EP2599540A1 - Élément de mélange pour un mélangeur statique - Google Patents
Élément de mélange pour un mélangeur statique Download PDFInfo
- Publication number
- EP2599540A1 EP2599540A1 EP12186959.8A EP12186959A EP2599540A1 EP 2599540 A1 EP2599540 A1 EP 2599540A1 EP 12186959 A EP12186959 A EP 12186959A EP 2599540 A1 EP2599540 A1 EP 2599540A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- wall
- inlet
- opening
- mixing
- mounting body
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
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- 238000001746 injection moulding Methods 0.000 description 11
- ORQBXQOJMQIAOY-UHFFFAOYSA-N nobelium Chemical compound [No] ORQBXQOJMQIAOY-UHFFFAOYSA-N 0.000 description 11
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Images
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
- B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
- B01F25/43—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
- B01F25/431—Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor
- B01F25/4317—Profiled elements, e.g. profiled blades, bars, pillars, columns or chevrons
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
- B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
- B01F25/421—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions by moving the components in a convoluted or labyrinthine path
- B01F25/423—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions by moving the components in a convoluted or labyrinthine path by means of elements placed in the receptacle for moving or guiding the components
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
- B01F23/47—Mixing liquids with liquids; Emulsifying involving high-viscosity liquids, e.g. asphalt
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
- B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
- B01F25/421—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions by moving the components in a convoluted or labyrinthine path
- B01F25/422—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions by moving the components in a convoluted or labyrinthine path between stacked plates, e.g. grooved or perforated plates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
- B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
- B01F25/43—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
- B01F25/431—Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor
- B01F25/4316—Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor the baffles being flat pieces of material, e.g. intermeshing, fixed to the wall or fixed on a central rod
- B01F25/43161—Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor the baffles being flat pieces of material, e.g. intermeshing, fixed to the wall or fixed on a central rod composed of consecutive sections of flat pieces of material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
- B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
- B01F25/43—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
- B01F25/432—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction with means for dividing the material flow into separate sub-flows and for repositioning and recombining these sub-flows; Cross-mixing, e.g. conducting the outer layer of the material nearer to the axis of the tube or vice-versa
- B01F25/4321—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction with means for dividing the material flow into separate sub-flows and for repositioning and recombining these sub-flows; Cross-mixing, e.g. conducting the outer layer of the material nearer to the axis of the tube or vice-versa the subflows consisting of at least two flat layers which are recombined, e.g. using means having restriction or expansion zones
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/50—Movable or transportable mixing devices or plants
- B01F33/501—Movable mixing devices, i.e. readily shifted or displaced from one place to another, e.g. portable during use
- B01F33/5011—Movable mixing devices, i.e. readily shifted or displaced from one place to another, e.g. portable during use portable during use, e.g. hand-held
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
- B01F2101/19—Mixing dentistry compositions
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
- B01F2101/20—Mixing of ingredients for bone cement
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05C—APPARATUS FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05C17/00—Hand tools or apparatus using hand held tools, for applying liquids or other fluent materials to, for spreading applied liquids or other fluent materials on, or for partially removing applied liquids or other fluent materials from, surfaces
- B05C17/005—Hand tools or apparatus using hand held tools, for applying liquids or other fluent materials to, for spreading applied liquids or other fluent materials on, or for partially removing applied liquids or other fluent materials from, surfaces for discharging material from a reservoir or container located in or on the hand tool through an outlet orifice by pressure without using surface contacting members like pads or brushes
- B05C17/00553—Hand tools or apparatus using hand held tools, for applying liquids or other fluent materials to, for spreading applied liquids or other fluent materials on, or for partially removing applied liquids or other fluent materials from, surfaces for discharging material from a reservoir or container located in or on the hand tool through an outlet orifice by pressure without using surface contacting members like pads or brushes with means allowing the stock of material to consist of at least two different components
Definitions
- the invention relates to a mixing element for a static mixer made of plastic comprising a mounting body for installation in a tubular mixer housing.
- a mixer and the associated mixer housing can, as in the W02008113196 A1 be connected to the outlets of a multi-component cartridge and in their entirety constitute a cartridge arrangement, which in Fig. 2 of the WO2008113196 A1 is shown.
- Such a static mixer is for example from the EP1426099 B1 known.
- this static mixer two components are mixed together in a three-part mixing process in which the mass is first divided, then expanded and displaced by means of a plurality of similar mixing elements. Depending on the physical properties of the components, this mixing process must be done several times. For this reason, the static mixer includes a plurality of structural bodies of the same type, which are arranged one behind the other. These mixers are used in particular for mixing small amounts of the components, that is, a few milliliters to about 1000 milliliters. As a result, these mixers have a mixing space with a diameter of less than 16 mm and a length of over 50 mm. As a consequence, that the wall thicknesses of the wall elements of this mixer can be less than 1 mm, often even less than 0.5 mm.
- Such a static mixer according to EP1426099 B1 made of plastic is preferably produced by injection molding.
- the production of a mixer of 30 mm length with a wall thickness of less than 3 mm by means of the injection molding process as in Fig. 1 This patent has not yet been possible because the flow path from the injection point of the injection molding tool to the opposite end of the mixer would require too high internal cavity pressures.
- each mounting body is connected to the adjacent mounting body via web elements. These web elements make it possible for the polymer melt in the injection molding tool to pass from an installation body to an adjacent installation body and to keep the tool internal pressures below 1000 bar, so that failure of the injection molding tool can be prevented.
- the installation bodies are preceded by an inlet element.
- the inlet member includes the two inlet channels which introduce the components from the cartridge outlets into the mixer housing.
- the mixing element contains mounting body. The components are deflected by the installation body, split and rejoined, resulting in a mixing of the components. At the outlet end of the mixer housing, the components are thus present as a uniformly mixed filling material.
- the mixer of WO2008113196 A1 has a configuration, according to which a flow of a component is prevented by providing a constriction in the flow channel, so deliberately incorporates a throttle effect.
- Fig. 13 of WO2008113196 A1 shows that, for this purpose, a web element is provided in the inlet region of the mixer adjacent to its inlet channel, which forms a flow obstacle and ensures the deflection of the flow around this web element. The left side flowing component is thus imposed a longer flow path than the right side flowing component.
- a divider is provided above each of the two inlet openings. This Divider is flowed around by the flowing through the respective inlet port component.
- the volume flows of the two components are different.
- the first component with the larger volume flow is led to the separating web by web elements parallel to the outer surface of the adapter element in the direction of the inlet opening of the second component.
- the second component which has a smaller volume flow, is detected by the first component and brought into contact before it enters the mixing element. This means that the first component with the larger volume flow reaches the mixer late in relation to the second component, ie its flow is delayed by additional path length.
- EP 0723 807 A2 shows a variant according to which the inlet chambers have different volumes when the components are present in a mixing ratio which is not equal to 1: 1.
- These inlet chambers receive the components conveyed from the cartridge before they enter the mixing element.
- the inlet chamber of the first component which forms the larger volume flow, has a larger volume than the inlet chamber of the second component, which forms the smaller volume flow.
- the second component simultaneously flows through the second inlet chamber, which has a much smaller volume.
- the volume ratio can be adjusted so that the first component and the second component reach the first mixing element simultaneously.
- the component which has a higher volume fraction is jammed.
- the flow path at the entrance of the static mixer is interrupted by a plate.
- a slot-shaped opening is provided, through which the components which have filled the storage space in front, get into the static mixer. As a result, a flow of the component is prevented with the larger volume flow.
- the volumes that are between the cartridge and mixer should be adapted to the appropriate mixing ratios in order to obtain as little flow as possible in order to avoid that unusually mixed material is obtained. Therefore, the first approach is to adjust the cross-sectional areas of the leads according to the desired mixing ratio. However, if very different mixing ratios are present, the cross-sectional area for the component with the smaller volume flow is no longer producible. Therefore, an additional volume is made available to the component with the larger volume flow, for example, an inlet chamber as in the EP 0 723 807 A2 or a chamber at the inlet end of the mixing element, as in EP 0 584 428 A1 described.
- the object of the invention is to provide a mixing element in which each of the two components reaches the first mounting body of the mixing element in the desired mixing ratio.
- the leading component reaches the mixing element in front of the other component.
- Another object of the invention is to reduce the pressure loss in comparison to previously known solutions, which also have the problem of a flow.
- a mixing element which contains at least one installation body and an inlet element, which has a body with a first and a second inlet channel. Through the inlet channels, the corresponding components are guided separately to each other to the mounting body.
- a first and a second mounting body can be arranged behind one another along the longitudinal axis of the mixing element.
- the inlet element is arranged upstream of the first installation body, wherein the inlet element and the installation body are connected to one another via a connecting element.
- the connecting element may be a helical element of a spiral mixer, which is at the same time its installation body or a web element which is part of the first installation body.
- the body of the inlet element is circumferentially in the mixer housing sealingly receivable.
- Each of the first inlet channels and the second inlet channels has an inlet opening and an outlet opening, so that the corresponding component can be guided through the corresponding inlet channel from the inlet opening to the outlet opening.
- the first inlet channel is spatially separated from the second inlet channel.
- the first inlet channel opens into an antechamber, wherein the antechamber is delimited by the outlet side of the body, the connecting element, the inner wall of the mixer housing and the first mounting body, wherein the second channel extends within the interior of the connecting element and opens from the connecting element into the first mounting body ,
- the ratio of the remaining free cross-sectional area to the cross-sectional area of the continuation channel in a sectional plane that is normal to the longitudinal axis and located at the mixer inlet is at least 4: 1.
- the mixing ratio of the components can be 4: 1, but also according to an alternative embodiment, at least 5: 1, it can also be at least 10: 1, or even more.
- a mixing element with the same dimensions is preferably used.
- the following additional geometric conditions thus apply analogously for cross-sectional ratios of 5: 1 to 10: 1 or more.
- at least 4: 1 is intended to mean ratios of 4: 1, 5: 1, 6: 1, 10: 1, 20: 1 as well as intervening ratios or ratios which are above it.
- the mixer housing according to an embodiment has a shoulder on which the outlet side of the body rests. In particular, the cutting plane can be arranged between this shoulder and the first mounting body.
- the cross-sectional area ratio of the cross-sectional areas available for the components at this point may be at least 5: 1.
- the ratio of the cross-sectional areas of the inlet openings is at least 5: 1.
- the cross-sectional area of the inlet opening to the cross-sectional area adjacent to the outlet opening increases by at least twice for at least one of the components.
- the cross-sectional area from the inlet opening to the cross-sectional area following the outlet opening for each of the components at least doubles.
- the second inlet channel narrows in the interior of the connecting element.
- the flow velocity of the second component which flows through this second inlet channel in the operating state, can be increased.
- the second component may be admixed in a smaller amount than the first component flowing through the first inlet channel. The constriction ensures that the second component already enters the static mixer with the first component in the correct mixing ratio at the beginning of the discharge process.
- the second inlet channel has in the interior of the connecting element on a clear diameter, which decreases continuously from the inlet side to the outlet side.
- the clear diameter decreases continuously, For example, the flow rate may increase with minimal losses, that is, maximum increase in flow rate can be achieved.
- the mixing element is provided for a static mixer for installation in a tubular mixer housing.
- the mixing element has a longitudinal axis, along which a plurality of mounting bodies are arranged one behind the other, wherein a first mounting body has a first wall element, which extends in the direction of the longitudinal axis.
- the wall member has a first sidewall and a second sidewall disposed opposite the first sidewall.
- the first wall element in particular forms the connecting element.
- a guide element may be arranged adjacent to the first wall element.
- the guide element can serve to extend the flow path of the first component, or to delay the inflow of the first component into the mixing element.
- the guide element may be formed as a deflecting element or formed as part of this deflecting element.
- the deflecting element has a deflecting surface extending transversely to the wall element on both sides of the wall element, a first opening being provided in the deflecting surface on the side facing the first side wall of the wall element.
- the deflecting element can at least partially cover the first outlet opening.
- the first inlet channel at the respective outlet opening may have a cross-sectional area which differs from the cross-sectional area of the corresponding outlet opening of the second inlet channel.
- the cross-sectional area of the first inlet channel at the first outlet opening is greater than the cross-sectional area of the second outlet opening of the second inlet channel.
- a second and a third wall element Adjacent to the first opening, a second and a third wall element are thus arranged in the direction of the longitudinal axis opposite to the first wall element, the second and third wall element delimiting a channel extending from the first opening and extending in the direction of the longitudinal axis.
- a second opening is provided in the deflection surface on the side facing the second side wall of the wall element, the second or third wall element being connected to the second opening.
- the first wall element of the second installation body adjoins the second and third wall elements. It has proven particularly advantageous if more than five mounting bodies are connected to one another via a common web element, because the pressure loss is surprisingly lower than without common web elements.
- a second and a third wall element Adjacent to the first opening, in turn, a second and a third wall element may be arranged, wherein the second and third wall elements extend in the direction of the longitudinal axis and each have an inner wall and an outer wall, which extend substantially in the direction of the longitudinal axis.
- Each of the inner walls and outer walls may enclose an angle between 20 ° and 160 ° to the first or second side wall of the first wall element.
- the first opening may be disposed between the inner walls of the second and third wall elements and a second opening may be located outside one of the outer walls of the second or third wall element, the second opening in the deflection surface on the side facing the second side wall of the first wall element is, can be provided.
- a second and a third wall element can be arranged in the direction of the longitudinal axis opposite to the first wall element, wherein the second and third wall element can define a channel extending from the first opening and extending in the direction of the longitudinal axis.
- a second opening can be provided in the deflection surface on the side facing the second side wall of the wall element, wherein the second or the third wall element can connect to the second opening, wherein the first wall element, the deflection element and the second and third wall element existing second mounting body can be arranged rotated about the longitudinal axis by an angle of 10 ° up to and including 180 ° with respect to the first mounting body.
- the second mounting body may have the same structure as the first mounting body.
- the first mounting body may be arranged rotated about the longitudinal axis by an angle of 180 ° with respect to the second mounting body.
- the wall element can enclose an angle of 90 to 130 ° with the deflection surface.
- the deflection surface may have a curved at least partially in the direction of the flowing fluid surface for deflecting the fluid flow in a deviating from the longitudinal axis direction, in particular, a progressive curvature in the flow direction and in the direction of the mixer housing may be provided.
- the deflection surface may be substantially planar.
- the deflection surface may extend substantially at an angle of 90 ° to the wall element.
- the surface of the deflecting element on the side facing the first side wall of the wall element at least partially lie in a transverse plane, which is aligned at an angle of 60 ° to 90 ° to the longitudinal axis.
- the surface of the deflecting element on the side facing the second side wall of the wall element may lie in a transverse plane which is oriented at an angle of 60 ° to 90 ° to the longitudinal axis.
- a reinforcing element may be provided at its connection point.
- the reinforcing element may be formed, for example, as a thickening or a rib.
- the static mixing element may in particular contain a foamed polymer.
- a propellant-containing polymer is used in this case for the production of the static mixer, which foams during or immediately after the injection.
- the injection molding process comprises the step of injecting a blowing agent-containing polymer into an injection mold at a cavity pressure of less than 600 bar, more preferably less than 500 bar.
- the mounting body has a length dimension and a diameter.
- the diameter corresponds to the edge length when the cross-sectional area of the tubular mixer housing is square.
- D a then stands for the equivalent diameter, A for the actual cross-sectional area.
- the ratio of length dimension to diameter is at least 1, using as diameter either the diameter of the circular cross section or the equivalent diameter for non-circular cross sections.
- the installation body or the entirety of the installation body may have a length dimension between 5 and 500 mm, preferably between 5 and 300 mm, preferably between 50 and 100 mm.
- the fluid to be mixed usually comprises two different components.
- the components are in the liquid state or as viscous masses.
- these include, for example, pastes, adhesives, but also fluids which find use in the medical field, which contain active pharmaceutical ingredients, or fluids for cosmetic applications, as well as foods.
- static mixers also find use as disposable mixers Mixture of a hardening mix of flowable components, such as the mixture of multi-component adhesives or sealants. Another preferred use is in the mixture of impression compounds in the dental field.
- a mixing element 100 for a static mixer according to a first embodiment of the invention is shown.
- the mixing element comprises an installation body 1, which is installed in a tubular housing, which is not shown.
- the tubular housing serves as a boundary of a mixing chamber 20, which is located in the interior of the tubular housing.
- a fluid to be mixed flows, which usually consists of at least two different components.
- the components are in a liquid state or as flowable, in particular viscous masses.
- These include, for example pastes, adhesives, but also fluids, which find use in the medical field, which contain active pharmaceutical ingredients, or fluids for cosmetic Applications, as well as food.
- static mixers also find use as disposable mixers for mixing a thermosetting mix of flowable components, such as the mixture of multicomponent adhesives. Another preferred use is in the mixture of impression compounds in the dental field.
- the mounting body 1 and the mounting body 101 have the same structure, however, the mounting body 101 is rotated by 180 ° about the longitudinal axis 10.
- the mixing space 120 has a flow cross-sectional area 122 in a plane 121 arranged normal to the longitudinal axis 10, which essentially corresponds to the flow cross-sectional area of the tubular mixer housing surrounding the installation body 101.
- the longitudinal axis lies in this plane of symmetry.
- the mixing chamber is peripherally limited by the mixer housing, not shown.
- the mixing element is to be installed in a mixer housing with a rectangular or square cross-section.
- the internal dimension of the mixer housing used to determine the equivalent diameter is indicated at reference 36.
- the mounting body 1 contains at least a first wall element 2, which serves to divide the fluid flow in two substreams flowing essentially parallel to the longitudinal axis 10.
- the wall element 2 has a first side wall 3 and a second side wall 4.
- the section of the first wall element 2 with the plane 21 results in a cross-sectional area 23.
- This cross-sectional area 23 is at most 1/5, preferably at most 1/10, particularly preferably at most 1/20, of the flow cross-sectional area 22 of the mixing chamber 20 without installation body.
- the fluid thus flows on both sides of the side walls 3, 4 of the wall element 2.
- the flow direction of the fluid is indicated by an arrow.
- the wall element has a substantially rectangular cross-section.
- the first wall element 2 has a first broad side 5, a second broad side 6 and a first and a second longitudinal side 25, 35.
- the first broad side 5, the second broad side 6, the first longitudinal side 25 and the second longitudinal side 35 form the circumference of each of the side walls 3, 4.
- the longitudinal sides 25, 35 extend substantially in the direction of the longitudinal axis 10 and the first broad side 5 and second broad side 6 extend transversely to the direction of the longitudinal axis.
- the first wall element 2 divides the mixing space into two parts.
- the wall element 2 has the function of a rod element which divides the fluid flow into two parts, the deflection of which, with the exception of the deflection at the edges of the first broad side 5, being negligible.
- the wall thickness 7 of the wall element 2 is usually less than 1 mm for a mixing element with a total length of up to 100 mm.
- the first wall element 2 includes a deflecting element 11, which serves to deflect the partial flows in a direction deviating from the longitudinal axis.
- the deflecting element has a deflecting surface extending transversely to the wall element 2 on both sides of the wall element.
- a first opening 12 is provided in the deflection surface on the side facing the first side wall 3 of the wall element 2.
- the crossing angle between the first wall element 2 and the second or third wall element 8, 9 is in the embodiment according to Fig. 1 90 °.
- Fig. 1 is the first wall element 2 with the second wall element 8 and the third wall element 9 via the deflecting element 11 connected.
- the deflecting element 11 is preferably located in a plane which is aligned parallel to the plane 21 or is arranged with an inclination angle to the plane, wherein the inclination angle is not more than 60 °, preferably not more than 45 °, particularly preferably not more than 30 ° , The smaller the angle of inclination between the surface of the deflecting element 11 and the plane 21, the lower the required overall length.
- the surface of the deflecting element 11 lies substantially in a transverse plane, which is oriented at an angle of 45 ° to 90 °, preferably 60 ° to 90 °, more preferably 75 ° to 90 ° to the longitudinal axis 10 ,
- the wall elements 8, 9 adjoining the deflection element 11 delimit a channel extending from the first opening 12 and extending in the direction of the longitudinal axis 10.
- adjoining the deflecting element is meant that the second and the third wall element 8, 9 are arranged in the direction of the longitudinal axis opposite to the first wall element 2, that is arranged downstream of the first wall element 2 in the flow direction.
- a second opening is provided in the deflection surface on the side facing the second side wall 4 of the wall element 2, the second or the third wall element 8, 9 adjoining the second opening.
- the second and third wall element 8, 9 defines the same channel, which also starts from the first opening 12.
- a second and a third wall element 8, 9 Adjacent to the first opening 12 thus a second and a third wall element 8, 9 are arranged.
- the second and third wall elements 8, 9 extend in the direction of the longitudinal axis 10 and each have an inner wall 81, 91 and an outer wall 82, 92, which extend substantially in the direction of the longitudinal axis 10.
- the second wall element 9 has the inner wall 81 and the outer wall 82.
- the third wall element has the inner wall 91 and the outer wall 92.
- the inner walls 81, 91 and extend Outer walls 82, 92 in the direction of the longitudinal axis, ie in the drawing direction in the vertical direction.
- Each of the inner walls 81, 91 and outer walls 82, 92 may include an angle between 20 ° and 160 ° to the first or second side wall 3, 4 of the first wall element 2.
- the first opening 12 is arranged between the inner walls 81, 91 of the second and third wall elements 8, 9.
- a second opening 13 and an optional third opening 14 are arranged outside one of the outer walls 82, 92 of the second or third wall element 8, 9.
- the second opening 13 and the third opening 14 are provided in the deflection surface on the side facing the second side wall 4 of the first wall member 2.
- the inner wall of each wall element can be parallel to its outer wall.
- the second and third wall elements may each have mutually parallel inner walls 81, 91 and outer walls 82, 92.
- the first wall element 102 of the second mounting body 101 adjoins.
- the second mounting body 101 has a first wall element 102, which extends in the direction of the longitudinal axis 10 of the mixing element and has a first side wall 103 and a second side wall 104, which is arranged opposite the first side wall 103.
- the first side wall 103 and the second side wall 104 are arranged substantially parallel to the longitudinal axis 10.
- the first opening 112 is arranged between the inner walls 181, 191 of the second and third wall elements 108, 109, and at least one second opening 113, 114 is arranged outside one of the outer walls 182, 192 of the second or third wall element 108, 109.
- the second opening 113 and / or a third opening 114 are provided in the deflection surface on the side facing the second side wall 104 of the first wall element 102.
- the second mounting body 101 containing the first wall element 102, the deflecting element 111 and the second and third wall elements 108, 109 is at an angle of 10 ° up to and including 180, about 180 ° in the specific example of 180 °, with respect to the longitudinal axis 10 the first mounting body 1 is arranged rotated.
- the first mounting body 1 and the second mounting body 101 have the same structure, that is, they contain the same wall elements and the same deflecting elements, which are arranged in each case at equal angles and distances from each other.
- Fig. 2 shows an embodiment of a section of a mixing element according to a second embodiment of the invention.
- the structure of the mixing element does not differ significantly from the mixing element according to Fig. 1 Therefore, the same reference numerals are used for the same parts as in Fig. 1 , Below is also only on the differences from the embodiment according to Fig. 1 To be received.
- a first mounting body 1 and a second mounting body 101 are shown.
- the mounting bodies are intended for installation in a mixer housing with a circular or elliptical cross section.
- the cross-sectional profile of the inner wall of the mixer housing, not shown, is indicated by a dash-dotted line.
- the diameter of the mixer housing is shown with a reference line 36.
- Fig. 3a to Fig. 3d each show a view of a first embodiment of a mixing element according to the invention.
- the mixing element 100 includes mounting bodies, as in Fig. 2 shown. All mounting bodies are connected to each other by web elements 15, 16, 17, 18. Furthermore, the mixing element 100 includes an inlet member 50 containing the inlet channels 51, 52 for the components to be mixed.
- the mixing ratio of the two components can be equal to 1: 1, but also differ, that is not equal to 1: 1.
- the components may be miscible in a ratio of 2: 1 to and at 20: 1, in particular 4: 1 to and 10: 1.
- the inlet member 50 is disposed upstream of the first mounting body 1.
- the inlet element 50 and the mounting body 1 are connected to one another via a connecting element 60.
- the inlet element 50 has a body 57, which is sealingly receivable on the circumference in the mixer housing.
- the body 57 has a first inlet channel 51 and a second inlet channel 52.
- Each of the inlet channels 51, 52 has an inlet opening 53, 54 and an outlet opening 55, 56, so that the corresponding component can be guided through the corresponding inlet channel 51, 52 from the inlet opening 53, 54 to the outlet opening 55, 56.
- the first The first inlet channel 51 opens into an antechamber 58.
- Fig. 5 shows a section through the second and third wall elements 8, 9 of the mounting body 1.
- the viewing direction is in the flow direction, so that the first wall element 102 of the mounting body 101 is visible.
- the deflecting element 111 adjoins the first wall element 102 of the installation body 101.
- the deflecting element 111 includes a first opening 112, which is arranged on the side of the second side wall 104.
- a second opening 113 and a third opening 114 are arranged on the side of the first side wall 103.
- the second opening 113 and the third opening 114 are offset from the first opening 112.
- the first second and third openings 112, 113, 114 are arranged such that opposite to each of the Opening is arranged in each case a sub-element, that is opposite to the first opening 112, a first sub-element 126, opposite to the second opening 113, a second sub-element 127 and opposite to the third opening, a third sub-element 128th
- Fig. 6a and Fig. 6b show a section through an inlet member 50 of a static mixer and a mixing element 100 according to 3a to Fig. 3d .
- the static mixer includes a mixer housing 99 in which the mixing element 100 and the inlet member 50 are received.
- the mixer housing 99 is received in a holding element 98, which serves for connection to a cartridge, not shown here.
- Fig. 6a shows a longitudinal section through the static mixer, which is placed along the longitudinal axis 10. The cut is made such that the nozzle 63, which contains the inlet channel 51, is not visible, because this nozzle 63 comes to lie in front of the plane of the drawing.
- the nozzle 64 which contains the inlet channel 52, is visible.
- the cap member 66 which is part of the body 57 of the inlet member, is held in the mixer housing. Through the cap member 66 extend the inlet channels 51, 52, which in Fig. 6b is visible.
- the cap member 66 may include a circumferential projection 72 extending along the skirt 71 of the cap member 66. The projection 72 is received in a corresponding recess 97 of the mixer housing 99.
- the cap member 66 can be held captive in the mixer housing 99. However, rotation of the cap member 66 relative to the mixer housing 99 is possible to ensure that the mixing element 50 can be correctly placed on the outlets of the cartridge.
- the connecting pieces 63, 64 are placed on the corresponding outlets or inserted into the corresponding outlets, so that the connecting pieces 63, 64 enclose the outlets or the outlets enclose the connecting pieces 63, 64.
- a flange member 67 serves as a support for the mixer housing 99.
- the mixer housing 99 is constructed in two stages.
- the inlet part 96 of the mixer housing 99 has a larger inner diameter than the main part 95 of the mixer housing.
- the main part 95 of the mixer housing 99 the fitting body of the mixing element, the inlet part 96 includes the cap member 66 of the body 57 of the inlet member 50.
- the flange member is also received in a holding member 98.
- the flange member 67 also forms the support of the end of the inlet part 96 of the mixing element.
- the retaining member 98 serves to secure the static mixer to the cartridge.
- the holding element 98 is provided for this purpose with Bayonettbefest Trentsmitteln.
- the inlet channel 51 extends within the nozzle 63 and continues through the flange 67 into the cap member 66.
- the inlet channel 51 thus begins at the inlet opening 53 and ends at the outlet opening 55.
- the inlet channel 52 extends inside the nozzle 64 and continues through the flange element 67 into the cap element 66.
- the inlet channel 52 thus begins at the inlet opening 54 and ends at the outlet opening 56.
- a continuation channel 62 leads into the interior 61 of the connecting element 60.
- the connecting element 60 can be designed in particular as the first wall element of the first installation body 1.
- the second inlet channel 52 in the interior 61 of the connecting element 60 can narrow.
- the second inlet channel 52 extends in the interior 61 of the connecting element 60 from an inlet side 75 to an outlet side 76.
- the inlet channel 52 has a clear diameter, which decreases continuously from the inlet side 75 to the outlet side 76.
- the first inlet channel 51 of the inlet element 50 has at the outlet opening 55 a cross-sectional area which differs from the cross-sectional area of the second inlet channel 52 at the outlet opening 56.
- Such an inlet element 50 is used for components which are miscible in a ratio of 2: 1 to and at 20: 1, in particular 4: 1 to and 10: 1.
- Fig. 7a and Fig. 7b each show a section through a complete mixing element 100, which is received in the mixer housing 99.
- the mixer housing 99 is constructed of an inlet part 96 and a main part 95.
- the inlet part 96 contains the inlet member 50 of the mixing element 100.
- the main part 95 contains the mounting bodies 1, 101 of the mixing element 100.
- the mixer housing has an inlet end 94 and an outlet end 93.
- Two or more components enter the mixer housing via the inlet element separated from each other and are brought into contact with each other in the first installation body 1.
- the wall elements of the installation body serve for the division of the component flow and the deflection elements of the deflection of the component flow, that is, the bringing about of a local redeployment of the component flow. By continuing over the length of the mixing element division and deflection of the component flow, the components are mixed.
- At the outlet end 93 of the mixer housing 99 exits a homogeneous filler.
- the web elements 15, 16, 17, 18 hold all the mounting body of the mixing element 100 connected to each other.
- Each of the web elements increases the flexural rigidity of the static mixer. Furthermore, it can be prevented by the web elements that it comes in the operation of the mixer to break the mixing element, in particular when at least two mixing elements are arranged on opposite sides of the first wall elements. Furthermore, it is ensured during the production of the mounting body in the injection molding via the web element that the polymer melt from the first mounting body 1 to the first and all other downstream mounted bodies 101 can flow. Without the web elements, the transition from the wall element 8 or 9 to the downstream wall element 102 would be exclusive in the common cut surface and a possible reinforcement of the same.
- the cut surface in this case consists of two squares, which would have a side length corresponding to the wall thickness 7. All of the polymer melt for the downstream installation bodies would have to pass through these orifices, resulting in local pressure spikes in the tool.
- a long residence time of the polymer melt would result, which would lead to changes in the polymer melt and possibly to a deterioration of the physical properties and inhomogeneity, so that in State of the art only by the use of a blowing agent-containing melt to produce a foamed structure, such a mixing element can be produced.
- the web elements for forwarding the polymer melt in the production process are provided by an installation body to each of the adjacent installation bodies.
- the static mixer is usually made of plastic, by means of which even comparatively complicated geometries can be realized in the injection molding process.
- the entirety of the installation bodies 1, 101 has a length dimension 24 and each of the cross-sectional areas 23, 123 has a wall thickness 7.
- the ratio of length dimension 24 to wall thickness 7 is at least 40, preferably at least 50, particularly preferred at least 75.
- the wall thickness 7 is less than 3 mm, preferably less than 2 mm, more preferably less than 1.5 mm.
- the entirety of the mounting body 1,101 has a length dimension 24 between 5 and 500 mm, preferably between 5 and 300 mm, preferably between 50 and 100 mm.
- Fig. 8 shows a section through the mixing element at the level of the continuation channel.
- the cut contains the holding element 98 in a partially cut-away form with the coding elements and the parts of a bayonet closure, by means of which the holding element 98 can be connected to a multi-component cartridge.
- the cap member 66 is arranged, which is part of the mixer housing 99.
- the cap member 66 has a centrally located circular opening 70 in which the connecting element 60 is received.
- the connecting element 60 does not completely fill the opening, but has two recesses which form the interior of the connecting element 61. These recesses are in Fig. 10 shown in detail.
- the recesses are the fluid-carrying channels through which the components to be mixed are supplied to the installation bodies of the mixing element.
- Fig. 9 shows a detail of Fig. 8 , namely the opening 70 in the cap member 66.
- the connecting element 60 which contains two recesses 73, 74, which form the interior of the connecting element 61.
- the recess 73 is provided for the component with the larger volume flow, the recess 74 serves as a channel for the component with the smaller volume flow.
- the recess 74 thus represents a section through the continuation channel 62.
- the ratio of the cross-sectional areas of the recess 73 to the recess 74 ie the ratio of the remaining free cross-sectional area to the cross-sectional area of the continuation channel 62 is between 4: 1 and 5: 1.
- the cross-sectional area of the recess 73 is 2.8 mm 2 and the cross-sectional area of the recess 74 is 0.6 mm 2 .
- Fig. 10 shows a section through the mixing element along the outlet side of the body 57, which the inlet channels 51, 52 (see Fig. 6b ) contains.
- the outlet opening 55 of the inlet channel 51 opens into the antechamber 58, which extends between the connecting element 60 and the outlet side 59 of the body 57.
- the outlet opening 56 of the inlet channel 52 is separated by the outlet side 59 forming wall elements 77 of the prechamber 58, so that the two components in the prechamber not yet in Come in contact.
- the wall elements 77 which define the connecting channel 78 leading to the connecting element 60 are in FIG Fig. 11 shown in detail.
- the ratio of the cross-sectional areas of the pre-chamber 58 to the connecting channel 78 as shown in the present section is at least 5: 1, wherein in the prechamber 58, the component with the larger volume flow is included.
- the cross-sectional area of the pre-chamber may be 32.4 mm 2
- the cross-sectional area of the connecting channel 78 may be 6.2 mm 2 .
- the cross-sectional area of the outlet opening 55 belonging to the inlet opening 53, the in Fig. 6b is shown, then is 15.9 mm 2 .
- the cross-sectional area of the exit opening 56 associated with the inlet opening 54 in Fig. 6b is shown, then is 2.8 mm 2 .
- the volume of the two components in the inlet region that is, from the corresponding inlet opening 53, 54 to the entry into the first mounting body of the mixing element for the component with the larger volume flow is 171 mm 3 and for the component with the smaller volume flow 28 mm 3 .
- Fig. 11 shows a detail of Fig. 10 , namely the wall elements 77, which bound the connecting channel 60 leading to the connecting element 60.
- the connecting channel 78 is narrowed from the outlet opening 56 until it enters the interior of the connecting element 61. This constriction can be done in particular by at least partially conical channel walls.
- the ratio of the cross-sectional area of the continuation channel and the remaining free cross-sectional area in a sectional plane which is normal to the longitudinal axis and located at the mixer inlet is at least 4: 1.
- the mixing ratio of the components can be 4: 1, but also according to an alternative embodiment, at least 5: 1, it can also be at least 10: 1, or even more.
- For all mixing ratios of the components is preferably a Used mixing element with the same dimensions. The following additional geometric conditions thus apply analogously for cross-sectional ratios of 5: 1 to 10: 1 or more.
- the cross-sectional area of the inlet opening to the cross-sectional area adjacent to the outlet opening increases by at least twice for at least one of the components.
- the cross-sectional area from the inlet opening to the cross-sectional area following the outlet opening for each of the components at least doubles.
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dispersion Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Civil Engineering (AREA)
- Structural Engineering (AREA)
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP12186959.8A EP2599540B1 (fr) | 2011-11-29 | 2012-10-02 | Élément de mélange pour un mélangeur statique et son utilisation |
PL12186959T PL2599540T3 (pl) | 2011-11-29 | 2012-10-02 | Element mieszający do mieszalnika statycznego oraz jego zastosowanie |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
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EP11191143 | 2011-11-29 | ||
EP12186959.8A EP2599540B1 (fr) | 2011-11-29 | 2012-10-02 | Élément de mélange pour un mélangeur statique et son utilisation |
Publications (2)
Publication Number | Publication Date |
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EP2599540A1 true EP2599540A1 (fr) | 2013-06-05 |
EP2599540B1 EP2599540B1 (fr) | 2014-01-08 |
Family
ID=46888969
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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EP12186959.8A Active EP2599540B1 (fr) | 2011-11-29 | 2012-10-02 | Élément de mélange pour un mélangeur statique et son utilisation |
Country Status (11)
Country | Link |
---|---|
US (1) | US10293311B2 (fr) |
EP (1) | EP2599540B1 (fr) |
JP (1) | JP6158496B2 (fr) |
KR (1) | KR102022572B1 (fr) |
CN (2) | CN107456889A (fr) |
AU (1) | AU2012254968B2 (fr) |
CA (1) | CA2789725C (fr) |
DK (1) | DK2599540T3 (fr) |
ES (1) | ES2443368T3 (fr) |
IL (1) | IL222512A (fr) |
PL (1) | PL2599540T3 (fr) |
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EP3034180A1 (fr) * | 2014-12-17 | 2016-06-22 | HILTI Aktiengesellschaft | Gerbe ayant au moins un récipient pour produit en vrac et d'un élément de tête |
WO2017027279A1 (fr) * | 2015-08-07 | 2017-02-16 | Nordson Corporation | Chicanes de déflecteur d'écoulement à double paroi et mélangeur statique associé, et procédés de mélange |
EP3338882A1 (fr) * | 2016-12-14 | 2018-06-27 | Felix Streiff | Élément mélangeur à résistance et à action de mélange élevés |
DE102017117198A1 (de) | 2017-07-28 | 2019-01-31 | 3lmed GmbH | Mischer |
WO2019020764A1 (fr) | 2017-07-28 | 2019-01-31 | Kettenbach Gmbh & Co. Kg | Mélangeur |
US10363526B2 (en) | 2015-08-07 | 2019-07-30 | Nordson Corporation | Entry mixing elements and related static mixers and methods of mixing |
US11020716B2 (en) | 2015-08-28 | 2021-06-01 | Sulzer Mixpac Ag | Static mixer, method of assembling a static mixer and dispensing apparatus |
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SG161141A1 (en) * | 2008-10-17 | 2010-05-27 | Sulzer Mixpac Ag | Static mixer |
US10737012B2 (en) * | 2015-03-31 | 2020-08-11 | Biomet Biologics, Inc. | Cell washing using acoustic waves |
ES2934154T3 (es) | 2015-10-30 | 2023-02-17 | Medmix Switzerland Ag | Mezclador estático |
DE102015121351A1 (de) * | 2015-12-08 | 2017-06-08 | Stamixco Ag | Mischereinsatz, statischer Mischer sowie Herstellverfahren |
US10281074B2 (en) * | 2016-01-14 | 2019-05-07 | Nordson Corporation | Adapters for connecting a separated-outlet fluid cartridge to a single-inlet mixer, and related methods |
EP3342478A1 (fr) * | 2016-12-29 | 2018-07-04 | Sulzer Mixpac AG | Mélangeur statique, kit de pièces et utilisation dudit mélangeur statique |
EP3342479A1 (fr) * | 2016-12-29 | 2018-07-04 | Sulzer Mixpac AG | Mélangeur statique, un kit de pièces et utilisation dudit mélangeur statique |
DE102017112440A1 (de) | 2017-06-06 | 2018-12-06 | Shin-Etsu Silicones Europe B.V. | Gebinde und Dosiervorrichtung für viskose Materialien |
DE102017117199A1 (de) | 2017-07-28 | 2019-01-31 | 3lmed GmbH | Mischer mit Kompensationskanal und/oder Staukammer |
DE102019101644B4 (de) | 2019-01-23 | 2021-02-18 | 3lmed GmbH | Mischer und Verfahren zum Vermischen zweier Komponenten |
US11813580B2 (en) * | 2020-09-02 | 2023-11-14 | Nov Canada Ulc | Static mixer suitable for additive manufacturing |
KR102674288B1 (ko) * | 2022-04-13 | 2024-06-11 | 주식회사 케이시티 | Uvc 고도산화공정을 연계한 유체 또는 기체 혼합용 스태틱 믹서 |
CN115178128B (zh) * | 2022-06-17 | 2023-09-29 | 合盛硅业股份有限公司 | 一种静态混合装置及气相二氧化硅生产系统 |
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- 2012-10-02 ES ES12186959.8T patent/ES2443368T3/es active Active
- 2012-10-02 DK DK12186959.8T patent/DK2599540T3/da active
- 2012-10-02 EP EP12186959.8A patent/EP2599540B1/fr active Active
- 2012-10-02 PL PL12186959T patent/PL2599540T3/pl unknown
- 2012-10-18 IL IL222512A patent/IL222512A/en active IP Right Grant
- 2012-11-05 JP JP2012243549A patent/JP6158496B2/ja active Active
- 2012-11-26 AU AU2012254968A patent/AU2012254968B2/en not_active Ceased
- 2012-11-28 CN CN201710866141.5A patent/CN107456889A/zh active Pending
- 2012-11-28 US US13/687,804 patent/US10293311B2/en active Active
- 2012-11-28 CN CN201210493063.6A patent/CN103127853B/zh active Active
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US10245565B2 (en) | 2015-08-07 | 2019-04-02 | Nordson Corporation | Double wall flow shifter baffles and associated static mixer and methods of mixing |
US10363526B2 (en) | 2015-08-07 | 2019-07-30 | Nordson Corporation | Entry mixing elements and related static mixers and methods of mixing |
US10427114B2 (en) | 2015-08-07 | 2019-10-01 | Nordson Corporation | Double wall flow shifter baffles and associated static mixer and methods of mixing |
US11020716B2 (en) | 2015-08-28 | 2021-06-01 | Sulzer Mixpac Ag | Static mixer, method of assembling a static mixer and dispensing apparatus |
EP3338882A1 (fr) * | 2016-12-14 | 2018-06-27 | Felix Streiff | Élément mélangeur à résistance et à action de mélange élevés |
DE102017117198A1 (de) | 2017-07-28 | 2019-01-31 | 3lmed GmbH | Mischer |
WO2019020764A1 (fr) | 2017-07-28 | 2019-01-31 | Kettenbach Gmbh & Co. Kg | Mélangeur |
Also Published As
Publication number | Publication date |
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JP6158496B2 (ja) | 2017-07-05 |
CN103127853A (zh) | 2013-06-05 |
IL222512A (en) | 2016-12-29 |
CA2789725A1 (fr) | 2013-05-29 |
US10293311B2 (en) | 2019-05-21 |
PL2599540T3 (pl) | 2014-06-30 |
US20130135963A1 (en) | 2013-05-30 |
AU2012254968A1 (en) | 2013-06-13 |
EP2599540B1 (fr) | 2014-01-08 |
KR20130060142A (ko) | 2013-06-07 |
CA2789725C (fr) | 2019-08-06 |
JP2013111574A (ja) | 2013-06-10 |
AU2012254968B2 (en) | 2015-01-29 |
CN107456889A (zh) | 2017-12-12 |
CN103127853B (zh) | 2017-08-22 |
ES2443368T3 (es) | 2014-02-19 |
KR102022572B1 (ko) | 2019-11-04 |
DK2599540T3 (da) | 2014-03-31 |
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