    • D21C3/228Automation of the pulping processes
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C7/00Digesters
    • D21C7/12Devices for regulating or controlling

Definitions

  • the invention refers to a method of controlling a pulping process wherein wood chips are conveyed to an impregnation vessel or to a digester where said wood chips are treated with a liquor comprising chemicals.
  • wood chips are treated with chemicals in a digester at enhanced pressure and temperature to dissolve the lignin that binds fibres together.
  • the predominating pulping process today is the Kraft process, wherein wood chips are treated with a mixture of sodium hydroxide and sodium sulphide, known as white liquor.
  • the pulp quality and the consumption of the chemicals used in the pulping process are highly dependent on the raw material, i.e. the wood chips.
  • the moisture content and other properties of the chips may vary due to, e.g., seasonal variations, different chip pile arrangements and the wood species used.
  • the variation of the properties of the raw material makes it difficult to set an accurate dosing of chemicals to the digester. Oftentimes more chemicals than required are used, which is detrimental from both an economical and an environmental perspective.
  • a system for controlling a continuous digester is further disclosed in CA919289.
  • the process is controlled on the basis of information obtained from measurements of the properties of the pulp or of the residual alkali content in spent cooking liquor, i.e. the process is controlled in a feed-back manner.
  • Such an approach fails to comply with short-term or sudden
  • the invention discloses a method of controlling a pulping process wherein wood chips are conveyed to an impregnation vessel and/or to a digester where said wood chips are treated with a liquor comprising chemicals.
  • the method of the invention comprises the steps of; a . estimating a mass flow of dry wood chips to the impregnation vessel or the digester needed to achieve a desired pulp production, b . measuring the actual mass flow of moisture wood chips conveyed to the impregnation vessel or the digester, c . calculating a ratio between the measured actual mass flow of moisture wood chips and the estimated mass flow of dry wood chips, d . controlling the pulping process based on said
  • the method according to the invention makes it, e.g.
  • a method comprising the steps of; a . estimating a dry density of the wood chips being treated, b . measuring the density of the moisture wood chips conveyed to the impregnation vessel or to the digester, c . calculating a ratio between said estimated dry density of the wood chips and said measured density of the moisture wood chips, and d . controlling the pulping process based on said calculated ratio.
  • a method comprising the steps of; a . estimating a dry density of the wood chips being treated, b . measuring the density of the moisture wood chips conveyed to the impregnation vessel or to the digester, c . calculating a ratio between said estimated dry density of the wood chips and said measured density of the moisture wood chips, which also involves compensating with a measured dry content, and d. controlling the pulping process based on said calculated ratio.
  • the invention relates to a method of controlling a pulping process wherein wood chips are treated with chemicals in an impregnation vessel and/or in a digester.
  • the pulping process may, e.g., be a kraft pulping process, a sulphite pulping process or a chemi-thermo mechanical pulping process.
  • the pulping process may be a batch or a continuous pulping process.
  • the process may, e.g., be a continuous Kraft pulping process, wherein the wood chips are treated with a mixture of sodium hydroxide and sodium sulphide at elevated temperature and pressure.
  • a ratio between the actual mass flow of fresh, moisture wood chips conveyed to the impregnation vessel or to the digester and an estimated mass flow of dry wood chips to the impregnation vessel or the digester needed to achieve a desired, pre-set, pulp production is calculated.
  • Said ratio below referred to as Wood Material Indicator (WMI)
  • WMI Wood Material Indicator
  • the WMI may be calculated in accordance with eq. 1.
  • the WMI may be calculated by dividing the estimated mass flow of dry wood chips with the actual mass flow of moisture wood chips.
  • An estimated mass flow of dry wood chips may be calculated by dividing the desired pulp production with the cooking yield in accordance with equation 2. pulp production
  • the Pulp Production is a targeted, pre-set, value.
  • the Pulp Production in the equation above is expressed in bone dry weight [kg/s], i.e. the weight of 100 % dry pulp.
  • the cooking yield is an estimated value of the cooking yield for the wood species that are being pulped.
  • the estimated cooking yield for kraft pulping of soft wood is, e.g., 46%.
  • the mass flow of moisture wood chips conveyed to the impregnation vessel or the digester may, e.g., be measured by use of a chip conveyor scale (preferred) , a mass flow scanner (by using X-ray) or a radiating wood flow meter.
  • a chip conveyor scale e.g., a mass flow scanner (by using X-ray) or a radiating wood flow meter.
  • the measured mass flow of moisture wood varies depending on the moisture content of the raw material and on other
  • the pulping process is controlled by use of a ratio between the actual, measured, value of the density of the moisture fresh chips and an estimated value of the density of dry chips.
  • the estimated value of the density of the dry chips depends on the wood species used.
  • the density of moisture, fresh, chips may be determined by measuring the weight of the chips in the chip silo and dividing said measured value with the volume of the chips in the silo. If the process is a batch pulping process, the density of moisture, fresh, chips may be determined by measuring the weight of the chips in the batch digester and dividing said measured value with the volume of the chips in the batch digester.
  • the Wood Material Indicator may be used to determine the Wood Material Indicator (WMI)
  • the cooking alkali dose may be continuously regulated based on the WMI value.
  • the Liquor to wood ratio may be regulated based on WMI by adjusting the internal circulation of spent cooking liquor or washing liquor in the digester.
  • the estimated dry mass flow is calculated by eq.2.
  • the production in a continuous digester system is normally controlled by a volumetric measurement such as a chip feeding screw or a chip meter. Based on the known feeding volume per revolution, filling degree and estimated chip density the chip feeding device will rotate with a certain speed in order to maintain the target production (estimated dry mass flow) .
  • Wet chip density WCF / (V x FD x rpm)
  • the WMI is defined as
  • WMI as described by the ratio above may then be used in the process control.
  • the estimated dry density is dependent on which raw material is used.
  • the method according to the invention is used in a feed forward loop (manner) taking into account what is fed into the system (variation in both dry matter and moisture is combined; in the Nordic conditions where variation in chip bulk density is very low this has worked well) .
  • the response to changes is further relatively fast.
  • Fig. 1 shows a schematic view of the flow of wood raw material from a chip pile to an impregnation vessel or to a digester. Total mass flow is measured preferably by using a chip conveyor scale.
  • the raw material of fresh, moisture wood chips is conveyed on a chip conveyor (1) to a chip silo
  • the material is further conveyed from the chip silo (2) to an impregnation vessel or a digester by use of a chip feed screw (3) .
  • a chip conveyor scale (4) arranged under the chip conveyor (1), measures the actual flow of fresh, moisture chips continuously. Since the mass of chips in the silo is held substantially constant, measuring of the flow on the chip conveyor gives an accurate value of the actual flow of fresh, moisture chips to the impregnation vessel or the digester. The measured fresh flow value is transmitted to a control unit (5) of a control system, (5) shown
  • the estimated dry wood flow is also entered into the control unit (5) .
  • a ratio between said flows is calculated (WMI) and used to regulate e.g. the set value for the alkali charge to the impregnation vessel or the digester and the liquid to wood ratio.
  • WMI is calculated
  • the process is further controlled on the basis of a theoretically calculated flow of wood chips to the impregnation vessel or the digester, i.e. in accordance with the traditional way of controlling a pulping process.
  • WMI is preferably used to regulate a certain percentage on top of the traditional control of the process.
  • a theoretically calculated set value (set-point) is thus also entered into the system.
  • Figure 2 shows an example how the WMI as set out above may be determined.
  • FIG 3 shows a control system in accordance with the invention.
  • the control system may comprise one or several sub control systems for regulating the alkali charge, cooking temperature and/or Liquor to wood ratio for long term, e.g. 24 hours, and/or short term, e.g. 2 hours, variations of the WMI.
  • the regulation is separated into two circuits; one for long term and one for short term variation of WMI.
  • the system (5) may comprise further control units (6, 7) where further variables (vl, v2, ... Vn) or preset values may be entered for controlling the process, such as the upper and lower limits of alkali charge, the current values of the liquor to wood ratio, cooking temperature (H-factor) and alkali charge etc.
  • Figure 4 shows more schematic how WMI according to the present invention may be used to control alkali dosage, which is only an example of a parameter which may be
  • Figure 5 shows the WMI control in action (c.f. the example below) .

Landscapes

  • Paper (AREA)

Abstract

The invention discloses a method of controlling a pulping process wherein wood chips are conveyed to an impregnation vessel and/or to a digester where said wood chips are treated with a liquor comprising chemicals. According to the method of the invention a ratio between a measured, actual mass flow of moisture wood chips to an impregnation vessel or to a digester and an estimated mass flow of dry wood chips conveyed to the impregnation vessel or to the digester is calculated. Said ratio is used to control the pulping process. The method makes it possible to control e.g. the supply of chemicals, the liquor to wood ratio and the pulping temperature on-line, in a feed-forward manner.

Description

A Method of Controlling a Pulping Process in a Feed-Forward Manner
Technical field
The invention refers to a method of controlling a pulping process wherein wood chips are conveyed to an impregnation vessel or to a digester where said wood chips are treated with a liquor comprising chemicals.
Background
In a chemical pulping process, wood chips are treated with chemicals in a digester at enhanced pressure and temperature to dissolve the lignin that binds fibres together. The predominating pulping process today is the Kraft process, wherein wood chips are treated with a mixture of sodium hydroxide and sodium sulphide, known as white liquor. The pulp quality and the consumption of the chemicals used in the pulping process are highly dependent on the raw material, i.e. the wood chips. The moisture content and other properties of the chips may vary due to, e.g., seasonal variations, different chip pile arrangements and the wood species used. The variation of the properties of the raw material makes it difficult to set an accurate dosing of chemicals to the digester. Oftentimes more chemicals than required are used, which is detrimental from both an economical and an environmental perspective. A system for controlling a continuous digester is further disclosed in CA919289.
In conventional chemical pulping processes, the process is controlled on the basis of information obtained from measurements of the properties of the pulp or of the residual alkali content in spent cooking liquor, i.e. the process is controlled in a feed-back manner. Such an approach fails to comply with short-term or sudden
variations of the properties of the chips. In the art, ther are commercial measurement systems available for measuring raw material properties. However, these prior art methods usually involve high investment costs, requires long time for analysis and/or are not accurate enough and are thus no typically used to control the process. Thus, there remains a need for a simple, on-line feed forward control of the pulping process.
Summary of the invention
It is an object of the invention to provide a simple, on- line method for controlling a pulping process. This, and other advantages, is achieved with the method according to the invention.
The invention discloses a method of controlling a pulping process wherein wood chips are conveyed to an impregnation vessel and/or to a digester where said wood chips are treated with a liquor comprising chemicals. The method of the invention comprises the steps of; a . estimating a mass flow of dry wood chips to the impregnation vessel or the digester needed to achieve a desired pulp production, b . measuring the actual mass flow of moisture wood chips conveyed to the impregnation vessel or the digester, c . calculating a ratio between the measured actual mass flow of moisture wood chips and the estimated mass flow of dry wood chips, d . controlling the pulping process based on said
calculated ratio.
The method according to the invention makes it, e.g.
possible to control the supply of chemicals, such as sodium hydroxide and sodium sulphide, to the impregnation vessel or to the digester, the liquor to wood ratio and/or the pulping temperature on-line, in a feed-forward manner. It has been shown, that by controlling the pulping process in accordance with the invention, the stability of the process is improved and a reduction in the variation of the kappa number and the quality of the pulp is achieved. The method is simple and does not require huge investment costs. Further we are using the estimation in a) to calculate the pre-set process parameters. The ratio is then used for fine tuning the process parameters. Thus you create first a set-point which later is used in the regulation of the process.
According to a second aspect of the invention, there is provided a method comprising the steps of; a . estimating a dry density of the wood chips being treated, b . measuring the density of the moisture wood chips conveyed to the impregnation vessel or to the digester, c . calculating a ratio between said estimated dry density of the wood chips and said measured density of the moisture wood chips, and d . controlling the pulping process based on said calculated ratio. According to a third aspect of the invention, there is provided a method comprising the steps of; a . estimating a dry density of the wood chips being treated, b . measuring the density of the moisture wood chips conveyed to the impregnation vessel or to the digester, c . calculating a ratio between said estimated dry density of the wood chips and said measured density of the moisture wood chips, which also involves compensating with a measured dry content, and d. controlling the pulping process based on said calculated ratio.
This may be used when the variations in wood density
dominate. Thus measuring the dry content provides a way to compensate for this variation.
Detailed description of the invention
The invention relates to a method of controlling a pulping process wherein wood chips are treated with chemicals in an impregnation vessel and/or in a digester. The term
"impregnation vessel" as used herein may be any kind of a vessel, pipe or the like suitable for processing of the wood chips. The pulping process may, e.g., be a kraft pulping process, a sulphite pulping process or a chemi-thermo mechanical pulping process. The pulping process may be a batch or a continuous pulping process. The process may, e.g., be a continuous Kraft pulping process, wherein the wood chips are treated with a mixture of sodium hydroxide and sodium sulphide at elevated temperature and pressure.
In accordance with the method of the invention, a ratio between the actual mass flow of fresh, moisture wood chips conveyed to the impregnation vessel or to the digester and an estimated mass flow of dry wood chips to the impregnation vessel or the digester needed to achieve a desired, pre-set, pulp production, is calculated. Said ratio, below referred to as Wood Material Indicator (WMI), may, e.g., be used to control the amount of chemicals, such as sodium hydroxide and sodium sulphide, supplied to the impregnation vessel or the digester and/or to control the liquor to wood ratio in the digester and/or to control the pulping temperature. The WMI may be calculated in accordance with eq. 1.
„ Actual mass flow of moisture chips [kg I s \ ,
WMI = - - - (eq. 1)
Estimated mass flow of dry chips [kg/ s\
Alternatively, the WMI may be calculated by dividing the estimated mass flow of dry wood chips with the actual mass flow of moisture wood chips.
An estimated mass flow of dry wood chips may be calculated by dividing the desired pulp production with the cooking yield in accordance with equation 2. pulp production
Estimated dry mass flow [kg/ s] xlOO (eq. 2)
Cooking Yield The Pulp Production is a targeted, pre-set, value. The Pulp Production in the equation above is expressed in bone dry weight [kg/s], i.e. the weight of 100 % dry pulp. The cooking yield is an estimated value of the cooking yield for the wood species that are being pulped. The estimated cooking yield for kraft pulping of soft wood is, e.g., 46%.
The mass flow of moisture wood chips conveyed to the impregnation vessel or the digester may, e.g., be measured by use of a chip conveyor scale (preferred) , a mass flow scanner (by using X-ray) or a radiating wood flow meter. The measured mass flow of moisture wood varies depending on the moisture content of the raw material and on other
properties, such as the density, of the raw material. In accordance with the second aspect of the invention, the pulping process is controlled by use of a ratio between the actual, measured, value of the density of the moisture fresh chips and an estimated value of the density of dry chips. The estimated value of the density of the dry chips depends on the wood species used. The density of moisture, fresh, chips may be determined by measuring the weight of the chips in the chip silo and dividing said measured value with the volume of the chips in the silo. If the process is a batch pulping process, the density of moisture, fresh, chips may be determined by measuring the weight of the chips in the batch digester and dividing said measured value with the volume of the chips in the batch digester.
The Wood Material Indicator (WMI) may be used to
continuously control the pulping process. This may, e.g., be achieved by regulating the chemical charge to the
impregnation vessel or the digester and/or the Liquor to wood ratio and/or the pulping temperature . The cooking alkali dose may be continuously regulated based on the WMI value. The Liquor to wood ratio may be regulated based on WMI by adjusting the internal circulation of spent cooking liquor or washing liquor in the digester. When the variation in raw material density is higher the wood material indicator can be used in combination with frequent analysis of the dry content of the chips conveyed to the digester as reflected by the third aspect of the present invention.
In such a way the possible variation from humidity and raw material density is separated from each other and this will further improve the precision of the process control if the variation in mass flow is dominated by raw material density variation. This is decided case by case on the conditions in the mill and used raw material.
The estimated dry mass flow is calculated by eq.2. The production in a continuous digester system is normally controlled by a volumetric measurement such as a chip feeding screw or a chip meter. Based on the known feeding volume per revolution, filling degree and estimated chip density the chip feeding device will rotate with a certain speed in order to maintain the target production (estimated dry mass flow) . By utilising the measured wet chip flow measured on the chip conveyor to the digester system in combination with an analysed chip dry content and the known volume (given by the rotation speed of the chip metering device) of chips fed to the digester system it is possible to calculate the measured wet chip density: Wet chip density = WCF / (V x FD x rpm)
Where WCF = wet chip mass flow (kg/min) V = fed volume per revolution (m3)
FD = filling degree rpm = rotation speed of the chip metering devise (rpm) The measured dry density is then calculated from:
Measured dry density = wet chip density x dry content.
In this case the WMI is defined as
WMI = Measured dry density/estimated dry density
WMI as described by the ratio above may then be used in the process control. The estimated dry density is dependent on which raw material is used.
Further the method according to the invention is used in a feed forward loop (manner) taking into account what is fed into the system (variation in both dry matter and moisture is combined; in the Nordic conditions where variation in chip bulk density is very low this has worked well) . The response to changes is further relatively fast.
In the following the invention will be described in more details by way of an example with reference to the drawings.
Description of the drawings Fig. 1 shows a schematic view of the flow of wood raw material from a chip pile to an impregnation vessel or to a digester. Total mass flow is measured preferably by using a chip conveyor scale. The raw material of fresh, moisture wood chips is conveyed on a chip conveyor (1) to a chip silo
(2) . The material is further conveyed from the chip silo (2) to an impregnation vessel or a digester by use of a chip feed screw (3) . The screw rotation of the chip feed screw
(3) is controlled based on the calculated estimated dry mass flow, i.e. it depends on the set value of the pulp
production. According to one example of the invention, a chip conveyor scale (4), arranged under the chip conveyor (1), measures the actual flow of fresh, moisture chips continuously. Since the mass of chips in the silo is held substantially constant, measuring of the flow on the chip conveyor gives an accurate value of the actual flow of fresh, moisture chips to the impregnation vessel or the digester. The measured fresh flow value is transmitted to a control unit (5) of a control system, (5) shown
schematically in fig. 3. The estimated dry wood flow is also entered into the control unit (5) . In the control system, a ratio between said flows is calculated (WMI) and used to regulate e.g. the set value for the alkali charge to the impregnation vessel or the digester and the liquid to wood ratio. Preferably, the process is further controlled on the basis of a theoretically calculated flow of wood chips to the impregnation vessel or the digester, i.e. in accordance with the traditional way of controlling a pulping process. Thus, WMI is preferably used to regulate a certain percentage on top of the traditional control of the process. A theoretically calculated set value (set-point) is thus also entered into the system.
Figure 2 shows an example how the WMI as set out above may be determined.
Figure 3 shows a control system in accordance with the invention. The control system may comprise one or several sub control systems for regulating the alkali charge, cooking temperature and/or Liquor to wood ratio for long term, e.g. 24 hours, and/or short term, e.g. 2 hours, variations of the WMI. In the control system (5) shown in fig. 3, the regulation is separated into two circuits; one for long term and one for short term variation of WMI. The system (5) may comprise further control units (6, 7) where further variables (vl, v2, ... Vn) or preset values may be entered for controlling the process, such as the upper and lower limits of alkali charge, the current values of the liquor to wood ratio, cooking temperature (H-factor) and alkali charge etc. Figure 4 shows more schematic how WMI according to the present invention may be used to control alkali dosage, which is only an example of a parameter which may be
controlled by using the WMI according to the present
invention .
Figure 5 shows the WMI control in action (c.f. the example below) . Example
A trial run was performed at the Oulu mill during 4 days where it was shown that WMI control reduces kappa variation.
WMI as a soft sensor appears to be usable and accurate enough to reduce the effects of raw material variations . The results are given below in Table 1.
With
No WMI WMI
control control
Devi Maxi Minim Devi Maxi Mini
Measurement Unit Average ation mum urn Average ation mum mum
Alkali to wood ratio % 19.1 0.10 19.2 19.0 19.0 0.05 19.2 18.8
Residual alkali extraction
[g/l] (average 2h) g/i 6.1 0.27 6.8 5.4 5.8 0.21 6.6 5.2
WMI value as % of DC in
wood (average 2h) % 47.7 0.47 48.7 46.9 48.0 0.41 49.0 47.3
On-line blow kappa value
from analyzer 27.1 1.27 31.5 24.4 26.7 0.74 28.8 25.0
167.
Cooking temperature °c 167.6 0.53 168.6 166.0 169.0 0.72 171.0 0
Cooking production t/d 1 123 6.98 1127 1099 1150 0.16 1150 1149
Table 1. Results from the 4-day Oulu trial. Each case period of 4d running. The raw material was softwood of Scandinavian origin (t/d=tonnes/day) . See also figure which reflects the example. C.f. also figure 2.
The benefits are given below in Table 2.
Benefits of using wood material
indicator (WMI) control
Change in residual alkali variation (black
liquor extraction) 22.1
Change in kappa variation (after digester
blow) 41.7 Table 2. The benefits from the 4-day Oulu trial.
Various embodiments of the present invention have been described above but a person skilled in the art realizes further minor alterations, which would fall into the scope of the present invention. The breadth and scope of the present invention should not be limited by any of the above- described exemplary embodiments, but should be defined only in accordance with the following claims and their
equivalents. Other aspects, advantages and modifications within the scope of the invention will be apparent to those skilled in the art to which the invention pertains. Thus the invention is therefore intended to cover various
modifications and equivalent methods included within the spirit and scope of the appended claims.
Any illustration and description in the drawings and in the foregoing description are to be considered exemplary and not restrictive .
Use of the word "comprising" in the claims does not exclude other elements or steps, and use of the article "a" or "an" does not exclude a plurality. Occurrence of features in different dependent claims does not per se exclude a combination of these features. Any reference signs in the claims are for increasing intelligibility and shall not be construed as limiting the scope of the claims.

Claims

A method of controlling a pulping process wherein wood chips are conveyed to an impregnation vessel and/or to a digester where said wood chips are treated with a liquor comprising chemicals, which method comprises the steps of; a . estimating a mass flow of dry wood chips to the impregnation vessel or to the digester needed to achieve a desired pulp production, b . measuring the actual mass flow of moisture wood chips conveyed to the impregnation vessel or to the digester, c . calculating a ratio between the actual mass flow of moisture wood chips and the estimated mass flow of dry wood chips, d . controlling the pulping process based on said
calculated ratio.
A method according to claim 1, wherein the estimated value of dry wood chips is achieved by dividing the desired pulp production with an estimated cooking yield .
3. A method according to any one of claims 1 - 2, wherein the mass flow of moisture wood chips is measured by use of a chip conveyor scale.
A method of controlling a pulping process wherein wood chips are conveyed to an impregnation vessel and/or to a digester where said wood chips are treated with a liquor comprising chemicals, which method comprises the steps of; a . estimating a dry density of the wood chips being treated, b . measuring the density of the moisture wood chips conveyed to the impregnation vessel and/or to the digester, c . calculating a ratio between said estimated dry density of the wood chips and said measured density of moisture wood chips, d . controlling the pulping process based on said
calculated ratio.
A method according to any one of claims 1 - 4, wherein the step (d) of controlling the pulping process comprises controlling the chemicals supplied to the impregnation vessel and/or to the digester based on said calculated ratio.
A method according to any one of claims 1 - 5, wherein the step (d) of controlling the pulping process comprises controlling the liquor to wood ratio in the digester based on said calculated ratio.
A method according to anyone of claims 1 - 6, wherein the step (d) of controlling the pulping process comprises controlling the pulping temperature based on said calculated ratio.
A method of controlling a pulping process wherein wood chips are conveyed to an impregnation vessel and/or to a digester where said wood chips are treated with a liquor comprising chemicals, which method comprises the steps of; a . estimating a dry density of the wood chips
being treated, b . measuring the density of the moisture wood
chips conveyed to the impregnation vessel or to the digester, c . calculating a ratio between said estimated dry density of the wood chips and said measured density of the moisture wood chips, which also involves compensating with a measured dry content, and d . controlling the pulping process based on said calculated ratio.
9. A method according to claim 8, wherein the step
(c) calculating a ratio between said estimated dry density of the wood chips and said measured density of the moisture wood chips, which also involves compensating with a measured dry content, involves multiplying with the dry content.
EP11851854.7A 2010-12-22 2011-12-16 A method of controlling a pulping process in a feed-forward manner Active EP2655731B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
SE1051361 2010-12-22
PCT/SE2011/051534 WO2012087228A1 (en) 2010-12-22 2011-12-16 A method of controlling a pulping process in a feed-forward manner

Publications (3)

Publication Number Publication Date
EP2655731A1 true EP2655731A1 (en) 2013-10-30
EP2655731A4 EP2655731A4 (en) 2017-05-17
EP2655731B1 EP2655731B1 (en) 2019-05-08

Family

ID=46314243

Family Applications (1)

Application Number Title Priority Date Filing Date
EP11851854.7A Active EP2655731B1 (en) 2010-12-22 2011-12-16 A method of controlling a pulping process in a feed-forward manner

Country Status (7)

Country Link
EP (1) EP2655731B1 (en)
CN (1) CN103270214B (en)
BR (1) BR112013015837A2 (en)
ES (1) ES2730759T3 (en)
PT (1) PT2655731T (en)
UY (1) UY33828A (en)
WO (1) WO2012087228A1 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FI130616B (en) * 2021-10-08 2023-12-14 Andritz Ab A method for chemical pulp production in a multi-stage process

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA919289A (en) * 1970-06-30 1973-01-16 Westinghouse Electric Corporation System for controlling the feed end of a continuous papermaking digester
US4239590A (en) * 1979-01-11 1980-12-16 Kamyr, Inc. Method of maintaining uniformity of fibrous material fed to a continuous digester
US5266159A (en) * 1991-10-25 1993-11-30 Kamyr, Inc. Mass flow measurement, preferably for controlling chip feed to a digester
SE500994C2 (en) * 1993-03-02 1994-10-17 Iggesund Tools Ab Method for controlling a defibration process by measuring the bulk density of the added chip
CN1179188A (en) * 1995-03-23 1998-04-15 西门子公司 Method and device for process control in cellulose and/or paper manufacture
SE517297E (en) * 1999-09-10 2004-12-07 Stora Enso Ab Method for producing mechanical pulp from a cellulose-containing material, pulp made according to the method and carton produced from the pulp
US6447639B1 (en) * 2001-03-05 2002-09-10 Sita Ruby Warren Process for controlling a digester using real time measurement of moisture content and species of wood
BR0213386A (en) * 2002-08-16 2005-02-01 Amec Americas Ltd Pulp Digester Control System Online
SE525872C2 (en) * 2002-09-06 2005-05-17 Stora Enso Ab Method of producing mechanical pulp with reduced energy consumption
FI123011B (en) * 2005-01-05 2012-09-28 Metso Paper Inc Method for regulating a cellulose cooking process
US20060278353A1 (en) * 2005-06-03 2006-12-14 Centre De Recherche Industrielle Du Quebec Method and apparatus for estimating relative proportion of wood chips species to be fed to a process for producing pulp

Also Published As

Publication number Publication date
CN103270214A (en) 2013-08-28
WO2012087228A1 (en) 2012-06-28
BR112013015837A2 (en) 2018-05-15
EP2655731A4 (en) 2017-05-17
ES2730759T3 (en) 2019-11-12
UY33828A (en) 2012-06-29
CN103270214B (en) 2016-11-16
EP2655731B1 (en) 2019-05-08
PT2655731T (en) 2019-06-26

Similar Documents

Publication Publication Date Title
US6319362B1 (en) Method and equipment for controlling properties of paper
CA1099058A (en) Process for controlling the supply of delignifying and/or bleaching chemicals in the continuous delignification of lignocellulosic material
CN104161300B (en) A kind of papermaking-method reconstituted tobaccos optimizes coating process
WO2015128808A1 (en) A system and a method for advanced optimization of continuous digester operation
US6328851B1 (en) Method and equipment for controlling properties of paper
CA2441055C (en) Pulp treatment and process
EP2655731B1 (en) A method of controlling a pulping process in a feed-forward manner
EP3036370B1 (en) A method and a system for controlling a refiner for refining a product containing cellulose and readable information about a quality index of the product
CN102268832A (en) Pulping and papermaking process for producing middle-grade and high-grade cultural paper by using larch chemical-mechanical pulp
CN113800459B (en) Quantitative control system, control method and production system for reconstituted tobacco by thick pulp papermaking method
EP2740839A1 (en) Method and system for manufacturing mechanical pulp and mechanical pulp obtainable by the method
CN103221607B (en) Method for adjusting the formation of a fiber web
US3816241A (en) Method and apparatus for feed-forward control of wood pulp refiners
FI58028C (en) REGLERINGSPROCESS OCH -ANORDNING FOER KOKARE
Tessier et al. Motor load and freeness control of CMP pulp refining
WO2006072653A1 (en) Method for controlling a pulping process
Badwe et al. Continuous digester optimization using advanced process control
KR20070103436A (en) Apparatus and method for producing a fibrous web
Smith A computerized pulp and paper mill instrumentation and control system
CA1130061A (en) Exothermic heat as a means of determining the degree of delignification
Rantanen et al. Prediction and control of blow-line kappa number
US3020765A (en) Method and apparatus for regulating consistency
JP3064616B2 (en) Method for controlling kappa number of pulp in vertical continuous digester with modified cooking method
SU926131A1 (en) Method for automatically controlling process of continuous cooking of sulphate pulp
JP2005256224A (en) Method of digestion using columnar vessel type continuous digester

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

17P Request for examination filed

Effective date: 20130722

AK Designated contracting states

Kind code of ref document: A1

Designated state(s): AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR

DAX Request for extension of the european patent (deleted)
RA4 Supplementary search report drawn up and despatched (corrected)

Effective date: 20170418

RIC1 Information provided on ipc code assigned before grant

Ipc: D21C 3/22 20060101ALI20170410BHEP

Ipc: D21C 7/12 20060101AFI20170410BHEP

RIC1 Information provided on ipc code assigned before grant

Ipc: D21C 3/22 20060101AFI20181008BHEP

Ipc: D21C 7/12 20060101ALI20181008BHEP

GRAP Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOSNIGR1

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: GRANT OF PATENT IS INTENDED

INTG Intention to grant announced

Effective date: 20181127

GRAS Grant fee paid

Free format text: ORIGINAL CODE: EPIDOSNIGR3

GRAA (expected) grant

Free format text: ORIGINAL CODE: 0009210

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: THE PATENT HAS BEEN GRANTED

AK Designated contracting states

Kind code of ref document: B1

Designated state(s): AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR

REG Reference to a national code

Ref country code: GB

Ref legal event code: FG4D

REG Reference to a national code

Ref country code: CH

Ref legal event code: EP

Ref country code: AT

Ref legal event code: REF

Ref document number: 1130297

Country of ref document: AT

Kind code of ref document: T

Effective date: 20190515

REG Reference to a national code

Ref country code: DE

Ref legal event code: R096

Ref document number: 602011058883

Country of ref document: DE

REG Reference to a national code

Ref country code: IE

Ref legal event code: FG4D

REG Reference to a national code

Ref country code: PT

Ref legal event code: SC4A

Ref document number: 2655731

Country of ref document: PT

Date of ref document: 20190626

Kind code of ref document: T

Free format text: AVAILABILITY OF NATIONAL TRANSLATION

Effective date: 20190617

REG Reference to a national code

Ref country code: SE

Ref legal event code: TRGR

REG Reference to a national code

Ref country code: NL

Ref legal event code: MP

Effective date: 20190508

REG Reference to a national code

Ref country code: LT

Ref legal event code: MG4D

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

Ref country code: NL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

Ref country code: AL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

Ref country code: NO

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190808

Ref country code: HR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

REG Reference to a national code

Ref country code: ES

Ref legal event code: FG2A

Ref document number: 2730759

Country of ref document: ES

Kind code of ref document: T3

Effective date: 20191112

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: GR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190809

Ref country code: LV

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

Ref country code: BG

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190808

Ref country code: RS

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

Ref country code: EE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

Ref country code: RO

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

Ref country code: DK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

REG Reference to a national code

Ref country code: DE

Ref legal event code: R097

Ref document number: 602011058883

Country of ref document: DE

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SM

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

Ref country code: IT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

PLBE No opposition filed within time limit

Free format text: ORIGINAL CODE: 0009261

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: TR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

26N No opposition filed

Effective date: 20200211

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: PL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SI

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

REG Reference to a national code

Ref country code: CH

Ref legal event code: PL

REG Reference to a national code

Ref country code: BE

Ref legal event code: MM

Effective date: 20191231

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: MC

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

GBPC Gb: european patent ceased through non-payment of renewal fee

Effective date: 20191216

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LU

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20191216

Ref country code: FR

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20191231

Ref country code: IE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20191216

Ref country code: GB

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20191216

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: BE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20191231

Ref country code: LI

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20191231

Ref country code: CH

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20191231

REG Reference to a national code

Ref country code: AT

Ref legal event code: UEP

Ref document number: 1130297

Country of ref document: AT

Kind code of ref document: T

Effective date: 20190508

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: CY

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IS

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190908

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: HU

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT; INVALID AB INITIO

Effective date: 20111216

Ref country code: MT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: MK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20190508

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: PT

Payment date: 20251121

Year of fee payment: 15

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: DE

Payment date: 20251126

Year of fee payment: 15

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: AT

Payment date: 20251121

Year of fee payment: 15

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: FI

Payment date: 20251119

Year of fee payment: 15

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: SE

Payment date: 20251119

Year of fee payment: 15

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: CZ

Payment date: 20251211

Year of fee payment: 15

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: ES

Payment date: 20260102

Year of fee payment: 15