EP2064369A4 - Electrochemical process for the recovery of metallic iron and chlorine values from iron-rich metal chloride wastes - Google Patents

Electrochemical process for the recovery of metallic iron and chlorine values from iron-rich metal chloride wastes

Info

Publication number
EP2064369A4
EP2064369A4 EP07701657A EP07701657A EP2064369A4 EP 2064369 A4 EP2064369 A4 EP 2064369A4 EP 07701657 A EP07701657 A EP 07701657A EP 07701657 A EP07701657 A EP 07701657A EP 2064369 A4 EP2064369 A4 EP 2064369A4
Authority
EP
European Patent Office
Prior art keywords
iron
recovery
metal chloride
electrochemical process
rich metal
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP07701657A
Other languages
German (de)
French (fr)
Other versions
EP2064369A1 (en
EP2064369B1 (en
Inventor
Francois Cardarelli
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rio Tinto Fer et Titane Inc
Original Assignee
Qit Fer et Titane Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Qit Fer et Titane Inc filed Critical Qit Fer et Titane Inc
Publication of EP2064369A1 publication Critical patent/EP2064369A1/en
Publication of EP2064369A4 publication Critical patent/EP2064369A4/en
Application granted granted Critical
Publication of EP2064369B1 publication Critical patent/EP2064369B1/en
Not-in-force legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25CPROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
    • C25C1/00Electrolytic production, recovery or refining of metals by electrolysis of solutions
    • C25C1/06Electrolytic production, recovery or refining of metals by electrolysis of solutions or iron group metals, refractory metals or manganese
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00Electrolytic production of inorganic compounds or non-metals
    • C25B1/01Products
    • C25B1/24Halogens or compounds thereof
    • C25B1/26Chlorine; Compounds thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Electrolytic Production Of Metals (AREA)
EP07701657A 2006-09-21 2007-01-09 Electrochemical process for the recovery of metallic iron and chlorine values from iron-rich metal chloride wastes Not-in-force EP2064369B1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US82645306P 2006-09-21 2006-09-21
CA2560407 2006-09-21
PCT/CA2007/000026 WO2008034212A1 (en) 2006-09-21 2007-01-09 Electrochemical process for the recovery of metallic iron and chlorine values from iron-rich metal chloride wastes

Publications (3)

Publication Number Publication Date
EP2064369A1 EP2064369A1 (en) 2009-06-03
EP2064369A4 true EP2064369A4 (en) 2009-11-04
EP2064369B1 EP2064369B1 (en) 2011-03-30

Family

ID=39200106

Family Applications (1)

Application Number Title Priority Date Filing Date
EP07701657A Not-in-force EP2064369B1 (en) 2006-09-21 2007-01-09 Electrochemical process for the recovery of metallic iron and chlorine values from iron-rich metal chloride wastes

Country Status (7)

Country Link
US (1) US20100044243A1 (en)
EP (1) EP2064369B1 (en)
JP (1) JP2010504423A (en)
AU (1) AU2007299519B2 (en)
CA (1) CA2663652C (en)
WO (1) WO2008034212A1 (en)
ZA (1) ZA200900950B (en)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2718585C (en) * 2008-03-20 2014-02-18 Qit-Fer & Titane Inc. Electrochemical process for the recovery of metallic iron and chlorine values from iron-rich metal chloride wastes
WO2009124393A1 (en) * 2008-04-11 2009-10-15 Cardarelli Francois Electrochemical process for the recovery of metallic iron and sulfuric acid values from iron-rich sulfate wastes, mining residues and pickling liquors
ITMI20111938A1 (en) * 2011-10-26 2013-04-27 Industrie De Nora Spa ANODIC COMPARTMENT FOR CELLS FOR ELECTROLYTIC EXTRACTION OF METALS
US20130233720A1 (en) * 2011-10-27 2013-09-12 Gagik Martoyan Extraction of metals
US9222147B2 (en) 2012-01-12 2015-12-29 Nichromet Extraction Inc. Method for selective precipitation of iron, arsenic and antimony
EP2966035A1 (en) * 2014-07-08 2016-01-13 Kronos International, Inc. Method for the recovery of hydrochloric acid from metal chloride solutions with a high iron chloride content
KR101723730B1 (en) * 2015-06-03 2017-04-06 조범래 High selective metals and acid recovery process from a multi-metallic solutio
CN105132936B (en) * 2015-07-07 2017-12-22 昆明理工大学 One kind prepares CaTiO with fused salt electrolysis process from ilmenite3The method of powder
US10364169B2 (en) * 2015-11-30 2019-07-30 The Board Of Trustees Of The University Of Illinois Ultrafiltration TIO2 magnéli phase reactive electrochemical membranes
DK202070078A1 (en) * 2017-07-07 2020-02-13 9203-5468 Quebec Inc. Dba Nmr360 Method for the oxidation and hydrothermal dissociation of metal chlorides for the separation of metals and hydrochloric acid
CN109628953B (en) * 2018-12-26 2020-10-23 浙江工业大学 Method for removing arsenic, antimony and bismuth in copper electrolyte
KR20220046589A (en) * 2019-08-01 2022-04-14 아쿠아 메탈스 인크. Metal recovery from lead-containing electrolytes
US20240263333A1 (en) 2021-03-24 2024-08-08 Electrasteel, Inc. Iron conversion system and applications
CN113215589B (en) * 2021-04-15 2023-03-17 中国恩菲工程技术有限公司 Method for separating iron and other metal elements in iron alloy
CN114740143B (en) * 2022-04-12 2023-10-27 四川大学 Deep dechlorination method and device based on occurrence form of chloride ions in chlorination tailings

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0215187A (en) * 1988-07-04 1990-01-18 Osaka Titanium Co Ltd Production of iron and chlorine from aqueous solution containing iron chloride
JPH0226802A (en) * 1988-07-15 1990-01-29 Osaka Titanium Co Ltd Method for recovering metal chloride
JP2006241568A (en) * 2005-03-07 2006-09-14 Sumitomo Metal Mining Co Ltd Electrowinning method for iron from acid chloride aqueous solution

Family Cites Families (47)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1752348A (en) * 1928-02-10 1930-04-01 Levy Stanley Isaac Electrolysis of ferrous chloride
US1980381A (en) * 1931-05-27 1934-11-13 Frederic A Eustis Method of making ductile electrolytic iron from sulphide ores
US2272899A (en) * 1940-06-06 1942-02-10 Firestone Tire & Rubber Co Method of making radioactive compositions
US2393582A (en) * 1942-08-08 1946-01-29 Nat Lead Co Method for utilizing iron chloride liquors
US3041253A (en) * 1956-02-08 1962-06-26 Electro Chimie Metal Electrolytic preparation of iron powder
US2954274A (en) * 1956-03-13 1960-09-27 Columbia Southern Chem Corp Metal chloride manufacture
US3016286A (en) * 1960-02-29 1962-01-09 Ishihara Sangyo Kaisha Method for the treatment of waste acid resulting from titanium dioxide production
US3216787A (en) * 1962-08-15 1965-11-09 Union Carbide Corp Selective arsenic impurity removal from aqueous vanadium bearing liquors
DE1521993B1 (en) * 1966-04-04 1970-02-19 Siemens Ag Process for regenerating a chromic acid solution for etching copper
GB1195871A (en) * 1967-02-10 1970-06-24 Chemnor Ag Improvements in or relating to the Manufacture of Electrodes.
US3617461A (en) * 1968-06-03 1971-11-02 Hooker Chemical Corp Spaced anode assembly for diaphragm cells
JPS4830226B1 (en) * 1969-03-28 1973-09-18
US3817843A (en) * 1971-04-13 1974-06-18 Electricity Council Electrodeposition of iron foil
BE795169A (en) * 1972-02-09 1973-08-08 Du Pont IRON CHLORIDE OXIDATION PROCESS
GB1407034A (en) 1972-07-21 1975-09-24 Laporte Industries Ltd Process for the recovery of chlorine
US3865920A (en) * 1973-03-14 1975-02-11 Rutile & Zircon Mines Newcastl Process for beneficiating a titaniferous ore and production of chlorine and iron oxide
FR2273082B1 (en) * 1974-05-28 1978-03-31 Seprac
US4043822A (en) * 1975-11-20 1977-08-23 Allied Chemical Corporation Treatment of water-soluble metal sulfate residues
DE2611667A1 (en) * 1976-03-19 1977-09-29 Kronos Titan Gmbh PROCESS FOR THE RECOVERY OF CHLORINE AND IRON OXIDE FROM CONTAMINATED IRON (II) -CHLORIDE-CONTAINING CHLORIDE MIXTURES, WHICH ARE PRODUCED IN THE CHLORINATION OF TITANIUM-CONTAINING RAW MATERIALS
US4282185A (en) * 1978-04-24 1981-08-04 E. I. Du Pont De Nemours And Company Chlorine and iron oxide from ferric chloride - apparatus
US4144316A (en) * 1978-04-24 1979-03-13 E. I. Du Pont De Nemours And Company Production of chlorine and iron oxide from ferric chloride
US4318794A (en) * 1980-11-17 1982-03-09 Edward Adler Anode for production of electrodeposited foil
DE3322668A1 (en) * 1983-06-23 1985-01-17 Bayer Ag, 5090 Leverkusen METHOD FOR PRODUCING URETHANES
JPS62158833A (en) * 1986-01-07 1987-07-14 Takeshi Aoki Recovering method for noble metal by electrolysis
DE3769855D1 (en) * 1986-06-10 1991-06-13 Tosoh Corp METHOD FOR RECOVERY OF METALS.
US4994255A (en) * 1986-07-24 1991-02-19 Scm Chemicals, Inc. Oxidation of ferrous chloride directly to chlorine in a fluid bed reactor
ZA899462B (en) * 1988-12-19 1990-09-26 Wimmera Ind Minerals Proprieta Improving the quality of heavy mineral concentrates
US4997533A (en) * 1989-08-07 1991-03-05 Board Of Control Of Michigan Technological University Process for the extracting oxygen and iron from iron oxide-containing ores
US5041196A (en) * 1989-12-26 1991-08-20 Olin Corporation Electrochemical method for producing chlorine dioxide solutions
ATE125310T1 (en) * 1991-05-30 1995-08-15 Sikel Nv ELECTRODE FOR AN ELECTROLYTIC CELL, USE AND METHOD THEREOF.
DE4326854A1 (en) * 1993-08-11 1995-02-16 Heraeus Elektrochemie Process for the regeneration of an aqueous solution containing metal ions and sulfuric acid, and device
JP2965442B2 (en) * 1993-09-03 1999-10-18 日鉄鉱業株式会社 Regeneration method of iron chloride waste liquid containing nickel
AUPM424894A0 (en) * 1994-03-04 1994-03-31 Spunboa Pty Limited Treatment of electrolyte solutions
US5856254A (en) * 1996-02-15 1999-01-05 Vaw Silizium Gmbh Spherical metal-oxide powder particles and process for their manufacture
JPH09263983A (en) * 1996-03-29 1997-10-07 Nittetsu Mining Co Ltd Treatment of iron chloride solution containing nickel and device for executing this method
MY115542A (en) * 1996-06-28 2003-07-31 Astec Irie Co Ltd Method for recovering etchand from etching waste liquid containing iron chloride
US5911869A (en) * 1997-12-09 1999-06-15 Exxon Research And Engineering Co. Method for demetallating petroleum streams (LAW639)
GB9803018D0 (en) * 1998-02-13 1998-04-08 Tioxide Group Services Ltd Treatment of metal chloride
DE10022867A1 (en) * 2000-05-10 2001-11-22 Kronos Titan Gmbh & Co Ohg Precipitation of nickel and lead ions from iron(II) salt solution, from e.g. lixiviation of cyclone dust from titanium dioxide production by chloride process, involves using excess alkali sulfide and filtration after dwell
US6375824B1 (en) * 2001-01-16 2002-04-23 Airborne Industrial Minerals Inc. Process for producing potassium hydroxide and potassium sulfate from sodium sulfate
US6843976B2 (en) * 2001-02-27 2005-01-18 Noranda Inc. Reduction of zinc oxide from complex sulfide concentrates using chloride processing
CA2408951C (en) * 2002-10-18 2008-12-16 Kvaerner Canada Inc. Mediated hydrohalic acid electrolysis
KR100500444B1 (en) * 2002-12-26 2005-07-12 삼성전자주식회사 fabrication method of a metal-insulator-metal capacitor
US7125610B2 (en) * 2003-03-17 2006-10-24 Kemet Electronics Corporation Capacitor containing aluminum anode foil anodized in low water content glycerine-phosphate electrolyte without a pre-anodizing hydration step
US7329396B2 (en) * 2003-05-16 2008-02-12 Jaguar Nickel Inc. Process for the recovery of value metals from material containing base metal oxides
US7332065B2 (en) * 2003-06-19 2008-02-19 Akzo Nobel N.V. Electrode
CA2718585C (en) * 2008-03-20 2014-02-18 Qit-Fer & Titane Inc. Electrochemical process for the recovery of metallic iron and chlorine values from iron-rich metal chloride wastes

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0215187A (en) * 1988-07-04 1990-01-18 Osaka Titanium Co Ltd Production of iron and chlorine from aqueous solution containing iron chloride
JPH0226802A (en) * 1988-07-15 1990-01-29 Osaka Titanium Co Ltd Method for recovering metal chloride
JP2006241568A (en) * 2005-03-07 2006-09-14 Sumitomo Metal Mining Co Ltd Electrowinning method for iron from acid chloride aqueous solution

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See also references of WO2008034212A1 *

Also Published As

Publication number Publication date
JP2010504423A (en) 2010-02-12
US20100044243A1 (en) 2010-02-25
AU2007299519B2 (en) 2011-12-15
WO2008034212A1 (en) 2008-03-27
CA2663652C (en) 2010-07-06
CA2663652A1 (en) 2008-03-27
EP2064369A1 (en) 2009-06-03
ZA200900950B (en) 2009-12-30
AU2007299519A1 (en) 2008-03-27
EP2064369B1 (en) 2011-03-30

Similar Documents

Publication Publication Date Title
ZA201006713B (en) Electrochemical process for the recovery of metallic iron and chlorine values from iron-rich metal chloride wastes
ZA200900950B (en) Electrochemical process for the recovery of metallic iron and chlorine values from iron-rich metal chloride wastes
EP2171108A4 (en) Method of recovering metal values from ores
ZA201007214B (en) Electrochemical process for the recovery of metallic iron and sulfuric acid values from iron-rich sulfate wastes,mining residues and pickling liquors
EP2065488A4 (en) Method for collection of valuable metal from ito scrap
EP2078768A4 (en) Method for collection of valuable metal from ito scrap
EP2078766A4 (en) Method for collection of valuable metal from ito scrap
ZA201101485B (en) Methods and systems for leaching a metal-bearing ore for the recovery of a metal value
ZA201004007B (en) Direct processing of metallic ore concentrates into ferroalloys
ZA200704039B (en) Leaching process in the presence of hydrochloric acid for the recovery of a value metal from an ore
ZA200809407B (en) Chloride heap leaching
EP1851172A4 (en) Method and system for recovering metal from metal-containing materials
EP1937857A4 (en) Process for recovery of metal values from materials containing arsenic and/or antimony
EP2078767A4 (en) Method for collection of valuable metal from ito scrap
HK1143613A1 (en) Process for producing pure metallic indium from zinc oxide and/or solution containing the metal
HK1133682A1 (en) Production method of blast furnace iron making by recycling usage of steel slag and the waste residue containing iron in chemistry or metallurgy
EP2093300A4 (en) Process for production of granular metallic iron and equipment for the production
GB2463441B (en) Extraction of metal from metal ore
ZA200804351B (en) Thiosulfate generation in situ in precious metal recovery
EP1957722A4 (en) Method for preventing metal leaching from copper and its alloys
ZA200808628B (en) Process for recovery of antimony and metal values from antimony- and metal value-bearing materials
ZA200800391B (en) Processing of metal chloride solutions and method and apparatus for producing direct iron
GB0717649D0 (en) Process for the direct reduction of iron ore
PT1922424E (en) Method and apparatus for the recovery of metals from refractory mineral ores
EP2226401A4 (en) Method for extracting precious metals from refractory ores and concentrates

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

17P Request for examination filed

Effective date: 20090316

AK Designated contracting states

Kind code of ref document: A1

Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HU IE IS IT LI LT LU LV MC NL PL PT RO SE SI SK TR

AX Request for extension of the european patent

Extension state: AL BA HR MK RS

A4 Supplementary search report drawn up and despatched

Effective date: 20091001

17Q First examination report despatched

Effective date: 20100128

DAX Request for extension of the european patent (deleted)
RIC1 Information provided on ipc code assigned before grant

Ipc: C25B 1/26 20060101ALI20100616BHEP

Ipc: C25C 1/06 20060101AFI20100616BHEP

GRAP Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOSNIGR1

GRAS Grant fee paid

Free format text: ORIGINAL CODE: EPIDOSNIGR3

GRAA (expected) grant

Free format text: ORIGINAL CODE: 0009210

AK Designated contracting states

Kind code of ref document: B1

Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HU IE IS IT LI LT LU LV MC NL PL PT RO SE SI SK TR

REG Reference to a national code

Ref country code: GB

Ref legal event code: FG4D

REG Reference to a national code

Ref country code: CH

Ref legal event code: EP

REG Reference to a national code

Ref country code: IE

Ref legal event code: FG4D

REF Corresponds to:

Ref document number: 602007013578

Country of ref document: DE

Date of ref document: 20110512

Kind code of ref document: P

REG Reference to a national code

Ref country code: DE

Ref legal event code: R096

Ref document number: 602007013578

Country of ref document: DE

Effective date: 20110512

REG Reference to a national code

Ref country code: NL

Ref legal event code: T3

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: GR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110701

Ref country code: LV

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110330

Ref country code: SE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110330

Ref country code: LT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110330

LTIE Lt: invalidation of european patent or patent extension

Effective date: 20110330

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SI

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110330

Ref country code: FI

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110330

Ref country code: CY

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110330

Ref country code: AT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110330

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: EE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110330

Ref country code: PT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110801

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IS

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110730

Ref country code: ES

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110711

Ref country code: SK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110330

Ref country code: CZ

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110330

Ref country code: RO

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110330

PLBE No opposition filed within time limit

Free format text: ORIGINAL CODE: 0009261

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: DK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110330

Ref country code: PL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110330

26N No opposition filed

Effective date: 20120102

REG Reference to a national code

Ref country code: DE

Ref legal event code: R097

Ref document number: 602007013578

Country of ref document: DE

Effective date: 20120102

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: FR

Payment date: 20120130

Year of fee payment: 6

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110330

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: DE

Payment date: 20120127

Year of fee payment: 6

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: BE

Payment date: 20120125

Year of fee payment: 6

Ref country code: GB

Payment date: 20120126

Year of fee payment: 6

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: NL

Payment date: 20120130

Year of fee payment: 6

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: MC

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20120131

REG Reference to a national code

Ref country code: CH

Ref legal event code: PL

REG Reference to a national code

Ref country code: IE

Ref legal event code: MM4A

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LI

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20120131

Ref country code: CH

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20120131

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20120109

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: BG

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110630

BERE Be: lapsed

Owner name: QIT-FER ET TITANE INC.

Effective date: 20130131

REG Reference to a national code

Ref country code: NL

Ref legal event code: V1

Effective date: 20130801

GBPC Gb: european patent ceased through non-payment of renewal fee

Effective date: 20130109

REG Reference to a national code

Ref country code: FR

Ref legal event code: ST

Effective date: 20130930

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: BE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20130131

Ref country code: DE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20130801

Ref country code: NL

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20130801

REG Reference to a national code

Ref country code: DE

Ref legal event code: R119

Ref document number: 602007013578

Country of ref document: DE

Effective date: 20130801

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: FR

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20130131

Ref country code: GB

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20130109

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: TR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110330

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: HU

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20070109

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LU

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20130109