EP1601943A1 - Self-cleaning optical sensor - Google Patents
Self-cleaning optical sensorInfo
- Publication number
- EP1601943A1 EP1601943A1 EP04719345A EP04719345A EP1601943A1 EP 1601943 A1 EP1601943 A1 EP 1601943A1 EP 04719345 A EP04719345 A EP 04719345A EP 04719345 A EP04719345 A EP 04719345A EP 1601943 A1 EP1601943 A1 EP 1601943A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- sensor
- heating
- combustion chamber
- tip
- lens
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01M—TESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
- G01M15/00—Testing of engines
- G01M15/04—Testing internal-combustion engines
- G01M15/10—Testing internal-combustion engines by monitoring exhaust gases or combustion flame
Definitions
- the invention relates to an optical sensor for detecting the light intensity of combustion processes in a combustion chamber.
- Optical sensors are used in combustion engines, for example in gasoline engines or diesel engines, to examine the combustion.
- the temporal recording of the light intensity in a combustion chamber provides important data as boundary conditions for computer models, since the temperature can be inferred from the light intensity.
- the soot concentration in the combustion chamber can be inferred when determining the light intensity. Due to the increasingly strict regulations of exhaust gas legislation, great efforts are being made to reduce the formation of soot during combustion in engines. Optical sensors provide valuable data for these developments.
- optical sensors which have a detection angle of up to 130 ° and such a small diameter that they can be installed in a spark plug or glow plug.
- the object of the present invention is to describe an optical sensor for detecting combustion processes in a combustion chamber, which is not impaired by soot deposits on the side facing the combustion chamber.
- Fig. 1 shows an embodiment of an optical sensor according to the invention
- FIG. 2 shows a detailed view of a sensor tip of an optical sensor according to the invention
- This sensor 1 shows an optical sensor 1.
- This sensor 1 has one or more lenses 2 on the side facing the combustion chamber 7.
- the light incident through the lenses 2 is passed on by means of a light guide running in the center of the sensor 1 and then processed for evaluation.
- the foremost surface of the lens 2 of the sensor 1 is soiled during a measurement by soot from the combustion chamber 7.
- This exemplary embodiment according to the invention has a heater 4 at the tip of the sensor 1, in the area of the foremost lens 2.
- the invention consists in that the sensor tip can be heated by means of this heater 4 to a temperature at which the soot is burned on the foremost lens 2. As a result, the sensor 1 can remain clean and functional for the entire desired measuring period.
- the heater 4 consists of a heating coil.
- a temperature sensor 6 attached to sensor 1 is used for temperature control.
- FIG. 2 shows the tip of an exemplary embodiment according to the invention of an optical sensor 1 with lenses 2 and with the subsequent light guide 3.
- the invention described here can also be used with other optical sensors. This figure is not intended to be limiting.
- the heating wire 4 was wound several times around the lenses 2. Windings between 1 and 8 turns, in particular 2 to 4 turns, are preferred. A heating wire 4 with a cross section between 0.25 and 1 mm is preferably used.
- the power with which the heating wire 4 is heated is preferably between 10 and 70 watts, in particular between 15 and 40 watts.
- the heater 4 is brought to the desired temperature before use of a measurement, which is necessary to keep the surface of the foremost lens 2 always clean.
- the temperature required for this is about 400 ° C, preferably about 600 ° C at the sensor tip. Soot, which would settle on the surface of the foremost lens 2, is immediately burned at these temperatures.
- the heating system ensures a clean lens 2 during the entire measurement and therefore reliable measurements in this regard.
- the required heating can also be generated by supplying energy in the form of electromagnetic waves. This energy can be generated by a laser, for example.
- the light can be directed onto the lens via the light guide 3. Deposits on the lens 2 absorb the incident energy and are burned as a result.
- One difference of this arrangement is that the heater cannot be in operation during the measurement. The measurement must therefore be interrupted and cleaned again after sooting again.
- lines or channels can be provided next to the lenses, which are filled with a fluid.
- This fluid is heated to the desired temperature in a suitable manner and brought to the sensor tip in lines or channels provided for this purpose. The release of heat in this area of the sensor tip in turn causes the soot to be burned on the foremost lens.
- the advantage of heating the sensor tip is that the measurement can be carried out at any operating point, irrespective of the degree of sooting, especially in the case of diesel engine combustion. Another advantage is that no complex calibration has to be carried out and that the sensor does not have to be removed.
- heating e.g. heating coil
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Photometry And Measurement Of Optical Pulse Characteristics (AREA)
- Testing Of Engines (AREA)
- Radiation Pyrometers (AREA)
- Combined Controls Of Internal Combustion Engines (AREA)
- Control Of Combustion (AREA)
Abstract
The invention relates to an optical sensor (1) for detecting light emission in combustion processes in a combustion chamber (7), comprising at least one lens (2) which faces the combustion chamber and is disposed on the tip of the sensor. The front surface of the sensor (1) is soiled by soot from the combustion chamber (7) during measurement. The inventive sensor (1) is provided with a heating device (4), which is disposed on the tip thereof, in the region of the front lens. The invention is characterized in that the tip of the sensor can be heated by means of said heating device (4) to a specific temperature at which the soot on the front lens (2) is combusted. As a result, the sensor (1) remains clean and operational during the entire measuring period as desired.
Description
Selbstreinigender optischer SensorSelf-cleaning optical sensor
Die Erfindung betrifft einen optischen Sensor zum Erfassen der Lichtintensität von Verbrennungsvorgängen in einem Brennraum.The invention relates to an optical sensor for detecting the light intensity of combustion processes in a combustion chamber.
Optische Sensoren dienen in Verbrennungsmotoren, beispielsweise in Ottomotoren oder Dieselmotoren, der Untersuchung der Verbrennung. Die zeitliche Aufnahme der Lichtintensität in einem Brennraum liefert einerseits wichtige Daten als Randbedingungen für Computermodelle, da von der Lichtintensität auf die Temperatur geschlossen werden kann. Andererseits kann bei der Ermittlung der Lichtintensität auf die Russkonzentration im Brennraum geschlossen werden. Aufgrund immer schärfer werdender Vorschriften der Abgas Gesetzgebung werden grosse Anstrengungen unternommen, um die Russbildung bei der Verbrennung in Motoren zu verringern. Optische Sensoren liefern für diese Entwicklungen wertvolle Daten.Optical sensors are used in combustion engines, for example in gasoline engines or diesel engines, to examine the combustion. The temporal recording of the light intensity in a combustion chamber on the one hand provides important data as boundary conditions for computer models, since the temperature can be inferred from the light intensity. On the other hand, the soot concentration in the combustion chamber can be inferred when determining the light intensity. Due to the increasingly strict regulations of exhaust gas legislation, great efforts are being made to reduce the formation of soot during combustion in engines. Optical sensors provide valuable data for these developments.
Von speziellem Interesse im Zusammenhang mit dieser Erfindung sind optische Sensoren, die einen Erf ssungswinkel von bis zu 130° und einen derart geringen Durchmesser aufweisen, dass sie in eine Zündkerze oder Glühkerze eingebaut werden kann.Of particular interest in connection with this invention are optical sensors which have a detection angle of up to 130 ° and such a small diameter that they can be installed in a spark plug or glow plug.
In Testversuchen stellte sich heraus, dass die dem Brennraum zugewandte Seite des optischen Sensors nach einer gewissen Betriebszeit, meistens schon nach wenigen Minuten, mit Russ bedeckt wird. Dadurch reduziert sich die Lichtdurchlässigkeit der vordersten Linse. Nach der Verrussung dieser Linse lassen die durch den optischen Sensor gemessenen Werte nur nach einer aufwändigen rechnerischen Kalibrierung Rückschlüsse auf die Lichtintensität im Brennraum zu. Zu diesem Zweck muss der Sensor ausgebaut und nach der Kalibrierung gereinigt werden. Dies unterbricht die Messung, ist sehr zeitaufwändig und teuer.
Erfahrungen haben gezeigt, dass der Russ weggebrannt und die vorderste Linse gereinigt werden kann, wenn die Temperatur an dieser Linse mindestens 400 °C beträgt. Zu diesem Zweck wird in einigen Anwendungen die vorderste Spitze des Sensors gezielt mit dem heissem Gas des Brennraums umströmt. Dadurch wird der Russ, je nach Temperatur im Brennraum, mit der Zeit wieder verbrannt und die Messung liefert wieder brauchbare Werte. Leider genügt die Umströmung in den meisten Fällen nicht, um die vorderste Linse wirklich sauber zu brennen.Test trials have shown that the side of the optical sensor facing the combustion chamber is covered with soot after a certain operating time, usually after a few minutes. This reduces the light transmission of the foremost lens. After the sooting of this lens, the values measured by the optical sensor only allow conclusions to be drawn about the light intensity in the combustion chamber after a complex mathematical calibration. For this purpose, the sensor must be removed and cleaned after calibration. This interrupts the measurement, is very time-consuming and expensive. Experience has shown that the soot can be burned away and the front lens can be cleaned if the temperature on this lens is at least 400 ° C. For this purpose, the hot gas of the combustion chamber flows around the front tip of the sensor in some applications. Depending on the temperature in the combustion chamber, the soot is burned again over time and the measurement provides usable values again. Unfortunately, the flow around is not enough in most cases to burn the front lens really clean.
Die Aufgabe der vorliegenden Erfindung ist es, einen optischen Sensor zum Erfassen von Verbrennungsvorgängen in einem Brennraum zu beschreiben, der nicht durch eine Russablagerung an der dem Brennraum zugewandten Seite beeinträchtigt ist.The object of the present invention is to describe an optical sensor for detecting combustion processes in a combustion chamber, which is not impaired by soot deposits on the side facing the combustion chamber.
Die Aufgabe wird gelöst durch die Merkmale des ersten Patentanspruchs .The object is achieved by the features of the first claim.
Die Erfindung wird unter Verwendung der folgenden Zeichnungen erläutert. Es zeigenThe invention is explained using the following drawings. Show it
Fig. 1 eine erfindungsgemässe Ausführungsform eines optischen SensorsFig. 1 shows an embodiment of an optical sensor according to the invention
Fig. 2 eine Detailansicht einer Sensorspitze eines erfin- dungsgemässen optischen Sensors2 shows a detailed view of a sensor tip of an optical sensor according to the invention
Fig. 1 zeigt einen optischen Sensor 1. Dieser Sensor 1 weist an der dem Brennraum 7 zugewandten Seite eine oder mehrere Linsen 2 auf . Das durch die Linsen 2 einfallende Licht wird mittels eines im Zentrum des Sensors 1 verlaufenden Lichtleiters weiter geleitet und anschliessend zur Auswertung aufbereitet.
Die vorderste Fläche der Linse 2 des Sensors 1 wird bei einer Messung durch Russ aus dem Brennraum 7 verschmutzt. Dieses er- findungsgemässe Ausführungsbeispiel weist an der Spitze des Sensors 1, im Bereich der vordersten Linse 2, eine Heizung 4 auf. Die Erfindung besteht darin, dass die Sensorspitze mittels dieser Heizung 4 auf eine Temperatur aufgeheizt werden kann, bei welcher der Russ an der vordersten Linse 2 verbrannt wird. Dadurch kann der Sensor 1 während der gesamten gewünschten Messdauer sauber und funktionstüchtig bleiben.1 shows an optical sensor 1. This sensor 1 has one or more lenses 2 on the side facing the combustion chamber 7. The light incident through the lenses 2 is passed on by means of a light guide running in the center of the sensor 1 and then processed for evaluation. The foremost surface of the lens 2 of the sensor 1 is soiled during a measurement by soot from the combustion chamber 7. This exemplary embodiment according to the invention has a heater 4 at the tip of the sensor 1, in the area of the foremost lens 2. The invention consists in that the sensor tip can be heated by means of this heater 4 to a temperature at which the soot is burned on the foremost lens 2. As a result, the sensor 1 can remain clean and functional for the entire desired measuring period.
In diesem Ausführungsbeispiel besteht die Heizung 4 aus einem Heizwendel. Ein am Sensor 1 angebrachter Temperaturmessfühler 6 dient der Temperaturregelung.In this embodiment, the heater 4 consists of a heating coil. A temperature sensor 6 attached to sensor 1 is used for temperature control.
Die Figur 2 zeigt die Spitze eines erfindungsgemässen Ausführungsbeispieles eines optischen Sensors 1 mit Linsen 2 und mit dem anschliessenden Lichtleiter 3. Die hier beschriebene Erfindung lässt sich bei anderen optischen Sensoren ebenso einsetzen. Diese Figur soll keine einschränkende Wirkung haben. Bei dem Ausführungsbeispiel der Fig. 2 wurde der Heizdraht 4 mehrfach um die Linsen 2 gewickelt. Bevorzugt sind Wicklungen zwischen 1 bis 8 Windungen, insbesondere 2 bis 4 Windungen. Bevorzugt wird ein Heizdraht 4 mit einem Querschnitt zwischen 0.25 und 1 mm verwendet. Die Leistung, mit welcher der Heizdraht 4 beheizt wird, liegt bevorzugt zwischen 10 und 70 Watt, insbesondere zwischen 15 und 40 Watt.FIG. 2 shows the tip of an exemplary embodiment according to the invention of an optical sensor 1 with lenses 2 and with the subsequent light guide 3. The invention described here can also be used with other optical sensors. This figure is not intended to be limiting. In the embodiment of FIG. 2, the heating wire 4 was wound several times around the lenses 2. Windings between 1 and 8 turns, in particular 2 to 4 turns, are preferred. A heating wire 4 with a cross section between 0.25 and 1 mm is preferably used. The power with which the heating wire 4 is heated is preferably between 10 and 70 watts, in particular between 15 and 40 watts.
Die Heizung 4 wird bereits vor Einsatz einer Messung auf die gewünschte Temperatur gebracht, die erforderlich ist, um die Oberfläche der vordersten Linse 2 stets sauber zu halten. Die dafür erforderliche Temperatur beträgt etwa 400 °C, vorzugsweise etwa 600 °C an der Sensorspitze. Russ, der sich auf die Oberfläche der vordersten Linse 2 absetzen würde, wird bei diesen Temperaturen sofort verbrannt. Während der gesamten Messung sorgt das Heizsystem für eine saubere Linse 2 und daher diesbezüglich zuverlässige Messungen.
Alternativ dazu kann die erforderliche Beheizung auch mittels Zuführung von Energie in Form von elektromagnetischen Wellen erzeugt werden. Diese Energie kann beispielsweise durch einen Laser erzeugt sein. Dabei kann das Licht über den Lichtleiter 3 auf die Linse geleitet werden. Ablagerungen auf der Linse 2 absorbieren die auftreffende Energie und werden dadurch verbrannt. Ein Unterschied dieser Anordnung ist allerdings, dass die Heizung nicht während der Messung in Betrieb sein kann. Die Messung muss demnach nach einer erneuten Verrussung wieder unterbrochen und gereinigt werden.The heater 4 is brought to the desired temperature before use of a measurement, which is necessary to keep the surface of the foremost lens 2 always clean. The temperature required for this is about 400 ° C, preferably about 600 ° C at the sensor tip. Soot, which would settle on the surface of the foremost lens 2, is immediately burned at these temperatures. The heating system ensures a clean lens 2 during the entire measurement and therefore reliable measurements in this regard. Alternatively, the required heating can also be generated by supplying energy in the form of electromagnetic waves. This energy can be generated by a laser, for example. The light can be directed onto the lens via the light guide 3. Deposits on the lens 2 absorb the incident energy and are burned as a result. One difference of this arrangement, however, is that the heater cannot be in operation during the measurement. The measurement must therefore be interrupted and cleaned again after sooting again.
Alternativ dazu können Leitungen oder Kanäle neben den Linsen vorgesehen sein, die mit einem Fluid gefüllt sind. Dieses Fluid wird auf geeignete Weise auf die gewünschte Temperatur erwärmt und in dafür vorgesehenen Leitungen oder Kanälen an die Sensorspitze gebracht. Das Abgeben der Wärme in diesem Bereich der Sensorspitze sorgt wiederum für die Verbrennung des Russes auf der vordersten Linse.Alternatively, lines or channels can be provided next to the lenses, which are filled with a fluid. This fluid is heated to the desired temperature in a suitable manner and brought to the sensor tip in lines or channels provided for this purpose. The release of heat in this area of the sensor tip in turn causes the soot to be burned on the foremost lens.
Der Vorteil einer Beheizung der Sensorspitze liegt darin, dass die Messung in jedem Betriebspunkt, ungeachtet des Verrussungs- grades, insbesondere bei der dieselmotorischen Verbrennung durchgeführt werden kann. Ein weiterer Vorteil besteht darin, dass keine aufwändige Kalibrierung durchgeführt werden muss und dass der Sensor nicht ausgebaut werden muss.The advantage of heating the sensor tip is that the measurement can be carried out at any operating point, irrespective of the degree of sooting, especially in the case of diesel engine combustion. Another advantage is that no complex calibration has to be carried out and that the sensor does not have to be removed.
Liste der BezeichnungenList of names
1 Sensor1 sensor
2 Linse2 lens
3 Lichtleiter3 light guides
4 Heizung, z.B. Heizwendel4 heating, e.g. heating coil
5 Heizleitung5 heating cable
6 Temperaturfühler6 temperature sensors
7 Brennraum
7 combustion chamber
Claims
1. Optischer Sensor (1) zum Erfassen von Verbrennungsvorgängen in einem Brennraum (7) mit mindestens einer dem Brennraum zugewandten Linse (2) an der Sensorspitze, dadurch gekennzeichnet, dass der Sensor (1) eine Heizvorrichtung (4) zum Erwärmen der Sensorspitze umfasst.1. Optical sensor (1) for detecting combustion processes in a combustion chamber (7) with at least one lens (2) facing the combustion chamber at the sensor tip, characterized in that the sensor (1) comprises a heating device (4) for heating the sensor tip ,
2. Sensor gemäss Anspruch 1, dadurch gekennzeichnet, dass die HeizVorrichtung (4) die Sensorspitze auf mindestens etwa 400 °C, vorzugsweise auf mindestens 600 °C erwärmt werden kann.2. Sensor according to claim 1, characterized in that the heating device (4), the sensor tip to at least about 400 ° C, preferably at least 600 ° C can be heated.
3. Sensor gemäss Anspruch 1 oder 2, dadurch gekennzeichnet, dass die Erwärmung mittels eines Heizdrahtes (4) erzeugt wird.3. Sensor according to claim 1 or 2, characterized in that the heating is generated by means of a heating wire (4).
4. Sensor gemäss Anspruch 3, dadurch gekennzeichnet, dass der Heizdraht (4) einen Durchmesser von 0.25 bis 1 mm aufweist.4. Sensor according to claim 3, characterized in that the heating wire (4) has a diameter of 0.25 to 1 mm.
5. Sensor gemäss Anspruch 3 oder 4, dadurch gekennzeichnet, dass sich der Heizdraht (4) mit einer Heizleistung von 10 bis 70 Watt, vorzugsweise mit 15 bis 40 Watt betreiben5. Sensor according to claim 3 or 4, characterized in that the heating wire (4) operate with a heating power of 10 to 70 watts, preferably 15 to 40 watts
J_clS S 17, .J_clS S 17,.
6. Sensor gemäss Anspruch 3, 4 oder 5, dadurch gekennzeichnet, dass der Heizdraht (4) 1 bis 8 Windungen, insbesondere 2 bis 4 Windungen um die Linse (2) aufweist.6. Sensor according to claim 3, 4 or 5, characterized in that the heating wire (4) has 1 to 8 turns, in particular 2 to 4 turns around the lens (2).
7. Sensor gemäss Anspruch 1 oder 2, dadurch gekennzeichnet, dass die Erwärmung mittels eines umströmenden Fluids erzeugt wird.7. Sensor according to claim 1 or 2, characterized in that the heating is generated by means of a flowing fluid.
8. Sensor gemäss Anspruch 1 oder 2, dadurch gekennzeichnet, dass die Erwärmung mittels elektromagnetischer Wellen erzeugt wird.8. Sensor according to claim 1 or 2, characterized in that the heating is generated by means of electromagnetic waves.
9. Sensor gemäss Anspruch 8, dadurch gekennzeichnet, dass die Erwärmung mittels eines Lasers erzeugt wird.9. Sensor according to claim 8, characterized in that the heating is generated by means of a laser.
10. Sensor gemäss einem der Ansprüche 1 bis 9, dadurch gekennzeichnet, dass die Erwärmung geregelt ist. 10. Sensor according to one of claims 1 to 9, characterized in that the heating is regulated.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH4162003 | 2003-03-13 | ||
CH4162003 | 2003-03-13 | ||
PCT/CH2004/000142 WO2004081511A1 (en) | 2003-03-13 | 2004-03-11 | Self-cleaning optical sensor |
Publications (1)
Publication Number | Publication Date |
---|---|
EP1601943A1 true EP1601943A1 (en) | 2005-12-07 |
Family
ID=32968390
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP04719345A Withdrawn EP1601943A1 (en) | 2003-03-13 | 2004-03-11 | Self-cleaning optical sensor |
Country Status (4)
Country | Link |
---|---|
US (1) | US7375314B2 (en) |
EP (1) | EP1601943A1 (en) |
JP (2) | JP4980050B2 (en) |
WO (1) | WO2004081511A1 (en) |
Families Citing this family (11)
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JP5012689B2 (en) * | 2008-06-24 | 2012-08-29 | 株式会社デンソー | Automatic cleaning optical sensor |
JP2010008077A (en) * | 2008-06-24 | 2010-01-14 | Denso Corp | Automatic cleaning type optical sensor |
US9194273B2 (en) | 2008-10-31 | 2015-11-24 | Cummins Inc. | Apparatus, system, and method for aftertreatment control and diagnostics |
US8648322B2 (en) * | 2008-10-31 | 2014-02-11 | Cummins Inc. | Optical sensing in an adverse environment |
DE102010003413B4 (en) | 2010-03-29 | 2016-12-22 | Von Ardenne Gmbh | Method for cleaning an optical position measuring system, optical position measuring system and coating system |
US8218147B2 (en) | 2010-06-18 | 2012-07-10 | Cummins Inc. | Apparatus, system, and method for detecting engine fluid constituents |
DE102011112698A1 (en) | 2011-06-21 | 2012-12-27 | Von Ardenne Anlagentechnik Gmbh | Optical control device used for vacuum treatment of glass substrate, has viewing window that is arranged at predetermined interior space within housing in which passage opening is extended within channel formed at housing |
WO2013187910A1 (en) | 2012-06-15 | 2013-12-19 | Empire Technology Development Llc | Self-cleaning lens |
US9816915B2 (en) | 2013-10-11 | 2017-11-14 | Fireye, Inc. | Couplings for flame observation devices |
CN104864411B (en) * | 2015-03-17 | 2017-06-23 | 厦门奥普拓自控科技有限公司 | A kind of grate firing boiler extinguishes the intelligent checking system of boundary |
ES2670830T3 (en) * | 2015-06-16 | 2018-06-01 | Kistler Holding Ag | Cable disassembly device, method for disassembling a cable using the disassembly device, as well as cable for use in the method |
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DE3321028A1 (en) * | 1982-06-17 | 1983-12-22 | Smiths Industries Public Ltd. Co., London | OPTICAL COMPONENT |
JPS59201934A (en) * | 1983-04-28 | 1984-11-15 | Toyota Motor Corp | Removing device of adhesive substance of ignition timing sensor |
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2004
- 2004-03-11 EP EP04719345A patent/EP1601943A1/en not_active Withdrawn
- 2004-03-11 JP JP2006504154A patent/JP4980050B2/en not_active Expired - Fee Related
- 2004-03-11 WO PCT/CH2004/000142 patent/WO2004081511A1/en active Application Filing
- 2004-03-11 US US10/548,167 patent/US7375314B2/en not_active Expired - Fee Related
-
2012
- 2012-02-28 JP JP2012041062A patent/JP2012150119A/en not_active Withdrawn
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Also Published As
Publication number | Publication date |
---|---|
WO2004081511A1 (en) | 2004-09-23 |
JP2012150119A (en) | 2012-08-09 |
US20070068495A1 (en) | 2007-03-29 |
JP4980050B2 (en) | 2012-07-18 |
US7375314B2 (en) | 2008-05-20 |
JP2006526142A (en) | 2006-11-16 |
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