CN103270214B - The method controlling pulping process with feed-forward mode - Google Patents

The method controlling pulping process with feed-forward mode Download PDF

Info

Publication number
CN103270214B
CN103270214B CN201180061867.2A CN201180061867A CN103270214B CN 103270214 B CN103270214 B CN 103270214B CN 201180061867 A CN201180061867 A CN 201180061867A CN 103270214 B CN103270214 B CN 103270214B
Authority
CN
China
Prior art keywords
wood flour
digester
wood
steeper
delivered
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201180061867.2A
Other languages
Chinese (zh)
Other versions
CN103270214A (en
Inventor
M.内史曼
M.哈里南
O.蒂莫南
K.劳霍尼米
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Stora Enso Oyj
Original Assignee
Stora Enso Oyj
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Stora Enso Oyj filed Critical Stora Enso Oyj
Publication of CN103270214A publication Critical patent/CN103270214A/en
Application granted granted Critical
Publication of CN103270214B publication Critical patent/CN103270214B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C1/00Pretreatment of the finely-divided materials before digesting
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00Pulping cellulose-containing materials
    • D21C3/22Other features of pulping processes
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00Pulping cellulose-containing materials
    • D21C3/22Other features of pulping processes
    • D21C3/228Automation of the pulping processes
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C7/00Digesters
    • D21C7/12Devices for regulating or controlling

Landscapes

  • Paper (AREA)

Abstract

The present invention discloses the method controlling pulping process, wherein wood flour is delivered to steeper and/or digester, process described wood flour herein with the serosity comprising chemicals.According to the inventive method, calculate the ratio between the actual mass flow being delivered to the measurement of moist wood flour of steeper or digester and the estimation mass flow of the dried wood chips that is delivered to steeper or digester.Described ratio is used for controlling pulping process.Described method allows to the supply with feed-forward mode On-line Control such as chemicals, serosity to wood ratio and slurrying temperature.

Description

The method controlling pulping process with feed-forward mode
Technical field
The method that the present invention relates to control pulping process, is wherein delivered to steeper or digestion by wood flour Pond (digester), processes described wood flour herein with the serosity comprising chemicals.
Background technology
In chemical pulping process, wood flour is used at chemicals with the pressure and temperature raised in digester Reason, lignin fiber being bonded together with dissolving.Current main pulping process is Kraft method, Wherein process wood flour with the mixture of the sodium hydroxide and sodium sulfide that are referred to as white liquor.
The consumption of the chemicals used in pulp quality and pulping process depends highly on raw material, i.e. wood Bits.The water capacity of wood flour and other character can due to such as seasonal variations, different wood flours stack arrange and Use seeds and change.The change of raw material makes it difficult to the accurate of the chemicals of setting digester Dosage.The commonly used chemicals exceeding needs, this is all harmful from the perspective of economy and environment.
Also disclose in CA919289 for controlling the system of continuous digester.
In conventional chemical pulping process, contain based on the however, residual base derived from pulp properties or cooking waste liquor The information of the measured value of amount controls described process, i.e. described process controls in feedback fashion.This way Footpath cannot be complied with the short-term of wood flour character or change suddenly.In the art, have can be used for measuring former The business of material character measures system.But, these art methods are usually directed to cost with high investment, Need long analysis time and/or be insufficient to accurately, and being therefore generally not used for controlling described method.
Therefore, it is still necessary to pulping process simple, the online feedforward.
Summary of the invention
It is an object of the invention to provide for controlling the simple at line method of pulping process.This and other Advantage the inventive method realizes.
The present invention discloses control pulping process method, wherein wood flour is delivered to steeper and/or Digester, processes described wood flour herein with the serosity comprising chemicals.The inventive method includes following step Rapid:
E. estimate to be delivered to the dry of steeper or digester required for realizing desired paper output The mass flow of dry wood flour,
F. the actual mass flow of the moist wood flour being delivered to steeper or digester is measured,
G. calculate in the actual mass flow of measurement of moist wood flour and the estimation mass flow of dried wood chips Between ratio,
H. rate control pulping process based on described calculating.
The inventive method allows to feed-forward mode On-line Control such as chemicals such as sodium hydroxide and sulfur Change sodium to steeper or to the supply of digester, serosity to wood ratio and/or slurrying temperature.? Verified, by controlling pulping process according to the present invention, improve technology stability and realize the Kappa of paper pulp The change of value (kappa number) and quality reduces.Described method is simple and need not big investment and becomes This.Additionally, the valuation during we are currently in use a) calculates predetermined process parameter.Then described ratio is used Fine setting technological parameter.Therefore, first you create set point, and it uses subsequently in the regulation of technique should Set point.
According to the second aspect of the invention, it is provided that the method comprised the following steps:
E. the dry density of pending wood flour is estimated,
F. the density of the moist wood flour being delivered to steeper or digester is measured,
G. calculate the dry density of estimation of described wood flour and the measurement of described moist wood flour density it Between ratio, and
H. rate control pulping process based on described calculating.
According to the third aspect of the invention we, it is provided that the method comprised the following steps:
E. the dry density of pending wood flour is estimated,
F. the density of the moist wood flour being delivered to steeper or digester is measured,
G. calculate the dry density of estimation of described wood flour and the measurement of described moist wood flour density it
Between ratio, its also include with measure dry content correction, and
H. rate control pulping process based on described calculating.
This can use when the change of density of wood prevails.Therefore, measure dry content to provide The approach that this change is modified.
Detailed description of the invention
The method that the present invention relates to control pulping process, wherein in steeper and/or in digester Use chemical treatments wood flour.Term used in this application " steeper " can be to be suitable to process any of wood flour The container of kind, pipeline etc..Pulping process can be such as kraft pulping process, sulphite slurrying Journey or chemi-thermal mechanical pulping process.Described pulping process can be in batches or continuous slurrying process. Described method can be such as continuously Kraft pulping process, wherein with the temperature and pressure hydroxide improved The mixture of sodium and sodium sulfide processes wood flour.
According to the inventive method, calculate at the fresh moist wood flour being delivered to steeper or digester Actual mass flow and required for realizing desired default paper output be delivered to steeper or Ratio between the estimation mass flow of the dried wood chips of person's digester.Described ratio, hereinafter referred to as timber Wood property index (Wood Material Indicator, WMI), can such as be used for controlling supplying to steeper or The chemicals of person's digester such as sodium hydroxide and the amount of sodium sulfide and/or control the serosity in digester to wood Material ratio and/or control slurrying temperature.WMI can calculate according to equation 1.
Selectively, WMI can calculate by the following method: removes by the estimation mass flow of dried wood chips Actual mass flow with moist wood flour.
The estimation mass flow of dried wood chips can calculate by the following method: according to equation 2, with desired Paper output is divided by steaming and decocting yield.
Paper output is the preset value as target.Paper output in equation above is with dry weight [kg/s], i.e. 100% weight being dried paper pulp represents.Steaming and decocting yield is by the steaming and decocting of the seeds of slurrying The estimated value of yield.Such as, the steaming and decocting yield of the estimation of the kraft slurrying of cork is 46%.
Such as, the mass flow of the moist wood flour being delivered to steeper or digester can be broken by using Bits belt scale (conveyor scale) (preferably), mass flow scanning device (by use X-ray) or Radiation wood flow flowmeter measurement.The mass flow of the measurement of live wood depend on raw-material water capacity and Raw-material other character such as density and change.
According to the second aspect of the invention, described pulping process is by using the density at moist fresh wood flour Actual measured value and dried wood chips density estimated value between ratio control.Dried wood chips close The estimated value of degree depends on the seeds used.The density of moist fresh wood flour can be surveyed by the following method Fixed: to measure the weight of wood flour in wood flour feed bin and with described measured value divided by the body of the wood flour in feed bin Long-pending.If described method is pulping process in batches, then the density of moist fresh wood flour can be by following Method measures: measure the weight of wood flour in digester in batches and with described measured value divided by digester in batches In the volume of wood flour.
Wood quality index (WMI) continuous control pulping process can be used.Such as, this can be by with lower section Method realizes: regulate the chemicals inventory to steeper or digester and/or serosity to wood ratio And/or slurrying temperature.Steaming and decocting alkaline agent amount can continuously adjust based on WMI value.Serosity can base to wood ratio Regulate by the following method in WMI: the cooking waste liquor in regulation digester or the interior circulation of cleaning mixture.
When the change of raw material density is higher, can be by wood quality index and the wood flour being delivered to digester The frequent analysis of dry content be applied in combination, as a third aspect of the present invention reflects.
In this way, by separated from one another for the possible change of humidity and raw material density, and if quality The change of flow is arranged by the change of raw material density, then this will improve the accurate of technology controlling and process further Degree.This is based on the condition in producing and the raw material concrete decision of use.
The dry mass flow estimated is calculated by equation 2.Yield in continuous digester system is usual By cubing such as chip feed worm (chip feeding screw) or wood flour gauge (chip Meter) control.Based on known each rotary feeding volume, compactedness and the wood flour density of estimation, broken Bits apparatus for feeding will rotate, at some speed to maintain target output (the dry mass flow of estimation).Pass through Utilize the wet wood flour flow of the measurement being delivered to digester system measured on wood flour conveyer belt, and combine The wood flour dry content analyzed and the known volume feeding the wood flour to digester system (are measured by wood flour The rotary speed of equipment is given), can the wet wood flour density of computation and measurement:
Wet wood flour density=WCF/ (V x FD x rpm)
Wherein, WCF=wet wood flour mass flow (kg/min)
Feed volume (the m that V=rotates every time3)
FD=compactedness
The rotary speed (rpm) of rpm=wood flour measuring equipment
Then from the dry density of following formula computation and measurement:
Dry density=wet wood flour density × the dry content measured.
In this case, WMI is defined as
The dry density of dry density/estimation that WMI=measures
Then the WMI described by ratio above can be used in technology controlling and process.That estimates is dry close Degree depends on using which kind of raw material.
Additionally, the inventive method uses in feed-forward loop (mode), this feed-forward loop (mode) considers will What feeds (change of dry matter and moisture being combined to system;In wood flour bulk density Change in low-down Northern Europe condition (Nordic condition), this method operational excellence).For The response of change is the most faster.
Hereinafter, by embodiment and referring to the drawings, the present invention be will be described in further detail.
Accompanying drawing explanation
Fig. 1 illustrates that wood raw material flows to the schematic diagram of steeper or digester from wood flour heap.Total matter Amount flow is preferably by using chip belt scale to measure.By defeated at wood flour for the raw material of fresh moist wood flour Send and on band (1), be delivered to wood flour hopper (2).By using chip feed worm (3), described material is entered one Step is delivered to steeper or digester from wood flour hopper (2).The screw rod of chip feed worm (3) rotates Dry mass flow based on the estimation calculated controls, i.e. it depends on the setting value of paper output. According to an example of the present invention, it is arranged on wood flour conveyer belt (1) chip belt scale (4) below and surveys continuously Measure the actual flow of fresh moist wood flour.Owing to the wood flour quality in hopper is held essentially constant, survey Amount flow on wood flour conveyer belt provides the fresh moist wood being delivered to steeper or digester The exact value of the actual flow of bits.The fresh flow value measured is sent to the control unit of control system (5) control unit (5), is schematically shown in figure 3.Also the desiccated wood flow input estimated is controlled In unit (5).In the controls, by the ratio calculation (WMI) between described flow, and it is used for regulating Such as it is delivered to alkali inventory and the liquid setting value to wood ratio of steeper or digester.Excellent Selection of land, Theoretical Calculation flow based on the wood flour being delivered to steeper or digester, i.e. according to control The traditional method of pulping process processed controls described process further.Therefore, except the tradition control of described process System, WMI is preferred for regulating certain percent.Therefore, also by the setting value (set point) of Theoretical Calculation Input in described system.
Fig. 2 illustrates how to determine the example of the WMI being set forth above.
Fig. 3 illustrates the control system of the present invention.Described control system can comprise one or several sub-control System, for long-term (such as, 24 hours) and/or short-term (such as, 2 hours) change for WMI Regulate alkali inventory, boiling temperature and/or serosity to wood ratio.The control system that figure 3 illustrates In system (5), regulation is divided into two loops;One loop is returned for the secular change of WMI and one Road is for the short term variations of WMI.System (5) can comprise other control unit (6,7), wherein can input Other variable (v1, v2 ... Vn) or preset value be used for controlling described process, such as alkali inventory is upper Limit and lower limit, serosity currency, boiling temperature (the H-factor) and alkali inventory etc. to wood ratio.
How Fig. 4 more schematically shows the WMI of the present invention for controlling alkali inventory, and it is only The example of the controllable parameter of WMI of the application of the invention.
Fig. 5 illustrates that operating WMI controls (seeing the following examples).
Embodiment
Trial run is carried out in Oulu maker (Oulu mill) is during 4 days, wherein shows, WMI controls to reduce kappa value change.
WMI as soft sensor (soft number) seems available and enough accurate to reduce raw material The impact of change.It is given in Table 1 below result.
The result that table 1. is tested from 4 days Oulu.Each situation is 4 day run.Raw material is next From the cork (t/d=metric ton/day) of Scandinavia (Scandinavian).Figure referring also to reflection embodiment 5.Referring also to Fig. 2.
It is given in Table 2 below benefit.
Use the benefit that wood quality index (WMI) controls
The benefit that table 2. is tested from 4 days Oulu
It is described above the multiple embodiments of the present invention, but skilled in the art realises that other Minor alteration, it will be within the scope of the present invention.The width of the present invention and scope should not shown by any of above Example embodiment limits, but should limit according only to claims and their equivalent.For For those skilled in the art of the invention, other side, advantage and modification within the scope of the present invention will For obviously.Therefore, the invention is intended to contain and be included in claims spirit and scope Various amendments and equivalent processes.
Any diagram in the accompanying drawings and in description above and description should be considered as exemplary and non- Restrictive.
The use that word " comprises " in the claims is not excluded for other element or step, and article " The use of one " or " one " is not excluded for plural number.In different dependent claims, the appearance of feature is originally Body is not excluded for the combination of these features.Any reference marks in the claims is to be appreciated that for raising Property, and be not construed as limiting the scope of the invention.

Claims (3)

1. the method controlling pulping process, is wherein delivered to steeper or digester, herein by wood flour Process described wood flour with the serosity comprising chemicals, said method comprising the steps of:
A. estimate realize desired paper output required for be delivered to described steeper or described in disappear Change the mass flow of the dried wood chips in pond,
B. the actual mass stream of the moist wood flour being delivered to described steeper or described digester is measured Amount,
C. calculate at the actual mass flow of described moist wood flour and the estimation quality stream of described dried wood chips Ratio between amount,
D. rate control pulping process based on described calculating, it includes rate control based on described calculating Supply is to described steeper or the chemicals of described digester or includes based on described calculating Serosity in rate control digester is to wood ratio or includes ratio control based on described calculating Slurrying temperature.
2. the process of claim 1 wherein that the estimated value of described dried wood chips is by with described desired paper Slurry yield obtains divided by the steaming and decocting yield estimated.
3. the method for any one in claim 12, the mass flow of wherein said moist wood flour is led to Cross use chip belt scale to measure.
CN201180061867.2A 2010-12-22 2011-12-16 The method controlling pulping process with feed-forward mode Active CN103270214B (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
SE1051361-2 2010-12-22
SE1051361 2010-12-22
PCT/SE2011/051534 WO2012087228A1 (en) 2010-12-22 2011-12-16 A method of controlling a pulping process in a feed-forward manner

Publications (2)

Publication Number Publication Date
CN103270214A CN103270214A (en) 2013-08-28
CN103270214B true CN103270214B (en) 2016-11-16

Family

ID=46314243

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201180061867.2A Active CN103270214B (en) 2010-12-22 2011-12-16 The method controlling pulping process with feed-forward mode

Country Status (7)

Country Link
EP (1) EP2655731B1 (en)
CN (1) CN103270214B (en)
BR (1) BR112013015837A2 (en)
ES (1) ES2730759T3 (en)
PT (1) PT2655731T (en)
UY (1) UY33828A (en)
WO (1) WO2012087228A1 (en)

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA919289A (en) * 1970-06-30 1973-01-16 Westinghouse Electric Corporation System for controlling the feed end of a continuous papermaking digester
WO1994020671A1 (en) * 1993-03-02 1994-09-15 Iggesund Tools Ab Method for controlling a process by measurement of wood chips
CN1179188A (en) * 1995-03-23 1998-04-15 西门子公司 Method and device for process control in cellulose and/or paper manufacture
CN1372611A (en) * 1999-09-10 2002-10-02 斯托拉·科帕伯格斯·伯格斯拉格斯公司 Method for production of mechanical pulp
CA2495713A1 (en) * 2002-08-16 2004-02-26 Amec E & C Services Limited On-line pulp digester control system
CN1681992A (en) * 2002-09-06 2005-10-12 斯托拉恩索公司 Method of producing mechanical pulp and the mechanical pulp thus produced
EP1846614A1 (en) * 2005-01-05 2007-10-24 Metso Paper, Inc. Method for controlling a pulping process

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4239590A (en) * 1979-01-11 1980-12-16 Kamyr, Inc. Method of maintaining uniformity of fibrous material fed to a continuous digester
US5266159A (en) * 1991-10-25 1993-11-30 Kamyr, Inc. Mass flow measurement, preferably for controlling chip feed to a digester
US6447639B1 (en) * 2001-03-05 2002-09-10 Sita Ruby Warren Process for controlling a digester using real time measurement of moisture content and species of wood
US20060278353A1 (en) * 2005-06-03 2006-12-14 Centre De Recherche Industrielle Du Quebec Method and apparatus for estimating relative proportion of wood chips species to be fed to a process for producing pulp

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA919289A (en) * 1970-06-30 1973-01-16 Westinghouse Electric Corporation System for controlling the feed end of a continuous papermaking digester
WO1994020671A1 (en) * 1993-03-02 1994-09-15 Iggesund Tools Ab Method for controlling a process by measurement of wood chips
CN1179188A (en) * 1995-03-23 1998-04-15 西门子公司 Method and device for process control in cellulose and/or paper manufacture
CN1372611A (en) * 1999-09-10 2002-10-02 斯托拉·科帕伯格斯·伯格斯拉格斯公司 Method for production of mechanical pulp
CA2495713A1 (en) * 2002-08-16 2004-02-26 Amec E & C Services Limited On-line pulp digester control system
CN1681992A (en) * 2002-09-06 2005-10-12 斯托拉恩索公司 Method of producing mechanical pulp and the mechanical pulp thus produced
EP1846614A1 (en) * 2005-01-05 2007-10-24 Metso Paper, Inc. Method for controlling a pulping process

Also Published As

Publication number Publication date
UY33828A (en) 2012-06-29
CN103270214A (en) 2013-08-28
EP2655731A4 (en) 2017-05-17
WO2012087228A1 (en) 2012-06-28
PT2655731T (en) 2019-06-26
EP2655731B1 (en) 2019-05-08
BR112013015837A2 (en) 2018-05-15
ES2730759T3 (en) 2019-11-12
EP2655731A1 (en) 2013-10-30

Similar Documents

Publication Publication Date Title
US6319362B1 (en) Method and equipment for controlling properties of paper
NO974358L (en) Process and apparatus for process control in cellulose and paper making
CA2757940C (en) Modelling of a property of paper, paperboard or board
US4419184A (en) Method for control of chemicals during gas treatment of suspensions
CN101163836A (en) System and method to control press section dewatering on paper and pulp drying machines using chemical dewatering agents
US6328851B1 (en) Method and equipment for controlling properties of paper
US20060278353A1 (en) Method and apparatus for estimating relative proportion of wood chips species to be fed to a process for producing pulp
US8540845B2 (en) Method and system for stabilizing dry-based density of wood chips to be fed to a chip refining process
CN103270214B (en) The method controlling pulping process with feed-forward mode
US4692210A (en) Method and apparatus for measuring the distribution of fiber widths and adjusting the refining of fibrous stock
US5266159A (en) Mass flow measurement, preferably for controlling chip feed to a digester
CN101611922B (en) Method for improving material water ratio uniformity after charging
EP3036370B1 (en) A method and a system for controlling a refiner for refining a product containing cellulose and readable information about a quality index of the product
CN103169147A (en) Papermaking tobacco sheet pulp grinding process
CA2592887C (en) Method for controlling a pulping process
CN201774947U (en) On-line detection control device for net part single-pass retention of papermaking method tobacco sheets
US7077930B2 (en) Method for controlling screening by measuring flow amount consistency of the pulp
EP2740839A1 (en) Method and system for manufacturing mechanical pulp and mechanical pulp obtainable by the method
Tessier et al. Motor load and freeness control of CMP pulp refining
FI58028C (en) REGLERINGSPROCESS OCH -ANORDNING FOER KOKARE
CN110302714A (en) A kind of system and equipment of automatic classification allotment albumen powder protein content
ES2359163T3 (en) METHOD FOR CONTROLLING A PROCEDURE FOR THE PRODUCTION OF SHORT FIBER CELLULOSE PASTE.
CN220619600U (en) High-strength corrugated paper production system
FI115976B (en) Method for quality sorting of pulpwood
WO1998030751A1 (en) Method for controlling consistency of papermaking pulp

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant