EP2326412A1 - Mixing in a container of content having a base component and a component to be mixed - Google Patents

Mixing in a container of content having a base component and a component to be mixed

Info

Publication number
EP2326412A1
EP2326412A1 EP09797569A EP09797569A EP2326412A1 EP 2326412 A1 EP2326412 A1 EP 2326412A1 EP 09797569 A EP09797569 A EP 09797569A EP 09797569 A EP09797569 A EP 09797569A EP 2326412 A1 EP2326412 A1 EP 2326412A1
Authority
EP
European Patent Office
Prior art keywords
mixing
container
facilitator
projection
component
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP09797569A
Other languages
German (de)
French (fr)
Other versions
EP2326412B1 (en
Inventor
Frédéric Bernard
Eric Chevalier
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sartorius Stedim Biotech SA
Original Assignee
Sartorius Stedim Biotech SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sartorius Stedim Biotech SA filed Critical Sartorius Stedim Biotech SA
Publication of EP2326412A1 publication Critical patent/EP2326412A1/en
Application granted granted Critical
Publication of EP2326412B1 publication Critical patent/EP2326412B1/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/70Spray-mixers, e.g. for mixing intersecting sheets of material
    • B01F25/72Spray-mixers, e.g. for mixing intersecting sheets of material with nozzles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/50Mixing liquids with solids
    • B01F23/51Methods thereof
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/50Mixing liquids with solids
    • B01F23/53Mixing liquids with solids using driven stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/808Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with stirrers driven from the bottom of the receptacle
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/50Mixing receptacles
    • B01F35/513Flexible receptacles, e.g. bags supported by rigid containers

Definitions

  • the invention relates to the mixing in a container of a content having a base component and a component to be mixed
  • the invention relates more particularly to a mixing method, a spraying and dispersing device, specially intended for the implementation of the mixing method and a mixing device, also specially intended for the implementation of the mixing process and including such a projection and dispersion device.
  • a method of mixing a content in a container of the type in which:
  • a container provided with means for introducing the components of the contents to be contained therein and to which may be associated means for mixing said content, the components of said content being available, at least one of which is substantially liquid (this component is hereinafter referred to as the “content base”) and at least one is intended to be mixed with the base of the contents (this component is hereafter referred to as a “mixing component” )
  • the components of the contents are introduced into the container and the various components in the container are mixed.
  • mixing and “mixing” is understood to mean the operation and the result of the operation, which consists of the fact that several distinct components form the same more or less viscous fluid phase or several phases with a high degree of homogenization.
  • a mixing method as just described is used for example in the case of bio-pharmaceutical fluids. It can then be implemented by means of a pocket of the type described in document FR-A-2 781 202.
  • Document FR-A-2 781 202 describes a plastic bag having two large walls and two bellows. Each bellows comprises two small walls connected to each other by an inner fold and each small wall is connected to the adjacent large wall by an outer fold. Such a pocket, once expanded, takes a three-dimensional shape (cylindrical, prismatic, parallelepipedic ...) and can have a volume of 50 liters or more, which justifies that some call it a 3D pocket.
  • the component to be mixed is in substantially solid form, in blocks or powder, while being able to be dissolved in the base of the contents.
  • such a component to be mixed in the absence of external action, may tend to float on the free surface of the base of the contents or to bulk. As a result, the dissolution of the component to be mixed and its mixing in the base of the contents are made difficult.
  • the component to be mixed is not in solid form but for example in the form of a gel, poorly or even immiscible in the base of the contents.
  • the high degree of homogenization that is then desired is made difficult to obtain.
  • US 2005/279687 discloses a water-gas pressurized device, especially for a multifunctional hydrogen peroxide machine.
  • the device in question comprises a hollow container having in the upper part, a water inlet, a gas inlet, a water collecting means disposed inside the hollow container, having lateral perforations which form outlet orifices of the nebulized water towards the inner face of the cylindrical wall of the hollow container.
  • the water is introduced via the inlet and is collected in the collector means. It leaves the collector means by perforations and is projected on the inner face of the cylindrical wall of the container. In its movement, it meets the gas flow introduced into the device via the corresponding arrival.
  • Such a device is not intended for the implementation of a mixing process such as that of the present invention.
  • projection and dispersion perforations these do not allow the projected product to reach substantially the entire free surface of the contents of the container, the projected product indeed reaching the inner face of the cylindrical wall hollow container.
  • the invention relates to a method of mixing a content in a container, of the type in which: on the one hand,
  • a container provided with means for introducing the components of the contents to be contained therein and to which may be associated means for mixing said contents,
  • the components of said content are available, at least one of which is substantially liquid (ie at least one substantially liquid component is referred to as the base of the contents) and at least one is intended to be mixed at the base of the contents (that is at least a component intended to be mixed is called a component to be mixed),
  • the components of the contents are introduced into the container and the various components in the container are mixed, characterized in that: on the one hand,
  • a mixing component is provided to form an integral part of said content by being mixed with the other components thereof, this mixing facilitator being liquid and having been specially selected for its compatibility with the required qualities of the content and its ability to promote the mixing operation of the component to be mixed in the content base,
  • a projection and dispersion device capable of being structurally associated with the container is provided at one of its introduction means (introduction means of the mixing facilitator), the said projection and dispersion device being able to find in a potentially or really active functional state in which it allows to project and disperse a liquid in the container, - then, on the other hand,
  • the base of the contents is introduced and then the component to be mixed into the container, without filling it, and
  • the projection and dispersion device then being associated with the introduction means of the mixing facilitator, the mixing facilitator is introduced into the container by the said introducing means, and is projected into the the dispersant to the component to be mixed by means of said projection and dispersion device returned to the potentially or really active functional state.
  • a component to be mixed in substantially solid form, in blocks or in powder which, in the absence of external action, tends to float on the free surface of the base of the contents, and one projects and scatters the mixing facilitator to wetting the floating mixing component on the surface of the base of the contents, this wetting facilitating the dissolution or dispersion of the component to be mixed in the base of the content and their mixture.
  • the mixing facilitator is projected by omni-directionally dispersing it over an opening angle to allow the mixing facilitator to substantially reach the entire free surface of the container contents and the floating mixing component which is There is in this realization.
  • the basic component in the first phase, is introduced into the container by an appropriate introduction means, distinct or not from the means for introducing the facilitator, whereas the projection and dispersion device is structurally associated with the means of introducing the facilitator and is in the inactive functional state.
  • the removable projection and dispersion device in the first phase, after having introduced into the container the basic component, the removable projection and dispersion device is structurally dissociated from the means for introducing the facilitator, and then the component to the container is introduced into the container. to mix by means of introduction of the facilitator.
  • the projection and dispersion device is structurally associated with the means of introduction of the facilitator, and then introduced into the container the mixing facilitator by the means of introduction of the facilitator.
  • the introduction, the projection and the dispersion of the mixing facilitator to the component to be mixed are continued, until a part of the component to be mixed is dissolved or dispersed in the base of the content. .
  • the mixing is started at the moment, or before or after the moment, when the introduction of the component to be mixed into the container is begun and the mixing is continued at least until the whole of the component to be mixed is mixed. dissolved or dispersed in the content base. According to one embodiment, there is a mixture of low to medium, depending on the components of the content, without the need for a strong mixture.
  • a closed container is used, except in the first phase for introducing into the container of the component to be mixed.
  • a container is used in the form of a foldable pouch with plastic bellows including a mixing means. More specifically, according to one embodiment, it starts from a collapsible bellows bag in the folded state and, in a preliminary phase, said bellows foldable pocket volume.
  • At least substantially the container is filled with the content base and / or the mixing facilitator, while the projection and dispersion device is associated with the means for introducing the facilitator.
  • the invention is directed to a projection and dispersion device, especially intended for the implementation of the mixing method which has just been described, which includes a wall provided on the one hand with peripheral means of structural association.
  • the wall is deformable between a substantially planar configuration when the said projection and dispersion device is in the inactive functional state and a convexly curved configuration turned towards the inside of the container when the said device of projection and dispersion is in the potentially or really active functional state, said curved configuration defining said omni directional dispersion on said opening angle, the wall being in its substantially flat configuration in the absence of external stress, in particular introducing the mixing facilitator and being responsive to the solicitation exerted on it by the mixing facilitator when introduced into the container so as to be in its curved configuration.
  • the wall is provided with perforations which, when the said projection and dispersion device is in the inactive functional state, are substantially closed and which, when the said projection and dispersion device is in the potentially or really active functional state, are open.
  • the wall is similar to that which has just been described, but rigid and not deformable.
  • the wall is provided with perforations which are always open, especially when said projection and dispersion device is in the active state inactive.
  • the perforations of a wall are identical to each other.
  • the perforations are differentiated from each other by their size and / or their shape according to their position on the wall and in order to best fulfill their function.
  • the peripheral means of structural association with a means for introducing a mixing facilitator of a container are in the form of an annular bead adapted to cooperate, removably, with complementary means.
  • means for introducing a mixing facilitator having the shape of an annular recess in the mixing facilitator introduction means.
  • the peripheral means of structural association with a means for introducing a mixing facilitator of a container are constituted by the wall formed by an elastically capable deformable part, by the tension which is exerted on it, to be enlarged and then strung on the collar that it can then grip and on which it is held removably.
  • the invention is directed to a mixing device specially designed for carrying out the mixing method described above, comprising:
  • a container provided with means for introducing components of the contents that it is intended to receive, including a means for introducing the mixing facilitator situated on its upper wall and in the form of an opening, the means for introducing the facilitator of mixing and the opening having an axis D, - mixing means of said content, associated with the container, and
  • a projection and dispersion device which comprises a wall provided on the one hand with peripheral means of structural association by means of introduction of a facilitator of mixing and, on the other hand, projection and dispersion perforations distributed over all or a substantial part of the surface intended to be located facing the opening and arranged omni directionally on an opening angle ( ⁇ ) around the axis D, able to allow the mixing facilitator (Fm) projected and dispersed by said projection and dispersion device to substantially reach the entire free surface (S) of the contents of the container, in particular the component to be mixed floating (Cm) that is there.
  • the container is closed except when the introduction means of the mixing facilitator is open.
  • the container is a foldable bag with plastic bellows including the mixing means.
  • the means for introducing the mixing facilitator is in the form of an opening formed by a peripheral collar adjoining the container, a cap with a liquid introduction port being mounted on the collar, the device for projection and dispersion being structurally associated, in a removable manner, by means of introduction of the mixing facilitator by its peripheral means of structural association cooperating with complementary means of the mixing facilitator introduction means.
  • FIG. 1 is a schematic view of the mixing method according to the invention; it comprises eight diagrams in perspective, respectively figure 1A, figure 1 B, figure
  • FIG. 3 is a diagrammatic cross-sectional view of the means for introducing the mixing facilitator forming part of a mixing device, to which is associated a projection and dispersion device, according to a first variant, which is in its functional state; inactive;
  • FIG. 4 is a schematic view similar to FIG. 3, the projection and dispersion device according to the first variant being in its active functional state;
  • FIG. 5 is a schematic elevational view of the projection and dispersion device according to the first variant in its active functional state;
  • FIG. 6 is a diagrammatic cross-sectional view of the means for introducing the mixing facilitator forming part of a mixing device, to which is associated a projection and dispersion device, according to a second variant, which is in its functional state; inactive.
  • a mixing device 1 specially designed for the implementation of the mixing method described above, comprises first of all a container 2.
  • the container 2 is closed, except when some introduction means 3 which it is provided and on which we will return is open ( Figures 1 D and 1 E).
  • the container 2 is a flexible pouch, foldable by means of bellows 4, plastic.
  • a pocket is for example a so-called 3D pocket of the general type described in document FR-A-2 781 202.
  • Such a bag 2 can have a volume that exceeds 50 I and reaches 3,000 I, which justifies that it can be described as a "large size" pocket.
  • such a pocket 2 When deployed and placed in volume, such a pocket 2 has a generally parallelepiped shape with a bottom wall 5, disposed substantially horizontally, four side walls 6, arranged substantially vertically, and an upper wall 7, disposed substantially horizontally.
  • Such a pocket 2 is intended to be used in association with a rigid rigid container 8 in which it is placed and removably.
  • container 2 may include rigid containers, which remain open permanently, metal, different capacity.
  • the container 2 is provided with means for introducing into the volume that it defines the components Co of the content C that it is intended to receive, able to allow these components to be introduced into this space, in the desired quantity.
  • these components Co, before being introduced into the container 2 are packaged in means provided for this purpose: tanks, cans, bags ...
  • the container 2 is provided with an introduction means 3 described as "means of introduction of the mixing facilitator".
  • the container 2 is provided with an introduction means 9 adapted to allow the introduction of a component of liquid constitution or, optionally, more or less viscous.
  • This introduction means 9 is different from the introduction means 3 or the same as him.
  • the container 2 comprises a larger number of such introduction means 3, 9.
  • the introduction means 3 is located on the upper wall 7 and the other separate introduction means 9 is located elsewhere, for example towards the junction between the bottom 5 and one side walls 6.
  • the introduction means 3 of the mixing facilitator is, in the embodiment shown in the drawings, in the form of an opening 10 formed and delimited by a peripheral flange 11 adjoining the upper wall 7 of the container and directed towards the outside of it.
  • the opening is here wide enough to allow the introduction of one or more components in solid form and more or less bulky.
  • a cap 12 provided with a liquid introduction port 13 is mounted on the flange 11, in a removable manner, by means of removable fastening means provided for this purpose.
  • the port 13 may have a structure identical to or similar to that of the corresponding port of the introduction means 9. This port 13 is therefore able to allow the introduction of a component of liquid constitution or, optionally, more or less pasty .
  • the introduction means 3 is versatile. When the cap 13 is mounted on the collar, it allows the introduction of a component of liquid constitution or, optionally, more or less pasty. When the cap 13 is removed from the collar, it allows the introduction of a component of solid constitution and more or less bulky.
  • the detachable fastening means of the cap 12 on the collar 1 1 are distinct from the cap 12 and attached to it, such as clamps. This achievement is not exclusive of others.
  • the mixing device 1 then comprises means 14 for mixing the content C of the container 2, associated with the container 2.
  • Such mixing means 14 per se, are known or within the abilities of those skilled in the art. It may be for example a mixing propeller mounted in the container on the bottom 5, driven by appropriate motor means.
  • the mixing device 1 finally comprises a device 15 for projection and dispersion.
  • the projection and dispersion device 15 is able to be associated structurally with the container 2, namely by means of introduction 3 of the mixing facilitator.
  • the projection and dispersion device 15 is structurally associated with the introduction means 3 of the mixing facilitator, in a removable manner, by means 16 of structural association device which it is provided arranged to cooperate with complementary means 17 provided with the introduction means 3 of mixing facilitator.
  • the peripheral means of structural association 16 are, in the embodiment shown in FIGS. 3 to 5 corresponding to a first variant, in the form of an annular bead adapted to cooperate, removably, with the complementary means 17 of which is equipped with the introduction means 3 for a mixing facilitator, in this case an annular recess in the means of introduction 3 of mixing facilitator, in particular between the collar 11 and the cap 12.
  • the peripheral means of structural association 16 are constituted by the wall 18 formed by a deformable part elastically adapted, by the tension that is exerted on it, to be widened and then strung on the collar 11 which it can then grip and on which it is held removably.
  • the projection and dispersion device 15 comprises a wall 18, which is provided at its periphery with means 16 of structural association, in particular the bead referred to above.
  • This wall 18 is provided with projection and dispersion perforations 19, distributed over all or a substantial part of the surface intended to be located facing the opening 10.
  • the perforations 19 of a wall 18 are identical to one another or, on the contrary, are differentiated from one another by their size and / or their shape according to their position on the wall 18 and this in order to best fulfill their function .
  • D is the axis - arranged generally vertically - of the opening 10 and the introduction means 3 of mixing facilitator.
  • the wall 18 is provided with projection and dispersion perforations 19 arranged omni-directionally over an opening angle ⁇ about the axis D, so as to allow the mixing facilitator Fm which is projected and dispersed by the device.
  • projection and dispersion 15 to substantially reach the entire free surface S of the contents of the container 2 and, as will be seen later in the embodiment aimed more specifically at a component to be mixed Cm in solid form, the said component to be mixed Cm lying at this free surface S and floating there.
  • the wall 18, made for example of a material such as silicone, is deformable between a substantially flat configuration (FIG. 3) and a convexly curved configuration turned towards the inside of the container. 2 and concavity turned towards the cap 12 and the port 13 (Figure 4).
  • the projection and dispersion device 15 is either associated with the container 2, namely with its introduction means 3 of mixing facilitator or dissociated from it. When it is associated, it is, when necessary in a potentially or really active functional state in which it allows to project and disperse a liquid introduced by the port 13 into the container 2. When no project and no does not disperse a liquid introduced by the port 13 into the container 2, the projection and dispersion device 15 is either in this same potentially or really active functional state or in an inactive functional state in which the introduction means 3 of the facilitator mixture is for example closed.
  • the wall 18 is in its substantially planar configuration (FIG. 3) when the projection and dispersion device 15 is in the inactive functional state. It is in its curved configuration (FIG. 4) when the projection and dispersion device 15 is in the potentially or actually active functional state.
  • the wall 18 is in its substantially flat configuration in the absence of external stress, including the introduction of a liquid through the port 13. It is responsive to the stress exerted on it by such a liquid introduced into the container through the port 13 and then, under the effect of the pressure exerted by the liquid in question, the curved configuration.
  • the perforations 19 are substantially closed, while they are open, when the projection and dispersion device 15 is at the same position. active functional state.
  • the wall 18 is similar to that described above, but it is rigid and not deformable. Such a rigid wall 18 can be either flat or curved as just described. Also, according to another embodiment, the wall 18, deformable or rigid, is provided with perforations 19 which are always open, especially when said projection and dispersion device 15 is in the inactive functional state.
  • the method according to the invention aims to ensure the mixing of the content C found in the container 2.
  • This content C comprises several distinct components Co, which are mixed in the container 2, thanks to the mixing device 1 which has just been described, notably thanks to the projection and dispersion device 15.
  • One of the components Co is substantially liquid. By this we mean that it is totally in liquid form or that it has a more or less pasty form. As indicated above, this component is hereafter conventionally called “content base” Cb.
  • One of the components Co is intended to be mixed at the base of the content Cb. As indicated above, this component is hereinafter conventionally referred to as “component to be mixed” Cm.
  • the number of these components is not limited to two. It can be provided several components forming the base of the content Cb, and / or several components forming the component to be mixed Cm.
  • the component to be mixed Cm has a substantially solid form, being either in blocks or in powder form. This component is apt, if it is miscible with the base of the content Cb to be dissolved in it, or if it is not miscible with it to be nevertheless dispersed in it with a high degree of homogenization.
  • the component to be mixed Cm has a fluid form and it is not miscible in the base of the content Cb.
  • This is for example a gel, suspended in the content base Cb.
  • the invention finds its interest in the case of a component to be mixed Cm in substantially solid form which, in the absence of external action, tends to float at the free surface S of the content base Cb.
  • One of the components Co is intended to be an integral part of the content C being mixed with the other components Cb and Cm thereof.
  • This component is liquid and has been specially selected for its compatibility with the required qualities of the content C and its ability to promote the mixing operation of the component to be mixed Cm in the content base Cb.
  • This component is conventionally referred to as a "mixing facilitator".
  • the mixing facilitator Fm is of the same nature as the content base Cb or, conversely, of a different nature.
  • the mixing facilitator Fm is water.
  • a first phase of the process (FIGS. 1C to 1F) the base of the content Cb is introduced and the component to be mixed Cm into the container 2 without completely filling it.
  • the method comprises a preliminary phase in which said volume is adjusted.
  • Foldable pocket with bellows and placed in the resistant container 8 ( Figures 1A and 1B).
  • the projection and dispersion device 15 is structurally associated with the introduction means 3 of the mixing facilitator by cooperating the respective means 16 and 17.
  • the projection and dispersion device 15 is then in the inactive functional state.
  • the base component Cb is introduced into the container 2 by the appropriate introduction means 9 provided for this purpose, distinct or not from the introduction means 3 of the mixing facilitator.
  • the basic component CB does not completely fill the container 2 and has a free surface S.
  • FIG. 1 The operation which has just been described is illustrated by FIG.
  • the projection and dispersion device 15 of the introduction means 3 of the mixing facilitator is structurally dissociated.
  • the cap 12 is removed, the projection and dispersion device 15 is removed and the opening 10 is left free.
  • FIG. 1 The operation that has just been described is illustrated by FIG. 1
  • the mixing component Cm is introduced into the container 2 via the introduction means 3 of the mixing facilitator, more precisely through the opening 10. This is possible even for a component to be mixed in solid form, because of sufficient size given at opening 10.
  • the component to be mixed Cm in solid form, may tend to float on the free surface S of the base of the content Cb.
  • FIG. 15 The operation which has just been described is illustrated by FIG. In a separate and subsequent second phase, the projection and dispersion device 15 is again associated with the introduction means 3 of the mixing facilitator by cooperating the respective means 16 and 17.
  • the mixing facilitator Fm is introduced into the container 2 by the introduction means 3 provided for this purpose.
  • the wall 18 which was in its substantially flat configuration is placed in its curved configuration, under the effect of the stress exerted on it by the mixing facilitator introduced through port 13.
  • the mixing facilitator is projected by dispersing it towards the base of the content Cb and towards the component to be mixed Cm.
  • the mixing facilitator Fm is projected and dispersed as just indicated to humidify the mixing component Cm which floats on the free surface S of the content base Cm.
  • the mixing facilitator Fm is projected by omni-directionally dispersing it over an opening angle ⁇ so that the mixing facilitator Fm substantially reaches the entire free surface S of the contents of the container 2 and the component to mix floating Cm found therein, in this variant embodiment.
  • the introduction, the projection and the dispersion of the mixing facilitator Fm to the component to be mixed Cm are continued, until a part of the component to be mixed Cm is dissolved or sufficiently dispersed in the base of the content.
  • Cb it is not essential to continue the projection and dispersion of the mixing facilitator Fm until the totality of the component to be mixed Cm is dissolved or dispersed in the base of the content Cb.
  • FIG. 1 The operation which has just been described is illustrated by FIG.
  • the contents of the container 2 are mixed by the mixing means 14.
  • the mixing is begun, at the moment, or most often before the moment, but also possibly after the moment, when the introduction of the component to be mixed Cm into the container (FIG. 1 E) is begun and the mixing is continued at least until at the moment when the whole of the component to be mixed is dissolved or dispersed in the base of the contents (FIG. 1H). This moment is generally subsequent to that when the introduction, the projection and the dispersion of the mixing facilitator Fm to the component to be mixed Cm are terminated.
  • the invention makes it possible to carry out a mixture of low to medium power, and this depending on the components Cb, Cm, content. It is not essential to use a mixture of high power, with the benefits that result.
  • the method also comprises a final phase in which at least substantially the container 2 is filled with the content base Cb and / or the mixing facilitator Fm, while the projection and dispersion device is associated with the introduction means 3 of the facilitator of mixing.
  • FIG. 1 The operation which has just been described is illustrated by FIG.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Containers And Packaging Bodies Having A Special Means To Remove Contents (AREA)
  • Packging For Living Organisms, Food Or Medicinal Products That Are Sensitive To Environmental Conditiond (AREA)
  • Nozzles (AREA)

Abstract

A mixing process, a spraying and dispersing device, and a mixing device for implementing the process. In the process, components are introduced into a container equipped with introduction elements and mixing elements and the contents are mixed. A mixing facilitator is provided, a spraying and dispersing device that can be connected to the container at one of its introduction element is provided, able to be in an active functional state in which it makes it possible to spray and to disperse a liquid in the container, and then, in a first phase, the base of the contents and then the components to be mixed are introduced into the container, without filling the latter, and in a second phase, the mixing facilitator is introduced into the container via an introduction element, and it is sprayed and dispersed to the components to be mixed by the spraying and dispersing device that is put into the active functional state.

Description

Mélange dans un conteneur d'un contenu ayant un composant de base et un composant à mélanger Mixing in a container of a content having a basic component and a component to be mixed
L'invention est relative au mélange dans un conteneur d'un contenu ayant un composant de base et un composant à mélangerThe invention relates to the mixing in a container of a content having a base component and a component to be mixed
L'invention concerne plus spécialement un procédé de mélange, un dispositif de projection et de dispersion, spécialement destiné à la mise en œuvre du procédé de mélange et un dispositif de mélange, également spécialement destiné à la mise en œuvre du procédé de mélange et incluant un tel dispositif de projection et de dispersion.The invention relates more particularly to a mixing method, a spraying and dispersing device, specially intended for the implementation of the mixing method and a mixing device, also specially intended for the implementation of the mixing process and including such a projection and dispersion device.
On connaît déjà un procédé de mélange d'un contenu se trouvant dans un conteneur, du type dans lequel :A method of mixing a content in a container, of the type in which:
• d'une part, - on dispose d'un conteneur pourvu de moyens d'introduction des composants du contenu devant s'y trouver et auquel peuvent être associés des moyens de mélange du dit contenu, - on dispose des composants du dit contenu, dont au moins un est substantiellement liquide (ce composant est dénommé par la suite conventionnellement « base du contenu ») et au moins un est destiné à être mélangé à la base du contenu (ce composant est dénommé par la suite conventionnellement « composant à mélanger »),On the one hand, there is a container provided with means for introducing the components of the contents to be contained therein and to which may be associated means for mixing said content, the components of said content being available, at least one of which is substantially liquid (this component is hereinafter referred to as the "content base") and at least one is intended to be mixed with the base of the contents (this component is hereafter referred to as a "mixing component" )
• puis, d'autre part, on introduit dans le conteneur les composants du contenu et on mélange les différents composants se trouvant dans le conteneur.And then, on the other hand, the components of the contents are introduced into the container and the various components in the container are mixed.
On entend par « mélanger » et « mélange », l'opération et le résultat de l'opération qui consiste à ce que plusieurs composants distincts forment une même phase fluide plus ou moins visqueuse ou plusieurs phases avec un degré d'homogénéisation élevé.The term "mixing" and "mixing" is understood to mean the operation and the result of the operation, which consists of the fact that several distinct components form the same more or less viscous fluid phase or several phases with a high degree of homogenization.
Un procédé de mélange tel qu'il vient d'être décrit est utilisé par exemple dans le cas de fluides bio-pharmaceutiques. Il peut alors être mis en œuvre au moyen d'une poche du type de celle décrite dans le document FR-A-2 781 202.A mixing method as just described is used for example in the case of bio-pharmaceutical fluids. It can then be implemented by means of a pocket of the type described in document FR-A-2 781 202.
Le document FR-A-2 781 202 décrit en effet une poche en matière plastique ayant deux grandes parois et deux soufflets. Chaque soufflet comprend deux petites parois reliées l'une à l'autre par un pli interne et chaque petite paroi est reliée à la grande paroi adjacente par un pli externe. Une telle poche, une fois expansée, prend une forme tridimensionnelle (cylindrique, prismatique, parallélépipédique...) et peut avoir un volume de 50 litres, voire plus, ce qui justifie que certains l'appellent poche 3D. Dans certains cas, le composant à mélanger est sous forme substantiellement solide, en blocs ou en poudre, tout en étant apte à être dissous dans la base du contenu. Typiquement, un tel composant à mélanger, en l'absence d'action extérieure, peut tendre à flotter à la surface libre de la base du contenu ou à prendre en masse. Il en résulte que la dissolution du composant à mélanger et son mélange dans la base du contenu sont rendus difficiles.Document FR-A-2 781 202 describes a plastic bag having two large walls and two bellows. Each bellows comprises two small walls connected to each other by an inner fold and each small wall is connected to the adjacent large wall by an outer fold. Such a pocket, once expanded, takes a three-dimensional shape (cylindrical, prismatic, parallelepipedic ...) and can have a volume of 50 liters or more, which justifies that some call it a 3D pocket. In some cases, the component to be mixed is in substantially solid form, in blocks or powder, while being able to be dissolved in the base of the contents. Typically, such a component to be mixed, in the absence of external action, may tend to float on the free surface of the base of the contents or to bulk. As a result, the dissolution of the component to be mixed and its mixing in the base of the contents are made difficult.
Pour tenter de surmonter cette difficulté, on a proposé de procéder à une opération de mélange forte, c'est-à-dire puissante, ce qui pose à son tour d'autres problèmes tel que l'apparition de mousse. En outre, dans certains cas, le contenu à mélanger peut se dégrader si le mélange qu'il subit est puissant.In an attempt to overcome this difficulty, it has been proposed to carry out a strong mixing operation, that is to say powerful, which in turn poses other problems such as the appearance of foam. In addition, in some cases, the content to be mixed can be degraded if the mixture it undergoes is powerful.
Dans d'autres cas, le composant à mélanger n'est pas sous forme solide mais par exemple sous forme d'un gel, mal ou même non miscible dans la base du contenu. Le degré d'homogénéisation élevé qui est alors souhaité est rendu difficile à obtenir.In other cases, the component to be mixed is not in solid form but for example in the form of a gel, poorly or even immiscible in the base of the contents. The high degree of homogenization that is then desired is made difficult to obtain.
Le document US 2005/279687 décrit un dispositif de mélange eau-gaz sous pression, tout spécialement destiné à une machine multifonctionnelle à eau oxygénée. Le dispositif en question comporte un contenant creux ayant en partie supérieure, une arrivée d'eau, une arrivée de gaz, un moyen collecteur d'eau disposé à l'intérieur du contenant creux, ayant des perforations latérales qui forment des orifices de sortie de l'eau nébulisée en direction la face interne de la paroi cylindrique du contenant creux. Avec un tel dispositif, l'eau est introduite via l'arrivée et est collectée dans le moyen collecteur. Elle sort du moyen collecteur par des perforations et est projetée sur la face interne de la paroi cylindrique du contenant. Dans son mouvement, elle rencontre le flux gazeux introduit dans le dispositif via l'arrivée correspondante. Un tel dispositif n'est pas destiné à la mise en œuvre d'un procédé de mélange tel que celui de la présente invention. De plus, s'il comporte des perforations de projection et de dispersion, celles-ci ne permettent pas au produit projeté d'atteindre substantiellement toute la surface libre du contenu du conteneur, le produit projeté atteignant en effet la face interne de la paroi cylindrique du contenant creux.US 2005/279687 discloses a water-gas pressurized device, especially for a multifunctional hydrogen peroxide machine. The device in question comprises a hollow container having in the upper part, a water inlet, a gas inlet, a water collecting means disposed inside the hollow container, having lateral perforations which form outlet orifices of the nebulized water towards the inner face of the cylindrical wall of the hollow container. With such a device, the water is introduced via the inlet and is collected in the collector means. It leaves the collector means by perforations and is projected on the inner face of the cylindrical wall of the container. In its movement, it meets the gas flow introduced into the device via the corresponding arrival. Such a device is not intended for the implementation of a mixing process such as that of the present invention. In addition, if it has projection and dispersion perforations, these do not allow the projected product to reach substantially the entire free surface of the contents of the container, the projected product indeed reaching the inner face of the cylindrical wall hollow container.
Il existe donc un problème lorsque l'on souhaite mélanger dans un conteneur une base du contenu et un composant à mélanger solide ou non - ou difficilement - miscible, lorsque ce dernier tend à flotter à la surface libre de la base du contenu ou à prendre en masse ou ne peut être mélangé avec le degré d'homogénéisation souhaité, ou encore lorsque l'opération de mélange est trop puissante. L'invention a donc pour but de pallier ces problèmes.There is therefore a problem when it is desired to mix in a container a base of the content and a component to mix solid or not - or difficultly - miscible, when the latter tends to float on the free surface of the base of the content or to take in bulk or can not be mixed with the desired degree of homogenization, or when the mixing operation is too powerful. The invention therefore aims to overcome these problems.
A cet effet, et selon un premier aspect, l'invention vise un procédé de mélange d'un contenu se trouvant dans un conteneur, du type dans lequel : - d'une part,For this purpose, and according to a first aspect, the invention relates to a method of mixing a content in a container, of the type in which: on the one hand,
- on dispose d'un conteneur pourvu de moyens d'introduction des composants du contenu devant s'y trouver et auquel peuvent être associés des moyens de mélange du dit contenu,a container provided with means for introducing the components of the contents to be contained therein and to which may be associated means for mixing said contents,
- on dispose des composants du dit contenu, dont au moins un est substantiellement liquide (ce dit au moins un composant substantiellement liquide est dénommé base du contenu) et au moins un est destiné à être mélangé à la base du contenu (ce dit au moins un composant destiné à être mélangé est dénommé composant à mélanger),the components of said content are available, at least one of which is substantially liquid (ie at least one substantially liquid component is referred to as the base of the contents) and at least one is intended to be mixed at the base of the contents (that is at least a component intended to be mixed is called a component to be mixed),
• puis, d'autre part, on introduit dans le conteneur les composants du contenu et on mélange les différents composants se trouvant dans le conteneur, caractérisé par le fait que : - d'une part,And then, on the other hand, the components of the contents are introduced into the container and the various components in the container are mixed, characterized in that: on the one hand,
- on dispose d'un composant - facilitateur de mélange - destiné à faire partie intégrante du dit contenu en étant mélangé aux autres composants de celui-ci, ce facilitateur de mélange étant liquide et ayant été spécialement sélectionné pour sa compatibilité avec les qualités requises du contenu et sa capacité à favoriser l'opération de mélange du composant à mélanger dans la base du contenu,a mixing component is provided to form an integral part of said content by being mixed with the other components thereof, this mixing facilitator being liquid and having been specially selected for its compatibility with the required qualities of the content and its ability to promote the mixing operation of the component to be mixed in the content base,
- on dispose d'un dispositif de projection et de dispersion apte à être associé structurellement au conteneur à l'un de ses moyens d'introduction (moyen d'introduction du facilitateur de mélange), le dit dispositif de projection et de dispersion pouvant se trouver dans un état fonctionnel potentiellement ou réellement actif dans lequel il permet de projeter et de disperser un liquide dans le conteneur, - puis, d'autre part,a projection and dispersion device capable of being structurally associated with the container is provided at one of its introduction means (introduction means of the mixing facilitator), the said projection and dispersion device being able to find in a potentially or really active functional state in which it allows to project and disperse a liquid in the container, - then, on the other hand,
- dans une première phase, on introduit la base du contenu puis le composant à mélanger dans le conteneur, sans remplir celui-ci, etin a first phase, the base of the contents is introduced and then the component to be mixed into the container, without filling it, and
- dans une deuxième phase distincte ultérieure, le dispositif de projection et de dispersion étant alors associé au moyen d'introduction du facilitateur de mélange, on introduit le facilitateur de mélange dans le conteneur par le dit moyen d'introduction, et on le projette en le dispersant vers le composant à mélanger au moyen du dit dispositif de projection et de dispersion rendu à l'état fonctionnel potentiellement ou réellement actif.in a second distinct subsequent phase, the projection and dispersion device then being associated with the introduction means of the mixing facilitator, the mixing facilitator is introduced into the container by the said introducing means, and is projected into the the dispersant to the component to be mixed by means of said projection and dispersion device returned to the potentially or really active functional state.
Selon une réalisation, on dispose d'un composant à mélanger sous forme substantiellement solide, en blocs ou en poudre, qui, en l'absence d'action extérieure, tend à flotter à la surface libre de la base du contenu, et on projette et disperse le facilitateur de mélange pour humidifier le composant à mélanger flottant à la surface de la base du contenu, cette humidification facilitant la dissolution ou la dispersion du composant à mélanger dans la base du contenu et leur mélange.According to one embodiment, there is provided a component to be mixed in substantially solid form, in blocks or in powder, which, in the absence of external action, tends to float on the free surface of the base of the contents, and one projects and scatters the mixing facilitator to wetting the floating mixing component on the surface of the base of the contents, this wetting facilitating the dissolution or dispersion of the component to be mixed in the base of the content and their mixture.
Selon une réalisation, on projette le facilitateur de mélange en le dispersant de façon omni directionnelle sur un angle d'ouverture apte à permettre au facilitateur de mélange d'atteindre substantiellement toute la surface libre du contenu du conteneur et le composant à mélanger flottant qui s'y trouve, dans cette réalisation.In one embodiment, the mixing facilitator is projected by omni-directionally dispersing it over an opening angle to allow the mixing facilitator to substantially reach the entire free surface of the container contents and the floating mixing component which is There is in this realization.
Selon une première réalisation, on dispose d'un facilitateur de mélange de même nature que le ou l'un des composants de la base du contenu. Selon une seconde réalisation, on dispose d'un facilitateur de mélange d'une nature différente des composants de la base du contenu.According to a first embodiment, there is a mixing facilitator of the same nature as the one or one of the components of the content base. According to a second embodiment, there is a mixing facilitator of a different nature of the components of the content base.
Selon une réalisation, dans la première phase, on introduit dans le conteneur le composant de base par un moyen d'introduction approprié, distinct ou non du moyen d'introduction du facilitateur, alors que le dispositif de projection et de dispersion est associé structurellement au moyen d'introduction du facilitateur et se trouve à l'état fonctionnel inactif.According to one embodiment, in the first phase, the basic component is introduced into the container by an appropriate introduction means, distinct or not from the means for introducing the facilitator, whereas the projection and dispersion device is structurally associated with the means of introducing the facilitator and is in the inactive functional state.
Selon une réalisation, dans la première phase, après avoir introduit dans le conteneur le composant de base, on dissocie structurellement le dispositif de projection et de dispersion, amovible, du moyen d'introduction du facilitateur, puis on introduit dans le conteneur le composant à mélanger par le moyen d'introduction du facilitateur.According to one embodiment, in the first phase, after having introduced into the container the basic component, the removable projection and dispersion device is structurally dissociated from the means for introducing the facilitator, and then the component to the container is introduced into the container. to mix by means of introduction of the facilitator.
Selon une réalisation, après avoir introduit dans le conteneur le composant à mélanger, on associe structurellement le dispositif de projection et de dispersion au moyen d'introduction du facilitateur, puis on introduit dans le conteneur le facilitateur de mélange par le moyen d'introduction du facilitateur.According to one embodiment, after having introduced into the container the component to be mixed, the projection and dispersion device is structurally associated with the means of introduction of the facilitator, and then introduced into the container the mixing facilitator by the means of introduction of the facilitator.
Selon une réalisation, dans la deuxième phase, on poursuit l'introduction, la projection et la dispersion du facilitateur de mélange vers le composant à mélanger, jusqu'au moment où une partie du composant à mélanger est dissous ou dispersé dans la base du contenu.According to one embodiment, in the second phase, the introduction, the projection and the dispersion of the mixing facilitator to the component to be mixed are continued, until a part of the component to be mixed is dissolved or dispersed in the base of the content. .
Selon une réalisation, on commence le mélange au moment, ou avant ou après le moment, où on commence l'introduction du composant à mélanger dans le conteneur et on poursuit le mélange au moins jusqu'au moment où la totalité du composant à mélanger est dissous ou dispersé dans la base du contenu. Selon une réalisation, on procède à un mélange de faible à moyen, en fonction des composants du contenu, sans nécessité d'un mélange fort.According to one embodiment, the mixing is started at the moment, or before or after the moment, when the introduction of the component to be mixed into the container is begun and the mixing is continued at least until the whole of the component to be mixed is mixed. dissolved or dispersed in the content base. According to one embodiment, there is a mixture of low to medium, depending on the components of the content, without the need for a strong mixture.
Selon une réalisation, on met en œuvre un conteneur clos, sauf dans la première phase pour l'introduction dans le conteneur du composant à mélanger.According to one embodiment, a closed container is used, except in the first phase for introducing into the container of the component to be mixed.
Selon une réalisation, on met en oeuvre un conteneur sous la forme d'une poche pliable à soufflets en matière plastique incluant un moyen de mélange. Plus précisément, selon une réalisation, on part d'une poche pliable à soufflets à l'état pliée et, dans une phase préliminaire, on met en volume ladite poche pliable à soufflets.According to one embodiment, a container is used in the form of a foldable pouch with plastic bellows including a mixing means. More specifically, according to one embodiment, it starts from a collapsible bellows bag in the folded state and, in a preliminary phase, said bellows foldable pocket volume.
Selon une réalisation, dans une phase finale, on remplit au moins substantiellement le conteneur avec la base du contenu et/ou le facilitateur de mélange, alors que le dispositif de projection et de dispersion est associé au moyen d'introduction du facilitateur.According to one embodiment, in a final phase, at least substantially the container is filled with the content base and / or the mixing facilitator, while the projection and dispersion device is associated with the means for introducing the facilitator.
Selon un deuxième aspect, l'invention vise un dispositif de projection et de dispersion, spécialement destiné à la mise en œuvre du procédé de mélange qui vient d'être décrit qui inclut une paroi pourvue d'une part des moyens périphériques d'association structurelle à un moyen d'introduction de facilitateur de mélange d'un conteneur ayant une ouverture et un axe D et, d'autre part, des perforations de projection et de dispersion réparties sur toute ou une partie substantielle de la surface destinée à être située en regard de l'ouverture et disposées de façon omni directionnelle sur un angle d'ouverture (α) autour de l'axe D, apte à permettre au facilitateur de mélange (Fm) projeté et dispersé par le dit dispositif de projection et de dispersion d'atteindre substantiellement toute la surface libre (S) du contenu du conteneur, notamment le composant à mélanger flottant (Cm) qui s'y trouve.According to a second aspect, the invention is directed to a projection and dispersion device, especially intended for the implementation of the mixing method which has just been described, which includes a wall provided on the one hand with peripheral means of structural association. means for introducing a mixing facilitator of a container having an aperture and an axis D and, on the other hand, projection and dispersion perforations distributed over all or a substantial portion of the surface to be located in view of the aperture and arranged omni directionally on an opening angle (α) about the axis D, adapted to allow the mixing facilitator (Fm) projected and dispersed by said projection and dispersion device d substantially reach the entire free surface (S) of the contents of the container, including the floating mixing component (Cm) therein.
Selon une première variante de réalisation, la paroi est déformable entre une configuration substantiellement plane lorsque le dit dispositif de projection et de dispersion se trouve à l'état fonctionnel inactif et une configuration incurvée à convexité tournée vers l'intérieur du conteneur lorsque le dit dispositif de projection et de dispersion se trouve à l'état fonctionnel potentiellement ou réellement actif, ladite configuration incurvée définissant ladite dispersion omni directionnelle sur le dit angle d'ouverture, la paroi étant dans sa configuration substantiellement plane en l'absence de sollicitation extérieure, notamment d'introduction du facilitateur de mélange et étant responsive à la sollicitation exercée sur elle par le facilitateur de mélange lors de son introduction dans le conteneur de manière à être dans alors sa configuration incurvée. Selon une réalisation, la paroi est pourvue de perforations qui, lorsque le dit dispositif de projection et de dispersion se trouve à l'état fonctionnel inactif, sont substantiellement fermées et qui, lorsque le dit dispositif de projection et de dispersion se trouve à l'état fonctionnel potentiellement ou réellement actif, sont ouvertes.According to a first variant embodiment, the wall is deformable between a substantially planar configuration when the said projection and dispersion device is in the inactive functional state and a convexly curved configuration turned towards the inside of the container when the said device of projection and dispersion is in the potentially or really active functional state, said curved configuration defining said omni directional dispersion on said opening angle, the wall being in its substantially flat configuration in the absence of external stress, in particular introducing the mixing facilitator and being responsive to the solicitation exerted on it by the mixing facilitator when introduced into the container so as to be in its curved configuration. According to one embodiment, the wall is provided with perforations which, when the said projection and dispersion device is in the inactive functional state, are substantially closed and which, when the said projection and dispersion device is in the potentially or really active functional state, are open.
Selon une seconde variante de réalisation, la paroi est analogue à celle qui vient d'être décrite, mais rigide et non pas déformable.According to a second variant embodiment, the wall is similar to that which has just been described, but rigid and not deformable.
Selon une autre réalisation, la paroi est pourvue de perforations qui sont toujours ouvertes, notamment lorsque le dit dispositif de projection et de dispersion se trouve à l'état fonctionnel in actif.In another embodiment, the wall is provided with perforations which are always open, especially when said projection and dispersion device is in the active state inactive.
Selon une première réalisation, les perforations d'une paroi sont identiques entre elles. Selon une seconde réalisation, les perforations sont différenciées les unes des autres par leur taille et/ou leur forme selon leur position sur la paroi et ce afin de remplir au mieux leur fonction.According to a first embodiment, the perforations of a wall are identical to each other. According to a second embodiment, the perforations are differentiated from each other by their size and / or their shape according to their position on the wall and in order to best fulfill their function.
Selon une première variante de réalisation, les moyens périphériques d'association structurelle à un moyen d'introduction de facilitateur de mélange d'un conteneur se présentent sous la forme d'un bourrelet annulaire apte à coopérer, de façon amovible, avec des moyens complémentaires du moyen d'introduction de facilitateur de mélange ayant la forme d'un creux annulaire ménagé dans le moyen d'introduction de facilitateur de mélange.According to a first variant embodiment, the peripheral means of structural association with a means for introducing a mixing facilitator of a container are in the form of an annular bead adapted to cooperate, removably, with complementary means. means for introducing a mixing facilitator having the shape of an annular recess in the mixing facilitator introduction means.
Selon une seconde variante de réalisation, les moyens périphériques d'association structurelle à un moyen d'introduction de facilitateur de mélange d'un conteneur sont constitués par la paroi formée par une pièce déformable élastiquement apte, par la tension que l'on exerce sur elle, à être élargie puis enfilée sur la collerette qu'elle peut alors enserrer et sur laquelle elle est maintenue de façon amovible.According to a second variant embodiment, the peripheral means of structural association with a means for introducing a mixing facilitator of a container are constituted by the wall formed by an elastically capable deformable part, by the tension which is exerted on it, to be enlarged and then strung on the collar that it can then grip and on which it is held removably.
Selon un troisième aspect, l'invention vise un dispositif de mélange spécialement destiné à la mise en œuvre du procédé de mélange décrit plus haut, comprenant :According to a third aspect, the invention is directed to a mixing device specially designed for carrying out the mixing method described above, comprising:
- un conteneur pourvu de moyens d'introduction de composants du contenu qu'il est destiné à recevoir, dont un moyen d'introduction du facilitateur de mélange situé sur sa paroi supérieure et en forme d'une ouverture, le moyen d'introduction de facilitateur de mélange et l'ouverture ayant un axe D, - des moyens de mélange du dit contenu, associés au conteneur, eta container provided with means for introducing components of the contents that it is intended to receive, including a means for introducing the mixing facilitator situated on its upper wall and in the form of an opening, the means for introducing the facilitator of mixing and the opening having an axis D, - mixing means of said content, associated with the container, and
- un dispositif de projection et de dispersion qui comporte une paroi pourvue, d'une part, des moyens périphériques d'association structurelle au moyen d'introduction de facilitateur de mélange et, d'autre part, de perforations de projection et de dispersion réparties sur toute ou une partie substantielle de la surface destinée à être située en regard de l'ouverture et disposées de façon omni directionnelle sur un angle d'ouverture (α) autour de l'axe D, apte à permettre au facilitateur de mélange (Fm) projeté et dispersé par le dit dispositif de projection et de dispersion d'atteindre substantiellement toute la surface libre (S) du contenu du conteneur, notamment le composant à mélanger flottant (Cm) qui s'y trouve.a projection and dispersion device which comprises a wall provided on the one hand with peripheral means of structural association by means of introduction of a facilitator of mixing and, on the other hand, projection and dispersion perforations distributed over all or a substantial part of the surface intended to be located facing the opening and arranged omni directionally on an opening angle (α) around the axis D, able to allow the mixing facilitator (Fm) projected and dispersed by said projection and dispersion device to substantially reach the entire free surface (S) of the contents of the container, in particular the component to be mixed floating (Cm) that is there.
Selon une réalisation, le conteneur est clos, sauf lorsque moyen d'introduction du facilitateur de mélange est ouvert.In one embodiment, the container is closed except when the introduction means of the mixing facilitator is open.
Selon une réalisation, le conteneur est une poche pliable à soufflets en matière plastique incluant le moyen de mélange.In one embodiment, the container is a foldable bag with plastic bellows including the mixing means.
Selon une réalisation, le moyen d'introduction du facilitateur de mélange se présente sous la forme d'une ouverture formée par une collerette périphérique attenante au conteneur, une coiffe avec un port d'introduction de liquide étant montée sur la collerette, le dispositif de projection et de dispersion étant associé structurellement, de façon amovible, au moyen d'introduction du facilitateur de mélange par ses moyens périphériques d'association structurelle coopérant avec des moyens complémentaires du moyen d'introduction de facilitateur de mélange.According to one embodiment, the means for introducing the mixing facilitator is in the form of an opening formed by a peripheral collar adjoining the container, a cap with a liquid introduction port being mounted on the collar, the device for projection and dispersion being structurally associated, in a removable manner, by means of introduction of the mixing facilitator by its peripheral means of structural association cooperating with complementary means of the mixing facilitator introduction means.
On décrit maintenant plusieurs modes de réalisation de l'invention à l'aide des dessins dans lesquels : la figure 1 est une vue schématique du procédé de mélange selon l'invention ; elle comporte huit schémas en perspective, respectivement figure 1A, figure 1 B, figureSeveral embodiments of the invention will now be described with the aid of the drawings in which: FIG. 1 is a schematic view of the mixing method according to the invention; it comprises eight diagrams in perspective, respectively figure 1A, figure 1 B, figure
1 C, figure 1 D, figure 1 E, figure 1 F, figure 1 G et figure 1 H, correspondant à des étapes successives du procédé, la première étant représentée par la figure 1A et la dernière par la figure 1 H ; la figure 2 est une vue schématique en perspective correspondant à la figure 1 G à plus grande échelle ; la figure 3 est une vue schématique en coupe transversale du moyen d'introduction du facilitateur de mélange faisant partie d'un dispositif de mélange, auquel est associé un dispositif de projection et de dispersion, selon une première variante, se trouvant dans son état fonctionnel inactif ; - la figure 4 est une vue schématique analogue à la figure 3, le dispositif de projection et de dispersion selon la première variante se trouvant dans son état fonctionnel actif ; Ia figure 5 est une vue schématique en élévation du dispositif de projection et de dispersion selon la première variante se trouvant dans son état fonctionnel actif ; la figure 6 est une vue schématique en coupe transversale du moyen d'introduction du facilitateur de mélange faisant partie d'un dispositif de mélange, auquel est associé un dispositif de projection et de dispersion, selon une seconde variante, se trouvant dans son état fonctionnel inactif.1 C, Figure 1 D, Figure 1 E, Figure 1 F, Figure 1 G and Figure 1 H, corresponding to successive steps of the method, the first being shown in Figure 1A and the last in Figure 1 H; Figure 2 is a schematic perspective view corresponding to Figure 1 G on a larger scale; FIG. 3 is a diagrammatic cross-sectional view of the means for introducing the mixing facilitator forming part of a mixing device, to which is associated a projection and dispersion device, according to a first variant, which is in its functional state; inactive; FIG. 4 is a schematic view similar to FIG. 3, the projection and dispersion device according to the first variant being in its active functional state; FIG. 5 is a schematic elevational view of the projection and dispersion device according to the first variant in its active functional state; FIG. 6 is a diagrammatic cross-sectional view of the means for introducing the mixing facilitator forming part of a mixing device, to which is associated a projection and dispersion device, according to a second variant, which is in its functional state; inactive.
Un dispositif de mélange 1 spécialement destiné à la mise en œuvre du procédé de mélange exposé ci-dessus, comprend tout d'abord un conteneur 2.A mixing device 1 specially designed for the implementation of the mixing method described above, comprises first of all a container 2.
Dans la réalisation représentée, le conteneur 2 est clos, sauf lorsqu'un certain moyen d'introduction 3 dont il est pourvu et sur lequel on reviendra est ouvert (figures 1 D et 1 E).In the embodiment shown, the container 2 is closed, except when some introduction means 3 which it is provided and on which we will return is open (Figures 1 D and 1 E).
Dans la réalisation représentée, le conteneur 2 est une poche souple, pliable au moyen de soufflets 4, en matière plastique. Une telle poche est par exemple une poche dite 3D du type général décrit dans le document FR-A-2 781 202.In the embodiment shown, the container 2 is a flexible pouch, foldable by means of bellows 4, plastic. Such a pocket is for example a so-called 3D pocket of the general type described in document FR-A-2 781 202.
Une telle poche 2 peut avoir un volume qui dépasse 50 I et atteint 3.000 I, ce qui justifie qu'elle puisse être qualifiée de poche de « grande taille ».Such a bag 2 can have a volume that exceeds 50 I and reaches 3,000 I, which justifies that it can be described as a "large size" pocket.
Lorsqu'elle est déployée et mise en volume, une telle poche 2 présente une forme générale parallélépipédique avec une paroi de fond 5, disposé sensiblement horizontalement, quatre parois latérales 6, disposées sensiblement verticalement, et une paroi supérieure 7, disposée sensiblement horizontalement.When deployed and placed in volume, such a pocket 2 has a generally parallelepiped shape with a bottom wall 5, disposed substantially horizontally, four side walls 6, arranged substantially vertically, and an upper wall 7, disposed substantially horizontally.
Une telle poche 2 est destinée à être utilisée en association avec un conteneur rigide résistant 8 dans laquelle elle est placée et ce de façon amovible.Such a pocket 2 is intended to be used in association with a rigid rigid container 8 in which it is placed and removably.
Il est entendu que l'invention s'applique à d'autres types de conteneur 2. Il peut s'agir notamment de conteneurs rigides, qui restent ouverts en permanence, en métal, de contenance différente.It is understood that the invention applies to other types of container 2. It may include rigid containers, which remain open permanently, metal, different capacity.
Le conteneur 2 est pourvu de moyens d'introduction dans le volume qu'il définit des composants Co du contenu C qu'il est destiné à recevoir, aptes à permettre d'introduire ces composants dans cet espace, en quantité voulue. En effet, ces composants Co, avant que d'être introduits dans le conteneur 2 sont conditionnés dans des moyens prévus à cet effet : réservoirs, bidons, poches... En l'espèce, il est prévu que le conteneur 2 est pourvu d'un moyen d'introduction 3 qualifié de « moyen d'introduction du facilitateur de mélange ».The container 2 is provided with means for introducing into the volume that it defines the components Co of the content C that it is intended to receive, able to allow these components to be introduced into this space, in the desired quantity. Indeed, these components Co, before being introduced into the container 2 are packaged in means provided for this purpose: tanks, cans, bags ... In this case, it is expected that the container 2 is provided with an introduction means 3 described as "means of introduction of the mixing facilitator".
II est prévu également que le conteneur 2 est pourvu d'un moyen d'introduction 9 apte à permettre l'introduction d'un composant de constitution liquide ou, éventuellement, plus ou moins visqueux.It is also expected that the container 2 is provided with an introduction means 9 adapted to allow the introduction of a component of liquid constitution or, optionally, more or less viscous.
Ce moyen d'introduction 9 est différent du moyen d'introduction 3 ou le même que lui.This introduction means 9 is different from the introduction means 3 or the same as him.
Le cas échéant, le conteneur 2 comporte un plus grand nombre de tels moyens d'introduction 3, 9.Where appropriate, the container 2 comprises a larger number of such introduction means 3, 9.
Dans la réalisation représentée sur les dessins, le moyen d'introduction 3 est situé sur la paroi supérieure 7 et l'autre moyen d'introduction 9, distinct, est situé ailleurs, par exemple vers la jonction entre le fond 5 et l'une des parois latérales 6.In the embodiment shown in the drawings, the introduction means 3 is located on the upper wall 7 and the other separate introduction means 9 is located elsewhere, for example towards the junction between the bottom 5 and one side walls 6.
Le moyen d'introduction 3 du facilitateur de mélange se présente, dans la réalisation représentée sur les dessins, sous la forme d'une ouverture 10 formée et délimitée par une collerette périphérique 11 attenante à la paroi supérieure 7 du conteneur et dirigée vers l'extérieur de celui-ci. L'ouverture est ici suffisamment large pour permettre l'introduction d'un ou de plusieurs composants sous forme solide et plus ou moins volumineux.The introduction means 3 of the mixing facilitator is, in the embodiment shown in the drawings, in the form of an opening 10 formed and delimited by a peripheral flange 11 adjoining the upper wall 7 of the container and directed towards the outside of it. The opening is here wide enough to allow the introduction of one or more components in solid form and more or less bulky.
Une coiffe 12 pourvue d'un port 13 d'introduction de liquide est montée sur la collerette 1 1 , de façon amovible, grâce à des moyens de fixation amovible prévus à cet effet.A cap 12 provided with a liquid introduction port 13 is mounted on the flange 11, in a removable manner, by means of removable fastening means provided for this purpose.
Le port 13 peut avoir une structure identique, analogue ou voisine de celle du port correspondant du moyen d'introduction 9. Ce port 13 est donc apte à permettre l'introduction d'un composant de constitution liquide ou, éventuellement, plus ou moins pâteux.The port 13 may have a structure identical to or similar to that of the corresponding port of the introduction means 9. This port 13 is therefore able to allow the introduction of a component of liquid constitution or, optionally, more or less pasty .
Ainsi, le moyen d'introduction 3 est polyvalent. Lorsque la coiffe 13 est montée sur la collerette, il permet l'introduction d'un composant de constitution liquide ou, éventuellement, plus ou moins pâteux. Lorsque la coiffe 13 est enlevée de la collerette, il permet l'introduction d'un composant de constitution solide et plus ou moins volumineux. Dans une réalisation, les moyens de fixation amovible de la coiffe 12 sur la collerette 1 1 sont distincts de la coiffe 12 et rapportés sur elle, tels que des colliers de fixation. Cette réalisation n'est pas exclusive d'autres.Thus, the introduction means 3 is versatile. When the cap 13 is mounted on the collar, it allows the introduction of a component of liquid constitution or, optionally, more or less pasty. When the cap 13 is removed from the collar, it allows the introduction of a component of solid constitution and more or less bulky. In one embodiment, the detachable fastening means of the cap 12 on the collar 1 1 are distinct from the cap 12 and attached to it, such as clamps. This achievement is not exclusive of others.
Le dispositif de mélange 1 comprend ensuite des moyens de mélange 14 du contenu C du conteneur 2, associés au conteneur 2.The mixing device 1 then comprises means 14 for mixing the content C of the container 2, associated with the container 2.
De tels moyens de mélange 14, en soi, sont connus ou à la portée de l'homme du métier. Il peut s'agir par exemple d'une hélice de mélange montée dans le conteneur sur le fond 5, mue par des moyens moteurs appropriés.Such mixing means 14, per se, are known or within the abilities of those skilled in the art. It may be for example a mixing propeller mounted in the container on the bottom 5, driven by appropriate motor means.
Le dispositif de mélange 1 comprend enfin un dispositif 15 de projection et de dispersion.The mixing device 1 finally comprises a device 15 for projection and dispersion.
Le dispositif de projection et de dispersion 15 est apte à être associé structurellement au conteneur 2, à savoir au moyen d'introduction 3 du facilitateur de mélange.The projection and dispersion device 15 is able to be associated structurally with the container 2, namely by means of introduction 3 of the mixing facilitator.
Plus précisément, le dispositif de projection et de dispersion 15 est associé structurellement au moyen d'introduction 3 du facilitateur de mélange, de façon amovible, par des moyens 16 périphériques d'association structurelle dont il est pourvu agencés pour coopérer avec des moyens 17 complémentaires dont est pourvu le moyen d'introduction 3 de facilitateur de mélange.More specifically, the projection and dispersion device 15 is structurally associated with the introduction means 3 of the mixing facilitator, in a removable manner, by means 16 of structural association device which it is provided arranged to cooperate with complementary means 17 provided with the introduction means 3 of mixing facilitator.
Les moyens périphériques d'association structurelle 16 se présentent, dans la réalisation représentée sur les figures 3 à 5 correspondant à une première variante, sous la forme d'un bourrelet annulaire apte à coopérer, de façon amovible, avec les moyens 17 complémentaires dont est pourvu le moyen d'introduction 3 de facilitateur de mélange, en l'espèce un creux annulaire ménagé dans le moyen d'introduction 3 de facilitateur de mélange, notamment entre la collerette 1 1 et la coiffe 12.The peripheral means of structural association 16 are, in the embodiment shown in FIGS. 3 to 5 corresponding to a first variant, in the form of an annular bead adapted to cooperate, removably, with the complementary means 17 of which is equipped with the introduction means 3 for a mixing facilitator, in this case an annular recess in the means of introduction 3 of mixing facilitator, in particular between the collar 11 and the cap 12.
Selon une autre réalisation représentée sur la figure 6 correspondant à une seconde variante, les moyens périphériques d'association structurelle 16 sont constitués par la paroi 18 formée par une pièce déformable élastiquement apte, par la tension que l'on exerce sur elle, à être élargie puis enfilée sur la collerette 11 qu'elle peut alors enserrer et sur laquelle elle est maintenue de façon amovible. Le dispositif de projection et de dispersion 15, comporte une paroi 18, laquelle est pourvue à sa périphérie des moyens 16 d'association structurelle, notamment le bourrelet dont il a été question plus haut.According to another embodiment shown in FIG. 6 corresponding to a second variant, the peripheral means of structural association 16 are constituted by the wall 18 formed by a deformable part elastically adapted, by the tension that is exerted on it, to be widened and then strung on the collar 11 which it can then grip and on which it is held removably. The projection and dispersion device 15 comprises a wall 18, which is provided at its periphery with means 16 of structural association, in particular the bead referred to above.
Cette paroi 18 est pourvue de perforations 19 de projection et de dispersion, réparties sur toute ou une partie substantielle de la surface destinée à être située en regard de l'ouverture 10.This wall 18 is provided with projection and dispersion perforations 19, distributed over all or a substantial part of the surface intended to be located facing the opening 10.
Selon les cas, les perforations 19 d'une paroi 18 sont identiques entre elles ou, au contraire sont différenciées les unes des autres par leur taille et/ou leur forme selon leur position sur la paroi 18 et ce afin de remplir au mieux leur fonction.Depending on the case, the perforations 19 of a wall 18 are identical to one another or, on the contrary, are differentiated from one another by their size and / or their shape according to their position on the wall 18 and this in order to best fulfill their function .
On définit par D, l'axe - disposé généralement verticalement - de l'ouverture 10 et du moyen d'introduction 3 de facilitateur de mélange.D is the axis - arranged generally vertically - of the opening 10 and the introduction means 3 of mixing facilitator.
La paroi 18 est pourvue de perforations 19 de projection et de dispersion disposées de façon omni directionnelle sur un angle d'ouverture α, autour de l'axe D, de manière à permettre au facilitateur de mélange Fm qui est projeté et dispersé par le dispositif de projection et de dispersion 15 d'atteindre substantiellement toute la surface libre S du contenu du conteneur 2 et, comme on le verra par la suite dans la réalisation visant plus spécialement un composant à mélanger Cm sous forme solide, le dit composant à mélanger Cm se trouvant à cette surface libre S et y flottant.The wall 18 is provided with projection and dispersion perforations 19 arranged omni-directionally over an opening angle α about the axis D, so as to allow the mixing facilitator Fm which is projected and dispersed by the device. projection and dispersion 15 to substantially reach the entire free surface S of the contents of the container 2 and, as will be seen later in the embodiment aimed more specifically at a component to be mixed Cm in solid form, the said component to be mixed Cm lying at this free surface S and floating there.
Dans une première variante de réalisation représentée sur les figures, la paroi 18, réalisée par exemple en une matière telle que du silicone, est déformable entre une configuration substantiellement plane (figure 3) et une configuration incurvée à convexité tournée vers l'intérieur du conteneur 2 et concavité tournée vers la coiffe 12 et le port 13 (figure 4).In a first embodiment shown in the figures, the wall 18, made for example of a material such as silicone, is deformable between a substantially flat configuration (FIG. 3) and a convexly curved configuration turned towards the inside of the container. 2 and concavity turned towards the cap 12 and the port 13 (Figure 4).
Le dispositif de projection et de dispersion 15 est soit associé au conteneur 2, à savoir à son moyen d'introduction 3 de facilitateur de mélange soit dissocié de lui. Lorsqu'il est associé, il se trouve, lorsque cela est nécessaire dans un état fonctionnel potentiellement ou réellement actif dans lequel il permet de projeter et de disperser un liquide introduit par le port 13 dans le conteneur 2. Lorsqu'on ne projette et ne disperse pas un liquide introduit par le port 13 dans le conteneur 2, le dispositif de projection et de dispersion 15 est soit dans ce même état fonctionnel potentiellement ou réellement actif soit dans un état fonctionnel inactif dans lequel le moyen d'Introduction 3 du facilitateur de mélange est par exemple fermé. La paroi 18 est dans sa configuration substantiellement plane (figure 3) lorsque le dispositif de projection et de dispersion 15 se trouve à l'état fonctionnel inactif. Elle est dans sa configuration incurvée (figure 4) lorsque le dispositif de projection et de dispersion 15 se trouve à l'état fonctionnel potentiellement ou réellement actif.The projection and dispersion device 15 is either associated with the container 2, namely with its introduction means 3 of mixing facilitator or dissociated from it. When it is associated, it is, when necessary in a potentially or really active functional state in which it allows to project and disperse a liquid introduced by the port 13 into the container 2. When no project and no does not disperse a liquid introduced by the port 13 into the container 2, the projection and dispersion device 15 is either in this same potentially or really active functional state or in an inactive functional state in which the introduction means 3 of the facilitator mixture is for example closed. The wall 18 is in its substantially planar configuration (FIG. 3) when the projection and dispersion device 15 is in the inactive functional state. It is in its curved configuration (FIG. 4) when the projection and dispersion device 15 is in the potentially or actually active functional state.
La paroi 18 est dans sa configuration substantiellement plane en l'absence de sollicitation extérieure, notamment d'introduction d'un liquide par le port 13. Elle est responsive à la sollicitation exercée sur elle par un tel liquide introduit dans le conteneur par le port 13 et prend alors, sous l'effet de la pression exercée par le liquide en question, la configuration incurvée.The wall 18 is in its substantially flat configuration in the absence of external stress, including the introduction of a liquid through the port 13. It is responsive to the stress exerted on it by such a liquid introduced into the container through the port 13 and then, under the effect of the pressure exerted by the liquid in question, the curved configuration.
Dans la réalisation envisagée, lorsque le dispositif de projection et de dispersion 15 se trouve à l'état fonctionnel inactif, les perforations 19 sont substantiellement fermées, tandis qu'elles sont ouvertes, lorsque le dispositif de projection et de dispersion 15 se trouve à l'état fonctionnel actif.In the embodiment envisaged, when the projection and dispersion device 15 is in the inactive functional state, the perforations 19 are substantially closed, while they are open, when the projection and dispersion device 15 is at the same position. active functional state.
La réalisation du dispositif de projection et de dispersion 15 qui vient d'être décrite n'est pas exclusive d'autres, de nature ou structure différentes, remplissant la même fonction et procurant des résultats identiques ou analogues. Ainsi, selon une seconde variante de réalisation, la paroi 18 est analogue à celle qui précédemment décrite, mais elle est rigide et non pas déformable. Une telle paroi 18 rigide peut être soit plane soit incurvée comme il vient d'être décrit. Egalement, selon une autre réalisation, la paroi 18, déformable ou rigide, est pourvue de perforations 19 qui sont toujours ouvertes, notamment lorsque le dit dispositif de projection et de dispersion 15 se trouve à l'état fonctionnel inactif.The embodiment of the projection and dispersion device 15 which has just been described is not exclusive of others, of a different nature or structure, fulfilling the same function and providing identical or similar results. Thus, according to a second embodiment, the wall 18 is similar to that described above, but it is rigid and not deformable. Such a rigid wall 18 can be either flat or curved as just described. Also, according to another embodiment, the wall 18, deformable or rigid, is provided with perforations 19 which are always open, especially when said projection and dispersion device 15 is in the inactive functional state.
Le procédé selon l'invention vise à assurer le mélange du contenu C se trouvant dans le conteneur 2.The method according to the invention aims to ensure the mixing of the content C found in the container 2.
Ce contenu C comporte plusieurs composants Co, distincts qui sont mélangés dans le conteneur 2, grâce au dispositif de mélange 1 qui vient d'être décrit, notamment grâce au dispositif de projection et de dispersion 15.This content C comprises several distinct components Co, which are mixed in the container 2, thanks to the mixing device 1 which has just been described, notably thanks to the projection and dispersion device 15.
L'un des composants Co est substantiellement liquide. On entend par là qu'il est totalement sous forme liquide ou qu'il a une forme plus ou moins pâteuse. Comme indiqué plus haut, ce composant est dénommé par la suite conventionnellement « base du contenu » Cb. L'un des composants Co est destiné à être mélangé à la base du contenu Cb. Comme indiqué plus haut, ce composant est dénommé par la suite conventionnellement « composant à mélanger » Cm.One of the components Co is substantially liquid. By this we mean that it is totally in liquid form or that it has a more or less pasty form. As indicated above, this component is hereafter conventionally called "content base" Cb. One of the components Co is intended to be mixed at the base of the content Cb. As indicated above, this component is hereinafter conventionally referred to as "component to be mixed" Cm.
II est entendu que le nombre de ces composants n'est pas limité à deux. Il peut être prévu plusieurs composants formant la base du contenu Cb, et/ou plusieurs composants formant le composant à mélanger Cm.It is understood that the number of these components is not limited to two. It can be provided several components forming the base of the content Cb, and / or several components forming the component to be mixed Cm.
Dans l'application plus spécialement décrite ici, le composant à mélanger Cm a une forme substantiellement solide, étant soit en blocs soit en poudre. Ce composant est apte, s'il est miscible avec la base du contenu Cb à être dissous dans elle, ou s'il n'est pas miscible avec elle à être néanmoins dispersé dans elle avec un degré d'homogénéisation élevé.In the application more specifically described herein, the component to be mixed Cm has a substantially solid form, being either in blocks or in powder form. This component is apt, if it is miscible with the base of the content Cb to be dissolved in it, or if it is not miscible with it to be nevertheless dispersed in it with a high degree of homogenization.
Selon une autre réalisation, le composant à mélanger Cm a une forme fluide et il n'est pas miscible dans la base du contenu Cb. Il s'agit par exemple d'un gel, mis en suspension dans la base du contenu Cb.According to another embodiment, the component to be mixed Cm has a fluid form and it is not miscible in the base of the content Cb. This is for example a gel, suspended in the content base Cb.
Plus spécialement, l'invention trouve tout son intérêt dans le cas d'un composant à mélanger Cm sous forme substantiellement solide qui, en l'absence d'action extérieure, tend à flotter à la surface libre S de la base du contenu Cb.More specifically, the invention finds its interest in the case of a component to be mixed Cm in substantially solid form which, in the absence of external action, tends to float at the free surface S of the content base Cb.
L'un des composants Co est destiné à faire partie intégrante du contenu C en étant mélangé aux autres composants Cb et Cm de celui-ci. Ce composant est liquide et il a été spécialement sélectionné pour sa compatibilité avec les qualités requises du contenu C et sa capacité à favoriser l'opération de mélange du composant à mélanger Cm dans la base du contenu Cb. Ce composant est dénommé conventionnellement « facilitateur de mélange ».One of the components Co is intended to be an integral part of the content C being mixed with the other components Cb and Cm thereof. This component is liquid and has been specially selected for its compatibility with the required qualities of the content C and its ability to promote the mixing operation of the component to be mixed Cm in the content base Cb. This component is conventionally referred to as a "mixing facilitator".
Selon les cas, le facilitateur de mélange Fm est de même nature que la base du contenu Cb ou, au contraire, d'une nature différente. Dans une réalisation, le facilitateur de mélange Fm est de l'eau.Depending on the case, the mixing facilitator Fm is of the same nature as the content base Cb or, conversely, of a different nature. In one embodiment, the mixing facilitator Fm is water.
Dans une première phase du procédé (figures 1 C à 1 F), on introduit la base du contenu Cb puis le composant à mélanger Cm dans le conteneur 2, sans remplir totalement celui-ci.In a first phase of the process (FIGS. 1C to 1F), the base of the content Cb is introduced and the component to be mixed Cm into the container 2 without completely filling it.
Dans la mesure où l'on part d'une poche 2 pliable à soufflets se trouvant initialement à l'état plié, le procédé comporte une phase préliminaire dans laquelle on met en volume ladite poche pliable à soufflets et on la place dans le conteneur résistant 8 (figures 1A et 1 B). De telles opérations sont en soi connues ou à la portée de l'homme du métier.Insofar as starting from a collapsible gusseted bag 2 initially located in the folded state, the method comprises a preliminary phase in which said volume is adjusted. Foldable pocket with bellows and placed in the resistant container 8 (Figures 1A and 1B). Such operations are in themselves known or within the abilities of those skilled in the art.
Dans cette situation, et dans la première phase, on associe structurellement le dispositif de projection et de dispersion 15 au moyen d'introduction 3 du facilitateur de mélange en faisant coopérer les moyens respectifs 16 et 17.In this situation, and in the first phase, the projection and dispersion device 15 is structurally associated with the introduction means 3 of the mixing facilitator by cooperating the respective means 16 and 17.
Le dispositif de projection et de dispersion 15 se trouve alors à l'état fonctionnel inactif.The projection and dispersion device 15 is then in the inactive functional state.
Dans cette situation, on introduit dans le conteneur 2 le composant de base Cb par le moyen d'introduction 9 approprié prévu à cet effet, distinct ou non du moyen d'introduction 3 du facilitateur de mélange.In this situation, the base component Cb is introduced into the container 2 by the appropriate introduction means 9 provided for this purpose, distinct or not from the introduction means 3 of the mixing facilitator.
Comme indiqué, le composant de base CB ne remplit pas totalement le conteneur 2 et il présente une surface libre S.As indicated, the basic component CB does not completely fill the container 2 and has a free surface S.
L'opération qui vient d'être décrite est illustrée par la figure 1 C.The operation which has just been described is illustrated by FIG.
Dans la même première phase, après avoir introduit dans le conteneur 2 le composant de base Cb, on dissocie structurellement le dispositif de projection et de dispersion 15 du moyen d'introduction 3 du facilitateur de mélange.In the same first phase, after having introduced in the container 2 the basic component Cb, the projection and dispersion device 15 of the introduction means 3 of the mixing facilitator is structurally dissociated.
Pour ce faire, on enlève la coiffe 12, on ôte le dispositif de projection et de dispersion 15 et on laisse libre l'ouverture 10.To do this, the cap 12 is removed, the projection and dispersion device 15 is removed and the opening 10 is left free.
L'opération qui vient d'être décrite est illustrée par la figure 1 D.The operation that has just been described is illustrated by FIG.
Dans cette situation, on introduit dans le conteneur 2 le composant à mélanger Cm par le moyen d'introduction 3 du facilitateur de mélange, plus précisément par l'ouverture 10. Cela est possible même pour un composant à mélanger sous forme solide, du fait de la taille suffisante donnée à l'ouverture 10.In this situation, the mixing component Cm is introduced into the container 2 via the introduction means 3 of the mixing facilitator, more precisely through the opening 10. This is possible even for a component to be mixed in solid form, because of sufficient size given at opening 10.
Comme indiqué, le composant à mélanger Cm, sous forme solide, peut avoir tendance à flotter à la surface libre S de la base du contenu Cb.As indicated, the component to be mixed Cm, in solid form, may tend to float on the free surface S of the base of the content Cb.
L'opération qui vient d'être décrite est illustrée par la figure 1 E. Dans une deuxième phase distincte et ultérieure, on associe de nouveau le dispositif de projection et de dispersion 15 au moyen d'introduction 3 du facilitateur de mélange en faisant coopérer les moyens respectifs 16 et 17.The operation which has just been described is illustrated by FIG. In a separate and subsequent second phase, the projection and dispersion device 15 is again associated with the introduction means 3 of the mixing facilitator by cooperating the respective means 16 and 17.
Dans cette situation, on introduit le facilitateur de mélange Fm dans le conteneur 2 par le moyen d'introduction 3 prévu à cet effet.In this situation, the mixing facilitator Fm is introduced into the container 2 by the introduction means 3 provided for this purpose.
Grâce à la présence du dispositif de projection et de dispersion 15, alors rendu à l'état fonctionnel actif, la paroi 18 qui était dans sa configuration substantiellement plane se place dans sa configuration incurvée, sous l'effet de la sollicitation exercée sur elle par le facilitateur de mélange introduit par le port 13.Thanks to the presence of the projection and dispersion device 15, then rendered in the active functional state, the wall 18 which was in its substantially flat configuration is placed in its curved configuration, under the effect of the stress exerted on it by the mixing facilitator introduced through port 13.
Ce faisant, on projette le facilitateur de mélange en le dispersant vers la base du contenu Cb et vers le composant à mélanger Cm.In doing so, the mixing facilitator is projected by dispersing it towards the base of the content Cb and towards the component to be mixed Cm.
On projette et disperse le facilitateur de mélange Fm comme il vient d'être indiqué, pour humidifier le composant à mélanger Cm qui flotte à la surface libre S de la base du contenu Cm.The mixing facilitator Fm is projected and dispersed as just indicated to humidify the mixing component Cm which floats on the free surface S of the content base Cm.
C'est cette humidification qui facilite la dissolution ou la dispersion du composant à mélanger Cm dans la base du contenu Cb et leur mélange respectif.It is this humidification which facilitates the dissolution or dispersion of the component to be mixed Cm in the base of the content Cb and their respective mixture.
Comme il résulte de la description qui précède, on projette le facilitateur de mélange Fm en le dispersant de façon omni directionnelle sur un angle d'ouverture α de manière que le facilitateur de mélange Fm atteigne substantiellement toute la surface libre S du contenu du conteneur 2 et le composant à mélanger Cm flottant qui s'y trouve, dans cette variante de réalisation.As is apparent from the foregoing description, the mixing facilitator Fm is projected by omni-directionally dispersing it over an opening angle α so that the mixing facilitator Fm substantially reaches the entire free surface S of the contents of the container 2 and the component to mix floating Cm found therein, in this variant embodiment.
Dans cette deuxième phase, on poursuit l'introduction, la projection et la dispersion du facilitateur de mélange Fm vers le composant à mélanger Cm, jusqu'au moment où une partie du composant à mélanger Cm est dissous ou suffisamment dispersée dans la base du contenu Cb. En général, il n'est pas indispensable de poursuivre la projection et la dispersion du facilitateur de mélange Fm jusqu'à ce que la totalité du composant à mélanger Cm est dissous ou dispersée dans la base du contenu Cb.In this second phase, the introduction, the projection and the dispersion of the mixing facilitator Fm to the component to be mixed Cm are continued, until a part of the component to be mixed Cm is dissolved or sufficiently dispersed in the base of the content. Cb. In general, it is not essential to continue the projection and dispersion of the mixing facilitator Fm until the totality of the component to be mixed Cm is dissolved or dispersed in the base of the content Cb.
L'opération qui vient d'être décrite est illustrée par la figure 1 G. On réalise le mélange du contenu du conteneur 2 grâce aux moyens de mélange 14.The operation which has just been described is illustrated by FIG. The contents of the container 2 are mixed by the mixing means 14.
On commence le mélange, au moment, ou le plus souvent avant le moment, mais également possiblement après le moment, où on commence l'introduction du composant à mélanger Cm dans le conteneur (figure 1 E) et on poursuit le mélange au moins jusqu'au moment où la totalité du composant à mélanger est dissous ou dispersé dans la base du contenu (figure 1 H). Ce moment est généralement postérieur à celui où on termine l'introduction, la projection et la dispersion du facilitateur de mélange Fm vers le composant à mélanger Cm.The mixing is begun, at the moment, or most often before the moment, but also possibly after the moment, when the introduction of the component to be mixed Cm into the container (FIG. 1 E) is begun and the mixing is continued at least until at the moment when the whole of the component to be mixed is dissolved or dispersed in the base of the contents (FIG. 1H). This moment is generally subsequent to that when the introduction, the projection and the dispersion of the mixing facilitator Fm to the component to be mixed Cm are terminated.
L'invention autorise de procéder à un mélange de faible à moyenne puissance, et ce en fonction des composants Cb, Cm, du contenu. Il n'est pas indispensable d'avoir recours à un mélange de forte puissance, avec les avantages qui en découlent.The invention makes it possible to carry out a mixture of low to medium power, and this depending on the components Cb, Cm, content. It is not essential to use a mixture of high power, with the benefits that result.
Le procédé comporte également une phase finale dans laquelle on remplit au moins substantiellement le conteneur 2 avec la base du contenu Cb et/ou le facilitateur de mélange Fm, alors que le dispositif de projection et de dispersion est associé au moyen d'introduction 3 du facilitateur de mélange.The method also comprises a final phase in which at least substantially the container 2 is filled with the content base Cb and / or the mixing facilitator Fm, while the projection and dispersion device is associated with the introduction means 3 of the facilitator of mixing.
L'opération qui vient d'être décrite est illustrée par la figure 1 H. The operation which has just been described is illustrated by FIG.

Claims

REVENDICATIONS
1. Procédé de mélange d'un contenu (C) se trouvant dans un conteneur (2), du type dans lequel : - d'une part,A method of mixing a content (C) in a container (2), of the type in which: - on the one hand,
- on dispose d'un conteneur (2) pourvu de moyens d'introduction des composants Co du contenu (C) devant s'y trouver et auquel peuvent être associés des moyens de mélange (14) du dit contenu (C),a container (2) provided with means for introducing the components Co of the content (C) to be there and to which may be associated mixing means (14) of said content (C),
- on dispose des composants du dit contenu (C), dont au moins un est substantiellement liquide (base du contenu Cb) et au moins un est destiné à être mélangé à la base du contenu (composant à mélanger),the components of said content (C) are available, at least one of which is substantially liquid (content base Cb) and at least one is intended to be mixed with the base of the content (component to be mixed),
• puis, d'autre part, on introduit dans le conteneur (2) les composants du contenu (C) et on mélange les différents composants se trouvant dans le conteneur (2), caractérisé par le fait que - d'une part,And then, on the other hand, the components of the contents (C) are introduced into the container (2) and the various components in the container (2) are mixed, characterized in that - on the one hand,
- on dispose d'un composant - facilitateur de mélange Fm - destiné à faire partie intégrante du dit contenu (C) en étant mélangé aux autres composants de celui-ci, ce facilitateur de mélange (Fm) étant liquide et ayant été spécialement sélectionné pour sa compatibilité avec les qualités requises du contenu (C) et sa capacité à favoriser l'opération de mélange du composant à mélanger dans la base du contenu (Cb),a component - a mixing facilitator Fm - is provided, intended to be an integral part of said content (C), being mixed with the other components thereof, this mixing facilitator (Fm) being liquid and having been specially selected for its compatibility with the required qualities of the content (C) and its ability to promote the mixing operation of the component to be mixed in the content base (Cb),
- on dispose d'un dispositif de projection et de dispersion (15) apte à être associé structurellement au conteneur (2) à l'un de ses moyens d'introduction (moyen d'introduction (3) du facilitateur de mélange), le dit dispositif de projection et de dispersion (15) pouvant se trouver dans un état fonctionnel potentiellement ou réellement actif dans lequel il permet de projeter et de disperser un liquide dans le conteneur (2), - puis, d'autre part,a projection and dispersion device (15) capable of being structurally associated with the container (2) is provided at one of its introduction means (introduction means (3) of the mixing facilitator); said projection and dispersion device (15) which can be in a potentially or really active functional state in which it allows to project and disperse a liquid in the container (2), - then, on the other hand,
- dans une première phase, on introduit la base du contenu (Cb) puis le composant à mélanger (Cm) dans le conteneur (2), sans remplir celui-ci, etin a first phase, introducing the base of the content (Cb) then the component to be mixed (Cm) into the container (2), without filling it, and
- dans une deuxième phase distincte ultérieure, le dispositif de projection et de dispersion (15) étant alors associé au moyen d'introduction (3) du facilitateur de mélange, on introduit le facilitateur de mélange (Fm) dans le conteneur (2) par le dit moyen d'introduction (3), et on le projette en le dispersant vers le composant à mélanger (Cm) au moyen du dit dispositif de projection et de dispersion (15) rendu à l'état fonctionnel potentiellement ou réellement actif.in a second distinct subsequent phase, the projection and dispersion device (15) being then associated with the introduction means (3) of the mixing facilitator, the mixing facilitator (Fm) is introduced into the container (2) by said introduction means (3), and is projected by dispersing it to the component to be mixed (Cm) by means of said projection and dispersion device (15) returned to the potentially or actually active functional state.
2. Procédé de mélange selon la revendication 1 , caractérisé par le fait que l'on dispose d'un composant à mélanger (Cm) sous forme fluide non ou mal miscible dans la base du contenu (Cb), par exemple un gel. 2. A method of mixing according to claim 1, characterized in that it has a mixing component (Cm) in fluid form not or miscible in the base of the content (Cb), for example a gel.
3. Procédé de mélange selon la revendication 1 , caractérisé par le fait que l'on dispose d'un composant à mélanger (Cm) sous forme substantiellement solide, en blocs ou en poudre, apte à être dissous ou dispersé avec un degré d'homogénéisation élevé dans la base du contenu (Cb).3. A method of mixing according to claim 1, characterized in that one has a mixing component (Cm) in substantially solid form, in blocks or powder, capable of being dissolved or dispersed with a degree of high homogenization in the content base (Cb).
4. Procédé de mélange selon la revendication 3, caractérisé par le fait que l'on dispose d'un composant à mélanger (Cm) sous forme substantiellement solide, en blocs ou en poudre, qui, en l'absence d'action extérieure, tend à flotter à la surface libre (S) de la base du contenu (Cb), et on projette et disperse le facilitateur de mélange (Fm) pour humidifier le composant à mélanger (Cm) flottant à la surface (S) de la base du contenu (Cb), cette humidification facilitant la dissolution ou la dispersion du composant à mélanger (Cm) dans la base du contenu (Cb) et leur mélange.4. A method of mixing according to claim 3, characterized in that one has a component to be mixed (Cm) in substantially solid form, in blocks or powder, which, in the absence of external action, tends to float on the free surface (S) of the base of the contents (Cb), and the mixing facilitator (Fm) is sprayed and dispersed to moisten the mixing component (Cm) floating on the surface (S) of the base content (Cb), this wetting facilitating the dissolution or dispersion of the component to mix (Cm) in the base of the content (Cb) and mixing.
5. Procédé de mélange selon la revendication 4, caractérisé par le fait que l'on projette le facilitateur de mélange (Fm) en le dispersant de façon omni directionnelle sur un angle d'ouverture (α) apte à permettre au facilitateur de mélange (Fm) d'atteindre substantiellement toute la surface libre (S) du contenu du conteneur (2) et le composant à mélanger (Cm) flottant qui s'y trouve.5. Mixing method according to claim 4, characterized in that the mixing facilitator (Fm) is projected by omni-directionally dispersing it over an opening angle (α) suitable for allowing the mixing facilitator ( Fm) to substantially reach the entire free area (S) of the contents of the container (2) and the floating mixing component (Cm) therein.
6. Procédé de mélange selon l'une quelconque des revendications 1 à 5, caractérisé par le fait que l'on dispose d'un facilitateur de mélange (Fm) de même nature que le ou l'un des composants de la base du contenu (Cb).6. A method of mixing according to any one of claims 1 to 5, characterized in that one has a mixing facilitator (Fm) of the same nature as the one or one of the components of the content base (Cb).
7. Procédé de mélange selon l'une quelconque des revendications 1 à 5, caractérisé par le fait que l'on dispose d'un facilitateur de mélange (Fm) d'une nature différente des composants de la base du contenu (Cb).7. A method of mixing according to any one of claims 1 to 5, characterized in that it has a mixing facilitator (Fm) of a different nature of the components of the content base (Cb).
8. Procédé de mélange selon l'une quelconque des revendications 1 à 7, caractérisé par le fait que dans la première phase, on introduit dans le conteneur (2) le composant de base par un moyen d'introduction (9) approprié, distinct ou non du moyen d'introduction (3) du facilitateur, alors que le dispositif de projection et de dispersion (15) est associé structurellement au moyen d'introduction (3) du facilitateur et se trouve à l'état fonctionnel in actif. 8. Mixing process according to any one of claims 1 to 7, characterized in that in the first phase, is introduced into the container (2) the base component by an introduction means (9) appropriate, separate or not the means for introducing (3) the facilitator, while the projection and dispersion device (15) is structurally associated with the introduction means (3) of the facilitator and is in the active state inactive.
9. Procédé de mélange selon la revendication 8, caractérisé par le fait que dans la première phase, après avoir introduit dans le conteneur (2) le composant de base (Cb), on dissocie structurellement le dispositif de projection et de dispersion (15), amovible, du moyen (3) d'introduction du facilitateur, puis on introduit dans le conteneur (2) le composant à mélanger (Cm) par le moyen d'introduction (3) du facilitateur.Mixing method according to claim 8, characterized in that in the first phase, after having introduced into the container (2) the basic component (Cb), the projection and dispersion device is structurally dissociated (15). , removable, medium (3) introduction of the facilitator, then introduced into the container (2) the component to be mixed (Cm) by the introduction means (3) of the facilitator.
10. Procédé de mélange selon la revendication 9, caractérisé par le fait que, après avoir introduit dans le conteneur (2) le composant à mélanger (Cm), on associe structurellement le dispositif de projection et de dispersion (15) au moyen d'introduction (3) du facilitateur, puis on introduit dans le conteneur (2) le facilitateur de mélange (Fm) par le moyen d'introduction (3) du facilitateur.Mixing method according to claim 9, characterized in that, after having introduced into the container (2) the component to be mixed (Cm), the projection and dispersion device (15) is structurally combined by means of introducing (3) the facilitator, then introducing into the container (2) the mixing facilitator (Fm) by the introduction means (3) of the facilitator.
1 1. Procédé de mélange selon l'une quelconque des revendications 1 à 10, caractérisé par le fait que dans la deuxième phase, on poursuit l'introduction, la projection et la dispersion du facilitateur de mélange (Fm) vers le composant à mélanger (Cm), jusqu'au moment où une partie du composant à mélanger (Cm) est dissous ou dispersée dans la base du contenu (Cb).1 1. A method of mixing according to any one of claims 1 to 10, characterized in that in the second phase, the introduction, projection and dispersion of the mixing facilitator (Fm) to the component to be mixed is continued. (Cm), until a part of the component to be mixed (Cm) is dissolved or dispersed in the base of the content (Cb).
12. Procédé de mélange selon l'une quelconque des revendications 1 à 1 1 , caractérisé par le fait que l'on commence le mélange au moment, ou avant ou après le moment, où on commence l'introduction du composant à mélanger (Cm) dans le conteneur (2) et on poursuit le mélange au moins jusqu'au moment où la totalité du composant à mélanger (Cm) est dissous ou dispersée dans la base du contenu (Cb).12. A method of mixing according to any one of claims 1 to 1 1, characterized in that one begins mixing at the moment, or before or after the moment, when one begins the introduction of the component to mix (Cm ) in the container (2) and mixing is continued at least until all the component to be mixed (Cm) is dissolved or dispersed in the content base (Cb).
13. Procédé de mélange selon l'une quelconque des revendications 1 à 12, caractérisé par le fait que l'on procède à un mélange de faible à moyen en fonction des composants du contenu (C), sans nécessité d'un mélange fort.13. A method of mixing according to any one of claims 1 to 12, characterized in that one proceeds to a mixture of low to medium depending on the components of the content (C), without the need for a strong mixture.
14. Procédé de mélange selon l'une quelconque des revendications 1 à 13, caractérisé par le fait que l'on met en œuvre un conteneur (2) clos, sauf dans la première phase pour l'introduction dans le conteneur (2) du composant à mélanger.14. Mixing method according to any one of claims 1 to 13, characterized in that it implements a closed container (2), except in the first phase for introduction into the container (2). component to mix.
15. Procédé de mélange selon l'une quelconque des revendications 1 à 14, caractérisé par le fait que l'on met en œuvre un conteneur (2) sous la forme d'une poche pliable à soufflets en matière plastique incluant un moyen de mélange (14).15. A method of mixing according to any one of claims 1 to 14, characterized in that it implements a container (2) in the form of a foldable pouch with plastic bellows including a mixing means (14).
16. Procédé de mélange selon la revendication 15, caractérisé par le fait que l'on part d'une poche pliable à soufflets (2) à l'état pliée et, dans une phase préliminaire, on met en volume ladite poche pliable à soufflets. 16. A method of mixing according to claim 15, characterized in that one starts from a collapsible pocket with bellows (2) in the folded state and, in a preliminary phase, is said volume said bellows foldable pocket .
17. Procédé de mélange selon l'une quelconque des revendications 1 à 16, caractérisé par le fait que, dans une phase finale, on remplit au moins substantiellement le conteneur (2) avec la base du contenu (Cb) et/ou le facilitateur de mélange (FM), alors que le dispositif de projection et de dispersion (15) est associé au moyen d'introduction (3) du facilitateur de mélange.17. Mixing method according to any one of claims 1 to 16, characterized in that, in a final phase, is filled at least substantially the container (2) with the base of the content (Cb) and / or the facilitator mixture (FM), while the projection and dispersion device (15) is associated with the introduction means (3) of the mixing facilitator.
18. Dispositif de projection et de dispersion, spécialement destiné à la mise en œuvre du procédé de mélange selon l'une quelconque des revendications 1 à 17, caractérisé par le fait qu'il comporte une paroi (18) pourvue d'une part des moyens (16) périphériques d'association structurelle à un moyen d'introduction (3) de facilitateur de mélange d'un conteneur (2) ayant une ouverture (10) et un axe D et, d'autre part, des perforations de projection et de dispersion (19) réparties sur toute ou une partie substantielle de la surface destinée à être située en regard de l'ouverture 10 et disposées de façon omni directionnelle sur un angle d'ouverture (α) autour de l'axe D, apte à permettre au facilitateur de mélange (Fm) projeté et dispersé par le dit dispositif de projection et de dispersion (15) d'atteindre substantiellement toute la surface libre (S) du contenu du conteneur (2), notamment le composant à mélanger flottant (Cm) qui s'y trouve.18. Apparatus for projection and dispersion, especially intended for the implementation of the mixing process according to any one of claims 1 to 17, characterized in that it comprises a wall (18) provided on the one hand with structurally associated peripheral means (16) for an introduction means (3) of a mixing facilitator of a container (2) having an opening (10) and an axis D and, on the other hand, projection perforations and dispersion (19) distributed over all or a substantial part of the surface intended to be located opposite the opening 10 and arranged omni directionally on an opening angle (α) about the axis D, suitable to allow the mixing facilitator (Fm) projected and dispersed by said projection and dispersion device (15) to substantially reach the entire free surface (S) of the contents of the container (2), in particular the floating mixing component ( Cm) who is there.
19. Dispositif de projection et de dispersion selon la revendication 18, caractérisé par le fait que la paroi (18) est déformable entre une configuration substantiellement plane lorsque le dit dispositif de projection et de dispersion (15) se trouve à l'état fonctionnel inactif et une configuration incurvée à convexité tournée vers l'intérieur du conteneur (2) lorsque le dit dispositif de projection et de dispersion (15) se trouve à l'état fonctionnel actif, ladite configuration incurvée définissant ladite dispersion omni directionnelle sur le dit angle d'ouverture (α), la paroi (18) étant dans sa configuration substantiellement plane en l'absence de sollicitation extérieure, notamment d'introduction du facilitateur de mélange (Fm) et étant responsive à la sollicitation exercée sur elle par le facilitateur de mélange (Fm) lors de son introduction dans le conteneur (2) de manière à être dans alors sa configuration incurvée.Projection and dispersion device according to Claim 18, characterized in that the wall (18) is deformable between a substantially flat configuration when the said projection and dispersion device (15) is in the inactive functional state. and an inwardly convex curved configuration of the container (2) when said projection and dispersion device (15) is in the active functional state, said curved configuration defining said omni directional dispersion on said angle of rotation. opening (α), the wall (18) being in its substantially flat configuration in the absence of external stress, in particular introduction of the mixing facilitator (Fm) and being responsive to the stress exerted on it by the mixing facilitator (Fm) when introduced into the container (2) so as to be in its curved configuration.
20. Dispositif de projection et de dispersion selon la revendication 19, caractérisé par le fait que la paroi (18) est pourvue de perforations (19) qui, lorsque le dit dispositif de projection et de dispersion (15) se trouve à l'état fonctionnel inactif, sont substantiellement fermées et qui, lorsque le dit dispositif de projection et de dispersion (15) se trouve à l'état fonctionnel actif, sont ouvertes. 20. A projection and dispersion device according to claim 19, characterized in that the wall (18) is provided with perforations (19) which, when the said projection and dispersion device (15) is in the state inactive, are substantially closed and which, when said projection and dispersion device (15) is in the active functional state, are open.
21. Dispositif de projection et de dispersion selon la revendication 18, caractérisé par le fait que la paroi (18) est rigide.21. Apparatus projection and dispersion according to claim 18, characterized in that the wall (18) is rigid.
22. Dispositif de projection et de dispersion selon l'une quelconque des revendications 18, 19, 21 , caractérisé par le fait que la paroi (18) est pourvue de perforations (19) qui sont toujours ouvertes, notamment lorsque le dit dispositif de projection et de dispersion se trouve à l'état fonctionnel inactif.22. Device for projection and dispersion according to any one of claims 18, 19, 21, characterized in that the wall (18) is provided with perforations (19) which are always open, especially when said projection device and dispersion is in the inactive functional state.
23. Dispositif de projection et de dispersion selon l'une quelconque des revendications 18 à 22, caractérisé par des perforations (19) identiques.23. Spraying and dispersing device according to any one of claims 18 to 22, characterized by identical perforations (19).
24. Dispositif de projection et de dispersion selon l'une quelconque des revendications 18 à 22, caractérisé par des perforations (19) différenciées par leur taille et/ou leur forme selon leur position sur la paroi (18).24. Device projection and dispersion according to any one of claims 18 to 22, characterized by perforations (19) differentiated by their size and / or their shape according to their position on the wall (18).
25. Dispositif de projection et de dispersion selon l'une quelconque des revendications 18 à 24, caractérisé par le fait que les moyens périphériques (16) d'association structurelle à un moyen d'introduction (3) de facilitateur de mélange d'un conteneur (2) se présentent sous la forme d'un bourrelet annulaire apte à coopérer, de façon amovible, avec des moyens complémentaires (17) du moyen d'introduction (3) de facilitateur de mélange ayant la forme d'un creux annulaire ménagé dans le moyen d'introduction (3) de facilitateur de mélange.25. Device for projection and dispersion according to any one of claims 18 to 24, characterized in that the peripheral means (16) of structural association with an introduction means (3) facilitator mixing a container (2) are in the form of an annular bead adapted to cooperate, removably, with complementary means (17) of the introduction means (3) of mixing facilitator having the shape of a hollow annular recess in the introduction means (3) of mixing facilitator.
26. Dispositif de projection et de dispersion selon l'une quelconque des revendications 18 à 24, caractérisé par le fait que les moyens périphériques (16) d'association structurelle à un moyen d'introduction (3) de facilitateur de mélange d'un conteneur (2) sont constitués par la paroi (18) formée par une pièce déformable élastiquement apte, par la tension que l'on exerce sur elle, à être élargie puis enfilée sur la collerette (1 1 ) qu'elle peut alors enserrer et sur laquelle elle est maintenue de façon amovible.26. projection and dispersion device according to any one of claims 18 to 24, characterized in that the peripheral means (16) of structural association with a means of introduction (3) facilitator mixing a container (2) are constituted by the wall (18) formed by a deformable piece elastically adapted, by the tension that is exerted on it, to be widened and then strung on the collar (1 1) that it can then grip and on which it is held removably.
27. Dispositif de mélange spécialement destiné à la mise en œuvre du procédé de mélange selon l'une quelconque des revendications 4 à 17, comprenant : - un conteneur (2) pourvu de moyens d'introduction (3, 9) de composants du contenu qu'il est destiné à recevoir, dont un moyen d'introduction (3) du facilitateur de mélange situé sur sa paroi supérieure (7) et en forme d'une ouverture (10), le moyen d'introduction (3) de facilitateur de mélange et l'ouverture (10) ayant un axe D, - des moyens de mélange (14) du dit contenu, associés au conteneur (2), et27. Mixing device specially adapted for carrying out the mixing process according to any one of claims 4 to 17, comprising: - a container (2) provided with means for introducing (3, 9) components of the content it is intended to receive, including an introduction means (3) of the mixing facilitator located on its upper wall (7) and in the form of an opening (10), the means (3) for introducing a facilitator of mixing and the opening (10) having an axis D, mixing means (14) for said content, associated with the container (2), and
- un dispositif de projection et de dispersion (15) qui comporte une paroi (18) pourvue, d'une part, des moyens (16) périphériques d'association structurelle au moyen d'introduction (3) de facilitateur de mélange et, d'autre part, de perforations de projection et de dispersion (19) réparties sur toute ou une partie substantielle de la surface destinée à être située en regard de l'ouverture (10) et disposées de façon omni directionnelle sur un angle d'ouverture (α) autour de l'axe D, apte à permettre au facilitateur de mélange (Fm) projeté et dispersé par le dit dispositif de projection et de dispersion (15) d'atteindre substantiellement toute la surface libre (S) du contenu du conteneur (2), notamment le composant à mélanger flottant (Cm) qui s'y trouve.a projection and dispersion device (15) which comprises a wall (18) provided, on the one hand, with means (16) for structural association with the introduction means (3) of a mixing facilitator, and on the other hand, projection and dispersion perforations (19) distributed over all or a substantial part of the surface intended to be situated facing the opening (10) and arranged omni-directionally over an opening angle ( α) about the axis D, able to allow the mixing facilitator (Fm) projected and dispersed by the said projection and dispersion device (15) to reach substantially the entire free surface (S) of the contents of the container ( 2), especially the floating mixing component (Cm) therein.
28. Dispositif de mélange selon la revendication 27, caractérisé par le fait que le conteneur (2) est clos, sauf lorsque moyen d'introduction (3) du facilitateur de mélange est ouvert.28. Mixing device according to claim 27, characterized in that the container (2) is closed, except when introduction means (3) of the mixing facilitator is open.
29. Dispositif de mélange selon l'une quelconque des revendications 27 et 28, caractérisé par le fait que le conteneur (2) est une poche pliable à soufflets en matière plastique incluant les moyens de mélange (14).29. Mixing device according to any one of claims 27 and 28, characterized in that the container (2) is a foldable pouch with plastic bellows including mixing means (14).
30. Dispositif de mélange selon l'une quelconque des revendications 27 à 29, caractérisé par le fait que le moyen d'introduction (3) du facilitateur de mélange se présente sous la forme d'une ouverture (10) formée par une collerette périphérique (1 1 ) attenante au conteneur (2), une coiffe (12) avec un port (13) d'introduction de liquide étant montée sur la collerette (1 1 ), le dispositif de projection et de dispersion (15) étant associé structurellement, de façon amovible, au moyen d'introduction (3) du facilitateur de mélange par ses moyens périphériques (16) d'association structurelle coopérant avec des moyens complémentaires (17) du moyen d'introduction (3) de facilitateur de mélange. Mixing device according to any one of Claims 27 to 29, characterized in that the means (3) for introducing the mixing facilitator is in the form of an opening (10) formed by a peripheral collar. (1 1) adjacent to the container (2), a cap (12) with a port (13) for introducing liquid being mounted on the flange (1 1), the projection and dispersion device (15) being structurally associated , removably, by means of introduction (3) of the mixing facilitator by its peripheral means (16) of structural association cooperating with complementary means (17) of the introduction means (3) of mixing facilitator.
EP09797569A 2008-07-16 2009-06-16 Mixing in a container of content having a base component and a component to be mixed Active EP2326412B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR0854827A FR2933881B1 (en) 2008-07-16 2008-07-16 MIXING IN A CONTAINER OF A CONTENT HAVING A BASE COMPONENT AND A MIXING COMPONENT
PCT/FR2009/051136 WO2010007273A1 (en) 2008-07-16 2009-06-16 Mixing in a container of content having a base component and a component to be mixed

Publications (2)

Publication Number Publication Date
EP2326412A1 true EP2326412A1 (en) 2011-06-01
EP2326412B1 EP2326412B1 (en) 2012-05-09

Family

ID=40386414

Family Applications (1)

Application Number Title Priority Date Filing Date
EP09797569A Active EP2326412B1 (en) 2008-07-16 2009-06-16 Mixing in a container of content having a base component and a component to be mixed

Country Status (5)

Country Link
US (1) US9073023B2 (en)
EP (1) EP2326412B1 (en)
AT (1) ATE556764T1 (en)
FR (1) FR2933881B1 (en)
WO (1) WO2010007273A1 (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018007691A1 (en) 2016-07-08 2018-01-11 Sartorius Stedim Fmt Sas 3-d flexible bag to be filled for biopharmaceutical fluids and method for creating such a bag
WO2018096226A1 (en) 2016-11-25 2018-05-31 Sartorius Stedim Fmt Sas Fillable 3d flexible pouch for biopharmaceutical fluids, and method for producing such a pouch
EP4316843A1 (en) 2022-08-03 2024-02-07 Sartorius Stedim Fmt Sas Method of assembling a bioreactor having a biological material depositing end that is movable with the top portion to allow bioprinting

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102006020461B3 (en) * 2006-04-28 2007-10-04 Sartorius Biotech Gmbh Flexible wall liquid container includes an agitator with through-wall magnetic coupled drive for longitudinal shaft movement from an external driver
FR2921905B1 (en) * 2007-10-04 2012-09-28 Sartorius Stedim Biotech CONTAINER FOR PROCESSING AND / OR CONTROLLING PRODUCTS COMPRISING A CHAMBER FOR PROTECTING MEANS OF PROCESSING AND / OR CONTROLLING THESE PRODUCTS, AND CONTAINER COMPRISING SUCH A CONTAINER
FR2929253B1 (en) * 2008-03-28 2013-09-13 Sartorius Stedim Biotech Sa RIGID FRAME FOR 3D CONTAINER CONTAINING AT LEAST PARTIALLY DEFORMABLE
FR2933881B1 (en) * 2008-07-16 2011-05-27 Sartorius Stedim Biotech Sa MIXING IN A CONTAINER OF A CONTENT HAVING A BASE COMPONENT AND A MIXING COMPONENT
FR2960425B1 (en) 2010-05-28 2013-03-08 Sartorius Stedim Biotech Sa CONNECTION WITH COMMUNICATION BETWEEN CONTAINERS AND / OR BIOPHARMACEUTICAL CONDUITS.
DE102010040923A1 (en) 2010-09-16 2012-03-22 Basf Se Process for the preparation of acrylic acid from ethanol and formaldehyde
DE102010040921A1 (en) 2010-09-16 2012-03-22 Basf Se Process for the preparation of acrylic acid from methanol and acetic acid
FR2997703B1 (en) * 2012-11-07 2016-12-30 Biomerieux Sa PROCESS FOR TREATING AT LEAST ONE BIOLOGICAL SAMPLE
US9827541B1 (en) 2012-11-29 2017-11-28 Emd Millipore Corporation 2D low level mixing bag for storage and shipping
WO2014085035A2 (en) 2012-11-29 2014-06-05 Emd Millipore Corporation 2d low level mixing bag for storage and shipping
EP2951452B1 (en) * 2013-02-01 2016-08-31 Asociación Centro de Investigación Cooperativa en Biomateriales - CIC biomaGUNE Non intrusive agitation system
US9073846B2 (en) 2013-06-05 2015-07-07 Celanese International Corporation Integrated process for the production of acrylic acids and acrylates
US9120743B2 (en) 2013-06-27 2015-09-01 Celanese International Corporation Integrated process for the production of acrylic acids and acrylates
US9248420B2 (en) * 2013-12-16 2016-02-02 Pall Corporation High turndown impeller
US9687852B2 (en) 2015-04-14 2017-06-27 Pall Corporation Support for biocontainer bag
JP6797417B2 (en) * 2015-04-16 2020-12-09 グローバル・ライフ・サイエンシズ・ソリューションズ・ユーエスエー・エルエルシー Bio process mixer
FR3039776B1 (en) * 2015-08-03 2017-08-25 Sartorius Stedim Fmt Sas METHOD FOR ASSEMBLING A CONTAINER-MIXER COMPRISING A TELESCOPIC TREE
US20170247167A1 (en) * 2016-02-25 2017-08-31 Master Payt-nt Ltd. Resealable package for mixing
EP3784372A1 (en) 2018-04-27 2021-03-03 Baxter International Inc. Method of mixing a pharmaceutical solution and mixing system
MX2020013891A (en) 2018-06-21 2021-03-09 Procter & Gamble Unitary dispensing nozzle for co-injection of two or more liquids and method of using same.
JP7299243B2 (en) 2018-06-22 2023-06-27 ザ プロクター アンド ギャンブル カンパニー Liquid filling system and method of use
WO2021119921A1 (en) 2019-12-16 2021-06-24 The Procter & Gamble Company Liquid dispensing system comprising an unitary dispensing nozzle
EP4108321A1 (en) 2021-06-24 2022-12-28 Sartorius Stedim Fmt Sas A mixing system including fillable 3d flexible pouch for biopharmaceutical fluids, and method for improving mixing in single-use bioreactors

Family Cites Families (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1782124A1 (en) * 1968-07-22 1971-03-18 Klinkhammer Handelsvertretunge Device for homogenizing powder-liquid mixtures
US3647397A (en) * 1969-11-19 1972-03-07 Charles M Coleman Reagent solution preparation
JP3195636B2 (en) * 1992-03-19 2001-08-06 ガンブロ株式会社 Dispensing method of undiluted solution for hemodialysate and soft bag for dispensing undiluted solution for hemodialysate
US5803137A (en) * 1995-07-24 1998-09-08 Beldex Corporation Liquid crystal delivering apparatus
US5750440A (en) * 1995-11-20 1998-05-12 Motorola, Inc. Apparatus and method for dynamically mixing slurry for chemical mechanical polishing
US5941635A (en) * 1997-06-11 1999-08-24 Hyclone Labortories, Inc. Mixing block for resuspension system
FR2781202B1 (en) 1998-07-16 2001-01-12 Stedim Sa POCKETS FOR BIO-PHARMACEUTICAL FLUID PRODUCTS
US7086778B2 (en) * 2000-10-09 2006-08-08 Levtech, Inc. System using a levitating, rotating pumping or mixing element and related methods
US6670171B2 (en) * 2001-07-09 2003-12-30 Wheaton Usa, Inc. Disposable vessel
US7153021B2 (en) * 2003-03-28 2006-12-26 Hyclone Laboratories, Inc. Container systems for mixing fluids with a magnetic stir bar
US20040245144A1 (en) * 2003-06-03 2004-12-09 Hurst William E. Preformed mixing bag for dry powder, apparatus, method and system for using same
EP1701780B8 (en) * 2004-01-07 2014-09-24 Pall Technology UK limited Bioprocessing vessel with integral sparger, and method of its manufacture
US20050279687A1 (en) * 2004-06-21 2005-12-22 Maxwell Hsu Pressurized gas-water mixing device
WO2008040567A1 (en) * 2006-10-03 2008-04-10 Artelis Flexible mixing bag, mixing device and mixing system
DE102006001623B4 (en) * 2006-01-11 2009-05-07 Sartorius Stedim Biotech Gmbh Container and method for mixing media
SE531572C2 (en) * 2006-04-05 2009-05-26 Millipore Ab Disposable unit for process products
FR2921905B1 (en) * 2007-10-04 2012-09-28 Sartorius Stedim Biotech CONTAINER FOR PROCESSING AND / OR CONTROLLING PRODUCTS COMPRISING A CHAMBER FOR PROTECTING MEANS OF PROCESSING AND / OR CONTROLLING THESE PRODUCTS, AND CONTAINER COMPRISING SUCH A CONTAINER
US7832922B2 (en) * 2007-11-30 2010-11-16 Levitronix Gmbh Mixing apparatus and container for such
EP2274084B1 (en) * 2008-03-19 2012-12-05 Sartorius Stedim Biotech GmbH Disposable mixing vessel comprising a magnetic stirrer
FR2929253B1 (en) * 2008-03-28 2013-09-13 Sartorius Stedim Biotech Sa RIGID FRAME FOR 3D CONTAINER CONTAINING AT LEAST PARTIALLY DEFORMABLE
FR2933881B1 (en) * 2008-07-16 2011-05-27 Sartorius Stedim Biotech Sa MIXING IN A CONTAINER OF A CONTENT HAVING A BASE COMPONENT AND A MIXING COMPONENT
SG10201504574RA (en) * 2010-07-30 2015-07-30 Emd Millipore Corp Plastic bag containing a disposable vortex breaker

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See references of WO2010007273A1 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018007691A1 (en) 2016-07-08 2018-01-11 Sartorius Stedim Fmt Sas 3-d flexible bag to be filled for biopharmaceutical fluids and method for creating such a bag
WO2018096226A1 (en) 2016-11-25 2018-05-31 Sartorius Stedim Fmt Sas Fillable 3d flexible pouch for biopharmaceutical fluids, and method for producing such a pouch
EP4316843A1 (en) 2022-08-03 2024-02-07 Sartorius Stedim Fmt Sas Method of assembling a bioreactor having a biological material depositing end that is movable with the top portion to allow bioprinting
WO2024028062A1 (en) 2022-08-03 2024-02-08 Sartorius Stedim Fmt Sas Method of assembling a bioreactor having a biological material depositing end that is movable with the top portion to allow bioprinting

Also Published As

Publication number Publication date
US20110158037A1 (en) 2011-06-30
US9073023B2 (en) 2015-07-07
FR2933881A1 (en) 2010-01-22
FR2933881B1 (en) 2011-05-27
EP2326412B1 (en) 2012-05-09
ATE556764T1 (en) 2012-05-15
WO2010007273A1 (en) 2010-01-21

Similar Documents

Publication Publication Date Title
EP2326412B1 (en) Mixing in a container of content having a base component and a component to be mixed
EP2943284B1 (en) Disposable assembly for preparing and working paint or for spraying a product resulting from mixing at least two components, to be used as a bucket on a spraying tool
EP2864216B1 (en) Dispensing and mixing device
EP1167231B1 (en) Assembly for the extemporaneous mixture of two products
EP2205496B1 (en) Vessel for processing a biopharmaceutical product including protection means, device and method
CA2180175C (en) Bottle for two separate products
FR2652567A1 (en) DISPENSING DEVICE COMPRISING AT LEAST ONE VIAL WITH A BREAKABLE TIP.
FR2610901A1 (en) SYSTEM AND METHOD FOR INTRODUCING A COUPLED ADDITIVE OF A CAPSULE IN A CONTAINER
FR2802180A1 (en) Container device for separate enclosure of two different substances comprises airtight closing unit fitted in the cap element and cutting device to release the second substance
EP0628495A1 (en) Packaging assembly for hair lightening products and corresponding hair lichtening process
WO1993012989A1 (en) Assembly for mixing two different separately-stored products
FR2507573A1 (en) PERFORABLE BEVERAGE CONTAINER WITH STRAW
FR2843373A1 (en) Container and applicator for for fluid product e.g. for hair care has inflatable chambers with movable spikes to pierce them
FR2552404A1 (en) SOLUTION PREPARATION AND DELIVERY ASSEMBLY, SHUTTER CAP FOR THIS ASSEMBLY, AND METHOD OF MANUFACTURING THE SAME
EP0626321B1 (en) Liquid dispensing device without dip tube
EP1976768A1 (en) Device for releasing a substance into a container
FR2709733A1 (en) Pouring or spraying packages without propellent gas
WO2004113184A2 (en) Device for releasing a liquid or powdered material into a sealed container, and container comprising one such device
EP3475190A1 (en) Mixing vessel adaptable to any receiving vessel
FR2982249A1 (en) Disposable cup for conditioning, preparing, application and holding of e.g. paints, has closure sealingly mounted on opening of body by screwing, clipping or interlocking unit, and tubular element retained in projection at one end
WO2011058272A1 (en) Container for fluid comprising a bag for containing said fluid and related barrel
FR2532280A1 (en) Packaging for the separate storage of mutually incompatible fluids which allows them to be mixed at the time of use
EP0377882B1 (en) Flexible packaging for liquid produce
FR2982250A1 (en) Closed disposable package for mounting on projecting or spraying gun for projecting and spraying e.g. paint, has shutter-vent for sealing product when package is closed, and exhibiting venting function when gun is in used condition
FR2926794A1 (en) Pre-dosed packaging for concentrated product e.g. powder product e.g. coffee, has concentrated dosette for receiving and conserving dose of concentrated product, and tube receiving product that is mixed to product stored in dosette

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

17P Request for examination filed

Effective date: 20110214

AK Designated contracting states

Kind code of ref document: A1

Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO SE SI SK TR

AX Request for extension of the european patent

Extension state: AL BA RS

GRAP Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOSNIGR1

DAX Request for extension of the european patent (deleted)
GRAC Information related to communication of intention to grant a patent modified

Free format text: ORIGINAL CODE: EPIDOSCIGR1

GRAS Grant fee paid

Free format text: ORIGINAL CODE: EPIDOSNIGR3

GRAA (expected) grant

Free format text: ORIGINAL CODE: 0009210

AK Designated contracting states

Kind code of ref document: B1

Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO SE SI SK TR

REG Reference to a national code

Ref country code: GB

Ref legal event code: FG4D

Free format text: NOT ENGLISH

REG Reference to a national code

Ref country code: AT

Ref legal event code: REF

Ref document number: 556764

Country of ref document: AT

Kind code of ref document: T

Effective date: 20120515

Ref country code: CH

Ref legal event code: EP

REG Reference to a national code

Ref country code: IE

Ref legal event code: FG4D

Free format text: LANGUAGE OF EP DOCUMENT: FRENCH

REG Reference to a national code

Ref country code: DE

Ref legal event code: R096

Ref document number: 602009006891

Country of ref document: DE

Effective date: 20120712

REG Reference to a national code

Ref country code: NL

Ref legal event code: VDEP

Effective date: 20120509

REG Reference to a national code

Ref country code: LT

Ref legal event code: MG4D

Effective date: 20120509

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IS

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120909

Ref country code: SE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

Ref country code: FI

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

Ref country code: PL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

Ref country code: NO

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120809

Ref country code: LT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

Ref country code: CY

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

REG Reference to a national code

Ref country code: AT

Ref legal event code: MK05

Ref document number: 556764

Country of ref document: AT

Kind code of ref document: T

Effective date: 20120509

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SI

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

Ref country code: GR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120810

Ref country code: LV

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

Ref country code: PT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120910

Ref country code: HR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

BERE Be: lapsed

Owner name: SARTORIUS STEDIM BIOTECH S.A.

Effective date: 20120630

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

Ref country code: NL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

Ref country code: MC

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20120630

Ref country code: CZ

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

Ref country code: AT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

Ref country code: RO

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

Ref country code: EE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

Ref country code: DK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

Ref country code: MK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

PLBE No opposition filed within time limit

Free format text: ORIGINAL CODE: 0009261

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT

REG Reference to a national code

Ref country code: IE

Ref legal event code: MM4A

26N No opposition filed

Effective date: 20130212

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20120616

Ref country code: BE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20120630

Ref country code: ES

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120820

REG Reference to a national code

Ref country code: DE

Ref legal event code: R097

Ref document number: 602009006891

Country of ref document: DE

Effective date: 20130212

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: MT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

Ref country code: BG

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120809

REG Reference to a national code

Ref country code: CH

Ref legal event code: PL

GBPC Gb: european patent ceased through non-payment of renewal fee

Effective date: 20130616

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: GB

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20130616

Ref country code: LI

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20130630

Ref country code: CH

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20130630

Ref country code: TR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20120509

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LU

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20120616

REG Reference to a national code

Ref country code: DE

Ref legal event code: R082

Ref document number: 602009006891

Country of ref document: DE

Representative=s name: OFFICE FREYLINGER S.A., LU

REG Reference to a national code

Ref country code: FR

Ref legal event code: TP

Owner name: SARTORIUS STEDIM FMT SAS, FR

Effective date: 20140602

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: HU

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20090616

REG Reference to a national code

Ref country code: DE

Ref legal event code: R082

Ref document number: 602009006891

Country of ref document: DE

Representative=s name: OFFICE FREYLINGER S.A., LU

Effective date: 20140630

Ref country code: DE

Ref legal event code: R081

Ref document number: 602009006891

Country of ref document: DE

Owner name: SARTORIUS STEDIM FMT SAS, FR

Free format text: FORMER OWNER: SARTORIUS STEDIM BIOTECH S.A., AUBAGNE, FR

Effective date: 20140630

REG Reference to a national code

Ref country code: FR

Ref legal event code: PLFP

Year of fee payment: 8

REG Reference to a national code

Ref country code: FR

Ref legal event code: PLFP

Year of fee payment: 9

REG Reference to a national code

Ref country code: FR

Ref legal event code: PLFP

Year of fee payment: 10

REG Reference to a national code

Ref country code: DE

Ref legal event code: R079

Ref document number: 602009006891

Country of ref document: DE

Free format text: PREVIOUS MAIN CLASS: B01F0003120000

Ipc: B01F0023500000

P01 Opt-out of the competence of the unified patent court (upc) registered

Effective date: 20230517

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: DE

Payment date: 20240617

Year of fee payment: 16

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: FR

Payment date: 20240621

Year of fee payment: 16