EP1713977B1 - Method and device for heating worn road coating materials - Google Patents
Method and device for heating worn road coating materials Download PDFInfo
- Publication number
- EP1713977B1 EP1713977B1 EP05717706.5A EP05717706A EP1713977B1 EP 1713977 B1 EP1713977 B1 EP 1713977B1 EP 05717706 A EP05717706 A EP 05717706A EP 1713977 B1 EP1713977 B1 EP 1713977B1
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- European Patent Office
- Prior art keywords
- heating
- recycled
- road materials
- chamber
- coated road
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- 238000010438 heat treatment Methods 0.000 title claims description 38
- 238000000034 method Methods 0.000 title claims description 21
- 239000000463 material Substances 0.000 title claims description 20
- 239000011248 coating agent Substances 0.000 title description 5
- 238000000576 coating method Methods 0.000 title description 5
- 239000010426 asphalt Substances 0.000 claims description 51
- 238000012546 transfer Methods 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 239000000654 additive Substances 0.000 claims description 5
- 238000001704 evaporation Methods 0.000 claims description 4
- 230000008020 evaporation Effects 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 230000005484 gravity Effects 0.000 claims description 3
- 239000003054 catalyst Substances 0.000 claims description 2
- 238000000354 decomposition reaction Methods 0.000 claims description 2
- 238000007599 discharging Methods 0.000 claims 2
- 239000000203 mixture Substances 0.000 description 12
- 239000007789 gas Substances 0.000 description 9
- 230000005855 radiation Effects 0.000 description 5
- 238000004064 recycling Methods 0.000 description 5
- 239000000567 combustion gas Substances 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 230000032683 aging Effects 0.000 description 3
- 230000015556 catabolic process Effects 0.000 description 3
- 238000006731 degradation reaction Methods 0.000 description 3
- 230000007613 environmental effect Effects 0.000 description 3
- 239000000446 fuel Substances 0.000 description 3
- 238000009434 installation Methods 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 230000008901 benefit Effects 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000009792 diffusion process Methods 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 238000001033 granulometry Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 230000008929 regeneration Effects 0.000 description 2
- 238000011069 regeneration method Methods 0.000 description 2
- 238000012958 reprocessing Methods 0.000 description 2
- 238000010792 warming Methods 0.000 description 2
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 230000004523 agglutinating effect Effects 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000007767 bonding agent Substances 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000002366 mineral element Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000013022 venting Methods 0.000 description 1
- 239000012855 volatile organic compound Substances 0.000 description 1
Images
Classifications
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- E—FIXED CONSTRUCTIONS
- E01—CONSTRUCTION OF ROADS, RAILWAYS, OR BRIDGES
- E01C—CONSTRUCTION OF, OR SURFACES FOR, ROADS, SPORTS GROUNDS, OR THE LIKE; MACHINES OR AUXILIARY TOOLS FOR CONSTRUCTION OR REPAIR
- E01C19/00—Machines, tools or auxiliary devices for preparing or distributing paving materials, for working the placed materials, or for forming, consolidating, or finishing the paving
- E01C19/02—Machines, tools or auxiliary devices for preparing or distributing paving materials, for working the placed materials, or for forming, consolidating, or finishing the paving for preparing the materials
- E01C19/10—Apparatus or plants for premixing or precoating aggregate or fillers with non-hydraulic binders, e.g. with bitumen, with resins, i.e. producing mixtures or coating aggregates otherwise than by penetrating or surface dressing; Apparatus for premixing non-hydraulic mixtures prior to placing or for reconditioning salvaged non-hydraulic compositions
- E01C19/1013—Plant characterised by the mode of operation or the construction of the mixing apparatus; Mixing apparatus
- E01C19/1027—Mixing in a rotary receptacle
- E01C19/1036—Mixing in a rotary receptacle for in-plant recycling or for reprocessing, e.g. adapted to receive and reprocess an addition of salvaged material, adapted to reheat and remix cooled-down batches
-
- E—FIXED CONSTRUCTIONS
- E01—CONSTRUCTION OF ROADS, RAILWAYS, OR BRIDGES
- E01C—CONSTRUCTION OF, OR SURFACES FOR, ROADS, SPORTS GROUNDS, OR THE LIKE; MACHINES OR AUXILIARY TOOLS FOR CONSTRUCTION OR REPAIR
- E01C19/00—Machines, tools or auxiliary devices for preparing or distributing paving materials, for working the placed materials, or for forming, consolidating, or finishing the paving
- E01C19/02—Machines, tools or auxiliary devices for preparing or distributing paving materials, for working the placed materials, or for forming, consolidating, or finishing the paving for preparing the materials
- E01C19/10—Apparatus or plants for premixing or precoating aggregate or fillers with non-hydraulic binders, e.g. with bitumen, with resins, i.e. producing mixtures or coating aggregates otherwise than by penetrating or surface dressing; Apparatus for premixing non-hydraulic mixtures prior to placing or for reconditioning salvaged non-hydraulic compositions
- E01C19/1004—Reconditioning or reprocessing bituminous mixtures, e.g. salvaged paving, fresh patching mixtures grown unserviceable; Recycling salvaged bituminous mixtures; Apparatus for the in-plant recycling thereof
-
- E—FIXED CONSTRUCTIONS
- E01—CONSTRUCTION OF ROADS, RAILWAYS, OR BRIDGES
- E01C—CONSTRUCTION OF, OR SURFACES FOR, ROADS, SPORTS GROUNDS, OR THE LIKE; MACHINES OR AUXILIARY TOOLS FOR CONSTRUCTION OR REPAIR
- E01C19/00—Machines, tools or auxiliary devices for preparing or distributing paving materials, for working the placed materials, or for forming, consolidating, or finishing the paving
- E01C19/02—Machines, tools or auxiliary devices for preparing or distributing paving materials, for working the placed materials, or for forming, consolidating, or finishing the paving for preparing the materials
- E01C19/10—Apparatus or plants for premixing or precoating aggregate or fillers with non-hydraulic binders, e.g. with bitumen, with resins, i.e. producing mixtures or coating aggregates otherwise than by penetrating or surface dressing; Apparatus for premixing non-hydraulic mixtures prior to placing or for reconditioning salvaged non-hydraulic compositions
- E01C2019/1081—Details not otherwise provided for
- E01C2019/109—Mixing containers having a counter flow drum, i.e. the flow of material is opposite to the gas flow
Definitions
- the present invention relates to a method and a device for heating road asphalt, in particular used asphalt for recycling.
- the manufacture of asphalt mix includes a first step of processing aggregates.
- These aggregates are of different particle sizes and mixed in suitable proportions to obtain a base of aggregates studied according to the coating to be produced.
- the aggregates must be free of water and facilities take advantage of the rise in temperature required for this coating to dry the aggregates in a preliminary step.
- One of the means for heating these aggregates is to use a rotary drum type oven, inclined, with a burner that emits a flame, this preferably against the flow of aggregates flow, the displacement of the aggregates being obtained by a suitable inclination of the drum .
- a suitable rotation and fins and other stirring means disposed on the internal walls of said drum to obtain the proper speed of movement and the desired brewing.
- the burner is fed with liquid or gaseous petroleum fuel and the flame generated is in profile adapted for propagation along the longitudinal axis of the drum.
- the aggregates are thus subjected to heating by the various transmission means: convection, conduction and radiation.
- hot aggregates are then optionally sieved and stored and then metered and stirred in kneaders in the presence of hot new bitumen otherwise preserved in order to coat them and obtain a mix ready to be used.
- the coating operation is carried out in the final part of the heating drum, before leaving.
- addition fines are added in addition to recovery fines after filtration of the heating gases at the time of coating so as to obtain more compact asphalt layers.
- the mix thus prepared is then deposited on a prepared surface to receive it and it is compacted energetically before cooling. During this cooling step, the bitumen acts as a cohesion and bonding agent.
- the hot recycling of asphalt mixes consists in using for a part or even all road costs.
- These recovered mixes consist of isolated aggregates but also agglomerates whose elements are strongly bound by bitumen.
- the analysis of the asphalt to be recycled indicates the granulometry of the mixture, the nature and the content of the bitumen present. The knowledge of these parameters will allow complementary bitumen supply operations and / or specific additives as well as additional new aggregates and / or correctors.
- the problem is the treatment of recycled asphalt because it is necessary to bring to temperature aggregates that are already coated with bitumen and which are in the form of small or large particles isolated or in the form of agglomerates with bitumen contained within even of these agglomerates.
- the flame which is of the order of 1100 ° C. at the burner outlet, propagates while maintaining 900 ° C. at its end.
- the gases then pass 700 ° C outside the flame zone to fall to about 200 ° C, that is to say 50 ° C above the temperature to be reached within the same asphalt.
- the fines present are entrained with the gaseous effluents.
- the small size and their limited mass induce a very rapid temperature rise compared to other aggregates and thus a quick and easy detachment of the support.
- Recycling must be able to be applied as well from production units established in a fixed place, from dismountable and mobile installations as for units operating directly on the roadway to be treated. For the latter operating by continuous reprocessing on costs also produced continuously, the problems mentioned above are intensified, especially the rejections. Similarly with the devices heating the surface of the roadway to be recycled, it is difficult to achieve diffusion in the thickness of the asphalt layer due to poor heat transfer and degradation consequences of the bitumen.
- a document DE-B-2916187 aims to solve some problems including the transfer of used asphalt through conveyors stacked superimposed into each other successively. Nevertheless, the The method does not provide heating at two temperatures in two modules in order to treat the different compounds of bitumens according to their degree of volatility.
- This device provides either a heating with heating conveyor soles or a flame heating but no radiant heating on top of used road asphalt is provided to refine the heating temperature of each sole or part of hearth.
- the present invention proposes solutions to overcome the problems mentioned in the preamble and uses heating means by radiant panels with a particular arrangement for illustrating the method and provide a solution in terms of device, satisfactory but not limiting.
- the method according to the present invention consists in treating asphalt mixes in a device equipped with radiant heating means by panels.
- milled mixes are used for the description of the description, but also the mixes resulting from mechanical block and crushed shrinkage.
- radiant heating panels used cover any surface arrangement capable of emitting radiation leading to radiant heating.
- the maximum point temperature reached can not exceed the deterioration temperature of the bitumens as will be indicated below.
- the aggregate mixture aggregate has a specific surface area of 15 to 20 m 2 per kilogram with about 50 grams of bitumen, which leads to thicknesses of bitumen films of a few microns.
- fractions of mineral elements small fine and very fine. These fractions concentrate a greater quantity of bitumen due to differences in specific surface area.
- the method also consists of mechanical conveying preferentially by gravity but also by forced conveying and with vibrations. These vibrations, in their emission, will have at least one vertical component, preferably with a high amplitude, so as to allow a regular reversal of the grains. This change of orientation allows a homogeneity of presentation of the entire surface of each grain in front of the infrared radiation of the radiant heating means.
- bitumen is not exposed in an extreme way to the air and therefore to the oxygen it contains, which can cause accelerated oxidation and aging.
- the associated device is represented on the figure 1 . It comprises a first enclosure 10 in which conveyors or transfer belts 12 are arranged. This enclosure is of substantially parallelepipedal shape in this embodiment to be the simplest.
- the device In the case of mobile machines, the device is necessarily the road gauge to allow movement and positioning in the immediate vicinity of construction sites. This same limitation to the road gauge is applicable to mobile machines moving continuously along the site to work the costs as and when continuous.
- the limitation of the size of the device and the need for a sufficient residence time of the mixes generate constraints.
- transfer mats arranged one below the other, these mats being inclined or horizontal and vibrated by any means 14 adapted to vibration and for example unbalance motors.
- heating means of radiant type in the form of panels 18. The power, the distribution and the power supply means must be adapted to the processing capacity.
- the materials to be treated contain a certain amount of water that must be removed and the residence time
- the heating power are parameters to be taken into account also when sizing the installation.
- the temperature of the asphalt to be reached at the outlet is of the order of 105 to 130 ° C. so as to bring the bitumen into the viscous state and cause complete evaporation of the water and completely dry the introduced materials.
- the method then provides a second step which consists of bringing the mix to the final working temperature, ie 160 to 220 ° C, into a second module.
- the grains and agglomerates derived from the first module are preferably continuously introduced into means for agglutinating fine elements, grains and agglomerates. The fines ensure cohesion.
- the heat output is modified to fill the heat sink and reach the desired temperature.
- the second module presented in figure 2 is substantially identical in design to the first module and the identical elements bear the same references with a "".
- the mixes resulting from this second module can be composed of 100% of materials to be recycled. It is necessary to add regeneration additives of the old bitumen, this operation to be carried out in a kneader, in a known manner. These additives are preheated and dosed in an amount related to the mass flow rate of recycled mixes in a continuous production unit or a mass of previously weighed mixes before introduction into the mixer for a discontinuous unit.
- the mixes from this second module can be recycled with a supply of virgin aggregates which are introduced together with the asphalt used in the first module.
- This virgin material is also prepared in a known manner.
- bitumen supplied by the used asphalt In addition to the bitumen supplied by the used asphalt, it is added regeneration additives and new bitumen as well as filler.
- the mix including all or part of the recycled mix is ready for use.
- the central cylinder 100 receives heating means 124, for example a burner 126 using liquid fuel.
- heating means 124 for example a burner 126 using liquid fuel.
- the flue gases are evacuated in known manner at the upper end 128 of the central cylinder, the burner being arranged at the bottom.
- the mixes are introduced into the space between the two cylinders, in the upper part and flow by gravity downwards.
- the rotation ensures the presentation of all the faces of the grains to the infrared radiation emitted by the outer wall of the central cylinder.
- the radiating surfaces are curved and can be equipped with any suitable mixing means.
- the methods and devices according to the present invention make it possible to solve the problems posed by the recycling of old mixes while respecting the environmental constraints.
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- Engineering & Computer Science (AREA)
- Architecture (AREA)
- Civil Engineering (AREA)
- Structural Engineering (AREA)
- Road Paving Machines (AREA)
- Processing Of Solid Wastes (AREA)
- Working-Up Tar And Pitch (AREA)
- Road Paving Structures (AREA)
Description
La présente invention concerne un procédé et un dispositif de mise en température d'enrobés routiers, notamment d'enrobés usagés à recycler.The present invention relates to a method and a device for heating road asphalt, in particular used asphalt for recycling.
On connaît par la demande de brevet
La fabrication des enrobés routiers présente plusieurs étapes successives, qui nécessitent des mises en température et/ou des maintiens en température, étapes qui engendrent des contraintes auxquelles il convient d'apporter des solutions.The manufacture of road asphalt has several successive stages, which require warming up and / or maintaining temperature, steps that generate constraints that should be provided solutions.
De plus, on a conscience des contraintes imposées par les nouvelles législations sur l'environnement, ce qui explique la recherche de nouveaux procédés pour la réalisation de certaines étapes, notamment celles de mises en température. Deux situations sont à étudier distinctement, le procédé et le dispositif selon l'invention trouvant une application indistinctement dans un cas comme dans l'autre, sans modification.In addition, we are aware of the constraints imposed by the new environmental legislation, which explains the search for new processes for the achievement of certain stages, especially those of warming up. Two situations are to be studied separately, the method and the device according to the invention finding an application indistinctly in one case as in the other, without modification.
Actuellement, de façon schématique, la fabrication d'enrobés routiers comprend une première étape de traitement des granulats.Currently, schematically, the manufacture of asphalt mix includes a first step of processing aggregates.
Ces granulats sont de granulométries différentes et mélangés en proportions adaptées pour l'obtention d'une base de granulats étudiée en fonction du revêtement à réaliser.These aggregates are of different particle sizes and mixed in suitable proportions to obtain a base of aggregates studied according to the coating to be produced.
Ces granulats doivent être mélangés à du bitume, lui-même préparé par ailleurs. Pour que l'adhésion du bitume sur les granulats s'opère de la meilleure façon, il faut que le bitume, avant mélange, soit porté en température mais que les granulats le soient aussi.These aggregates must be mixed with bitumen, itself prepared elsewhere. In order for the bitumen to adhere to aggregates in the best possible way, it is necessary that the bitumen, before mixing, be raised in temperature but that the aggregates are also heated.
De plus, les granulats doivent être exempts d'eau et les installations profitent de la montée en température nécessaire pour cet enrobage pour sécher les granulats dans une étape préalable.In addition, the aggregates must be free of water and facilities take advantage of the rise in temperature required for this coating to dry the aggregates in a preliminary step.
Un des moyens pour chauffer ces granulats consiste à utiliser un four de type tambour rotatif, incliné, avec un brûleur qui émet une flamme, ceci de préférence à contre courant du flux de granulats, le déplacement des granulats étant obtenu par une inclinaison adaptée du tambour. Une rotation adaptée et des ailettes et autres moyens de brassage disposés sur les parois internes dudit tambour permettent d'obtenir la bonne vitesse de déplacement et le brassage recherché.One of the means for heating these aggregates is to use a rotary drum type oven, inclined, with a burner that emits a flame, this preferably against the flow of aggregates flow, the displacement of the aggregates being obtained by a suitable inclination of the drum . A suitable rotation and fins and other stirring means disposed on the internal walls of said drum to obtain the proper speed of movement and the desired brewing.
Le brûleur est alimenté par du combustible pétrolier liquide ou gazeux et la flamme générée est de profil adapté pour une propagation suivant l'axe longitudinal du tambour.The burner is fed with liquid or gaseous petroleum fuel and the flame generated is in profile adapted for propagation along the longitudinal axis of the drum.
Les granulats sont ainsi soumis à un chauffage par les différents moyens de transmission : convection, conduction et rayonnement.The aggregates are thus subjected to heating by the various transmission means: convection, conduction and radiation.
L'essentiel du transfert de calories est issu de la convection générée par le flux gazeux chaud de la flamme. Un courant d'air est même associé aux gaz de combustion pour faire progresser de façon adaptée ce flux gazeux chaud.Most of the heat transfer comes from the convection generated by the hot gas flow of the flame. An air stream is even associated with the combustion gases to suitably advance this hot gas stream.
Les autres modes de transfert sont mineurs, la conduction étant limitée aux contacts avec les parois et les éléments métalliques de brassage. Quant aux radiations, ce transfert n'est significatif qu'à proximité des parois et/ou de la flamme.The other modes of transfer are minor, the conduction being limited to the contacts with the walls and the metallic stirring elements. As for radiation, this transfer is significant only near the walls and / or the flame.
Les différents paramètres : débit de granulats, sens de passage des granulats par rapport à celui de la flamme, énergie de brassage et vitesses de circulation, longueur du tambour, puissance du brûleur, débit d'air, nature des combustibles et pouvoir calorifique, sont adaptés pour atteindre le résultat souhaité.The different parameters: aggregate flow rate, direction of passage of the aggregates with respect to that of the flame, stirring energy and circulation velocities, drum length, burner output, air flow rate, type of fuel and calorific value, are adapted to achieve the desired result.
On constate que durant cette étape de chauffage, il se produit une émission de gaz de combustion qui sont évacués dans l'atmosphère tout comme l'eau d'évaporation.It is found that during this heating step, there is an emission of combustion gases which are discharged into the atmosphere as the evaporation water.
Par contre, lors du brassage des granulats, il faut répondre à deux contraintes antinomiques puisque dès que les granulats sont brassés, ils génèrent des poussières et comme le débit gazeux est nécessairement important, il faut pouvoir traiter les gaz et recueillir toutes les particules fines, la quantité pouvant atteindre des valeurs de l'ordre de 200g/m3 de gaz évacué.On the other hand, when mixing aggregates, two antinomic constraints have to be met: as soon as the aggregates are stirred, they generate dust and since the gas flow is necessarily important, it is necessary to be able to treat the gases and to collect all the fine particles, the quantity that can reach values of the order of 200 g / m 3 of evacuated gas.
On peut ainsi travailler en température les granulats d'entrée, les sécher et tenir compte des contraintes environnementales pour les rejets.It is thus possible to work on the temperature of the input aggregates, to dry them and to take into account environmental constraints for discharges.
Ces granulats chauds sont ensuite éventuellement tamisés et stockés puis dosés et brassés dans des malaxeurs en présence de bitume neuf chaud conservé par ailleurs afin des les revêtir et d'obtenir un enrobé prêt à être utilisé. Dans certains cas, l'opération d'enrobage s'effectue dans la partie finale du tambour de chauffage, avant sortie.These hot aggregates are then optionally sieved and stored and then metered and stirred in kneaders in the presence of hot new bitumen otherwise preserved in order to coat them and obtain a mix ready to be used. In some cases, the coating operation is carried out in the final part of the heating drum, before leaving.
A ces enrobés sont ajoutées des fines d'apport en plus des fines de récupération après filtration des gaz de chauffage au moment de l'enrobage en sorte d'obtenir des couches d'enrobés plus compactes.To these mixes, addition fines are added in addition to recovery fines after filtration of the heating gases at the time of coating so as to obtain more compact asphalt layers.
L'enrobé ainsi préparé est ensuite déposé sur une surface préparée pour le recevoir et il est compacté de façon énergique avant son refroidissement. Lors de cette étape de refroidissement, le bitume joue son rôle d'agent de cohésion et de liaison.The mix thus prepared is then deposited on a prepared surface to receive it and it is compacted energetically before cooling. During this cooling step, the bitumen acts as a cohesion and bonding agent.
La formulation originale de l'enrobé, nature et composition du mélange de granulats, quantité et caractère évolutif du bitume, la compacité des ouches, l'intensité du trafic et la climatologie du lieu d'emploi de l'enrobé, puis les modifications de granulométrie produites par les opérations de broyage pour sa récupération ont des incidences importantes sur le recyclage des enrobés.The original formulation of the asphalt mix, nature and composition of the aggregate mix, quantity and evolutionary nature of the bitumen, the compactness of the layers, the intensity of the traffic and the climatology of the place of use of the asphalt, then the Granulometry changes produced by grinding operations for its recovery have important implications for asphalt recycling.
En effet, le recyclage à chaud des enrobés consiste à utiliser pour une part voire pour la totalité des fraisats routiers. Ces enrobés récupérés sont constitués de granulats isolés mais aussi d'agglomérats dont les éléments sont fortement liés par le bitume. L'analyse de l'enrobé à recycler indique la granulométrie du mélange, la nature et le contenu du bitume présent. La connaissance de ces paramètres permettra les opérations d'apport de bitume complémentaire et/ou d'additifs spécifiques ainsi que des granulats neufs complémentaires et/ou correcteurs.In fact, the hot recycling of asphalt mixes consists in using for a part or even all road costs. These recovered mixes consist of isolated aggregates but also agglomerates whose elements are strongly bound by bitumen. The analysis of the asphalt to be recycled indicates the granulometry of the mixture, the nature and the content of the bitumen present. The knowledge of these parameters will allow complementary bitumen supply operations and / or specific additives as well as additional new aggregates and / or correctors.
Par contre, le problème est le traitement des enrobés recyclés car il convient de porter en température des granulats qui sont déjà enrobés de bitume et qui se présentent sous forme de particules petites ou grosses isolées ou sous forme d'agglomérats avec du bitume contenu au sein même de ces agglomérats.On the other hand, the problem is the treatment of recycled asphalt because it is necessary to bring to temperature aggregates that are already coated with bitumen and which are in the form of small or large particles isolated or in the form of agglomerates with bitumen contained within even of these agglomerates.
Les installations connues qui retraitent ces enrobés sont identiques à celles pour granulats neufs. Le four rotatif équipé d'un brûleur est utilisé mais des agencements évitent de mettre en contact les enrobés directement au contact de la flamme.The known installations which reprocess these mixes are identical to those for new aggregates. The rotary kiln equipped with a burner is used but arrangements avoid contacting the asphalt directly in contact with the flame.
Or on sait que la flamme qui est de l'ordre de 1100°C en sortie de brûleur, se propage en conservant 900°C en son extrémité. Les gaz passent ensuite de 700°C hors zone de la flamme pour tomber à environ 200°C, c'est-à-dire 50°C au-dessus de la température à atteindre au sein même de l'enrobé.However, it is known that the flame, which is of the order of 1100 ° C. at the burner outlet, propagates while maintaining 900 ° C. at its end. The gases then pass 700 ° C outside the flame zone to fall to about 200 ° C, that is to say 50 ° C above the temperature to be reached within the same asphalt.
Il se produit alors différents phénomènes néfastes au sein du bitume.There are then various harmful phenomena within the bitumen.
Tout d'abord, compte tenu des températures maximales atteintes dans certaines zones du four, bien au-delà des températures d'élaboration du bitume en raffinerie, on obtient des phénomènes de dégradation par cracking et pyrolyse notamment. Ces phénomènes engendrent un vieillissement du bitume recyclé. Les gaz de combustion entraînent avec eux des composés organiques volatils, en quantité très supérieures aux normes autorisées.Firstly, given the maximum temperatures reached in certain areas of the furnace, well beyond the refining temperatures of the bitumen refinery, degradation phenomena by cracking and pyrolysis in particular. These phenomena cause an aging of bitumen recycled. The combustion gases carry with them volatile organic compounds, in quantities much higher than the authorized standards.
De plus, parallèlement au phénomène de vieillissement, le flux gazeux issu de la combustion, auquel sont ajoutées de très fortes quantités d'air pour sa diffusion dans l'enceinte, provoque une oxydation et une évaporation supplémentaire ajoutant à sa dégradation.In addition, parallel to the aging phenomenon, the gas stream from combustion, which are added very large amounts of air for its diffusion into the chamber, causes oxidation and additional evaporation adding to its degradation.
Comme dans le cas des granulats neufs, les fines présentes sont entraînées avec les effluents gazeux. Les faible taille et leur masse limitée induisent une montée en température très rapide par rapport aux autres granulats et donc un détachement rapide et aisé du support.As in the case of new aggregates, the fines present are entrained with the gaseous effluents. The small size and their limited mass induce a very rapid temperature rise compared to other aggregates and thus a quick and easy detachment of the support.
A la différence des granulats neufs, ces fines entraînées sont imprégnées de bitume donc fortement adhésives.Unlike new aggregates, these fines entrained are impregnated with bitumen therefore strongly adhesive.
Lors du retraitement mécanique par filtration, quel que soit le mode retenu, il se produit un colmatage des conduits de circulation.During mechanical reprocessing by filtration, whatever the mode chosen, clogging of the circulation ducts occurs.
Quant aux filtres, ils se colmatent rapidement et définitivement interdisant leur bon fonctionnement.As for filters, they clog quickly and permanently prohibiting their proper operation.
Le recyclage doit pouvoir s'appliquer aussi bien à partir des unités de fabrication établies en lieu fixe, d'installations démontables et mobiles comme pour les unités opérant directement sur la chaussée à traiter. Pour ces dernières opérant par retraitement en continu sur des fraisats également produits en continu, les problèmes mentionnés ci-dessus se trouvent intensifiés, notamment les rejets. De même avec les dispositifs chauffant la surface de la chaussée à recycler, on se heurte à la diffusion impossible dans l'épaisseur de la couche d'enrobés à cause du mauvais transfert thermique et aux conséquences de dégradation du bitume.Recycling must be able to be applied as well from production units established in a fixed place, from dismountable and mobile installations as for units operating directly on the roadway to be treated. For the latter operating by continuous reprocessing on costs also produced continuously, the problems mentioned above are intensified, especially the rejections. Similarly with the devices heating the surface of the roadway to be recycled, it is difficult to achieve diffusion in the thickness of the asphalt layer due to poor heat transfer and degradation consequences of the bitumen.
Un document
Ce dispositif prévoit soit un chauffage avec des soles de convoyeurs chauffantes soit un chauffage par flamme mais aucun chauffage radiant sur le dessus des enrobés routiers usagés n'est prévu pour affiner la température de chauffage de chaque sole ou partie de sole.This device provides either a heating with heating conveyor soles or a flame heating but no radiant heating on top of used road asphalt is provided to refine the heating temperature of each sole or part of hearth.
La présente invention propose des solutions pour pallier les problèmes évoqués en préambule et recourt à des moyens de chauffage par panneaux radiants avec un agencement particulier permettant d'illustrer le procédé et d'apporter une solution en terme de dispositif, satisfaisante mais non limitative.The present invention proposes solutions to overcome the problems mentioned in the preamble and uses heating means by radiant panels with a particular arrangement for illustrating the method and provide a solution in terms of device, satisfactory but not limiting.
Afin de mieux expliciter ce dispositif, le procédé et le dispositif sont maintenant décrits en détail, selon un mode de réalisation, en regard des dessins annexés sur lesquels les différentes figures représentent :
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figure 1 : une vue schématique en élévation latérale d'un premier module de traitement selon la présente invention permettant la mise en oeuvre du procédé -
figure 2 : une vue schématique en élévation latérale d'un second module de traitement selon la présente invention, et -
figure 3 , une vue d'une variante de réalisation d'une enceinte du module de traitement.
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figure 1 : a schematic view in side elevation of a first processing module according to the present invention for carrying out the method -
figure 2 a schematic side elevational view of a second processing module according to the present invention, and -
figure 3 , a view of an alternative embodiment of an enclosure of the treatment module.
Le procédé selon la présente invention consiste à traiter les fraisats d'enrobés dans un dispositif équipé de moyens de chauffage radiant par panneaux.The method according to the present invention consists in treating asphalt mixes in a device equipped with radiant heating means by panels.
On entend pour la suite de la description par fraisats les enrobés issus de fraisage mais aussi les enrobés issus de retrait mécanique par blocs et concassés.For the remainder of the description, the milled mixes are used for the description of the description, but also the mixes resulting from mechanical block and crushed shrinkage.
De même les termes "chauffage radiant par panneaux" utilisé couvrent tout agencement surfacique apte à émettre des rayonnements conduisant à un chauffage radiant.Similarly, the term "radiant heating panels" used cover any surface arrangement capable of emitting radiation leading to radiant heating.
Ceci permet de traiter les fraisats sans provoquer les mouvements de courants d'air violents imposés par les modes de mise en température de l'art antérieur, par combustion.This makes it possible to treat the charges without causing the movements of violent air currents imposed by the heating modes of the prior art, by combustion.
De plus, il est impossible d'atteindre différentes températures au sein d'un même module puisqu'il suffit de régler l'émission de chaleur en fonction de la charge.In addition, it is impossible to achieve different temperatures within the same module since it is sufficient to adjust the heat emission according to the load.
On note dès lors que, grâce à ce mode de chauffage, même en cas de baisse de puissance de chauffe, celle-ci reste parfaitement répartie, grâce aux panneaux qui émettent des calories de façon homogène. Dans le cas d'une flamme, lorsque la puissance est diminuée, la répartition est également modifiée de façon importante.It is therefore noted that, thanks to this mode of heating, even in the event of a fall in heating power, it remains perfectly distributed, thanks to the panels which emit calories in a homogeneous way. In the case of a flame, when the power is decreased, the distribution is also significantly modified.
De fait, la température ponctuelle maximale atteinte ne peut excéder la température de détérioration des bitumes comme cela sera indiqué ci-après. Ces caractéristiques conduisent à des avantages immédiats qui solutionnent les premiers problèmes importants qui ont été mentionnés en préambule. Néanmoins, il faut ensuite obtenir le résultat final recherché à savoir la mise en température des granulats déjà enrobés de bitume.In fact, the maximum point temperature reached can not exceed the deterioration temperature of the bitumens as will be indicated below. These characteristics lead to immediate benefits that solve the first important problems that were mentioned in the preamble. Nevertheless, it is then necessary to obtain the final result sought namely to warm up the aggregates already coated with bitumen.
Or, pour donner un ordre d'idée, on sait que l'ensemble du mélange de granulats présente une surface spécifique de 15 à 20 m2 par kilogramme avec 50 grammes de bitume environ, ce qui conduit à des épaisseurs de pellicules de bitume de quelques microns.However, to give an idea, it is known that the aggregate mixture aggregate has a specific surface area of 15 to 20 m 2 per kilogram with about 50 grams of bitumen, which leads to thicknesses of bitumen films of a few microns.
La majorité des ces pellicules est emprisonnée dans les agglomérats constituant le fraisats et il convient qu'il conserve cette structure durant la mise en température pour réduire la création de nouvelles surfaces mettant à l'air libre le bitume.The majority of these films are trapped in agglomerates constituting the costs and it should maintain this structure during warm-up to reduce the creation of new surfaces venting the bitumen.
Entre les gros éléments composant les agglomérats se trouvent des fractions d'éléments minéraux petits fins et très fins. Ces fractions concentrent à masse égale une quantité plus importante de bitume en raison des différences de surface spécifique.Between the large elements composing the agglomerates are fractions of mineral elements small fine and very fine. These fractions concentrate a greater quantity of bitumen due to differences in specific surface area.
Ces agglomérats doivent rester cohésionnés de façon préférentielle. Il faut donc un procédé de traitement mécaniquement suffisamment souple.These agglomerates must remain cohesive preferentially. Therefore, a mechanically flexible treatment process is required.
Le procédé consiste aussi en un convoyage mécanique préférentiellement par gravité mais aussi par convoyage forcé et avec des vibrations. Ces vibrations, dans leur émission, auront au moins une composante verticale, de préférence avec une amplitude élevée, en sorte de permettre régulièrement un retournement des grains. Cette modification d'orientation permet une homogénéité de présentation de l'ensemble de la surface de chaque grain devant les radiations infrarouges des moyens de chauffage radiant.The method also consists of mechanical conveying preferentially by gravity but also by forced conveying and with vibrations. These vibrations, in their emission, will have at least one vertical component, preferably with a high amplitude, so as to allow a regular reversal of the grains. This change of orientation allows a homogeneity of presentation of the entire surface of each grain in front of the infrared radiation of the radiant heating means.
On constate à cette occasion que le bitume n'est pas exposé de façon extrême à l'air donc à l'oxygène qu'il contient susceptible de provoquer une oxydation et un vieillissement accélérés.It is noted on this occasion that the bitumen is not exposed in an extreme way to the air and therefore to the oxygen it contains, which can cause accelerated oxidation and aging.
Le dispositif associé est représenté sur la
Dans le cas de machines mobiles, le dispositif est nécessairement au gabarit routier pour permettre les déplacement et positionnement à proximité immédiate des chantiers. Cette même limitation au gabarit routier est applicable aux machines mobiles se déplaçant en continu le long du chantier pour travailler les fraisats au fur et à mesure en continu. La limitation de l'encombrement du dispositif et la nécessité d'un temps de séjour suffisant des enrobés engendrent des contraintes.In the case of mobile machines, the device is necessarily the road gauge to allow movement and positioning in the immediate vicinity of construction sites. This same limitation to the road gauge is applicable to mobile machines moving continuously along the site to work the costs as and when continuous. The limitation of the size of the device and the need for a sufficient residence time of the mixes generate constraints.
Aussi, il est prévu plusieurs tapis de transfert disposés les uns au dessous des autres, ces tapis étant inclinés ou horizontaux et mis en vibration par tous moyens 14 adaptés de mise en vibration et par exemple des moteurs à balourd. Au-dessus de ces tapis, il est prévu des moyens 16 de chauffage de type radiant, sous forme de panneaux 18. La puissance, la répartition et les moyens d'alimentation en énergie devront être adaptés à la capacité de traitement.Also, there is provided several transfer mats arranged one below the other, these mats being inclined or horizontal and vibrated by any means 14 adapted to vibration and for example unbalance motors. Above these mats, there are provided heating means of radiant type, in the form of panels 18. The power, the distribution and the power supply means must be adapted to the processing capacity.
En effet, il faut tenir compte du fait que les matériaux à traiter contiennent une certaine quantité d'eau qu'il faut éliminer et la durée de séjour, la puissance de chauffe sont des paramètres à prendre en compte également lors du dimensionnement de l'installation.Indeed, it must be taken into account that the materials to be treated contain a certain amount of water that must be removed and the residence time, the heating power are parameters to be taken into account also when sizing the installation.
Dans le procédé retenu, la température de l'enrobé à atteindre en sortie est de l'ordre de 105 à 130°C en sorte de mettre la bitume à l'état visqueux et de provoquer l'évaporation complète de l'eau et sécher totalement les matériaux introduits.In the process chosen, the temperature of the asphalt to be reached at the outlet is of the order of 105 to 130 ° C. so as to bring the bitumen into the viscous state and cause complete evaporation of the water and completely dry the introduced materials.
Les gaz générés lors du chauffage, la vapeur d'eau ainsi que les produits organiques les plus volatils, issus du bitume, sont évacués à l'atmosphère mais on constate que les effluents gazeux contiennent des proportions de substances organiques très réduites à ces températures.The gases generated during heating, water vapor and the most volatile organic products, derived from bitumen, are discharged to the atmosphere, but it is found that the gaseous effluents contain very small proportions of organic substances at these temperatures.
Le procédé prévoit ensuite une seconde étape qui consiste à amener l'enrobé à température finale de travail, soit 160 à 220°C, dans un second module. Préalablement, les grains et les agglomérats issus du premier module sont de façon préférentielle introduits en continu dans des moyens pour agglutiner les éléments fins, les grains et agglomérats. Les fines assurent la cohésion.The method then provides a second step which consists of bringing the mix to the final working temperature, ie 160 to 220 ° C, into a second module. Beforehand, the grains and agglomerates derived from the first module are preferably continuously introduced into means for agglutinating fine elements, grains and agglomerates. The fines ensure cohesion.
C'est un matériau chaud et totalement sec, à environ 105 à 130°C, constitué d'agglomérats d'éléments cohésionnés, qui est ensuite porté selon le procédé de l'invention à une température de 160 à 220°C.It is a hot and completely dry material, at about 105 to 130 ° C, consisting of agglomerates of cohesive elements, which is then carried according to the process of the invention at a temperature of 160 to 220 ° C.
De fait, il se produit des émissions de produits organiques car les températures sont plus élevées et ces émissions doivent être traitées avant leur rejet à l'atmosphère. On note néanmoins que les courants d'air étant supprimés et les éléments ayant été agglutinés, l'entraînement des fines est extrêmement réduit, voire supprimé.In fact, there are emissions of organic products because the temperatures are higher and these emissions must be treated before their release to the atmosphere. It is noted, however, that the air currents being removed and the elements having been agglutinated, the entrainment of fines is extremely reduced or even eliminated.
Dans le second module sensiblement identique au premier, on modifie la puissance calorifique pour combler le delta calorifique et atteindre la température voulue.In the second module substantially identical to the first, the heat output is modified to fill the heat sink and reach the desired temperature.
Un autre problème susceptible de se poser est le traitement des effluents gazeux. Ceux-ci peuvent être traités de façon efficace par passage à travers des catalyseurs de décomposition qui, pour beaucoup d'entre eux, sont sensibles à l'humidité. De fait l'élimination de l'eau dans le premier module est d'une grande importance également pour résoudre ce problème.Another problem that may arise is the treatment of gaseous effluents. These can be effectively treated by passage through decomposition catalysts which, for many of them, are sensitive to moisture. In fact the elimination of water in the first module is of great importance also to solve this problem.
Le second module présenté en
Par contre, de façon non représentée mais en recourant à des dispositifs connus, il convient de prévoir des moyens racleurs pour éliminer la partie de mortiers bitumineux qui se dépose sur les convoyeurs ou tapis.By cons, not shown but using known devices, it is necessary to provide scraper means to remove the portion of bituminous mortar that is deposited on conveyors or carpets.
Les enrobés issus de ce second module peuvent être composés de 100% de matériaux à recycler. Il convient d'adjoindre des additifs de régénération du vieux bitume, cette opération devant être effectuée dans un malaxeur, de façon connue. Ces additifs sont préalablement mis en température et dosés suivant une quantité en rapport avec le débit massique d'enrobés recyclés dans une unité de production en continu ou une masse d'enrobés préalablement pesés avant introduction dans le malaxeur pour une unité discontinue.The mixes resulting from this second module can be composed of 100% of materials to be recycled. It is necessary to add regeneration additives of the old bitumen, this operation to be carried out in a kneader, in a known manner. These additives are preheated and dosed in an amount related to the mass flow rate of recycled mixes in a continuous production unit or a mass of previously weighed mixes before introduction into the mixer for a discontinuous unit.
On retrouve de nouveau l'importance de l'élimination de l'eau dans le premier module.The importance of water removal in the first module is again found.
Les enrobés issus de ce second module peuvent être recyclés avec un apport de granulats vierges qui sont introduits conjointement à l'enrobé usagé dans le premier module. Ce matériau vierge est préparé par ailleurs de façon connue.The mixes from this second module can be recycled with a supply of virgin aggregates which are introduced together with the asphalt used in the first module. This virgin material is also prepared in a known manner.
En plus du bitume apporté par l'enrobé usagé, il est adjoint des additifs de régénération et du bitume neuf ainsi que des fines d'apport.In addition to the bitumen supplied by the used asphalt, it is added regeneration additives and new bitumen as well as filler.
En sortie de malaxeur, l'enrobé incluant pour tout ou partie de l'enrobé recyclé est prêt à l'emploi.At the end of the mixer, the mix including all or part of the recycled mix is ready for use.
Selon une variante du dispositif de l'invention il est possible d'utiliser la surface rayonnante de façon différente. Dans ce cas, voir
Le cylindre central 100 reçoit des moyens de chauffage 124 par exemple un brûleur 126 utilisant du combustible liquide. Les gaz de combustion sont évacués de façon connue à l'extrémité 128 haute de ce cylindre central, le brûleur étant disposé en partie basse.The central cylinder 100 receives heating means 124, for example a burner 126 using liquid fuel. The flue gases are evacuated in known manner at the upper end 128 of the central cylinder, the burner being arranged at the bottom.
Les enrobés sont introduits dans l'espace entre les deux cylindres, en partie haute et circulent par gravité vers le bas.The mixes are introduced into the space between the two cylinders, in the upper part and flow by gravity downwards.
La rotation assure la présentation de toutes les faces des grains aux rayonnements infrarouges émis par la paroi extérieure du cylindre central.The rotation ensures the presentation of all the faces of the grains to the infrared radiation emitted by the outer wall of the central cylinder.
On note dès lors que les grains et le bitume qui leur est lié, ne sont jamais en contact avec les gaz de combustion, ce qui élimine tout problème d'envol des fines enrobées. En sortie, les effluents sont traités comme précédemment avant renvoi à l'atmosphère.It is therefore noted that the grains and the bitumen which is bound to them, are never in contact with the combustion gases, which eliminates any problem of flight of the coated fines. At the outlet, the effluents are treated as before before returning to the atmosphere.
Dans cette variante, les surfaces radiantes sont courbes et peuvent être équipées de tout moyen de brassage adapté.In this variant, the radiating surfaces are curved and can be equipped with any suitable mixing means.
Les procédé et dispositifs selon la présente invention permettent de résoudre les problèmes posés par le recyclage des vieux enrobés en respectant les contraintes environnementales.The methods and devices according to the present invention make it possible to solve the problems posed by the recycling of old mixes while respecting the environmental constraints.
Claims (9)
- A method for heating a material comprising at least partly old coated road materials to be recycled, in particular issuing from milled road surface or crushed conglomerates, which comprises heating these old coated road materials to be recycled by exposing the various faces of these aggregates and/or coated road materials to the heating, characterised in that:- heating is carried out, in a first chamber (10) of a first module, at a first temperature by means of first radiant heating means (16) disposed close to the old coated road materials to be recycled so as to make the bitumen viscous and to cause evaporation of the water and to completely dry the materials, that is to say from 105° to 130°C,- these coated road materials heated to a temperature of 105° to 130°C are heated in a second chamber (10') of a second module to a second temperature by means of second radiant heating means (16') disposed close to the old coated road materials to be recycled so as to raise the coated road materials to a working temperature, that is to say 160° to 220°C.
- A method according to claim 1, characterised in that, between the two heating steps, the old coated road materials to be recycled are caked.
- A method according to claim 1 or 2, characterised in that at least additives are added at the discharge from the second heating step so as to regenerate the bitumen or reconstitute a novel type of bitumen, by mixing.
- A method according to claim 3, characterised in that at least a proportion of untreated aggregates prepared elsewhere is added.
- A device for implementing the method according to any one of the preceding claims, characterised in that it comprises at least one first chamber (10) of a first module provided with mechanical transfer means (12) and heating means (16) of the radiant type making it possible to expose all the faces of the old coated road materials to be recycled and to reach a first temperature of between 105° and 130°C, means for discharging the gaseous effluent and a second chamber (10') of a second module provided with mechanical transfer means (12') and heating means (16') of the radiant type, enabling the old coated road materials to be recycled to reach a second temperature of between 160° and 220°C and means for discharging the gaseous effluent.
- A device according to claim 5, characterised in that it comprises means for caking the old coated road materials to be recycled disposed at the discharge from the first chamber (10).
- A device according to claim 5 or 6, characterised in that it comprises a substantially parallelepipidal chamber (10, 10') and in that the mechanical means comprise inclined and/or horizontal conveyors (12, 12') equipped with vibration means (14, 14') and heating means (16, 16') of the radiant type in the form of panels (18, 18').
- A device according to claim 5 or 6, characterised in that each chamber (10, 10') comprises first and second chambers (100, 100'), cylindrical, coaxial, rotary and inclined, and heating means (124), the old coated road materials to be recycled flowing in the space between the two chambers, by gravity from top to bottom.
- A device according to one of claims 5 to 7, characterised in that it comprises means for treating the gaseous effluent emitted in the second chamber, including decomposition catalysts.
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FR0450225A FR2866037B1 (en) | 2004-02-09 | 2004-02-09 | METHOD AND DEVICE FOR TEMPERATURING GRANULATES AND / OR ROAD COVERS, IN PARTICULAR COATED USES FOR RECYCLING |
PCT/FR2005/050075 WO2005075742A1 (en) | 2004-02-09 | 2005-02-07 | Method and device for heating worn road coating materials |
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EP1713977B1 true EP1713977B1 (en) | 2016-07-20 |
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US6164809A (en) * | 1998-11-30 | 2000-12-26 | Hawkins; Michael R. | Counter-flow asphalt plant with independently rotatable dryer and mixer |
US6672751B2 (en) * | 2001-01-18 | 2004-01-06 | Michael R. Hawkins | Counter-flow asphalt plant with combustion zone feed and exhaust gas heater |
US20070070801A1 (en) * | 2005-09-23 | 2007-03-29 | Cedarapids, Inc. | Pre-combustion mix drum |
US20110110177A1 (en) * | 2006-05-22 | 2011-05-12 | Wesley Van Velsor | System for producing asphalt from reclaimed asphalt pavement |
US7681326B2 (en) * | 2006-06-25 | 2010-03-23 | Marusho-Giken Co., Ltd. | All weather passive-type solar Ogako drying house |
US20080220133A1 (en) * | 2007-03-05 | 2008-09-11 | Gary Bruce Carman | Food sanitation system |
-
2004
- 2004-02-09 FR FR0450225A patent/FR2866037B1/en not_active Expired - Fee Related
-
2005
- 2005-02-07 US US10/588,763 patent/US9045867B2/en active Active
- 2005-02-07 EP EP05717706.5A patent/EP1713977B1/en active Active
- 2005-02-07 PT PT57177065T patent/PT1713977T/en unknown
- 2005-02-07 WO PCT/FR2005/050075 patent/WO2005075742A1/en active Application Filing
- 2005-02-07 ES ES05717706.5T patent/ES2598130T3/en active Active
Also Published As
Publication number | Publication date |
---|---|
PT1713977T (en) | 2016-10-25 |
ES2598130T3 (en) | 2017-01-25 |
FR2866037B1 (en) | 2006-04-28 |
EP1713977A1 (en) | 2006-10-25 |
US20070172313A1 (en) | 2007-07-26 |
FR2866037A1 (en) | 2005-08-12 |
WO2005075742A1 (en) | 2005-08-18 |
US9045867B2 (en) | 2015-06-02 |
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