EP2482989A1 - Dispositif, machine de flottation munie de ce dispositif et son procédé d'exploitation - Google Patents

Dispositif, machine de flottation munie de ce dispositif et son procédé d'exploitation

Info

Publication number
EP2482989A1
EP2482989A1 EP10760327A EP10760327A EP2482989A1 EP 2482989 A1 EP2482989 A1 EP 2482989A1 EP 10760327 A EP10760327 A EP 10760327A EP 10760327 A EP10760327 A EP 10760327A EP 2482989 A1 EP2482989 A1 EP 2482989A1
Authority
EP
European Patent Office
Prior art keywords
gas
suspension
nozzle
mixing chamber
channels
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP10760327A
Other languages
German (de)
English (en)
Inventor
Norbert Becker
Wolfgang Krieglstein
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Primetals Technologies Germany GmbH
Original Assignee
Siemens AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=41727990&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=EP2482989(A1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Siemens AG filed Critical Siemens AG
Priority to EP10760327A priority Critical patent/EP2482989A1/fr
Publication of EP2482989A1 publication Critical patent/EP2482989A1/fr
Withdrawn legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D1/00—Flotation
    • B03D1/02—Froth-flotation processes
    • B03D1/028—Control and monitoring of flotation processes; computer models therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20—Mixing gases with liquids
    • B01F23/23—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/232—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using flow-mixing means for introducing the gases, e.g. baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/30—Injector mixers
    • B01F25/31—Injector mixers in conduits or tubes through which the main component flows
    • B01F25/312—Injector mixers in conduits or tubes through which the main component flows with Venturi elements; Details thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/30—Injector mixers
    • B01F25/31—Injector mixers in conduits or tubes through which the main component flows
    • B01F25/312—Injector mixers in conduits or tubes through which the main component flows with Venturi elements; Details thereof
    • B01F25/3124—Injector mixers in conduits or tubes through which the main component flows with Venturi elements; Details thereof characterised by the place of introduction of the main flow
    • B01F25/31243—Eductor or eductor-type venturi, i.e. the main flow being injected through the venturi with high speed in the form of a jet
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D1/00—Flotation
    • B03D1/14—Flotation machines
    • B03D1/1431—Dissolved air flotation machines
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D1/00—Flotation
    • B03D1/14—Flotation machines
    • B03D1/1493—Flotation machines with means for establishing a specified flow pattern
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D1/00—Flotation
    • B03D1/14—Flotation machines
    • B03D1/24—Pneumatic
    • B03D1/242—Nozzles for injecting gas into the flotation tank
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F2025/91—Direction of flow or arrangement of feed and discharge openings
    • B01F2025/913—Vortex flow, i.e. flow spiraling in a tangential direction and moving in an axial direction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/30—Injector mixers
    • B01F25/31—Injector mixers in conduits or tubes through which the main component flows
    • B01F25/312—Injector mixers in conduits or tubes through which the main component flows with Venturi elements; Details thereof
    • B01F25/3125—Injector mixers in conduits or tubes through which the main component flows with Venturi elements; Details thereof characteristics of the Venturi parts
    • B01F25/31252—Nozzles
    • B01F25/312522—Profiled, grooved, ribbed nozzle, or being provided with baffles

Definitions

  • the invention relates to a device for dispersing a suspension with at least one gas, in particular for a flotation machine, comprising a dispersion nozzle, one after the other in flow direction of the suspension, a tapered in the flow direction suspension nozzle, a mixing chamber into which the suspension nozzle opens, a to the Mixing chamber subsequent, in the flow direction tapered mixing tube and at least one gas supply line for supplying the at least one gas into the mixing chamber, wherein the suspension nozzle has at least a number N> 3 with the at least one gas supply line connected gas channels, which at one of the mixing chamber facing end of the Open suspension nozzle.
  • the invention also relates to a method for operating such
  • the invention further relates to a flotation machine equipped with at least one such device, to a method for operating the flotation machine and to the use thereof.
  • Flotation is a physical separation process for
  • Suspension contained particles It is used for the treatment of mineral resources and in the processing of preferably mineral substances with a low to medium
  • Flotation machines are already known.
  • WO 2006/069995 A1 describes a flotation machine with a housing, which comprises a flotation chamber, with at least one
  • Dispergierdüse here referred to as an ejector, further with at least one gassing, when using air ventilation devices or aerators called, as well as a collection container for a formed during the flotation foam product.
  • a suspension of water and fine-grained solid mixed with reagents is generally passed over at least one
  • Dispergierdüse introduced into a flotation chamber.
  • the purpose of the reagents is to ensure that, in particular, the valuable particles, which are preferably to be separated off, are rendered hydrophobic in the suspension.
  • the at least one dispersing nozzle is supplied with gas, in particular air or nitrogen, which comes into contact with the hydrophobic particles in the suspension.
  • Gassing is introduced more gas in.
  • the hydrophobic particles adhere to forming gas bubbles, so that the gas bubble structures, also called aeroflocs, float and on the surface of the suspension
  • the foam product is in a
  • Collision probability the greater the number of hydrophobic particles that adhere to a gas bubbles, rise to the surface and together with the particles form the foam product.
  • the probability of collision is influenced, inter alia, by the dispersion of suspension and gas in the dispersing nozzle. Dispergierdüsen according to FIG 1 are already in
  • FIG 2 a longitudinal section through the dispersing 1 is shown, in each of the
  • This known dispersing nozzle 1 comprises one after the other, seen in the flow direction (see arrow direction) of the suspension 2, a tapering in the flow direction
  • Suspension nozzle 3 opens, a subsequent to the mixing chamber 4, tapering in the flow direction
  • the suspension 2 is connected via a connecting piece 9 in the
  • Suspension nozzle 3 fed and occurs at the end face 3a of the suspension nozzle 3 as a free jet 8 in the mixing chamber 4 a.
  • the gas 7 fed into the mixing chamber 4 is mixed with the suspension 2 emerging from the suspension nozzle 3 and reaches the mixing tube 5, where a further dispersion of suspension 2 and gas 7 takes place.
  • At the outlet la from the dispersing 1 is a suspension. 2
  • the flotation machine 100 used with a known per se structure according to FIG 20, wherein usually the installation is carried out such that the longitudinal axis of the dispersing nozzle 1 is aligned horizontally.
  • the flotation machine 100 comprises a housing 101 with a flotation chamber 102 into which at least one dispersing nozzle 1 for supplying gas 7 and suspension 2 opens into the flotation chamber 102.
  • the housing 101 has a cylindrical housing portion 101 a, at the lower end at least one
  • Gassing arrangement 103 is arranged.
  • Foam gutter 104 with nozzle 105 for discharging the formed Foam product The upper edge of the outer wall of the housing
  • the housing 101 is located above the upper edge of the foam channel 104, whereby an overflow of the foam product on the upper edge of the housing 101 is excluded.
  • the housing 101 further has a bottom discharge opening 106. Particles of
  • Suspension 2 which are provided, for example, with an insufficiently hydrophobized surface or have not collided with a gas bubble, and hydrophilic particles sink in the direction of the bottom discharge opening 106.
  • the gassing device 103 which is connected to a gas feed 103a, additional gas 7 is blown into the cylindrical housing section 101a, so that more
  • hydrophobic particles are bound to it and ascend. Ideally, especially the hydrophilic particles continue to sink and are removed from the process via the bottom discharge opening 106. The foam product comes out of the flotation chamber
  • the suction of the gas 7 is subject to the
  • Dispersion nozzle 1 fluctuates.
  • An amount of gas 7 supplied via the at least one gas supply line 6 can be obtained
  • the arrangement of the at least one gas supply line 6 plays a decisive role with regard to the dispersion result.
  • the gas supply line 6 In the known dispersing nozzle 1 according to FIGS. 1 and 2, the gas supply line 6
  • Mixing chamber 4 are arranged. In order to prevent clogging of a gas supply line 6 by solid particles from the suspension 2, which up to 50 wt .-% in the suspension. 2 However, a gas supply line 6 is preferably arranged in the upper region of the mixing chamber 4 of the horizontally oriented dispersing 1. This can be
  • German Offenlegungsschrift No. 27 000 49 discloses a dispersing nozzle for a flotation machine, in which a water stream containing impurities to be separated off is dispersed with air. The air is displaced by a spiral air chamber in a rotational movement.
  • Dispergierdüsen for flotation operations in the aforementioned type in the suspension nozzle has gas channels, which open at the front of the suspension nozzle, are known for example from DE 42 06 715 AI.
  • Dispersing result of suspension and gas improved device comprising a dispersing nozzle and a
  • the object is with regard to the device for
  • At least one gas supply line for supplying the
  • the suspension nozzle has at least a number N> 3 with the at least one gas supply line connected gas channels, which open at one of the mixing chamber facing end side of the suspension nozzle, and wherein the device
  • each of the at least N gas channels depending on a gas control valve for metering a gas amount of the
  • Suspension is assigned by the respective gas channel supplied gas.
  • the supply of gas to be dispersed in the suspension in the region of the end face of the suspension nozzle means that a particularly uniform gas distribution takes place in the region of the surface of the free jet that is being formed and a particularly large amount of gas is uniformly sucked into the free jet.
  • a gassing pattern M is understood to mean here a gas injection that changes over time and in succession at certain time intervals in succession via specific individual gas channels or groups of gas channels.
  • a gas control valve of the device may also be such that a switching between
  • the insert is piezoelectronic
  • the gas control valves are preferably electronically controllable via at least one central control unit.
  • fumigation patterns M can be set and performed quickly and above all automatically.
  • the device according to the invention is particularly suitable for use in general on any type of flotation machine, preferably for use on pneumatic flotation machines. Here is due to the achieved higher
  • Collision probability between a gas bubbles and a particle to be separated achieved in terms of quantity and quality improved foam product.
  • the device according to the invention can also be used in other
  • Processes are used in which a suspension and at least one gas to be dispersed.
  • At least one pressurized water line for supplying water with an amount of dissolved therein, in the mixing chamber at least partially escaping gas in the suspension nozzle and / or in the mixing tube is available.
  • the gas can be in the water until the
  • Dispersing nozzle is preferably carried out at a point at which the water passes directly into the suspension or already dispersed with gas suspension. Due to the occurring at the transition between pressurized water pipe and suspension
  • a microbubble is understood as meaning a gas bubble having a diameter of ⁇ 100 ⁇ m.
  • Microbubbles is capable of producing the finest particles
  • the at least one pressurized water line can be guided through a wall of the suspension nozzle and / or the mixing tube.
  • the at least one pressurized water line may alternatively be guided into the mixing chamber, in order to open at a location within the mixing tube, which leads to a
  • the suspension nozzle is at least one
  • the at least one device comprises at least one web arranged on an inner side of the suspension nozzle facing the suspension, which extends spirally from one side of the suspension nozzle facing away from the mixing chamber to the front side of the suspension nozzle facing the mixing chamber ,
  • the at least one device which is able to set the suspension in a spiral rotation about a longitudinal center axis of the suspension nozzle, alternatively to a formation as swirl grooves or webs by at least one spiral nozzle insert and the like or a combination of such a nozzle insert with swirl grooves and / or webs, be formed.
  • the suspension nozzle has at least a number N> 8 of gas ducts which, at the end face facing the mixing chamber, of the gas channels
  • the number of gas channels can vary depending on Dimension of the suspension nozzle can be freely selected within wide limits. In order to change the gas volume to be introduced into the suspension and the inflow velocity, an optimal number and configuration of the gas channels will also be
  • the N gas channels are, viewed in the direction of the end face of the suspension nozzle, preferably arranged at a uniform distance from one another centered on at least one circular path about the longitudinal central axis of the suspension nozzle.
  • the object is achieved for the method for operating a device according to the invention, i. comprising one
  • Dispersion nozzle and further gas control valves achieved in that the at least N gas channels associated gas control valves are operated clocked such that at any time at least one gas control valve is closed and at least one other gas control valve is open, the gas supply to the suspension a gassing M following at each gas control valve temporarily interrupted.
  • a gassing pattern M is a sequence which changes in time sequence and repeats in a certain time interval in the sequence
  • the gas control valves for a maximum gas supply to the suspension are controlled so that only one gas channel is closed at any time, the gas supply to the suspension a first Begasungsmuster Ml following one after the other at each of the gas channel is temporarily interrupted. This promotes uniform intake into and distribution of the gas in the suspension. Furthermore, it has for a minimal gas supply to
  • Gassing pattern M2 is carried out sequentially and successively through each gas channel. This reliably prevents a
  • the second gassing pattern M2 is preferably formed such that in the direction of the front side of
  • Suspension nozzle seen the at least one gas sequentially by adjacent gas channels arranged side by side
  • the gassing pattern M is formed in an alternative manner such that viewed in the direction of the end face of the suspension nozzle, the at least one gas is successively supplied by adjacent groups of adjacent adjacent gas ducts. This to a
  • the gas supply can be over two or more
  • Gas control valve to be regulated. It has proven useful to supply a subset of the N gas channels via a first gas supply line with a first gas and to supply a remainder of the gas channels via a second gas supply line with a second gas different from the first gas. It can be different gases such
  • air and nitrogen are used, but other gases are usable.
  • the object is achieved for the flotation machine, in that it comprises at least one device according to the invention.
  • a foam product improved in terms of quantity and quality is achieved.
  • the discharge rate of particles to be discharged is effectively increased.
  • the flotation machine preferably comprises a housing with a flotation chamber, into which the dispersing nozzle of the at least one device opens, and at least one gassing arrangement for the further supply of gas into the flotation chamber, which is arranged in the flotation chamber below the dispersing nozzle (s).
  • the flotation machine can also have a different structure.
  • a use of a flotation machine according to the invention for segregating an ore of gangue contained in the suspension has proven itself, since a particularly effective discharge of the ore takes place.
  • Suspension is injected by means of the dispersing in the flotation and the device is operated according to the invention, wherein the mixing chamber gas is supplied via the at least one gas supply, wherein the gas control valves associated with the at least N gas channels operated in a clocked manner at least one
  • Gas control valve is closed and at least one other gas control valve is open, with the gas supply to
  • Gas control valve is temporarily interrupted.
  • FIGS. 1 to 20 are intended to illustrate the invention by way of example. So shows:
  • Dispergierdüse according to FIG 1; 3 shows a suspension nozzle in longitudinal section
  • FIG. 4 shows the suspension nozzle according to FIG. 3 seen from below;
  • FIG 6 shows the suspension nozzle according to FIG 5 in plan view
  • FIG. 7 shows the suspension nozzle according to FIG. 5 seen from below;
  • FIG. 8 shows a dispersion nozzle for the invention
  • the centers of the eight gas channels 31 lie on a circular line, wherein the Circle to the center of the suspension nozzle 3 '' centered
  • suspension nozzle 3 '' according to the figures 3 and 4 can not be replaced directly against a suspension nozzle 3 of a conventional dispersing 1 to one for the
  • the eight gas channels 31 allow a targeted introduction of gas 7 into the suspension 2 with regard to the amount of gas and / or location of the injection and / or distribution of the injection.
  • the gas channels 31 are individually supplied with gas 7 and are each connected to a gas control valve Va, Vb, Vc, Vd, Ve, Vf, Vg, Vh (compare FIGS. 10 to 19).
  • a specific gassing pattern M can be set.
  • a gassing pattern M is understood to mean a gas injection 7 which changes over time and in sequence at certain time intervals in the sequence, via specific individual gas channels 31 or groups of gas channels 31. This will be explained in more detail below with reference to FIGS. 10 to 19.
  • Means 30 is equipped, which are able to put the suspension 2 (see also Figures 8 and 9) in a spiral rotation about a longitudinal central axis of the suspension nozzle 3 ' .
  • the required gas channels 31 have been omitted in this illustration.
  • the devices 30 are called helical grooves, as well
  • the means 30 may alternatively be formed as a swirl grooves by webs, spiral inserts and the like or a combination of such devices, possibly also in combination with swirl grooves, be formed.
  • Number, the depth and the pitch angle of the grooves are freely selectable within wide limits and limited only by the dimensions and the material of the suspension nozzle used.
  • FIG. 6 shows the suspension nozzle 3 '(without gas channels) according to FIG. 5 in plan view, the course of the four existing swirl grooves on the inner wall of the suspension nozzle
  • FIG. 7 shows the suspension nozzle 3 '(without gas channels) according to FIG. 5 from below, wherein the front side 3a' of the suspension nozzle 3 'can be seen with the swirl grooves on which the suspension 2 (see also FIGS. 8 and 9) offset from rotation Suspension nozzle 3 'emerges.
  • FIG. 8 shows a dispersion nozzle 10 for a device according to the invention in longitudinal section, which is equipped with a suspension nozzle 3 '' ', which shows the gas channels 31 and the means 30 in the form of swirl grooves, as shown in Figures 5 to 7, has.
  • the dispersing nozzle 10 is particularly suitable for use in the device according to the invention and thus for use in flotation machines or hybrid flotation cells (see FIG. 20).
  • the longitudinal section through the dispersing nozzle 10 shows in each case the flow path of suspension 2 and gas 7.
  • the dispersing 10 comprises successively, in the flow direction (see arrow) of the suspension 2, the tapering in the flow direction suspension nozzle 3 ''', a Mixing chamber 4, in which the suspension nozzle 3 ''' opens, a subsequent to the mixing chamber 4, in
  • Suspension 2 is connected via a connector 9 in the
  • the gas 7 fed into the mixing chamber 4 via the gas channels 31 is mixed with the suspension 2 emerging from the suspension nozzle 3 '".
  • Gas 7 and suspension 2 enter the mixing tube 5, where a further intensive dispersion takes place.
  • At the outlet opening 10a from the dispersing nozzle 10 is a
  • the dispersing nozzle 10 ' is likewise suitable in particular for use in flotation machines or hybrid flotation cells
  • the longitudinal section through the dispersing nozzle 10 'in each case shows the flow course of suspension 2 and gas 7a, 7b.
  • the dispersing nozzle 10 ' is, in principle, constructed as the dispersion nozzle 10 according to FIG. 8. However, different gases 7a, 7b, for example air and nitrogen, are fed into the gas channels 31 via the gas supply lines 6a, 6b.
  • the dispersion nozzle 10 has at least one
  • the dispersing nozzle 10' At the outlet opening 10a 'from the dispersing nozzle 10' is a dilute with water suspension 2 with therein particularly finely and intimately dispersed gas 7a, 7b and microbubbles before.
  • FIGS. 10 to 14 are intended to schematically illustrate a method according to the invention for operating a device according to the invention, of which, for a better overview, only the suspension nozzle is representative of the dispersion nozzle 10, 10 '
  • 3 '', 3 '' 'with N 8 gas channels 31 and the associated gas control valves Va, Vb, Vc, Vd, Ve, Vf, Vg, Vh are shown schematically, with maximum gas supply to gas 7, 7a, 7b explain.
  • the maximum gas supply is realized simultaneously over seven of the eight existing gas channels 31, which changes over time, which of the eight gas channels
  • FIG. 10 shows the end face of a suspension nozzle 3 '' , 3 '''of a dispersion nozzle 10, 10' of the invention
  • each gas channel 31 is controlled by means of a gas control valve V.
  • the gas passage 31a is connected to a gas control valve Va which controls a gas supply of the gas 7, 7a, 7b (see FIGS. 8 and 9) into the gas passage 31a.
  • the gas passage 31b is connected to a gas control valve Vb which controls gas supply of the gas 7, 7a, 7b into the gas passage 31b.
  • the gas passage 31c is connected to a gas control valve Vc which controls gas supply of the gas 7, 7a, 7b into the gas passage 31c.
  • the gas passage 31d is connected to a gas control valve Vd, which is a
  • the gas passage 31e is connected to a gas control valve Ve, which controls gas supply of the gas 7, 7a, 7b into the gas passage 31e.
  • the gas passage 31f is connected to a gas control valve Vf which controls a gas supply of the gas 7, 7a, 7b into the gas passage 31f.
  • the gas channel 31g is with a
  • Gas control valve Vg connected, which regulates a gas supply of the gas 7, 7a, 7b in the gas passage 31g.
  • the gas passage 31h is connected to a gas control valve Vh which controls gas supply of the gas 7, 7a, 7b into the gas passage 31h.
  • Gas control valves V are preferably via a central
  • Control unit electronically controllable.
  • FIG. 10 shows the first stage of the first gassing pattern M1.
  • FIG 11 shows the after a time interval
  • Gas control valve Vb which is connected upstream of the clockwise to the gas channel 31a adjacent the gas channel 31b, opened simultaneously.
  • the remaining gas control valves Vc to Vh are
  • FIG 12 shows the after a time interval, here
  • Gas control valve Vc which is connected upstream of the adjacent clockwise to the gas channel 31b gas channel 31c, open simultaneously.
  • the following remaining gas control valves Vd to Va are opened unchanged.
  • FIG. 13 shows that after a time interval, here
  • Gas control valve Vd which is the upstream of the gas channel 31c adjacent to the gas channel 31c upstream, opened simultaneously.
  • the following remaining gas control valves Ve to Vb are opened unchanged.
  • the closed gas channel travels clockwise per time interval, so that
  • FIG. 14 shows the eighth stage of the first following after a further time interval, here for example by ls
  • the first gassing pattern Ml which on the end face 3a '', 3a '' 'of the suspension nozzle 3' ', 3' '' seen a circulation of a closed gas channel clockwise, is now complete and is repeated.
  • the following stage is identical to the first stage according to FIG. 10.
  • the first to eighth stages in succession are repeated again and again until a modified fumigation pattern M is desired.
  • FIGS. 15 to 19 are intended to schematically show a preferred one
  • a method for operating a device according to the invention with a dispersion nozzle 10, 10 'comprising a suspension nozzle 3' ', 3' '' with N 8 gas channels 31 with minimal gas supply explain.
  • gas channels 31 are also not critical here. Of course, more or fewer gas channels 31 may be present.
  • the other gas control valves Vb, Vc, Vd, Ve, Vf, Vg, Vh and thus also the gas channels 31b, 31c, 31d, 31e, 31f, 31g, 31h are closed and do not allow access of the gas 7, 7a, 7b to the mixing chamber, not shown here.
  • the valve setting according to FIG. 15 will only be of a specific, experimental nature in its optimum length Maintaining the time interval to be determined and then changing it.
  • a second gassing pattern M2 is selected, in which, in a clockwise direction, a single activation of the
  • FIG. 15 shows the first stage of the second gassing pattern M2.
  • FIG. 16 shows that after a time interval, here
  • Gas control valve Vb which is connected upstream of the clockwise to the gas channel 31a adjacent the gas channel 31b, opened simultaneously.
  • the remaining gas control valves Vc to Vh are
  • FIG. 17 shows the after a time interval, here
  • Gas control valve Vc which is connected upstream of the adjacent clockwise to the gas channel 31b gas channel 31c, open simultaneously.
  • the following remaining gas control valves Vd to Va are closed unchanged.
  • FIG. 18 shows that after a time interval, here
  • Gas control valve Vd which clockwise to the gas channel 31c adjacent gas channel 31d is connected, opened at the same time.
  • the following remaining gas control valves Ve to Vb are closed unchanged.
  • the open gas channel travels clockwise per time interval, so that in each case the gas control valve Ve, Vf, Vg is open one after the other at each time interval.
  • FIG. 19 shows the eighth stage of the second following after a further time interval, here for example from ls
  • Stage 1 Va, Ve open; Vb to Vd and Vf to Vh closed;
  • Stage 2 Vb, Vf open; Vc to Ve and Vg to Va closed;
  • Stage 3 Vc, Vg open; Vd to Vf and Vh to Vb closed;
  • Stage 4 Vd, Vh open; Ve to Vg and Va to Vc closed;
  • Step 1 Va, Vc, Ve, Vg open; Vb, Vd, Vf, Vh closed; Stage 2: Vb, Vd, Vf, Vh open; Va, Vc, Ve, Vg closed: This is followed by a repetition of the fifth
  • the gassing pattern M5 can still be varied by feeding different gases into stage 1 and stage 2, for example in stage 1 in the form of air and stage 2 in the form of nitrogen.
  • Level 1 Va open; Vb to Vh closed;
  • Stage 3 Vf open; Vg to Ve closed; Level 4 Vg open; Vh to Vf closed;
  • Stage 12 Vc open; Vd to Vb closed;
  • Stage 13 Vg open; Vh to Vf closed;
  • Stage 14 Vh open; Va to Vg closed;
  • Gas supply used gas channels and / or the selection of the injected gas via a gas channel a variety of other gassing M are possible to influence an amount and distribution of at least one gas in the suspension 2 and thus the dispersion result.
  • FIG 20 shows a
  • Flotation chamber 102 of the flotation machine 100 opens, the dispersion of suspension and gas is improved at the same or similar installation position of the dispersion nozzle 10, 10 'and thus increases the probability of collision between a gas bubbles and a particle 2 separated from the suspension. As a result, increased deposition rates and an optimal foam product can be achieved.
  • the use of the device according to the invention is not on a flotation machine in general or a
  • a device according to the invention comprising a
  • Dispersion nozzle and gas control valves can be used on flotation systems of any structure or equipment in which at least one gas in a suspension is to be finely and evenly distributed.

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biotechnology (AREA)
  • General Engineering & Computer Science (AREA)
  • Nozzles (AREA)
  • Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)

Abstract

L'invention concerne un dispositif pour assurer la dispersion d'une suspension, avec au moins un gaz, qui comporte une buse de dispersion qui comprend, vus successivement dans la direction d'écoulement de la suspension : une buse de suspension qui s'effile dans la direction de l'écoulement; une chambre de mélange dans laquelle la buse de suspension débouche; un tube de mélange qui s'effile dans la direction de l'écoulement et est contigu à la chambre de mélange, et au moins une conduite d'alimentation en gaz pour l'introduction du ou des gaz dans la chambre de mélange. Selon l'invention, la buse de suspension comprend au moins un nombre N ≥ 3 de canaux à gaz reliés avec la ou les conduites d'alimentation en gaz, qui débouchent au niveau d'une face frontale de la buse de suspension, qui est tournée vers la chambre de mélange. Le dispositif comporte également un nombre A de soupapes à gaz, avec N étant égal à A, une soupape à gaz de régulation étant associée à chacun des au moins N canaux à gaz pour le dosage d'une quantité du gaz introduit dans la suspension par le canal à gaz respectif. L'invention concerne également une machine de flottation munie d'un tel dispositif et un procédé d'exploitation du dispositif et de la machine de flottation.
EP10760327A 2009-09-29 2010-09-28 Dispositif, machine de flottation munie de ce dispositif et son procédé d'exploitation Withdrawn EP2482989A1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
EP10760327A EP2482989A1 (fr) 2009-09-29 2010-09-28 Dispositif, machine de flottation munie de ce dispositif et son procédé d'exploitation

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09171568A EP2308601A1 (fr) 2009-09-29 2009-09-29 Buse de dispersion, machine de flottation en étant équipée et son procédé de fonctionnement
EP10760327A EP2482989A1 (fr) 2009-09-29 2010-09-28 Dispositif, machine de flottation munie de ce dispositif et son procédé d'exploitation
PCT/EP2010/064366 WO2011039190A1 (fr) 2009-09-29 2010-09-28 Dispositif, machine de flottation munie de ce dispositif et son procédé d'exploitation

Publications (1)

Publication Number Publication Date
EP2482989A1 true EP2482989A1 (fr) 2012-08-08

Family

ID=41727990

Family Applications (2)

Application Number Title Priority Date Filing Date
EP09171568A Withdrawn EP2308601A1 (fr) 2009-09-29 2009-09-29 Buse de dispersion, machine de flottation en étant équipée et son procédé de fonctionnement
EP10760327A Withdrawn EP2482989A1 (fr) 2009-09-29 2010-09-28 Dispositif, machine de flottation munie de ce dispositif et son procédé d'exploitation

Family Applications Before (1)

Application Number Title Priority Date Filing Date
EP09171568A Withdrawn EP2308601A1 (fr) 2009-09-29 2009-09-29 Buse de dispersion, machine de flottation en étant équipée et son procédé de fonctionnement

Country Status (11)

Country Link
US (1) US20120218852A1 (fr)
EP (2) EP2308601A1 (fr)
CN (1) CN102548662A (fr)
AU (1) AU2010303034B2 (fr)
CA (1) CA2775614C (fr)
CL (1) CL2012000449A1 (fr)
MX (1) MX2012003285A (fr)
PE (1) PE20130166A1 (fr)
RU (1) RU2503502C1 (fr)
WO (1) WO2011039190A1 (fr)
ZA (1) ZA201200731B (fr)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2450106B1 (fr) 2010-11-03 2016-06-01 Primetals Technologies Germany GmbH Appareil de flottation et procédé de flottation
KR20140049987A (ko) * 2011-04-26 2014-04-28 지 테크 라이센싱 엘엘씨 기체 용해 장치
DK2572778T3 (en) * 2011-09-23 2017-06-06 Primetals Technologies Germany Gmbh Flotation machine with a dispersing nozzle and method for operating it
DE102012209342A1 (de) * 2012-06-04 2013-12-05 Siemens Aktiengesellschaft Verfahren zum Anpassen der Geometrie einer Dispergierdüse
WO2014188232A1 (fr) * 2013-05-23 2014-11-27 Dpsms Tecnologia E Inovação Em Mineração Ltda Système automatique de colonnes de flottation par mousse avec buses d'injection d'aérateurs et procédé
CN103506227B (zh) * 2013-09-27 2015-04-29 北京科技大学 一种脉冲喷射式泡沫浮选机
FR3031099B1 (fr) * 2014-12-24 2019-08-30 Veolia Water Solutions & Technologies Support Buse optimisee d'injection d'eau pressurisee contenant un gaz dissous.
CN105664748A (zh) * 2016-04-05 2016-06-15 李理 一种螺旋提升机油汽混合箱
CN105689158B (zh) * 2016-04-06 2017-12-15 北京科技大学 一种用于射流式浮选机的旋转射流充气搅拌装置
AU2018256837A1 (en) * 2017-04-28 2019-12-19 Nano Gas Technologies, Inc. Nanogas shear processing
CN111256367B (zh) * 2018-11-30 2021-10-26 宁波方太厨具有限公司 一种燃气热水器及其控制方法

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU149367A1 (ru) * 1960-01-21 1961-11-30 Д.А. Кириллов Устройство дл диспергировани воздуха
DE2700049C3 (de) 1977-01-03 1980-10-02 Oskar Werner Dipl.-Ing. 6463 Freigericht Pawel Flotationsanlage
DE2756894A1 (de) * 1977-12-20 1979-06-21 Clevepak Corp Verfahren zum betreiben einer vorrichtung zum vermischen eines gases mit einer fluessigkeit und vorrichtung zur durchfuehrung dieses verfahrens
CH665962A5 (de) * 1985-07-19 1988-06-30 Escher Wyss Gmbh Begasungsvorrichtung fuer eine flotationseinrichtung und deren verwendung.
JPH0660640B2 (ja) * 1985-09-09 1994-08-10 清之 堀井 管路に螺旋流体流を生成させる装置
SU1377151A1 (ru) * 1985-12-26 1988-02-28 Всесоюзный научно-исследовательский и проектный институт механической обработки полезных ископаемых "Механобр" Вибрационна флотационна машина
GB8610636D0 (en) * 1986-04-30 1986-06-04 Pringle J M Induced flow mixers
SU1411044A1 (ru) * 1986-11-24 1988-07-23 Всесоюзный научно-исследовательский и проектный институт механической обработки полезных ископаемых "Механобр" Аэратор флотационной машины
DE4029982C2 (de) * 1990-09-21 2000-08-10 Steinecker Anton Entwicklung Vorrichtung zum Begasen einer Flüssigkeit
DE4206715C2 (de) * 1992-03-04 1997-06-26 Gaston M Wopfner Verfahren und Vorrichtung zum Einbringen eines Gases in eine Flüssigkeit
GB2294646B (en) * 1994-10-29 1999-03-17 Transvac Systems Ltd Material treatment
CN2279216Y (zh) * 1996-10-16 1998-04-22 中国矿业大学 浮选柱节能微泡发生器
CN2304475Y (zh) * 1997-08-22 1999-01-20 中国矿业大学 自吸组合式微泡发生器
US6682057B2 (en) * 2001-05-01 2004-01-27 Estr, Inc. Aerator and wastewater treatment system
RU2004138727A (ru) 2004-12-28 2006-06-10 Марк Григорьевич Видуецкий (RU) Флотационная пневматическая колонная машина
RU2289479C9 (ru) * 2005-04-06 2007-06-10 Эмерик Панкратьевич Ячушко Флотационная машина для пенной сепарации ячушко
RU2332263C2 (ru) * 2005-06-30 2008-08-27 Эмерик Панкратьевич Ячушко Центробежная пневматическая машина для флотации и обессеривания мелкого угля
CN201124121Y (zh) * 2007-11-21 2008-10-01 昆明理工大学 组合式射流微泡发生器

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See references of WO2011039190A1 *

Also Published As

Publication number Publication date
PE20130166A1 (es) 2013-02-16
CA2775614C (fr) 2015-11-03
CA2775614A1 (fr) 2011-04-07
US20120218852A1 (en) 2012-08-30
AU2010303034A1 (en) 2012-04-19
EP2308601A1 (fr) 2011-04-13
RU2012117617A (ru) 2013-11-10
WO2011039190A1 (fr) 2011-04-07
CL2012000449A1 (es) 2012-07-13
CN102548662A (zh) 2012-07-04
RU2503502C1 (ru) 2014-01-10
AU2010303034B2 (en) 2013-07-04
MX2012003285A (es) 2012-04-30
ZA201200731B (en) 2012-09-26

Similar Documents

Publication Publication Date Title
EP2482989A1 (fr) Dispositif, machine de flottation munie de ce dispositif et son procédé d'exploitation
DE2634496C2 (de) Injektor zur Begasung einer Flüssigkeit
EP2500102B1 (fr) Dispositif de flottation avec un élément de distribution d'un fluide pouvant générer un courant du fluide vers le collecteur en mousse
DE10164735C2 (de) Verfahren zur Aerosolerzeugung
EP2572778B1 (fr) Machine de flottaison avec une buse de dispersion et procédé de fonctionnementen
DE102011005031A1 (de) Flotationsvorrichtung, Verfahren zum Betreiben der Flotationsvorrichtung sowie deren Verwendung
EP3183052B1 (fr) Procédé et dispositif pour épurer des suspensions de matières fibreuses par flottation
EP2266704A1 (fr) Machine de flottation pneumatique et procédé de flottation
EP1293255B1 (fr) Procédé et dispositif de séparation de saletés de suspensions par flottation
EP3630368B1 (fr) Dispositif aérosol et procédé de production d'un aérosol
WO2012059415A1 (fr) Appareil de flottation et procédé de flottation
EP2415527B1 (fr) Dispositif d'aération pour une cellule de flottation, cellule de flottation et procédé de flottation
DE19920237B4 (de) Verfahren und Vorrichtung zum mechanischen Trennen eines dispersen Systems
WO2015052056A1 (fr) Procédé et dispositif de dispersion pour produire un mélange dispersé de fluides
DE102008056040A1 (de) Verfahren zur Entfernung von Störstoffen aus einer wässrigen Papierfasersuspension durch Flotation sowie Vorrichtung zu seiner Durchführung
WO2011128154A1 (fr) Dispositif d'alimentation en gaz pour une cellule de flottation
WO2013189685A1 (fr) Dispositif pour isoler des particules magnétiques et/ou magnétisables présentes dans une suspension et son utilisation
EP2512737B1 (fr) Procédé et dispositif de nettoyage, d'activation et de prétraitement d'une pièce au moyen de particules de neige carbonique
DE60109613T2 (de) Verfahren und vorrichtung zur beschickung von dynamischen separatoren
DE102009040318A1 (de) Verfahren zur Entfernung von Störstoffen aus einer Fasersuspension durch Flotation sowie Flotationsvorrichtung zu seiner Durchführung
EP3820821B1 (fr) Procédé de purification d'eaux usées par flottation
AT504955B1 (de) Diffusor für einen injektor in einer flotationszelle und verfahren zum zuführen einer fasersuspension in die flotationszelle
DE102006031540A1 (de) Vorrichtung und Verfahren zur Flotation einer Flüssigkeit
EP2397220B1 (fr) Générateur d'écoulement
DE102012200900A1 (de) Schaumrückführung

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

17P Request for examination filed

Effective date: 20120309

AK Designated contracting states

Kind code of ref document: A1

Designated state(s): AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO SE SI SK SM TR

DAX Request for extension of the european patent (deleted)
RAP1 Party data changed (applicant data changed or rights of an application transferred)

Owner name: SIEMENS AKTIENGESELLSCHAFT

RAP1 Party data changed (applicant data changed or rights of an application transferred)

Owner name: PRIMETALS TECHNOLOGIES GERMANY GMBH

RIC1 Information provided on ipc code assigned before grant

Ipc: B01F 5/00 20060101ALI20151202BHEP

Ipc: B01F 5/04 20060101ALI20151202BHEP

Ipc: B03D 1/24 20060101AFI20151202BHEP

Ipc: B01F 3/04 20060101ALI20151202BHEP

Ipc: B03D 1/14 20060101ALI20151202BHEP

Ipc: B03D 1/02 20060101ALI20151202BHEP

GRAP Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOSNIGR1

INTG Intention to grant announced

Effective date: 20160114

GRAS Grant fee paid

Free format text: ORIGINAL CODE: EPIDOSNIGR3

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: THE APPLICATION IS DEEMED TO BE WITHDRAWN

18D Application deemed to be withdrawn

Effective date: 20160525