EP2035587B1 - A method and a system for producing hot-rolled strip silicon steel based on thin slabs - Google Patents

A method and a system for producing hot-rolled strip silicon steel based on thin slabs Download PDF

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EP2035587B1
EP2035587B1 EP07764798.0A EP07764798A EP2035587B1 EP 2035587 B1 EP2035587 B1 EP 2035587B1 EP 07764798 A EP07764798 A EP 07764798A EP 2035587 B1 EP2035587 B1 EP 2035587B1
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rolling
temperature
hot
stage
train
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German (de)
French (fr)
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EP2035587A1 (en
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Ingo Schuster
Christoph Klein
Mario Sucker
Heribert Neifer
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SMS Group GmbH
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SMS Group GmbH
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    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/12Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/12Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
    • C21D8/1216Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the working step(s) being of interest
    • C21D8/1222Hot rolling
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B1/00Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
    • B21B1/46Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling metal immediately subsequent to continuous casting
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B1/00Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
    • B21B1/46Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling metal immediately subsequent to continuous casting
    • B21B1/463Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling metal immediately subsequent to continuous casting in a continuous process, i.e. the cast not being cut before rolling
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B3/00Rolling materials of special alloys so far as the composition of the alloy requires or permits special rolling methods or sequences ; Rolling of aluminium, copper, zinc or other non-ferrous metals
    • B21B3/02Rolling special iron alloys, e.g. stainless steel
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/52Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for wires; for strips ; for rods of unlimited length

Definitions

  • the invention relates to a method and a plant for the production of hot strip (pre-material) from silicon-alloyed steels for further processing into grain-oriented sheets, such as electric sheets.
  • the further processing is not the subject of the present invention; it takes place in cold rolling mills.
  • the EP 1 097 764 describes a device and method for surface treatment of a continuously cast steel product in the hot state for the removal of surface defects, surface contaminants and the like where surface treatments are to provide long service life.
  • the parts to be machined are subjected to cooling before the surface processing step.
  • the EP 0 392 535 describes a method for producing a grain oriented electrical steel sheet comprising the steps of: heating, hot rolling and winding. Subsequently, the hot-rolled sheet is annealed again as needed, and subjected to a cold rolling process. The cold rolling is divided into different degrees of deformation. Depending on requirements and application, an intermediate annealing is then carried out again and the cold-rolled sheet is subjected to a decarburization annealing and a final finish annealing and a subsequent hot rolling process.
  • Multi-stage temperature-adjusting systems for heating a cast product before it enters a rolling mill are known from EP 1 469 954 known.
  • the thin slabs are produced on Bogenstranggelloanlagen with horizontal outlet direction.
  • the method comprises the process steps: rolling the thin slab after solidification of the strand in an arcuate guide shaft at temperatures of more than 1100 ° C, cooling the slabs during radiation or descaling, inductive reheating to a temperature of about 1100 ° C and rolling the thin slab in at least one rolling mill.
  • a temperature is set in the slab, so that sets a temperature gradient at the deformation means of the rolling train in such a way that when tapping into the last roll stand, the temperature is within sufficient for a good deformation order of magnitude.
  • the rolling stock temperature dropped, for example, to 988 ° C and sufficient as a tapping temperature for the last forming step.
  • the rolling stock leaves the last mill stand with a temperature of 953 ° C or less and is then separated at a further lowered temperature in the desired lengths, stacked or reeled. If necessary, one or more stages of inductive intermediate heating may be provided between the individual stands.
  • the invention has for its object to optimize the heat treatment in hot strip pre-material of silicon-alloyed steels for further processing to grain-oriented sheets to the effect that in the rolling mill a desired final temperature and thus a desired microstructure can be set in the strand.
  • an inlet temperature is set in the finishing train, which ensures a favorable precipitation morphology in the rolling stock.
  • single-stage temperature-adjusting systems are not able to heat the cast product to the required for setting the desired / required recrystallization state high temperatures of preferably more than 1250 ° C inlet temperature in the rolling mill.
  • the high temperatures are advantageously achieved in the claimed method in that a two-stage preheating of the cast product, comprising a Primärergiebeauchte and an inductively heated stage is performed.
  • the claimed two-stage heat treatment also has the advantage that it can heat the cast product not only - if necessary - to temperatures above 1250 ° C, but also to lower inlet temperatures, should this be necessary to set other desired structural or recrystallization conditions; In this respect, the claimed method is very universally applicable.
  • the control of the temperature in the subsequent finishing train depends on the final structure to be achieved and is set via a combination of rolling speed and use of inter-frame cooling.
  • the final rolling temperature (T WE ) and the final rolling speed of the rolling stock are set to values at which no complete recrystallization of the steel takes place, and the rolling stock becomes after the last
  • the final rolling temperature (T WE ) of the rolling stock to temperatures of at least 950 ° C, preferably above 1000 ° C, set and then, preferably in immediate connection, the rolling stock to temperatures (T A ) of below 450 ° C within 10 s deterred.
  • the temperature of the cast product is set to values between 1000 and 1100 ° C and that in the subsequent intensive heating stage, the temperature is increased to values of 1250 ° C.
  • the preheating stage is carried out in a gas- or oil-fired oven and the subsequent intensive stage in an induction heating stage. This has the particular advantage that the preheating can take place in a roller hearth furnace, while the heating step is shifted to temperatures above 1200 ° C in an inductive heating zone. This prevents that the roller hearth furnace is charged too much, which could possibly lead to its thermal destruction.
  • the slab surface is descaled.
  • descaling is carried out in a descaling device between the preheating stage and the intensive heating stage.
  • the setting of the inlet temperature in the finish rolling stage is then carried out by means of induction heating.
  • the finish rolling stage can consist of a single or multi-stand Pre-season and a Mergerüstigen final season consist. The distance between these two can be bridged by a roller table or bezeizten heat tunnel.
  • the device for cooling the rolling stock comprises components for quenching the rolling stock to temperatures below 450 ° C.
  • the hot rolling train is designed as a compact finishing line.
  • the hot rolling line is formed divided into at least one pre-and at least one Endwalzstaffel.
  • Fig. 1 shows a plant 1 for the production of rolling stock in the form of sheets or strips of silicon-alloyed steel for further processing into grain-oriented sheets, such as electric sheets, which are heat treated and rolled without intermediate cooling to room temperature, so that then the rolling stock with desired structural properties available stands.
  • the plant 1 comprises a continuous casting plant 1a.
  • the near net cast strand in the form of a cast product 2 is cut in front of the roller hearth furnace 3 using a pair of scissors 4, which then come directly from the casting heat in the roller hearth furnace 3 to be heated to temperatures of 1000 to 1100 ° C or to learn a temperature compensation.
  • the slabs are preferably thin slabs with a thickness of up to 120 mm.
  • the heated slabs then preferably pass through a descaling device 5 and then enter an intensive heating stage 6.
  • the slabs are heated in a short rapid heating process at inlet temperatures of 1100 to 1300 ° C, preferably above 1250 ° C.
  • the preheating stage 3 is carried out in a gas or oil-fired furnace such as a roller hearth furnace 3 and the subsequent Intensivheittress 6 in an induction heating.
  • the Intensivannecut 6 must be designed to ensure an inlet temperature T a of the cast product 2 in the rolling mill of more than 1200 ° C.
  • the preheating stage 3 and the intensive heating stage 6 form a temperature Adjusting System 7.
  • the means for performing the heat treatment include the preheating stage 3, the intensive heating stage 6, and the interstand cooling means 10.
  • the cast product 2 is again descaled (second descaling stage 8) and introduced into a hot rolling line 9a or 9b.
  • the hot rolling train 9a or 9b may be a compact finishing line 9a or divided into a preliminary and a final rolling 9b.
  • the number of scaffolds in each of the two partial scales is not fixed.
  • an inlet temperature T a of the cast product 2 in the hot rolling line 9a or 9b is preferably set above 1250 ° C by a multi-stage heat treatment of the mill of at least 1200 ° C, wherein the cast product from the casting heat coming directly to the heat pretreatment is performed.
  • the multi-stage heat pretreatment takes place with the temperature setting system 7, which includes the preheating stage 3 for preheating the cast product 2 and the intensive heating stage 6 for adjusting the inlet temperature T a of the cast product 2 in the hot rolling line.
  • the final rolling temperature T WE and the final rolling speed of the rolling stock are set to values at which complete recrystallization of the steel no longer takes place.
  • the rolling stock is quenched after the last pass in the hot rolling line in the context of post-heat treatment from the final rolling temperature T WE to a temperature T A , whereby the desired Rekristallistionsschreib of the rolling stock at the end of the hot rolling over the strip thickness is ensured.
  • the final rolling temperature T WE of the rolling stock to temperatures of at least 950 ° C, preferably above 1000 ° C, adjusted, and then the rolling stock to temperatures T A of below 450 ° C within 10 seconds, quenched.
  • the post-rolling heat post-treatment is a combination of a rapid-cooling device 12 and normal cooling bars with water cooling 13.
  • the cooled rolling stock is subsequently wound on a reeling device 14.

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Metallurgy (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Electromagnetism (AREA)
  • Metal Rolling (AREA)
  • Manufacturing Of Steel Electrode Plates (AREA)
  • Soft Magnetic Materials (AREA)

Description

Die Erfindung bezieht sich auf ein Verfahren und eine Anlage zur Herstellung von Warmband (-vormaterial) aus Silizium-legierten Stählen zur Weiterverarbeitung zu kornorientierten Blechen, wie beispielsweise Elektroblechen. Die Weiterverarbeitung ist nicht Gegenstand der vorliegenden Erfindung; sie erfolgt in Kaltwalzwerken.The invention relates to a method and a plant for the production of hot strip (pre-material) from silicon-alloyed steels for further processing into grain-oriented sheets, such as electric sheets. The further processing is not the subject of the present invention; it takes place in cold rolling mills.

Aus dem Stand der Technik sind verschiedene Verfahren und Anlagen der gattungsgemäßen Art bekannt; es sei dazu beispielhaft auf die folgenden beiden Druckschriften verwiesen:

  • Verfahren und Anlagen zum Walzen von Bändern und Blechen aus der Gießhitze sind bekannt, zum Beispiel beschrieben in Stahl & Eisen, Vol. 2, 1993, S. 37 ff . Bei der hier beschriebenen Anlage wird mittels einer Stranggießmaschine mit speziell ausgestalteter Kokille eine Dünnbramme erzeugt, in Einzellängen unterteilt und zum Temperaturausgleich einem Rollenherdofen zugeführt. Anschließend wird die Bramme auf eine deutlich höhere Einlaufgeschwindigkeit der sich anschließenden Walzstrasse beschleunigt, entzundert und der Walzstrasse zugeführt. Im stationären Produktionsbetrieb mit einer Gießgeschwindigleit von 5,5 m/min erreicht die Dünnbramme den Rollenherdofen mit einer Durchschnittstemperatur von 1080°C. Die Auslauftemperatur aus dem Rollenherdofen liegt etwa bei 1100°C. Die für den Walzprozess notwendige Energie wird somit fast vollständig aus der Wärmemenge gedeckt, die im gegossenen Strang enthalten ist. Im Walzwerk werden die Temperaturen durch Veränderung der Walzengeschwindigkeit, durch Kühlung und aus dem Walzenkontakt gesteuert, so dass sich eine Endwalztemperatur von 880°C einstellt. Es folgt eine langsame Abkühlung in der Kühlstrecke sowie ein sich anschließendes Aufhaspeln.
Various methods and systems of the generic type are known from the prior art; by way of example, reference is made to the following two publications:
  • Processes and plants for the rolling of strips and sheets from the casting heat are known, for example described in Stahl & Eisen, Vol. 2, 1993, p. 37 ff , In the plant described here, a thin slab is produced by means of a continuous casting machine with specially designed mold, divided into individual lengths and fed to a roller hearth furnace for temperature compensation. Subsequently, the slab is accelerated to a much higher inlet speed of the subsequent rolling train, descaled and fed to the rolling train. In stationary production operation with a casting speed of 5.5 m / min, the thin slab reaches the roller hearth furnace with an average temperature of 1080 ° C. The outlet temperature from the roller hearth furnace is approximately 1100 ° C. The energy required for the rolling process is thus almost completely covered by the amount of heat contained in the cast strand. In the rolling mill, the temperatures are controlled by changing the roller speed, by cooling and from the roller contact, so that sets a final rolling temperature of 880 ° C. It follows a slow cooling in the cooling section and a subsequent coiling.

Aus der EP-A1-1 469 954 ist ein Verfahren und eine Anlage zur Herstellung von Warmband aus austhenitischen nichtrostenden Stählen bekannt. Dabei wird das Gießprodukt einem Walzvorgang in einer Walzstraße unterworfen und in einem zweiten Schritt einer Wärmebehandlung zur Verhinderung einer Korrosionsanfälligkeit.From the EP-A1-1 469 954 A method and plant for producing hot strip of austenitic stainless steels is known. The cast product is subjected to a rolling process in a rolling train and in a second step of a heat treatment to prevent corrosion.

Die EP 1 097 764 beschreibt eine Einrichtung und ein Verfahren zur Oberflächenbearbeitung eines kontinuierlich gegossenen Stahlproduktes im warmen Zustand zur Beseitigung von Oberflächenfehlern, Oberflächenverunreinigungen und dergleichen wobei Oberflächenbearbeitungen lange Standzeiten bereitstellen sollen. Die zu bearbeitenden Teile werden vor dem Schritt der Oberflächenbearbeitung einer Kühlung unterzogen.The EP 1 097 764 describes a device and method for surface treatment of a continuously cast steel product in the hot state for the removal of surface defects, surface contaminants and the like where surface treatments are to provide long service life. The parts to be machined are subjected to cooling before the surface processing step.

Die EP 0 392 535 beschreibt ein Verfahren zur Herstellung eines kornorientierten Elektrobleches mit den Schritten: Erwärmen, Warmwalzen und Wickeln. Anschließend wird das warmgewalzte Blech nach Bedarf nochmals geglüht, und einem Kaltwalzprozess unterzogen. Das Kaltwalzen ist in verschiedene Umformgrade aufgeteilt. Je nach Bedarf und Anwendung wird anschließend noch einmal ein Zwischenglühen durchgeführt und das kaltgewalzte Blech einem Entkohlungsglühen und einem letzten Fertigglühen unterzogen sowie einem anschließendem Warmwalzprozess.The EP 0 392 535 describes a method for producing a grain oriented electrical steel sheet comprising the steps of: heating, hot rolling and winding. Subsequently, the hot-rolled sheet is annealed again as needed, and subjected to a cold rolling process. The cold rolling is divided into different degrees of deformation. Depending on requirements and application, an intermediate annealing is then carried out again and the cold-rolled sheet is subjected to a decarburization annealing and a final finish annealing and a subsequent hot rolling process.

Weiterhin ist in der DE 31 50 946 eine Vorrichtung zum Entzundern eines von einer Stranggießanlage kommenden Stahlstranges beschrieben, wobei dessen Gesamtoberfläche mit so wenig Wasser wie möglich vor der Brennschneidemaschine entzundert wird.Furthermore, in the DE 31 50 946 Described an apparatus for descaling a steel strand coming from a continuous casting plant, wherein the total surface is descaled with as little water as possible before the flame cutting machine.

Die Druckschrift EP 0 0771 596 A1 beschreibt eine Produktionsanlage zum kontinuierlichen oder diskontinuierlichen Auswalzen von Warmband.The publication EP 0 0771 596 A1 describes a production plant for continuous or discontinuous rolling of hot strip.

Mehrstufige Temperatur-Einstellsysteme zum Aufheizen eines Gießproduktes vor dessen Eintritt in eine Walzstraße sind aus der EP 1 469 954 bekannt.Multi-stage temperature-adjusting systems for heating a cast product before it enters a rolling mill are known from EP 1 469 954 known.

Weiterhin ist aus der EP 0 415 987 B2 ein Verfahren zur kontinuierlichen Herstellung von Bandstahl oder Stahlblech aus Dünnbrammen von ca. 50 mm Dicke bekannt, wobei die Dünnbrammen auf Bogenstranggießanlagen mit horizontaler Auslaufrichtung hergestellt werden. Das Verfahren umfasst die Verfahrensschritte: Walzen der Dünnbrammen nach der Erstarrung des Stranges in einem bogenförmigen Führungsschacht bei Temperaturen von mehr als 1100°C, Abkühlen der Brammen während Strahlung oder Entzundern, induktives Wiederaufheizen auf eine Temperatur von ca. 1100°C sowie Walzen der Dünnbramme in mindestens einer Walzstrasse. Mittels des Erwärmens wird eine Temperatur in der Bramme eingestellt, so dass sich an den Verformungseinrichtungen der Walzstrasse ein Temperaturgefälle einstellt und zwar derart, dass beim Anstich in das letzte Walzgerüst die Temperatur innerhalb der für eine gute Verformung noch ausreichenden Größenordnung liegt. Hier ist bei einem dritten und letzten Walzgerüst der Walzstrasse die Walzguttemperatur beispielsweise auf 988°C abgefallen und als Anstichtemperatur für den letzten Umformschritt ausreichend. Das Walzgut verlässt das letzte Walzgerüst mit einer Temperatur von 953°C oder weniger und wird danach bei noch weiter abgesenkter Temperatur in die gewünschten Längen abgetrennt, gestapelt oder gehaspelt. Falls erforderlich, kann zwischen den einzelnen Walzgerüsten eine oder mehrere Stufen einer induktiven Zwischenerwärmung vorgesehen sein.Furthermore, from the EP 0 415 987 B2 a method for the continuous production of strip steel or sheet steel from thin slabs of about 50 mm thickness known, the thin slabs are produced on Bogenstranggießanlagen with horizontal outlet direction. The method comprises the process steps: rolling the thin slab after solidification of the strand in an arcuate guide shaft at temperatures of more than 1100 ° C, cooling the slabs during radiation or descaling, inductive reheating to a temperature of about 1100 ° C and rolling the thin slab in at least one rolling mill. By means of the heating, a temperature is set in the slab, so that sets a temperature gradient at the deformation means of the rolling train in such a way that when tapping into the last roll stand, the temperature is within sufficient for a good deformation order of magnitude. Here, in a third and last roll stand of the rolling train, the rolling stock temperature dropped, for example, to 988 ° C and sufficient as a tapping temperature for the last forming step. The rolling stock leaves the last mill stand with a temperature of 953 ° C or less and is then separated at a further lowered temperature in the desired lengths, stacked or reeled. If necessary, one or more stages of inductive intermediate heating may be provided between the individual stands.

Beiden bekannten Verfahren ist gemeinsam, dass die Einlauftemperatur in die Fertigwalzstufe so eingestellt wird, dass die festgelegte Endwalztemperatur eingehalten werden kann.Both known methods have in common that the inlet temperature is set in the finish rolling stage so that the specified Endwalztemperatur can be maintained.

Der Erfindung liegt die Aufgabe zugrunde, die Wärmebehandlung bei Warmbandvormaterial aus Silizium -legierten Stählen für die Weiterverarbeitung zu kornorientierten Blechen dahingehend zu optimieren, dass in der Walzstraße eine gewünschte Endtemperatur und damit ein gewünschtes Gefüge im Strang eingestellt werden kann.The invention has for its object to optimize the heat treatment in hot strip pre-material of silicon-alloyed steels for further processing to grain-oriented sheets to the effect that in the rolling mill a desired final temperature and thus a desired microstructure can be set in the strand.

Die Aufgabe wird durch das in Anspruch 1 beanspruchte Verfahren gelöst.The object is achieved by the method claimed in claim 1.

Mit dem erfindungsgemäßen Verfahren wird erstmalig auf einfache Weise eine Einlauftemperatur in die Fertigstrasse eingestellt, welche eine günstige Ausscheidungsmorphologie bei dem Walzgut gewährleistet. Im Stand der Technik bekannte einstufige Temperatur-Einstellsysteme sind nicht in der Lage, das Gießprodukt auf die für die Einstellung des hier gewünschten / erforderlichen Rekristallisationszustandes erforderlichen hohen Temperaturen von vorzugsweise über 1250 °C Einlauftemperatur in die Walzstraße aufzuheizen. Die hohen Temperaturen werden bei dem beanspruchten Verfahren vorteilhafterweise dadurch erreicht, dass eine zweistufige Vorerwärmung des Gießproduktes, umfassend eine primärenergiebeheizte und eine induktiv beheizte Stufe, durchgeführt wird. Die beanspruchte zweistufige Wärmevorbehandlung hat weiterhin den Vorteil, dass sie das Gießprodukt nicht nur - falls erforderlich - auf Temperaturen über 1250 °C, sondern auch auf niedrigere Einlauftemperaturen aufheizen lassen, wenn dies zur Einstellung anderer gewünschter Gefüge- bzw. Rekristallisationszustände erforderlich sein sollte; insofern ist das beanspruchte Verfahren sehr universell einsetzbar.With the method according to the invention, for the first time in a simple manner, an inlet temperature is set in the finishing train, which ensures a favorable precipitation morphology in the rolling stock. Known in the art single-stage temperature-adjusting systems are not able to heat the cast product to the required for setting the desired / required recrystallization state high temperatures of preferably more than 1250 ° C inlet temperature in the rolling mill. The high temperatures are advantageously achieved in the claimed method in that a two-stage preheating of the cast product, comprising a Primärergiebeheizte and an inductively heated stage is performed. The claimed two-stage heat treatment also has the advantage that it can heat the cast product not only - if necessary - to temperatures above 1250 ° C, but also to lower inlet temperatures, should this be necessary to set other desired structural or recrystallization conditions; In this respect, the claimed method is very universally applicable.

Die Steuerung der Temperatur in der nachfolgenden Fertigwalzstrasse richtet sich nach dem zu erreichenden Endgefüge und wird über eine Kombination von Walzgeschwindigkeit und Nutzung von Zwischengerüstkühlungen eingestellt.The control of the temperature in the subsequent finishing train depends on the final structure to be achieved and is set via a combination of rolling speed and use of inter-frame cooling.

Bei einer bevorzugten Ausführungsform der vorliegenden Erfindung hinsichtlich des Verfahrens wird die Endwalztemperatur (TWE) und die Endwalzgeschwindigkeit des Walzgutes auf Werte eingestellt, bei denen keine vollständige Rekristallisation des Stahles mehr erfolgt und das Walzgut wird nach dem letztenIn a preferred embodiment of the present invention with regard to the method, the final rolling temperature (T WE ) and the final rolling speed of the rolling stock are set to values at which no complete recrystallization of the steel takes place, and the rolling stock becomes after the last

Stich in der Warmwalzstrasse von der Endwalztemperatur (TWE) auf eine Temperatur (TA) abgeschreckt, die die Einstellung bzw. Einfrierung eines gewünschten Rekristallistionszustandes über die Banddicke sicherstellt. Dabei wird die Endwalztemperatur (TWE) des Walzgutes auf Temperaturen von mindestens 950°C, vorzugsweise oberhalb von 1000°C, eingestellt und anschließend, vorzugsweise im unmittelbaren Anschluss, das Walzgut auf Temperaturen (TA) von unterhalb 450 °C innerhalb von 10 s abgeschreckt.Stitch in the hot rolling line of the final rolling temperature (T WE ) to a temperature (T A ) quenched, which ensures the setting or freezing a desired Rekristallistionszustandes over the strip thickness. In this case, the final rolling temperature (T WE ) of the rolling stock to temperatures of at least 950 ° C, preferably above 1000 ° C, set and then, preferably in immediate connection, the rolling stock to temperatures (T A ) of below 450 ° C within 10 s deterred.

Dabei wird eine vollständige Rekristallisation des Warmbandes unterdrückt. Durch die Wahl der Haspeltemperatur lässt sich der Anteil des rekristallisierten Gefüges über die Banddicke einstellen.In this case, a complete recrystallization of the hot strip is suppressed. By selecting the reel temperature, the proportion of the recrystallized structure can be adjusted via the strip thickness.

Nach einem weiteren Ausgestaltungsmerkmal der vorliegenden Erfindung ist vorgesehen, dass in der Vorwärmstufe die Temperatur des Gießproduktes auf Werte zwischen 1000 und 1100 °C eingestellt wird und dass in der sich anschließenden Intensivheizstufe die Temperatur auf Werte von 1250 °C erhöht wird. Dabei wird in bevorzugter Ausgestaltung die Vorwärmstufe in einem gas- oder ölbeheiztem Ofen und die sich anschließende Intensivheitstufe in einer Induktionsheizstufe durchgeführt. Dies weist den besonderen Vorteil auf, dass die Vorwärmung in einem Rollenherdofen stattfinden kann, während der Aufheizschritt bis zu Temperaturen oberhalb 1200°C in eine induktive Heizzone verlagert wird. Damit wird verhindert, dass der Rollenherdofen zu sehr belastet wird, was gegebenenfalls zu seiner thermischen Zerstörung führen könnte.According to a further embodiment feature of the present invention, it is provided that in the preheating stage, the temperature of the cast product is set to values between 1000 and 1100 ° C and that in the subsequent intensive heating stage, the temperature is increased to values of 1250 ° C. In this case, in a preferred embodiment, the preheating stage is carried out in a gas- or oil-fired oven and the subsequent intensive stage in an induction heating stage. This has the particular advantage that the preheating can take place in a roller hearth furnace, while the heating step is shifted to temperatures above 1200 ° C in an inductive heating zone. This prevents that the roller hearth furnace is charged too much, which could possibly lead to its thermal destruction.

Um die nachteilige Auswirkung einer stark erhitzten Primärzunderschicht auf die Oberflächenqualität des Walzgutes zu vermeiden, wird die Brammenoberfläche entzundert. Hierzu wird nach einem weiteren Ausgestaltungsmerkmal der vorliegenden Erfindung zwischen der Vorwärmstufe und der Intensivheizstufe eine Entzunderung in einer Entzunderungseinrichtung durchgeführt. Die Einstellung der Einlauftemperatur in die Fertigwalzstufe erfolgt also danach mittels Induktionsheizstufe. Die Fertigwalzstufe kann dabei aus einer ein- oder mehrgerüstigen Vorstaffel und einer mehrgerüstigen Endstaffel bestehen. Die Distanz zwischen diesen beiden kann dabei durch einen Rollgang oder bezeizten Wärmetunnel überbrückt werden.In order to avoid the adverse effect of a highly heated primary scale on the surface quality of the rolling stock, the slab surface is descaled. For this purpose, according to a further embodiment feature of the present invention, descaling is carried out in a descaling device between the preheating stage and the intensive heating stage. The setting of the inlet temperature in the finish rolling stage is then carried out by means of induction heating. The finish rolling stage can consist of a single or multi-stand Pre-season and a mehrgerüstigen final season consist. The distance between these two can be bridged by a roller table or bezeizten heat tunnel.

Um die Oberflächenqualität weiterhin zu verbessern, ist nach einem weiteren Ausgestaltungsmerkmal der vorliegenden Erfindung vorgesehen, dass nach der Intensivheizstufe eine weitere Entzunderung in einer zweiten Entzunderungsstufe durchgeführt wird.In order to further improve the surface quality, it is provided according to a further embodiment feature of the present invention that, after the intensive heating stage, further descaling is carried out in a second descaling stage.

Im Übrigen ist vorgesehen, zusätzlich oder allein zu den genannten Entzunderungen bereits vor dem Rollenherdofen eine Entfernung des Zunders durchzuführen, um die Rollen des Ofens vor Zunderanwachsungen und damit die Brammenunterseite vor unerwünschten Markierungen zu schützen und den Wärmeübergang in die Bramme zu verbessern.Incidentally, it is envisaged, in addition to or in addition to said descaling already before the roller hearth furnace to perform a removal of the scale to protect the roles of the furnace against scale growth and thus the slab underside against unwanted marks and to improve the heat transfer into the slab.

Die der Erfindung zu Grunde liegende oben genannte Aufgabe wird weiterhin durch die in Anspruch 7 beanspruchte Anlage gelöst. Bezüglich der sich dabei ergebenden Vorteile wird zur Vermeidung von Wiederholungen auf die oben beschriebenen Vorteile des erfindungsgemäßen Verfahrens verwiesen.The object of the invention underlying above is further solved by the claimed in claim 7 system. With regard to the resulting advantages, reference is made to avoid repetition on the above-described advantages of the method according to the invention.

Bei der erfindungsgemäßen Anlage ist vorgesehen, dass die Einrichtung zum Abkühlen des Walzgutes Komponenten zum Abschrecken des Walzgutes auf Temperaturen unterhalb von 450 °C umfasst.In the system according to the invention it is provided that the device for cooling the rolling stock comprises components for quenching the rolling stock to temperatures below 450 ° C.

Es empfiehlt sich nach einem weiteren Ausgestaltungsmerkmal der vorliegenden Erfindung, dass die Warmwalzstrasse als kompakte Fertigstrasse ausgebildet ist. Nach einem dazu alternativen Ausgestaltungsmerkmal ist vorgesehen, dass die Warmwalzstrasse in wenigstens eine Vor- und wenigstens eine Endwalzstaffel aufgeteilt ausgebildet ist.It is recommended according to a further embodiment feature of the present invention that the hot rolling train is designed as a compact finishing line. According to an alternative design feature, it is provided that the hot rolling line is formed divided into at least one pre-and at least one Endwalzstaffel.

Weitere Vorteile und Einzelheiten der Erfindung ergeben sich aus den Unteransprüchen und aus der nachfolgenden Beschreibung, in der die in den Figuren dargestellten Ausführungsformen der Erfindung näher erläutert werden. Dabei sind neben den oben angeführten Kombinationen von Merkmalen auch Merkmale allein oder in anderen Kombinationen erfindungswesentlich.Further advantages and details of the invention will become apparent from the dependent claims and from the following description in which the embodiments of the invention shown in the figures are explained in more detail. In addition to the above-mentioned combinations of features, features alone or in other combinations are essential to the invention.

Es zeigt:

Fig. 1
eine schematische Darstellung einer Anlage zur Durchführung des erfindungsgmäßen Verfahrens.
It shows:
Fig. 1
a schematic representation of a system for carrying out the erfindungsgmäßen process.

Fig. 1 zeigt eine Anlage 1 zur Herstellung von Walzgut in Form von Blechen oder Bändern aus Silizium-legiertem Stahl zur Weiterverarbeitung zu kornorientierten Blechen, wie beispielsweise Elektroblechen, welche ohne zwischenzeitliche Abkühlung auf Raumtemperatur wärmebehandelt und gewalzt werden, so dass danach das Walzgut mit gewünschten Gefügeeigenschaften zur Verfügung steht. Die Anlage 1 umfasst eine Stranggießanlage 1a. Der endabmessungsnah gegossene Strang in Form eines Gießproduktes 2 wird vor dem Rollenherdofen 3 mit Hilfe einer Schere 4 in Brammen geschnitten, welche dann aus der Gießhitze kommend direkt in den Rollenherdofen 3 eintreten, um auf Temperaturen von 1000 bis 1100°C erwärmt zu werden bzw. einen Temperaturausgleich zu erfahren. Bei den Brammen handelt es sich vorzugsweise um Dünnbrammen mit einer Dicke von bis zu 120 mm. Die erwärmten Brammen durchlaufen danach vorzugsweise eine Entzunderungseinrichtung 5 und laufen anschließend in eine Intensivheizstufe 6 ein. Hier werden die Brammen in einem kurzen schnellen Erwärmungsprozess auf Einlauftemperaturen von 1100 bis 1300°C, vorzugsweise über 1250°C aufgeheizt. Die Vorwärmstufe 3 wird dabei in einem gas- oder ölbeheiztem Ofen wie einem Rollenherdofen 3 und die sich anschließende Intensivheitstufe 6 in einer Induktionsheizstufe durchgeführt. Die Intensivheizstufe 6 muss dabei ausgebildet sein, um eine Einlauftemperatur Tein des Gießproduktes 2 in das Walzwerk von mehr als 1200°C zu gewährleisten. Die Vorwärmstufe 3 und die Intensivheizstufe 6 bilden ein Temperatur- Einstellsystem 7. Die Mittel zur Durchführung der Wärmebehandlung umfassen die Vorwärmstufe 3, die Intensivheizstufe 6 sowie Zwischengerüstkühleinrichtungen 10. Fig. 1 shows a plant 1 for the production of rolling stock in the form of sheets or strips of silicon-alloyed steel for further processing into grain-oriented sheets, such as electric sheets, which are heat treated and rolled without intermediate cooling to room temperature, so that then the rolling stock with desired structural properties available stands. The plant 1 comprises a continuous casting plant 1a. The near net cast strand in the form of a cast product 2 is cut in front of the roller hearth furnace 3 using a pair of scissors 4, which then come directly from the casting heat in the roller hearth furnace 3 to be heated to temperatures of 1000 to 1100 ° C or to learn a temperature compensation. The slabs are preferably thin slabs with a thickness of up to 120 mm. The heated slabs then preferably pass through a descaling device 5 and then enter an intensive heating stage 6. Here, the slabs are heated in a short rapid heating process at inlet temperatures of 1100 to 1300 ° C, preferably above 1250 ° C. The preheating stage 3 is carried out in a gas or oil-fired furnace such as a roller hearth furnace 3 and the subsequent Intensivheitstufe 6 in an induction heating. The Intensivheizstufe 6 must be designed to ensure an inlet temperature T a of the cast product 2 in the rolling mill of more than 1200 ° C. The preheating stage 3 and the intensive heating stage 6 form a temperature Adjusting System 7. The means for performing the heat treatment include the preheating stage 3, the intensive heating stage 6, and the interstand cooling means 10.

Nach dem Durchlaufen der Intensivheizstufe 6 wird das Gießprodukt 2 nochmals entzundert (zweite Entzunderungsstufe 8) und in eine Warmwalzstrasse 9a oder 9b eingeführt. Die Warmwalzstrasse 9a oder 9b kann eine kompakte Fertigstrasse 9a darstellen oder in eine Vor- und eine Endwalzstaffel 9b aufgeteilt sein. Die Anzahl der Gerüste in jeder der beiden Teilstaffeln ist nicht festgelegt.After passing through the intensive heating stage 6, the cast product 2 is again descaled (second descaling stage 8) and introduced into a hot rolling line 9a or 9b. The hot rolling train 9a or 9b may be a compact finishing line 9a or divided into a preliminary and a final rolling 9b. The number of scaffolds in each of the two partial scales is not fixed.

Bei dem erfindungsgemäßen Verfahren ist nun vorgesehen, dass zur Einstellung der Endwalztemperatur TWE eine Einlauftemperatur Tein des Gießproduktes 2 in die Warmwalzstrasse 9a oder 9b des Walzwerkes von mindestens 1200 °C, bevorzugt oberhalb von 1250°C, durch eine mehrstufige Wärmebehandlung eingestellt wird, wobei das Gießprodukt aus der Gießhitze kommend direkt der Wärmevorbehandlung zu geführt wird. Die mehrstufige Wärmevorbehandlung erfolgt mit dem Temperatur-Einstellsystem 7, welches die Vorwärmstufe 3 zum Vorwärmen des Gießproduktes 2 und die Intensivheizstufe 6 zur Einstellung der Einlauftemperatur Tein des Gießproduktes 2 in die Warmwalzstrasse umfasst. Bei dem erfindungsgemäßen Verfahren wird die Endwalztemperatur TWE und die Endwalzgeschwindigkeit des Walzgutes auf Werte eingestellt, bei denen keine vollständige Rekristallisation des Stahles mehr erfolgt. Das Walzgut wird nach dem letzten Stich in der Warmwalzstrasse im Rahmen einer Wärmenachbehandlung von der Endwalztemperatur TWE auf eine Temperatur TA abgeschreckt, wodurch der gewünschte Rekristallistionszustand des Walzgutes am Ende der Warmwalzstraße über die Banddicke sicherstellt wird. Dabei wird die Endwalztemperatur TWE des Walzgutes auf Temperaturen von mindestens 950°C, vorzugsweise oberhalb von 1000°C, eingestellt, und anschließend wird das Walzgut auf Temperaturen TA von unterhalb 450 °C innerhalb von 10 s, abgeschreckt. Fig. 1 In the inventive process is now provided that for setting the finish rolling temperature T WE an inlet temperature T a of the cast product 2 in the hot rolling line 9a or 9b is preferably set above 1250 ° C by a multi-stage heat treatment of the mill of at least 1200 ° C, wherein the cast product from the casting heat coming directly to the heat pretreatment is performed. The multi-stage heat pretreatment takes place with the temperature setting system 7, which includes the preheating stage 3 for preheating the cast product 2 and the intensive heating stage 6 for adjusting the inlet temperature T a of the cast product 2 in the hot rolling line. In the method according to the invention, the final rolling temperature T WE and the final rolling speed of the rolling stock are set to values at which complete recrystallization of the steel no longer takes place. The rolling stock is quenched after the last pass in the hot rolling line in the context of post-heat treatment from the final rolling temperature T WE to a temperature T A , whereby the desired Rekristallistionszustand of the rolling stock at the end of the hot rolling over the strip thickness is ensured. In this case, the final rolling temperature T WE of the rolling stock to temperatures of at least 950 ° C, preferably above 1000 ° C, adjusted, and then the rolling stock to temperatures T A of below 450 ° C within 10 seconds, quenched. Fig. 1

Bei der Wärmenachbehandlung nach dem Walzen handelt es sich um eine Kombination aus einer Schnellkühleinrichtung 12 und normalen Kühlbalken mit Wasserkühlung 13. Das abgekühlte Walzgut wird nachfolgend auf einer Haspeleinrichtung 14 aufgewickelt.The post-rolling heat post-treatment is a combination of a rapid-cooling device 12 and normal cooling bars with water cooling 13. The cooled rolling stock is subsequently wound on a reeling device 14.

BezugszeichenlisteLIST OF REFERENCE NUMBERS

11
Anlage zur Herstellung von WarmbandPlant for the production of hot strip
1a1a
Stranggießanlagecontinuous casting plant
22
Gießprodukt (Strang)Cast product (strand)
33
Einrichtung zum Vorwärmen (Rollenherdofen)Device for preheating (roller hearth furnace)
44
Scherescissors
55
Entzunderungseinrichtungdescaling
66
IntensivheizstufeIntensivheizstufe
77
Temperatur- EinstellsystemTemperature adjustment system
88th
zweite Entzunderungsstufesecond descaling step
9a9a
kompakte Fertigstrasse als Warmwalzstrassecompact finishing mill as hot rolling mill
9b9b
Vor- und Endwalzstaffel der WarmwalzstrassePre and final rolling of the hot rolling line
1010
ZwischengerüstkühleinrichtungIntermediate stand cooling device
1111
Einrichtung zum Abkühlen (Kühlstrecke)Device for cooling (cooling section)
1212
SchnellkühleinrichtungQuick cooling device
1313
Kühlbalken mit WasserkühlungChilled beam with water cooling
1414
Haspeleinrichtungcoiler

Claims (9)

  1. Method of producing hot-strip rolling material from a cast product, for example a thin slab, wherein the cast product (2) is subjected to a heat pretreatment in a first step and the preheated cast product is subjected to a rolling process in a hot-rolling train in a second step, wherein the rolling material is in this way transferred to a recrystallisation state, which is suitable with respect to later further processing, at a desired final rolling temperature (TWE), and the final rolling temperature (TWE) of the rolling material is set to temperatures of at least 950° C, preferably above 1,000° C, wherein the cast product (2) within the scope of the heat pretreatment for setting the final rolling temperature (TWE) of the rolling material in the hot-rolling train runs through at least one preheating stage (3) and intensive heating stage (6) and in this way is preheated to an entry temperature (Tein) of at least 1,200° C for entry into the hot-rolling train (9a or 9b) and wherein descaling is carried out in a descaling device ahead of the preheating stage (3),
    characterised in that
    for producing silicon-alloyed steels for further processing to form grain-oriented sheets such as, for example, magnetic steel sheets the control of the temperature in the rolling train (9a and 9b) is set by way of a combination of rolling speed and use of intermediate stand cooling devices (10), wherein after hot rolling the rolling material is quenched to temperatures (TA) of below 450° C within 10 seconds.
  2. Method according to claim 1, characterised in that the final rolling temperature (TWE) and the final rolling speed of the rolling speed of the rolling material are set to a value in which complete recrystallisation of the steel no longer takes place and the rolling material after the last pass in the hot-rolling train is quenched from final rolling temperature (TWE) to a temperature (TA) which ensures freezing of the desired recrystallisation state, which is set at the end of the hot-rolling train, over the strip thickness.
  3. Method according to one of claims 1 and 2, characterised in that in the preheating stage (3) the temperature of the cast product (2) is set to values between 1,000 and 1,100° C and that in the subsequent intensive heating stage (6) the temperature is increased to values of 1,250° C.
  4. Method according to any one of claims 1 to 3, characterised in that the preheating stage (3) is carried out in a gas-heated or oil-heated furnace and the subsequent intensive heating stage (6) in an induction heating stage.
  5. Method according to any one of claims 1 to 4, characterised in that descaling in a descaling device (5) is carried out between the preheating stage (3) and the intensive heating stage (6).
  6. Method according to any one of claims 1 to 5, characterised in that after the intensive heating stage (6) a further descaling is carried out in a second descaling stage (8).
  7. Plant (1) for producing hot-strip rolling material for later further processing to form grain-oriented sheets, through use of the method according to any one of claims 1 to 6, wherein the plant comprises:
    a continuous casting plant (1 a) for producing the cast product (2);
    a temperature setting system (7) for preheating the cast products; and
    a rolling mill (9a or 9b) downstream of the temperature setting system (7), wherein the temperature setting system (7) and the rolling mill (9) serve the purpose of transferring the cast product (2) into the rolling material with a recrystallisation state, which is suitable with respect to later further processing, at a specific final rolling temperature (TWE), wherein the temperature setting system (7) comprises, for setting the final rolling temperature (TWE) of the rolling material in the rolling train, a preheating stage (3) for preheating the cast product (2) and an intensive heating stage (6) for intensive heating of the cast product (2) to an entry temperature (Tein) in the hot-rolling train above 1,200° C, preferably above 1,250° C, and a descaling device is provided in front of the preheating stage (3);
    characterised in that
    a device (11) for cooling the rolling material comprises components for quenching the rolling material to temperatures below 450° C within 10 seconds and the rolling material is constructed in the form of silicon-alloyed steels such as, for example, magnetic steel plates, and the hot-rolling mill (9a, 9b) comprises intermediate stand cooling devices (10), which serve in combination with the rolling speed for controlling the final rolling temperature (TWE).
  8. Plant according to claim 7, characterised in that the hot-rolling train is constructed as a compact finishing train (9a).
  9. Plant according to claim 7, characterised in that the hot-rolling train is constructed to be divided into at least one pre-rolling echelon and at least one final rolling echelon (9b).
EP07764798.0A 2006-06-26 2007-06-22 A method and a system for producing hot-rolled strip silicon steel based on thin slabs Active EP2035587B1 (en)

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WO2021038108A1 (en) 2019-08-30 2021-03-04 Sms Group Gmbh Method for the heat treatment of a primary steel product

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