EP1627938A1 - Ceramic coating for parts of a microscope - Google Patents
Ceramic coating for parts of a microscope Download PDFInfo
- Publication number
- EP1627938A1 EP1627938A1 EP05102893A EP05102893A EP1627938A1 EP 1627938 A1 EP1627938 A1 EP 1627938A1 EP 05102893 A EP05102893 A EP 05102893A EP 05102893 A EP05102893 A EP 05102893A EP 1627938 A1 EP1627938 A1 EP 1627938A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- microscope
- ceramic coating
- layer
- stage
- insert
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000005524 ceramic coating Methods 0.000 title claims description 36
- 238000007745 plasma electrolytic oxidation reaction Methods 0.000 claims description 8
- 238000000576 coating method Methods 0.000 claims description 6
- 229910000838 Al alloy Inorganic materials 0.000 claims description 5
- 239000011248 coating agent Substances 0.000 claims description 5
- 239000003960 organic solvent Substances 0.000 claims description 5
- 239000002585 base Substances 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 3
- 150000007513 acids Chemical class 0.000 claims description 3
- 239000000919 ceramic Substances 0.000 abstract description 11
- 239000010410 layer Substances 0.000 description 16
- 239000004411 aluminium Substances 0.000 description 4
- 229910052782 aluminium Inorganic materials 0.000 description 4
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 230000008901 benefit Effects 0.000 description 3
- 239000011247 coating layer Substances 0.000 description 3
- 230000003287 optical effect Effects 0.000 description 3
- 230000003678 scratch resistant effect Effects 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000010422 painting Methods 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 239000004809 Teflon Substances 0.000 description 1
- 229920006362 Teflon® Polymers 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 238000002048 anodisation reaction Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 238000007429 general method Methods 0.000 description 1
- 238000003780 insertion Methods 0.000 description 1
- 230000037431 insertion Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 238000004901 spalling Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C30/00—Coating with metallic material characterised only by the composition of the metallic material, i.e. not characterised by the coating process
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C8/00—Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C8/02—Pretreatment of the material to be coated
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/02—Anodisation
- C25D11/026—Anodisation with spark discharge
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/02—Anodisation
- C25D11/04—Anodisation of aluminium or alloys based thereon
Definitions
- the present invention relates generally to microscopes; and more particularly; to a ceramic coating for parts of a microscope.
- the hardness of the layer of the ceramic coating is related to the thickness of the layer.
- the ceramic coating can be produced in different colours so that the part on which the ceramic coating is provided differs from the other parts of the microscope. It is especially advantageous in the case where the upper stage element is black and the colour of the ceramic coating on the insert is of a different colour so that the ceramic coating provides a good contrast between the upper stage element and the insert. It is clear to every person skilled in the art that a ceramic coating can also be provided on the insert and on the upper stage element wherein both ceramic coatings are of different colours.
- the ceramic coating is extremely scratch resistant. In addition, the ceramic coating is resistant to organic solvents, acids and bases.
- a microscope stage including a means for creating contrasts between a microscope stage and a specimen, such that the specimen may be orientated correctly on the stage prior to insertion into the optical path.
- the upper stage or at least the insert in the upper stage has to be scratch resistant in order to avoid wear on the stage or the insert due to intensive use of the microscope.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electrochemistry (AREA)
- Mechanical Engineering (AREA)
- Microscoopes, Condenser (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
Description
- The present invention relates generally to microscopes; and more particularly; to a ceramic coating for parts of a microscope.
- Painting is the general method used on various parts of a microscope. The scratch resistance of the parts painted or coated in a conventional way is not very satisfactory. Other traditional technologies, such as chrome plating, anodisation or spraying of teflon did not also provide the required features.
- The Russian patent RU 2224828 discloses a method of microarc oxidation and a device for its realisation. Nothing is disclosed about the use of the part made by the process disclosed in the above document.
- Another patent application RU 2199613 discloses anticorrosive coatings for components of stop valves. The parts of the valves include the application of an aluminium layer or that of an anodised aluminium containing alloy upon which a layer of microarc oxidation material is applied. The components covered with such a coating show a high strength, mechanical endurance, corrosion resistance, adhesion, microhardness, resistance to cyclic temperature variations and resistance against organic solvents. The above disclosure does not show any application of a layer produced by microarc oxidation for microscopic parts.
- The document RU 2147324 shows the application of microarc oxidation on body parts of gear-type pumps. No application for optical instruments, such as microscopes, is mentioned or disclosed in the above document.
- In the object of the present invention to provide a coating for parts of a microscope which show a high scratch resistance and provide a good contrast compared to the other parts of the microscope. The above object is solved by a microscope which comprises several parts wherein the parts are for example a stand, a stage, a nose piece and several elements used to operate a microscope. At least one part of the microscope is provided with a ceramic coating. It is advantageous if the ceramic coating is provided on a part which is made of an aluminium alloy. It is extremely advantageous if the part with the ceramic coating is the upper stage element. It is of importance if the ceramic coating is provided on an insert which fits in a recess on the upper stage element. The ceramic coating is a microarc coating. The hardness of the layer of the ceramic coating is related to the thickness of the layer. The ceramic coating can be produced in different colours so that the part on which the ceramic coating is provided differs from the other parts of the microscope. It is especially advantageous in the case where the upper stage element is black and the colour of the ceramic coating on the insert is of a different colour so that the ceramic coating provides a good contrast between the upper stage element and the insert. It is clear to every person skilled in the art that a ceramic coating can also be provided on the insert and on the upper stage element wherein both ceramic coatings are of different colours. The ceramic coating is extremely scratch resistant. In addition, the ceramic coating is resistant to organic solvents, acids and bases.
- Therefore, what is needed is a microscope stage including a means for creating contrasts between a microscope stage and a specimen, such that the specimen may be orientated correctly on the stage prior to insertion into the optical path. In addition, the upper stage or at least the insert in the upper stage has to be scratch resistant in order to avoid wear on the stage or the insert due to intensive use of the microscope.
- These and other objects, features and advantages of the invention will become readily apparent to one having ordinary skill in the art upon study of the following detailed description in view of the drawings and appended claims.
- Figure 1
- is a perspective view of a microscope comprising a microscope stage, contrasting means according to the present invention;
- Figure 2
- is a perspective view of a microscope stage according to the present invention;
- Figure 3
- is an exploded perspective view of the microscope stage of Figure 2; and
- Figure 4
- is a cross-sectional side view of the insert showing the ceramic coating provided as a layer on the surface of the insert.
- At the outset it should be noted that the same reference numbers on different figures represent similar structural elements. It should also be appreciated that, while a number of different embodiments and variations of the present invention are shown in the various drawings, the invention disclosed it is not intended to be limited to these specific embodiments as the claims define a broader invention that can take many different shapes and structures. Finally, in the present disclosure and claims, it should be appreciated that the terms insert and/or plate are not intended to be limited to the removable plate-like structures as illustrated in the present figures, but may include other parts of the microscope that require a ceramic coating on their surfaces.
- Figure 1 shows a perspective view of a
microscope 10 comprising amicroscope stage 24 and aremovable insert 28. In addition, the microscope comprises abinocular head 12, aneyepiece 14, astand 16, an objective turret ornose piece 17, astage drive control 18, coarsefocus adjustment knob 20, finefocus adjustment knob 22 and thestage assembly 24. In this embodiment, thestage assembly 24 is generally adjustable in left/right and forward/backward directions via thestage drive control 18 and stage drive means (not shown). - Referring now to figures 2 and 3,
stage assembly 24 of the present invention broadly comprises anupper stage element 26, which additionally includescontrasting stage insert 28. In a preferred embodiment,upper stage element 26 is black, and more preferably flat black, for purposes of limiting the incidence of light that might be reflected off the stage and into the optical beam path. Theupper stage element 26 could, however, comprise a different colour if desired. Typically, theupper stage element 26 is made of aluminium or of an aluminium alloy that is anodised and painted to provide a flat black colour.Optional stage insert 28 is preferably made of an aluminium alloy as well and is of a lighter colour than theupper stage element 26. The contrasting stage insert is, thus configured, for providing a good contrast between a specimen and the contrasting stage insert 28 when the specimen is placed thereon. In addition to the lighter colour of the stage insert 28 or the lighter colour of theupper stage element 26, the surfaces of both elements may be provided with a ceramic coating. The ceramic coating has the properties that it is of lighter colour than a black element surrounding it, that it is scratch resistant and that is resistant to organic solvents, acids and bases. As already mentioned, the ceramic coating may be provided on different parts of the microscope, such as the stand, theupper stage element 26 or the stage insert 28. The ceramic coating is a microarc oxidation coating. Thestage insert 28 also comprises anaperture 29, which allows light to pass through for performing microscopic methods. The scratch resistance of the stage insert 28 or the whole stageupper element 26 is of great benefit to a microscope, since there is no wear of the surfaces of the stage insert 28 or theupper stage element 26 due to the intense use by the persons working with the microscope. - As shown more clearly in Figure 3, the stage assembly of the present invention is operatively arranged that the
contrasting stage insert 28 is removable from theupper stage element 26. In such an embodiment,upper stage 26 comprises arecess 32 which is configured for accepting a complementarilyshaped stage insert 28, which in this embodiment is removable from theupper stage element 26. For purposes of correctly aligning the stage insert 28 therein,recess 32 comprises an alignment means 34, which may comprise a pair of pins of nubs operatively arranged for mateable fit withbores 30 of thecontrasting stage insert 28. Of course, other means for ensuring the proper alignment of the stage insert 28 withrecess 32 are contemplated, for example, notches, keyways or the like could be used to ensure a correct fit of the stage insert 28 in therecess 32. Figure 3 also illustrates thatrecess 32 further comprises fastening means 36 for securing the stage insert 28 in therecess 32. Fastening means 36 may comprise magnets, hook and loop type fasteners, detents, spring ball bearings, etc. Finally,recess 32 comprisesaperture 39, which is larger thanaperture 29 of thestage insert 28 allowing the stage insert 28 to be easily removed from the recess from below theupper stage element 26. - Figure 4 shows a partial cross-sectional view through a part of a microscope provided with a
ceramic layer 41. The part of the microscope 40, which may be a stand portion, a focussing knob, anupper stage element 26 or astage insert 28, has asurface 42 on which theceramic coating layer 41 is provided. The part 40 is made of a metal and preferably of aluminium or of an aluminium alloy. Theceramic coating layer 41 combines with the base material of the part 40, therefore, the part will show no crusting or spalling during the course of its use. Theceramic layer 41 is formed through physical action, thus the filming speed is several times faster than in conventional technology such as spraying or painting. Additionally, the thickness of theceramic layer 41 can be adjusted according to the requirements which leads to a further enhancement of the hardness of the parts. The resulting hardness is related to the thickness of theceramic layer 41. Additionally, the colour of the part can be treated into pure white, beige, coffee or black during the course of oxidation. Moreover, theceramic coating layer 41 will not fade even if organic solvents, such as alcohol, acetone, ditoluene and the like are used. The part, on which theceramic layer 41 is provided, is treated by microarc oxidation. Microarc oxidation has the advantage that during or after the process the part is not deformed. Additionally, the resulting surface of theceramic layer 41 has an excellent scratch resistance and corruption resistance. Theceramic layer 41 can be applied to the part of the microscope with athickness 42 ranging from 30µm to 50µm. - Moreover, as mentioned above, the
ceramic layer 41 was not attacked by chemicals. The hardness of theceramic layer 41 ranges from HV 500-2500, wherein the hardness is related to thickness ofceramic layer 41. Thus, it is seen that the objectives of the present invention are effectively achieved, although modification and changes to the invention should be readily apparent to those having ordinary skill in the art, which modifications are intended to be within the spirit and scope of the invention as claimed.
Claims (10)
- A microscope comprises several parts, wherein the parts are a stand, a stage, a nosepiece, and several elements used to operate a microscope, characterized in that, at least one part of the microscope is provided with a layer of a ceramic coating.
- The microscope as claimed in claim 1, wherein the part provided with the layer of the ceramic coating is made of an aluminium alloy.
- The microscope as claimed in claim 1 wherein the part provided with the layer of the ceramic coating in an upper stage element.
- The microscope as claimed in claim 3 wherein the part provided with the layer of the ceramic coating in an insert provided in a recess of the upper stage element.
- The microscope as claimed in any of the previous claims wherein the layer of the ceramic coating is a microarc oxidation coating.
- The microscope as claimed in any of the previous claims wherein the hardness of the layer of the ceramic coating is related to the thickness of the layer.
- The microscope as claimed in any of the previous claims wherein the layer of the ceramic coating has a different color than the other part of the microscope.
- The microscope as claimed in claim 7 wherein the upper stage element is of black color and the layer of the ceramic coating of the insert is of a different color, so that the ceramic coating support color contrast.
- The microscope as claimed in any of the previous claims wherein the layer of the ceramic coating is scratch resistent.
- The microscope as claimed in any of the previous claims wherein the layer of the ceramic coating is resistant against organic solvents, acids and bases.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 200410053868 CN1737209A (en) | 2004-08-20 | 2004-08-20 | Ceramic coating of microscope parts |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1627938A1 true EP1627938A1 (en) | 2006-02-22 |
EP1627938B1 EP1627938B1 (en) | 2013-09-25 |
Family
ID=35351706
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP20050102893 Active EP1627938B1 (en) | 2004-08-20 | 2005-04-13 | Ceramic coating for parts of a microscope |
Country Status (2)
Country | Link |
---|---|
EP (1) | EP1627938B1 (en) |
CN (1) | CN1737209A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AT506125B1 (en) * | 2007-12-10 | 2011-07-15 | Herbert Luttenberger | MICROSCOPIC SYSTEM |
GB2538121A (en) * | 2014-12-29 | 2016-11-09 | Leica Microsystems Ltd Shanghai | Embedder |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH05150168A (en) | 1991-11-30 | 1993-06-18 | Olympus Optical Co Ltd | Stage of microscope and production thereof |
JPH06308392A (en) | 1993-04-19 | 1994-11-04 | Olympus Optical Co Ltd | Microscope stage and its production |
RU2070622C1 (en) | 1993-06-24 | 1996-12-20 | Василий Александрович Большаков | Method of applying ceramic coating onto a metal surface by microarc anodizing technique and used electrolyte |
US5781338A (en) | 1994-11-17 | 1998-07-14 | Carl Zeiss Stiftung | Microscope stage |
JPH10253641A (en) | 1997-03-07 | 1998-09-25 | Jeol Ltd | Probe holder for scan type probe microscope |
RU2147324C1 (en) | 1999-03-22 | 2000-04-10 | Орловская государственная сельскохозяйственная академия | Gear for microarc oxidation of body wells of gear-type pump |
RU2199613C2 (en) | 2001-05-22 | 2003-02-27 | Агабабян Размик Енокович | Method for covering components of stop valves with protective coatings (alternatives) |
RU2224828C2 (en) | 2002-05-22 | 2004-02-27 | Московский государственный технический университет "МАМИ" | Method of microarc oxidation and device for its implementation |
-
2004
- 2004-08-20 CN CN 200410053868 patent/CN1737209A/en active Pending
-
2005
- 2005-04-13 EP EP20050102893 patent/EP1627938B1/en active Active
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH05150168A (en) | 1991-11-30 | 1993-06-18 | Olympus Optical Co Ltd | Stage of microscope and production thereof |
JPH06308392A (en) | 1993-04-19 | 1994-11-04 | Olympus Optical Co Ltd | Microscope stage and its production |
RU2070622C1 (en) | 1993-06-24 | 1996-12-20 | Василий Александрович Большаков | Method of applying ceramic coating onto a metal surface by microarc anodizing technique and used electrolyte |
US5781338A (en) | 1994-11-17 | 1998-07-14 | Carl Zeiss Stiftung | Microscope stage |
JPH10253641A (en) | 1997-03-07 | 1998-09-25 | Jeol Ltd | Probe holder for scan type probe microscope |
RU2147324C1 (en) | 1999-03-22 | 2000-04-10 | Орловская государственная сельскохозяйственная академия | Gear for microarc oxidation of body wells of gear-type pump |
RU2199613C2 (en) | 2001-05-22 | 2003-02-27 | Агабабян Размик Енокович | Method for covering components of stop valves with protective coatings (alternatives) |
RU2224828C2 (en) | 2002-05-22 | 2004-02-27 | Московский государственный технический университет "МАМИ" | Method of microarc oxidation and device for its implementation |
Non-Patent Citations (3)
Title |
---|
PATENT ABSTRACTS OF JAPAN vol. 017, no. 539 (P - 1621) 28 September 1993 (1993-09-28) * |
PATENT ABSTRACTS OF JAPAN vol. 1995, no. 02 31 March 1995 (1995-03-31) * |
PATENT ABSTRACTS OF JAPAN vol. 1998, no. 14 31 December 1998 (1998-12-31) * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AT506125B1 (en) * | 2007-12-10 | 2011-07-15 | Herbert Luttenberger | MICROSCOPIC SYSTEM |
GB2538121A (en) * | 2014-12-29 | 2016-11-09 | Leica Microsystems Ltd Shanghai | Embedder |
US9518902B2 (en) | 2014-12-29 | 2016-12-13 | Leica Microsystems Ltd. Shanghai | Embedder |
GB2538121B (en) * | 2014-12-29 | 2018-05-09 | Leica Microsystems Ltd Shanghai | Embedder |
Also Published As
Publication number | Publication date |
---|---|
CN1737209A (en) | 2006-02-22 |
EP1627938B1 (en) | 2013-09-25 |
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