EP1326713B1 - Flotation device - Google Patents

Flotation device Download PDF

Info

Publication number
EP1326713B1
EP1326713B1 EP01986275A EP01986275A EP1326713B1 EP 1326713 B1 EP1326713 B1 EP 1326713B1 EP 01986275 A EP01986275 A EP 01986275A EP 01986275 A EP01986275 A EP 01986275A EP 1326713 B1 EP1326713 B1 EP 1326713B1
Authority
EP
European Patent Office
Prior art keywords
plates
flotation device
set forth
space
suspension
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP01986275A
Other languages
German (de)
French (fr)
Other versions
EP1326713A2 (en
Inventor
Lucas Menke
George Troubounis
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Meri Environmental Solutions GmbH
Original Assignee
Meri Entsorgungstechnik Fuer Die Papierindustrie GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Meri Entsorgungstechnik Fuer Die Papierindustrie GmbH filed Critical Meri Entsorgungstechnik Fuer Die Papierindustrie GmbH
Publication of EP1326713A2 publication Critical patent/EP1326713A2/en
Application granted granted Critical
Publication of EP1326713B1 publication Critical patent/EP1326713B1/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B03SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03DFLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D1/00Flotation
    • B03D1/14Flotation machines
    • B03D1/1443Feed or discharge mechanisms for flotation tanks
    • B03D1/1456Feed mechanisms for the slurry
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B03SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03DFLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D1/00Flotation
    • B03D1/02Froth-flotation processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B03SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03DFLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D1/00Flotation
    • B03D1/14Flotation machines
    • B03D1/1481Flotation machines with a plurality of parallel plates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B03SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03DFLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D1/00Flotation
    • B03D1/14Flotation machines
    • B03D1/1493Flotation machines with means for establishing a specified flow pattern
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B03SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03DFLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D1/00Flotation
    • B03D1/02Froth-flotation processes
    • B03D1/028Control and monitoring of flotation processes; computer models therefor
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/24Treatment of water, waste water, or sewage by flotation

Definitions

  • the invention relates to a flotation device for the separation of substances or mixtures of substances from suspensions to form at least one rich and a low-fluff fraction, with several in a flotation tank above each other to parent, rotationally symmetric lamellae, wherein the low-carbon fraction enters during the separation process in blade interstices between the slats and a clear fluid Gets collected and horizontally outside the slats, a vertically extending annular separation space is formed, which communicates with a provided above the slats drain for the rich fraction.
  • the present invention seeks to provide a generic flotation, which avoids the disadvantages mentioned above and is characterized in particular by an effective separation of the desired substances of the suspension in a low-material and a rich fraction.
  • the most significant advantages of the invention are that compared to horizontal flotation devices, the installation area is reduced and thus the flotation performance per installation area is greater.
  • the combination of the lamellar arrangement with the eccentrically charged reaction and mixing chamber results in improved flocculation and thus better process values in the filtrate.
  • the deposition by means of the double-lamellar principle results in better deposition values.
  • FIG. 1 shows, in a schematic axial section, a first embodiment of the invention, that is to say a flotation device 10a .
  • Figures 2a, 2b and 2c are three cross-sections through the flotation device 10a along the lines AA ( Figure 2a).
  • BB Figure 2b
  • CC Figure 2c).
  • the flotation device 10a consists essentially of a round flotation tank 12 at the lower end of the suspension inlet and the clear fluid outlet and at the top end of the drain is intended for the flotate.
  • the flotation tank may be constructed of a plurality of segments.
  • a suspension feed 16 is provided in the lower region of the flotation device 10a , which opens into a double conical reaction and mixing chamber 18 eccentrically.
  • a sediment outlet 20 is provided in the conical bottom region of the reaction and mixing chamber 18 , which is connected to a sediment conduit 22 which is closed by a timed sediment valve 24 .
  • the upper cone of the reaction and mixing chamber 18 opens into at least one suspension distribution tube 26 arranged vertically approximately centrally in the flotation tank 12 , which has a multiplicity of preferably slit-like suspension outlets 28 into the interior of the flotation tank 12 .
  • each second slat 30a is made shorter in the radial direction and each other slat 30b longer.
  • the suspension outlets 28 open into first annular lamellae 31 a , each of which is bounded below by a long lamella 30 b and above by a short lamina 30 a .
  • second lamellar annular spaces 31b Arranged in alternation with the first lamination annular spaces 31a are second lamellar annular spaces 31b , each of which is bounded at the bottom by a short lamella 30a and at the top by a long lamella 30b .
  • an annular separation space 32 which communicates with a provided in the upper part of the flotation tank 12 Flotatsammelraum 34 .
  • a Räumpaddelvorraum 36 is mounted on the flotation tank 12 , the more about two roller assemblies 38a, 38b and endless belts 40 circumferential Räumpaddel 42 include, which dip into the Flotatsammelraum 34 and lead to a circumferential Flotatab procurrinne 461 .
  • the second finned annular spaces 31b preferably have slot-like clear fluid outlets 46 on the inside, via which a connection to at least one clear fluid collecting pipe 48 is formed.
  • the at least one clear fluid collection tube 48 in turn opens into a clear fluid reservoir 50 , which communicates with a clear fluid discharge port 52 , which is provided with a control valve, not shown, to adjust the liquid level in the flotation tank 12 .
  • a cell tube consisting of a plurality of circular cross-section shaped parallel tubes, each second sector tube being a suspension distributor tube 26 and each other sector tube being a clear fluid collection tube 48 forms.
  • the cell tube is circular in cross-section in the illustrated embodiment. It may alternatively be polygonal, in particular square, and in particular four square arranged side by side in turn square tubes, of which two opposite tubes suspension distribution tubes 26 and the other tubes clear fluid collecting tubes 48 are.
  • the fins 30 are shown in Figure 2b with a circular cross-section. Other shapes such as polygons, especially a square, may also be used.
  • the shorter fins 30a are about 5% to 40%, preferably 10% to 20%, shorter than the longer fins 26b .
  • the separation space 26 preferably has a width which corresponds to between 10% and 30% of the length of the longer lamellae 30b .
  • a suspension preferably water, which may also contain heavy particles
  • the suspension can either be mixed with gas bubbles before entry into the reaction and mixing chamber 18 or shortly afterwards and / or chemical or physical flocculation aids can be added. Due to the tangential inflow of the suspension into the reaction and mixing chamber 18, there is an effective separation of the heavy parts, which sink downwards and are discharged via the sediment outlet 20 .
  • the suspension mixed with flocculants and / or gas bubbles flows into the suspension distribution tube 26 arranged above, and from there via the suspension outlets 28 into the first annular disc spaces 31a .
  • the suspension then flows with continuous deceleration radially outwards and upwards and enters the separation space 32 .
  • the clear fluid flows obliquely downwards and inwards, with a further separation of the solids, dissolved and partially dissolved substances, which flow back upwards and outwards to the separation space 32 .
  • the clear fluid flows via the slit-type clear fluid outlets 46 into the clear fluid collection pipe 48 and thence to the clear fluid discharge line 50 where it is discharged from the flotation device 10a via the controlled-fluid clearing discharge port 52 .
  • a second embodiment of the invention is shown, in which like reference numerals designate the same components as in Figures 1 and 2.
  • This second embodiment of the invention differs from the first only in that the inflow of the suspension from the suspension distribution pipe 26 takes place via the suspension outlets 28 into second lamella annular spaces 31b , which are delimited at the bottom by a short lamella 30a and at the top by a long lamella 30b . Accordingly, the flow of the clarified fluid from the separation chamber 32 is effected in the first annular plate spaces 31a, which are bounded by a long blade 30b and the top of a short blade 30a respectively below.
  • the invention is preferably used in the treatment of water in paper mills or sewage treatment.
  • the suspension contains, for example, as solids: fibers, mineral particles or microorganisms, as partially dissolved substances colloidal substances, fats, color pigments and as solutes carbon hydrates, salts, organic or inorganic acids.

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Physical Water Treatments (AREA)
  • Paper (AREA)
  • Fish Paste Products (AREA)
  • Separation Of Solids By Using Liquids Or Pneumatic Power (AREA)

Abstract

A flotation device for separating materials or mixtures of materials from suspensions includes a reaction and mixing space (18) with eccentric inlet (16) for the mixture of suspension particles with gas bubbles and for further transport into at least one centrally arranged vertical suspension distribution tube (26), wherein the suspension distribution tube (26) and the clarified fluid collecting tube (48) are arranged adjacently, the plates (30) surround the suspension distribution tube (26) and the clarified fluid collecting tube (48) in an annular manner; and every second annular plate space (31) between adjacent plates (30) is connected to the suspension distribution tube (26) and every other space (31) between plates is connected to the clarified fluid collecting tube (48), so that the flow takes place out of one space (31) between plates from the inside towards the outside to the separating space (32), and subsequently into an adjacent space (31) between plates from the outside towards the inside. The substantive advantages of the invention are in that by combination of the plate arrangement with the eccentrically loaded reaction and mixing space, improved flocculation and thus better processing values are obtained in the filtrate. Better separation values are obtained by separation using the double-plate principle.

Description

Die Erfindung betrifft Flotationsvorrichtung zur Trennung von Stoffen oder Stoffgemischen aus Suspensionen zur Bildung mindestens einer stoffreichen und einer stoffarmen Fraktion, mit mehreren in einem Flotationstank übereinander an geordneten, rotationssymmetrischen Lamellen, wobei die stoffarme Fraktion beim Trennvorgang in Lamellenzwischenräume zwischen den Lamellen eintritt und zu einem Klarfluid-Sammelrohr gelangt und horizontal außerhalb der Lamellen ein vertikal sich erstreckender ringförmiger Trennraum ausgebildet ist, der mit einem oberhalb der Lamellen vorgesehenen Ablauf für die stoffreiche Fraktion kommuniziert.The invention relates to a flotation device for the separation of substances or mixtures of substances from suspensions to form at least one rich and a low-fluff fraction, with several in a flotation tank above each other to parent, rotationally symmetric lamellae, wherein the low-carbon fraction enters during the separation process in blade interstices between the slats and a clear fluid Gets collected and horizontally outside the slats, a vertically extending annular separation space is formed, which communicates with a provided above the slats drain for the rich fraction.

Aus der US 3,182,799 ist eine Flotationsvorrichtung mit rechteckigem Grundriß bekannt, bei der aufwärts gerichtete Lamellen vorhanden sind, wobei im Zwischenraum zwischen je zwei Lamellen oben ein Suspensionseinlaß und darunter ein Klarfluid-Auslaß vorgesehen sind, wobei zwischen Ein- und Auslaß kurze Ablenkbleche vorhanden sind. Diese Anordnung hat den Nachteil, daß aufgrund der Dimensionierung vor allem der Ablenkbleche bei hoher hydraulischer Belastung (hohe Drücke oder Durchsätze) ein "Kurzschlußstrom" vom Zulauf zum Ablauf entsteht, der drastisch verschlechterte Wirkungsgrade bei der Trennung bewirkt. Ferner die Reinigung der Anlage, wie diese insbesondere in der Papierindustrie bei der Farbumstellung erforderlich ist, sehr aufwendig aufgrund der separaten Zulaufleitungen.From US 3,182,799 a flotation device with a rectangular outline is known, in which upward slats are present, wherein in the space between two slats above a suspension inlet and below a clear fluid outlet are provided, between the inlet and outlet short baffles are present. This arrangement has the disadvantage that due to the dimensioning of the baffles especially at high hydraulic load (high pressures or flow rates), a "short-circuit current" from the inlet to the process is created, which causes drastically deteriorated efficiencies in the separation. Furthermore, the cleaning of the plant, as this particular in the paper industry in the color change is required, very expensive due to the separate supply lines.

Hiervon ausgehend liegt der Erfindung die Aufgabe zugrunde, eine gattungsgemäße Flotationsvorrichtung zu schaffen, welche die oben genannten Nachteile vermeidet und sich insbesondere durch eine wirksame Trennung der gewünschten Stoffe der Suspension in eine stoffarme und eine stoffreiche Fraktion auszeichnet.Proceeding from this, the present invention seeks to provide a generic flotation, which avoids the disadvantages mentioned above and is characterized in particular by an effective separation of the desired substances of the suspension in a low-material and a rich fraction.

Diese Aufgabe wird durch die im Patentanspruch 1 angegebenen Merkmale gelöst. Vorteilhafte Weiterbildungen ergeben sich aus den Unteransprüchen.This object is achieved by the features specified in claim 1. Advantageous developments emerge from the subclaims.

Die wesentlichsten Vorteile der Erfindung bestehen darin, daß gegenüber horizontalen Flotationsvorrichtungen die Installationsfläche reduziert ist und damit die Flotationsleistung pro Installationsfläche größer ist. Durch die Kombination der Lamellenanordnung mit dem exzentrisch beschickten Reaktions- und Mischraum ergibt sich eine verbesserte Flockenbildung und damit bessere Prozeßwerte im Filtrat. Durch die Abscheidung mittels des doppellamelligen Prinzips ergeben sich bessere Abscheidungswerte.The most significant advantages of the invention are that compared to horizontal flotation devices, the installation area is reduced and thus the flotation performance per installation area is greater. The combination of the lamellar arrangement with the eccentrically charged reaction and mixing chamber results in improved flocculation and thus better process values in the filtrate. The deposition by means of the double-lamellar principle results in better deposition values.

Die Erfindung wird nachfolgend anhand der beigefügten Zeichnungen weiter erläutert. Dabei zeigt:

Fig. 1:
einen schematischen Axialschnitt durch eine erste Ausführungsform der erfindungsgemäßen mit einer Flotationsvorrichtung;
Fig. 2:
drei schematische Querschnitte durch die Flotationsvorrichtung gemäß Figur 1 entlang der Linien A-A, B-B und C-C;
Fig. 3:
einen schematischen Axialschnitt durch eine zweite Ausführungsform der erfindungsgemäßen mit einer Flotationsvorrichtung;
The invention will be further explained with reference to the accompanying drawings. Showing:
Fig. 1:
a schematic axial section through a first embodiment of the invention with a flotation device;
Fig. 2:
three schematic cross sections through the flotation device according to Figure 1 along the lines AA, BB and CC;
3:
a schematic axial section through a second embodiment of the invention with a flotation device;

In Figur 1 ist im schematischen Axialschnitt eine erste Ausführungsform der Erfindung dargestellt, mithin eine Flotationsvorrichtung 10a. In den Figuren 2a, 2b und 2c sind drei Querschnitte durch die Flotationsvorrichtung 10a entlang der Linien A-A (Fig. 2a); B-B (Fig. 2b) und C-C (Fig. 2c) dargestellt.FIG. 1 shows, in a schematic axial section, a first embodiment of the invention, that is to say a flotation device 10a . In Figures 2a, 2b and 2c are three cross-sections through the flotation device 10a along the lines AA (Figure 2a). BB (Figure 2b) and CC (Figure 2c).

Unter Bezugnahme auf die Figuren 1 und 2 besteht die Flotationsvorrichtung 10a im wesentlichen aus einem runden Flotationstank 12, an dessen Unterende der Suspensionseinlauf sowie der Klarfluid-Auslaß und an dessen Oberende der Ablauf für das Flotat vorgesehen ist. Wie durch die Flansche 14 angedeutet, kann der Flotationstank aus mehreren Segmenten aufgebaut sein.With reference to Figures 1 and 2, the flotation device 10a consists essentially of a round flotation tank 12 at the lower end of the suspension inlet and the clear fluid outlet and at the top end of the drain is intended for the flotate. As indicated by the flanges 14 , the flotation tank may be constructed of a plurality of segments.

Im einzelnen ist im unteren Bereich der Flotationsvorrichtung 10a ein Suspensionszulauf 16 vorgesehen, der in einen doppelkonischen Reaktions- und Mischraum 18 exzentrisch einmündet. Im kegelförmigen Bodenbereich des Reaktions- und Mischraums 18 ist ein Sedimentauslaß 20 vorgesehen, der mit einer Sedimentleitung 22 verbunden ist, die mit einem zeitgetakteten Sedimentventil 24 verschlossen ist.In detail, a suspension feed 16 is provided in the lower region of the flotation device 10a , which opens into a double conical reaction and mixing chamber 18 eccentrically. In the conical bottom region of the reaction and mixing chamber 18 , a sediment outlet 20 is provided, which is connected to a sediment conduit 22 which is closed by a timed sediment valve 24 .

Der obere Konus des Reaktions- und Mischraums 18 mündet in mindestens ein vertikal etwa mittig im Flotationstank 12 angeordnetes Suspensionsverteilrohr 26, das eine Vielzahl von vorzugsweise schlitzartigen Suspensionsauslässen 28 in das Innere des Flotationstanks 12 aufweist.The upper cone of the reaction and mixing chamber 18 opens into at least one suspension distribution tube 26 arranged vertically approximately centrally in the flotation tank 12 , which has a multiplicity of preferably slit-like suspension outlets 28 into the interior of the flotation tank 12 .

Im Flotationstank 12 und das mindestens eine Suspensionsverteilrohr 26 ringförmig umschließend sind eine Vielzahl konisch sich nach oben erweiternde ringförmige Lamellen angeordnet, wovon jede zweite Lamelle 30a in Radialrichtung kürzer und jede andere Lamelle 30b länger ausgeführt ist. Die Suspensionsauslässe 28 münden in erste Lamellenringräume 31a, die jeweils unten von einer langen Lamelle 30b und oben von einer kurzen Lamelle 30a begrenzt werden. Alternierend mit den ersten Lamellenringräumen 31a sind zweite Lamellenring-räume 31b ausgebildet, die jeweils unten von einer kurzen Lamelle 30a und oben von einer langen Lamelle 30b begrenzt werden.In the flotation tank 12 and the at least one Suspensionsverteilrohr 26 annularly surrounding a plurality of conically widening upward annular slats are arranged, of which each second slat 30a is made shorter in the radial direction and each other slat 30b longer. The suspension outlets 28 open into first annular lamellae 31 a , each of which is bounded below by a long lamella 30 b and above by a short lamina 30 a . Arranged in alternation with the first lamination annular spaces 31a are second lamellar annular spaces 31b , each of which is bounded at the bottom by a short lamella 30a and at the top by a long lamella 30b .

Radial außerhalb der langen Lamellen 30b erstreckt sich bis zur Wandung des Flotationstankes 12 ein ringförmiger Trennraum 32, der mit einem im oberen Bereich des Flotationstankes 12 vorgesehenen Flotatsammelraum 34 kommuniziert. Dort ist am Flotationstank 12 eine Räumpaddelvorrichtung 36 montiert, die mehrere über zwei Walzenanordnungen 38a, 38b und Endlosbänder 40 umlaufende Räumpaddel 42 umfassen, welche in den Flotatsammelraum 34 eintauchen und zu einer umlaufenden Flotatabführrinne 461 führen.Radially outside the long fins 30b extends to the wall of the flotation tank 12, an annular separation space 32 which communicates with a provided in the upper part of the flotation tank 12 Flotatsammelraum 34 . There, a Räumpaddelvorrichtung 36 is mounted on the flotation tank 12 , the more about two roller assemblies 38a, 38b and endless belts 40 circumferential Räumpaddel 42 include, which dip into the Flotatsammelraum 34 and lead to a circumferential Flotatabführrinne 461 .

Die zweiten Lamellenringräume 31b weisen innenendig vorzugsweise schlitzartige Klarfluidauslässe 46 auf, über die eine Verbindung zu mindestens einem Klarfluid-Sammelrohr 48 gebildet wird. Das mindestens eine Klarfluid-Sammelrohr 48 mündet wiederum in einen Klarfluid-Reservoir 50, der mit einer Klarfluid-Ableitöffnung 52 kommuniziert, welche mit einem nicht gezeigten Regelventil versehen ist, um das Flüssigkeitsniveau im Flotationstank 12 einzustellen.The second finned annular spaces 31b preferably have slot-like clear fluid outlets 46 on the inside, via which a connection to at least one clear fluid collecting pipe 48 is formed. The at least one clear fluid collection tube 48 in turn opens into a clear fluid reservoir 50 , which communicates with a clear fluid discharge port 52 , which is provided with a control valve, not shown, to adjust the liquid level in the flotation tank 12 .

Wie sich aus Fig. 2b ergibt, sind mehrere Suspensionsverteilrohre 26 und mehrere Klarfluid-Sammelrohre 48 zu einem Zellrohr zusammengefaßt, das aus mehreren im Querschnitt kreissektorartig geformten parallelen Rohren besteht, wobei jedes zweite Sektorrohr ein Suspensionsverteilrohr 26 und jedes anderes Sektorrohr ein Klarfluid-Sammelrohr 48 bildet. Das Zellrohr ist in der dargestellten Ausführung im Querschnitt kreisrund. Es kann alternativ auch vieleckig, insbesondere quadratisch ausgebildet sind,und insbesondere auch vier im Quadrat nebeneinander angeordneten wiederum quadratischen Rohren bestehen, von denen je zwei gegenüberliegende Rohre Suspensionsverteilrohre 26 und die anderen Rohre Klarfluid-Sammelrohre 48 sind.As can be seen from Fig. 2b, several suspension distribution tubes 26 and a plurality of clear fluid collection tubes 48 are combined to form a cell tube consisting of a plurality of circular cross-section shaped parallel tubes, each second sector tube being a suspension distributor tube 26 and each other sector tube being a clear fluid collection tube 48 forms. The cell tube is circular in cross-section in the illustrated embodiment. It may alternatively be polygonal, in particular square, and in particular four square arranged side by side in turn square tubes, of which two opposite tubes suspension distribution tubes 26 and the other tubes clear fluid collecting tubes 48 are.

Die Lamellen 30 sind in Figur 2b mit kreisrundem Querschnitt dargestellt. Andere Formen wie Vielecke, insbesondere ein Quadrat, können ebenfalls zur Anwendung kommen. Die kürzeren Lamellen 30a sind ca. 5% bis 40%, vorzugsweise 10% bis 20%, kürzer als die längeren Lamellen 26b.The fins 30 are shown in Figure 2b with a circular cross-section. Other shapes such as polygons, especially a square, may also be used. The shorter fins 30a are about 5% to 40%, preferably 10% to 20%, shorter than the longer fins 26b .

Der Trennraum 26 hat vorzugsweise eine Breite, die zwischen 10% und 30% der Länge der längeren Lamellen 30b entspricht.The separation space 26 preferably has a width which corresponds to between 10% and 30% of the length of the longer lamellae 30b .

Im Betrieb wird eine Suspension, vorzugsweise aus Wasser, die auch Schwerteile enthalten kann, über den Suspensionszulauf 16 exzentrisch tangential in den Reaktions- und Mischraum 18 eingeleitet. Die Suspension kann entweder vor dem Eintritt in den Reaktions- und Mischraum 18 oder kurz danach mit Gasblasen versetzt werden und/oder es können chemische oder physikalische Flockungshilfsmittel zugesetzt werden. Durch die tangentiale Einströmung der Suspension in den Reaktions- und Mischraum 18 erfolgt eine wirksame Abscheidung der Schwerteile, die nach unten sinken und über den Sedimentauslaß 20 abgeführt werden.In operation, a suspension, preferably water, which may also contain heavy particles, on the suspension feed 16 eccentrically introduced tangentially into the reaction and mixing chamber 18 . The suspension can either be mixed with gas bubbles before entry into the reaction and mixing chamber 18 or shortly afterwards and / or chemical or physical flocculation aids can be added. Due to the tangential inflow of the suspension into the reaction and mixing chamber 18, there is an effective separation of the heavy parts, which sink downwards and are discharged via the sediment outlet 20 .

Aus dem Reaktions- und Mischraum 18 strömt die mit Flockungsmitteln und/oder Gasblasen versetzte Suspension in das oberhalb angeordnete Suspensionsverteilrohr 26, und von dort über die Suspensionsauslässe 28 in die ersten Lamellenringräume 31a. Die Suspension strömt anschließend unter stetiger Verlangsamung radial nach außen und oben und gelangt in den Trennraum 32. Dabei erfolgt zunehmend eine Auftrennung der Suspension in Klarfluid und die abzutrennenden Stoffe, also Feststoffe, gelöste und teilgelöste Stoffe. Während die abzutrennenden Stoffe im Trennraum nach oben zum Flotatsammelraum 34 hin strömen, strömt die Masse des Klarfluides in die zweiten Lamellenringräume 31b, die alternierend zu den ersten Lamellenringräumen 31a angeordnet sind. Durch die Lamellenringräume 31b strömt das Klarfluid schräg nach unten und innen, wobei eine weitere Abtrennung der Feststoffe, gelösten und teilgelösten Stoffe erfolgt, die nach oben und außen zum Trennraum 32 zurückströmen. Das Klarfluid strömt über die schlitzartigen Klarfluidauslässe 46 in das Klarfluid-Sammelrohr 48 und von dort zur Klarfluid-Ableitung 50, von wo es über die mit einem Regelventil versehene Klarfluid-Ableitöffnung 52 aus der Flotationsvorrichtung 10a geregelt abgeleitet wird.From the reaction and mixing chamber 18 , the suspension mixed with flocculants and / or gas bubbles flows into the suspension distribution tube 26 arranged above, and from there via the suspension outlets 28 into the first annular disc spaces 31a . The suspension then flows with continuous deceleration radially outwards and upwards and enters the separation space 32 . In this case, there is increasingly a separation of the suspension in clear fluid and the substances to be separated, ie solids, dissolved and partially dissolved substances. While the substances to be separated flow upwards in the separation space to the flotation collection chamber 34 , the mass of the clear fluid flows into the second lamella annular spaces 31b , which are arranged alternately with the first lamella annular spaces 31a . Through the laminar annular spaces 31b , the clear fluid flows obliquely downwards and inwards, with a further separation of the solids, dissolved and partially dissolved substances, which flow back upwards and outwards to the separation space 32 . The clear fluid flows via the slit-type clear fluid outlets 46 into the clear fluid collection pipe 48 and thence to the clear fluid discharge line 50 where it is discharged from the flotation device 10a via the controlled-fluid clearing discharge port 52 .

In Fig. 3 ist eine zweite Ausführungsform der Erfindung dargestellt, in der gleiche Bezugszeichen die gleichen Bauteile wie in den Figuren 1 und 2 bezeichnen. Diese zweite Ausfü h-rungsform der Erfindung unterscheidet sich von der ersten lediglich dadurch, daß die Einströmung der Suspension aus dem Suspensionsverteilrohr 26 über die Suspensionsauslässe 28 in zweite Lamellenringräume 31b erfolgt, die jeweils unten von einer kurzen Lamelle 30a und oben von einer langen Lamelle 30b begrenzt werden. Dementsprechend erfolgt die Strömung des Klarfluides aus dem Trennraum 32 in die ersten Lamellenringräume 31a, die jeweils unten von einer langen Lamelle 30b und oben von einer kurzen Lamelle 30a begrenzt werden.In Fig. 3, a second embodiment of the invention is shown, in which like reference numerals designate the same components as in Figures 1 and 2. This second embodiment of the invention differs from the first only in that the inflow of the suspension from the suspension distribution pipe 26 takes place via the suspension outlets 28 into second lamella annular spaces 31b , which are delimited at the bottom by a short lamella 30a and at the top by a long lamella 30b . Accordingly, the flow of the clarified fluid from the separation chamber 32 is effected in the first annular plate spaces 31a, which are bounded by a long blade 30b and the top of a short blade 30a respectively below.

Durch diesen Unterschied erfolgt die Hauptströmung des Kla r-fluides nach unten und somit entgegen dem Hauptstrom der Feststoffe, gelösten und teilgelösten Stoffe, die nach oben zum Flotatsammelraum 34 hin erfolgt. Durch diesen Gegenstrom und die damit erzeugten Verwirbelungen ergibt sich für spezielle Suspensionszusammensetzungen ein besserer Trennungsgrad als mit der Ausführung gemäß den Figuren 1 und 2.Due to this difference, the main flow of the Kl-r-fluid down and thus against the main flow of solids, dissolved and partially dissolved substances, which takes place up to the Flotatsammelraum 34 out. As a result of this countercurrent and the turbulences generated therewith, a better degree of separation results for special suspension compositions than with the embodiment according to FIGS. 1 and 2.

Die Erfindung ist vorzugsweise bei der Wasseraufbereitung in Papierfabriken oder Abwasserklärung einsetzbar. Die Suspension enthält beispielsweise als Feststoffe: Fasern, Mineralpartikel oder Mikroorganismen, als teilgelöste Stoffe Kolloidalstoffe, Fette, Farbpigmente und als gelöste Stoffe Kohle - hydrate, Salze, organische oder anorganische Säuren.The invention is preferably used in the treatment of water in paper mills or sewage treatment. The suspension contains, for example, as solids: fibers, mineral particles or microorganisms, as partially dissolved substances colloidal substances, fats, color pigments and as solutes carbon hydrates, salts, organic or inorganic acids.

Claims (16)

  1. A flotation device for separating materials or mixtures of materials from suspensions to form at least one high material content fraction and one low material content fraction, with several rotationally symmetrical plates arranged one above another in a flotation tank, wherein during the separating procedure, the low material content fraction enters into plate spaces between the plates and arrives at a clarified fluid collecting tube, wherein horizontally outside the plates, a vertically extending annular separating space is formed that communicates with a run-off for the high material content provided above the plates, characterised by
    a reaction and mixing space (18) with eccentric inlet (16) for mixing the suspension particles with gas bubbles and for further conveyance into at least one centrally arranged vertical suspension distribution tube (26);
    wherein the suspension distribution tube (26) and the clarified fluid collecting tube (48) are arranged adjacently;
    the plates (30) surround the suspension distribution tube (26) and the clarified fluid collecting tube (48) in an annular manner;
    every second annular plate space (31) between adjacent plates (30) is connected to the suspension distribution tube (26) and every other space between plates (31) is connected to the clarified fluid collecting tube (48), so the flow takes place from one space between plates (31) from the inside to the outside towards the separating space (32) and subsequently into an adjacent space between plates (31) from the outside to the inside.
  2. The flotation device as set forth in claim 1, characterised in that the plates (30) and/or the flotation tank (12) are configured round or regularly polygonal.
  3. The flotation device as set forth in claim 2, characterised in that the plates (30) are configured substantially conically or, conversely, pyramid-shaped.
  4. The flotation device as set forth in claim 3, characterised in that the plates (30) are inclined upwards in the radial direction.
  5. The flotation device as set forth in claim 1, characterised in that in the radial direction, shorter plates (30a) and longer plates (30b) are arranged alternately one above another.
  6. The flotation device as set forth in claim 5, characterised in that a first annular plate spacing (31a) formed below by a longer plate (30b) and above by a shorter plate (30a) is connected to the suspension distribution tube (26) and a second annular plate spacing (31a) formed below by a shorter plate (30a) and above by a longer plate (30b) is connected to the clarified fluid collecting tube (48).
  7. The flotation device as set forth in claim 5, characterised in that a second annular plate spacing (31b) formed below by a shorter plate (30a) and above by a longer plate (30b) is connected to the suspension distribution tube (26) and a first annular plate spacing (31a) formed below by a longer plate (30b) and above by a shorter plate (30a) is connected to the clarified fluid collecting tube (48).
  8. The flotation device as set forth in claim 5, characterised in that the shorter plates (30a) are 5% to 40% shorter in the radial direction than the longer plates (30b).
  9. The flotation device as set forth in claim 5, characterised in that the separating space (32) between the ends of the plates (30) and the wall of the flotation tank (12) has an extent between 10% and 30% of the extent of the longer plates (30b) in the radial direction.
  10. The flotation device as set forth in claim 1, characterised in that the inclination of the plates with respect to the horizontal is between 10° and 60°, preferably between 30° and 50°.
  11. The flotation device as set forth in claim 1, characterised in that arranged centrally in the flotation tank (12) is a conduit comprising both the at least one suspension distribution tube (26) and the at least one clarified fluid collecting tube (48).
  12. The flotation device as set forth in claim 11, characterised in that the conduit is divided into at least two sector-shaped conduits, one of which sector-shaped conduits forms the suspension distribution tube (26) and the second sector-shaped conduit of which forms the clarified fluid collecting tube (48).
  13. The flotation device as set forth in claim 12, characterised in that the conduit is divided into 4 to 8, preferably 6 sector-shaped conduits, wherein the suspension distribution tubes (26) and clarified fluid collecting tubes (48) alternate circumferentially.
  14. The flotation device as set forth in claim 11, characterised in that in the conduit, horizontal throughflow slots (28, 46) are configured approximately the width of the sectors for discharge of the suspension from the suspension distribution tube (26), and for letting in the clarified fluid into the clarified fluid tube (48) into and respectively out of the associated annular plate spaces (31).
  15. The flotation device as set forth in claim 1, characterised in that the reaction and mixing space (18) is configured as a double cone, wherein the upper cone merges into the at least one suspension distribution tube (26) and the lower cone into a sediment drain (20).
  16. The flotation device as set forth in claim 1, characterised in that it includes a base unit, a lid unit and several plate units that can be assembled vertically one above another, wherein each plate unit includes distribution and collecting tube sections, annular space external wall sections, and several plates (30).
EP01986275A 2000-09-27 2001-09-26 Flotation device Expired - Lifetime EP1326713B1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE10047958A DE10047958C2 (en) 2000-09-27 2000-09-27 A flotation device
DE10047958 2000-09-27
PCT/DE2001/003769 WO2002028538A2 (en) 2000-09-27 2001-09-26 Flotation device

Publications (2)

Publication Number Publication Date
EP1326713A2 EP1326713A2 (en) 2003-07-16
EP1326713B1 true EP1326713B1 (en) 2007-01-24

Family

ID=7657891

Family Applications (1)

Application Number Title Priority Date Filing Date
EP01986275A Expired - Lifetime EP1326713B1 (en) 2000-09-27 2001-09-26 Flotation device

Country Status (12)

Country Link
US (1) US6773586B2 (en)
EP (1) EP1326713B1 (en)
JP (1) JP3585231B2 (en)
AT (1) ATE352376T1 (en)
AU (1) AU2002223451A1 (en)
BR (1) BR0107285B1 (en)
CA (1) CA2394164C (en)
DE (2) DE10047958C2 (en)
ES (1) ES2281454T3 (en)
MX (1) MXPA02005463A (en)
PT (1) PT1326713E (en)
WO (1) WO2002028538A2 (en)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7232476B2 (en) * 2004-12-28 2007-06-19 Council Of Scientific And Industrial Research Apparatus for scum removal
GB2423734B (en) * 2005-03-03 2007-02-07 Yorkshire Water Services Ltd Dissolved gas flotation system and nozzle assembly
CN101746909B (en) * 2009-12-24 2011-03-02 吴少杰 Method for pretreating machining waste emulsion liquid and equipment therefor
US11207614B2 (en) 2019-07-23 2021-12-28 University Of Kentucky Research Foundation Single stage clarifier and mixing assembly
US11596912B2 (en) 2019-07-23 2023-03-07 University Of Kentucky Research Foundation Single stage clarifier and mixing assembly
CN112897620A (en) * 2021-03-06 2021-06-04 无锡大驰环境技术有限公司 Air floatation system with super-strong treatment capacity

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1213223C2 (en) * 1960-02-15 1973-02-01 Milos Krofta Dr Ing Device for cleaning uncleared waste water in the paper, pulp and similar industries
US3754656A (en) * 1970-09-28 1973-08-28 Kurita Water Ind Ltd Floatation separators
CH548795A (en) * 1972-09-12 1974-05-15 Escher Wyss Ag DECANTER.
DE2640803C2 (en) * 1975-09-18 1982-03-11 Thune-Eureka A/S, Tranby Lamella separator for sedimentation
FR2457127A1 (en) * 1979-05-23 1980-12-19 Alsthom Atlantique SEPARATOR OF A MIXTURE OF TWO LIQUIDS
US4936990A (en) * 1989-05-01 1990-06-26 Brunsell Dennis A Apparatus for multiple fluid phase separator
FR2699421B1 (en) * 1992-12-21 1995-02-10 Alsthom Gec Lamellar settling tank with double flow.
FR2717192B1 (en) * 1994-03-11 1996-04-26 Lamort E & M Method for deinking paper pulp and apparatus for carrying out this method.
AUPM714794A0 (en) * 1994-07-29 1994-08-18 International Fluid Separation Pty Limited Separation apparatus and method
GB9505891D0 (en) * 1995-03-23 1995-05-10 Dufour Reneau Series multi-staged clarifier
FR2774307B1 (en) * 1998-01-30 2000-03-10 Roumen Kaltchev DEVICE AND METHOD FOR LAMELLAR CLARIFICATION OF LIQUID LOADED IN SUSPENSION MATERIAL

Also Published As

Publication number Publication date
WO2002028538A2 (en) 2002-04-11
ATE352376T1 (en) 2007-02-15
DE10047958A1 (en) 2002-04-18
MXPA02005463A (en) 2002-11-29
WO2002028538A3 (en) 2002-06-27
PT1326713E (en) 2007-04-30
ES2281454T3 (en) 2007-10-01
DE10047958C2 (en) 2002-08-01
CA2394164A1 (en) 2002-04-11
US20020096475A1 (en) 2002-07-25
JP3585231B2 (en) 2004-11-04
CA2394164C (en) 2007-03-20
EP1326713A2 (en) 2003-07-16
BR0107285B1 (en) 2010-09-08
AU2002223451A1 (en) 2002-04-15
DE50111974D1 (en) 2007-03-15
US6773586B2 (en) 2004-08-10
BR0107285A (en) 2002-08-13
JP2004510568A (en) 2004-04-08

Similar Documents

Publication Publication Date Title
DE2349702C2 (en) Method and device for fractionating a suspension by means of hydrocyclones
DE69320954T2 (en) WATER CLEARING DEVICE WITH INSULATION OF THE FIRST FILTRATE IMPROVED BACKWASH AND BUBBLE FORMATION
DE1929974C3 (en) Inclined plate clarifier
WO2009138192A1 (en) Three-phase cascade separator
DE69816068T2 (en) DEVICE FOR SEPARATING SOLIDS FROM A LIQUID
DE3134871C2 (en) Disc press
DE3046969A1 (en) DEVICE FOR TREATING MOVING SUSPENSIONS
DE3940334A1 (en) SCREEN FOR PRINT SORTING FOR FIBER SUSPENSIONS
EP1326713B1 (en) Flotation device
AT395325B (en) DEVICE FOR SEPARATING A CELLULOSE-FIBER-MIXED SUSPENSION
DE2129349C3 (en) Floating filter clarifier for clarifying liquids
DE19850320C2 (en) Compact system for the mechanical treatment of waste water
EP2627426B1 (en) Device for precipitating suspended materials
DE1517391C3 (en) Device for clarifying water
EP2957683B1 (en) Waste water treatment assembly
DE4006633A1 (en) Fibre suspension sieve - has projecting blades at mantle with downwards angled ends to give two fractions without clogging
DE60309210T2 (en) POLYGONAL PIPE WALL WITH A REJUVENZONE ZONE
CH677194A5 (en)
DE102005033701A1 (en) plate precipitator
WO2008135124A1 (en) Flotation apparatus with plate containing holes
EP0789611B1 (en) Multiple tube filter device for filtering beer
DE2908003C2 (en) Device for dry, absorptive binding of air pollutants to additives
EP0951326A1 (en) Sedimentation basin with rectangular layout for separating sludge from waste water
DE3711114A1 (en) Service water backwash filter
EP0864344A1 (en) Inlet distributor and settling tank incorporating the same

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

17P Request for examination filed

Effective date: 20030326

AK Designated contracting states

Designated state(s): AT BE CH CY DE DK ES FI FR GB GR IE IT LI LU MC NL PT SE TR

AX Request for extension of the european patent

Extension state: AL LT LV MK RO SI

GRAP Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOSNIGR1

GRAS Grant fee paid

Free format text: ORIGINAL CODE: EPIDOSNIGR3

GRAA (expected) grant

Free format text: ORIGINAL CODE: 0009210

AK Designated contracting states

Kind code of ref document: B1

Designated state(s): AT BE CH CY DE DK ES FI FR GB GR IE IT LI LU MC NL PT SE TR

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: FI

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20070124

Ref country code: DK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20070124

Ref country code: IE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20070124

Ref country code: NL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20070124

REG Reference to a national code

Ref country code: GB

Ref legal event code: FG4D

Free format text: NOT ENGLISH

REG Reference to a national code

Ref country code: CH

Ref legal event code: EP

REG Reference to a national code

Ref country code: IE

Ref legal event code: FG4D

Free format text: LANGUAGE OF EP DOCUMENT: GERMAN

REF Corresponds to:

Ref document number: 50111974

Country of ref document: DE

Date of ref document: 20070315

Kind code of ref document: P

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20070424

REG Reference to a national code

Ref country code: PT

Ref legal event code: SC4A

Free format text: AVAILABILITY OF NATIONAL TRANSLATION

Effective date: 20070403

REG Reference to a national code

Ref country code: CH

Ref legal event code: NV

Representative=s name: ZIMMERLI, WAGNER & PARTNER AG

ET Fr: translation filed
NLV1 Nl: lapsed or annulled due to failure to fulfill the requirements of art. 29p and 29m of the patents act
REG Reference to a national code

Ref country code: IE

Ref legal event code: FD4D

REG Reference to a national code

Ref country code: ES

Ref legal event code: FG2A

Ref document number: 2281454

Country of ref document: ES

Kind code of ref document: T3

PLBE No opposition filed within time limit

Free format text: ORIGINAL CODE: 0009261

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT

26N No opposition filed

Effective date: 20071025

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: GR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20070425

Ref country code: MC

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20070930

Ref country code: IT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20070124

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: CY

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20070124

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LU

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20070926

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: TR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20070124

REG Reference to a national code

Ref country code: CH

Ref legal event code: PFA

Owner name: MERI ENTSORGUNGSTECHNIK FUER DIE PAPIERINDUSTRIE

Free format text: MERI ENTSORGUNGSTECHNIK FUER DIE PAPIERINDUSTRIE GMBH#LEVELINGSTRASSE 18#81673 MUENCHEN (DE) -TRANSFER TO- MERI ENTSORGUNGSTECHNIK FUER DIE PAPIERINDUSTRIE GMBH#LEVELINGSTRASSE 18#81673 MUENCHEN (DE)

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: DE

Payment date: 20100928

Year of fee payment: 10

REG Reference to a national code

Ref country code: DE

Ref legal event code: R081

Ref document number: 50111974

Country of ref document: DE

Owner name: MERI ENVIRONMENTAL SOLUTIONS GMBH, DE

Free format text: FORMER OWNER: MERI ENTSORGUNGSTECHNIK FUER DIE PAPIERINDUSTRIE GMBH, 81673 MUENCHEN, DE

Effective date: 20110411

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: CH

Payment date: 20110926

Year of fee payment: 11

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: ES

Payment date: 20110923

Year of fee payment: 11

Ref country code: FR

Payment date: 20111005

Year of fee payment: 11

Ref country code: PT

Payment date: 20110915

Year of fee payment: 11

Ref country code: GB

Payment date: 20110923

Year of fee payment: 11

Ref country code: AT

Payment date: 20110922

Year of fee payment: 11

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: BE

Payment date: 20110926

Year of fee payment: 11

BERE Be: lapsed

Owner name: MERI ENTSORGUNGSTECHNIK FUR DIE PAPIERINDUSTRIE G

Effective date: 20120930

REG Reference to a national code

Ref country code: PT

Ref legal event code: MM4A

Free format text: LAPSE DUE TO NON-PAYMENT OF FEES

Effective date: 20130326

REG Reference to a national code

Ref country code: CH

Ref legal event code: PL

REG Reference to a national code

Ref country code: AT

Ref legal event code: MM01

Ref document number: 352376

Country of ref document: AT

Kind code of ref document: T

Effective date: 20120926

GBPC Gb: european patent ceased through non-payment of renewal fee

Effective date: 20120926

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: PT

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20130326

REG Reference to a national code

Ref country code: FR

Ref legal event code: ST

Effective date: 20130531

REG Reference to a national code

Ref country code: DE

Ref legal event code: R119

Ref document number: 50111974

Country of ref document: DE

Effective date: 20130403

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: CH

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20120930

Ref country code: LI

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20120930

Ref country code: BE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20120930

Ref country code: AT

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20120926

Ref country code: DE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20130403

Ref country code: GB

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20120926

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: FR

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20121001

REG Reference to a national code

Ref country code: ES

Ref legal event code: FD2A

Effective date: 20131021

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: ES

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20120927