EP1220714A2 - Verfahren und vorrichtung für einen optimal integrierten homogenisierungsproze - Google Patents

Verfahren und vorrichtung für einen optimal integrierten homogenisierungsproze

Info

Publication number
EP1220714A2
EP1220714A2 EP00907456A EP00907456A EP1220714A2 EP 1220714 A2 EP1220714 A2 EP 1220714A2 EP 00907456 A EP00907456 A EP 00907456A EP 00907456 A EP00907456 A EP 00907456A EP 1220714 A2 EP1220714 A2 EP 1220714A2
Authority
EP
European Patent Office
Prior art keywords
ultrasound
continuous
lamellas
chamber
charateristic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP00907456A
Other languages
English (en)
French (fr)
Inventor
Peter Sendal From
Helge V. Petersen
Poul Melby
Hans H. Haraldsted
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Teledyne Reson AS
Original Assignee
Reson AS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Reson AS filed Critical Reson AS
Publication of EP1220714A2 publication Critical patent/EP1220714A2/de
Withdrawn legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • B01F23/41Emulsifying
    • B01F23/411Emulsifying using electrical or magnetic fields, heat or vibrations
    • B01F23/4111Emulsifying using electrical or magnetic fields, heat or vibrations using vibrations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F31/00Mixers with shaking, oscillating, or vibrating mechanisms
    • B01F31/80Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F31/00Mixers with shaking, oscillating, or vibrating mechanisms
    • B01F31/80Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations
    • B01F31/83Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations comprising a supplementary stirring element
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/07Stirrers characterised by their mounting on the shaft
    • B01F27/072Stirrers characterised by their mounting on the shaft characterised by the disposition of the stirrers with respect to the rotating axis
    • B01F27/0725Stirrers characterised by their mounting on the shaft characterised by the disposition of the stirrers with respect to the rotating axis on the free end of the rotating axis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/11Stirrers characterised by the configuration of the stirrers
    • B01F27/112Stirrers characterised by the configuration of the stirrers with arms, paddles, vanes or blades
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/50Mixing receptacles
    • B01F35/53Mixing receptacles characterised by the configuration of the interior, e.g. baffles for facilitating the mixing of components
    • B01F35/532Mixing receptacles characterised by the configuration of the interior, e.g. baffles for facilitating the mixing of components with guide tubes on the wall or the bottom

Definitions

  • the invention relates to a method as an apparatus for continuous homogenising or emulsification of liquid, where the liquid in a ultrasound chamber with lamellas or guiding plates, especially placed on the outer walls of the chamber, but also possibly with a place in the area up to this, can be submitted to a cinematic- mechanical treatment, as an example by stirring , and with an continuous stream, which subsequently is guided over the surface of several ultrasound generators.
  • this can be obtained respectively by a driving form for ultra sound transducers, and by the establish dynamic-physical state of the lamellas, and characteristic of, that a majority of transducers are driven in displaced succession, while at least in change one transducer is in rest, as that the lamellas during work can be given a rotating movement.
  • the ultrasound head can cool down, before its critical temperature for destruction has been reached.
  • Another advantage is also that the ultrasound head and its electrical resistence is lowering by cooling, why there further also here has been obtained an advantage.
  • one now can couple as drive the ultrasound heads more stabile, inside a lesser range of temperature.
  • a further advantage is also that one, by continuous shift between the heads, further can obtain a higher degree of efficiency of the arrangement. As a shift and stop will change the condition of cavitation, so that the cavitation or emulsification can be more effective or maintain optimum driving in the liquid.
  • FigJ shows in perspective a ultrasound chamber for homogenisation as emulsification of liquid, with guiding plates and driving or working of the ultrasound transducers in displaced order ,-
  • Fig.2 shows a ring of lamella- or guiding plates, which rotate together or jointly around or in the centre axle of the ultrasound chamber
  • Fig.3 shows in perspective and seen from the side a single vertical lamella-or guiding plate, which rotate around itself, -
  • Fig.3B shows a single rotating lamella-or guiding plate as Fig.3, but seen from upper, and
  • Fig.4 shows a picture of pulsing guiding ultrasound signals.
  • FIGJ Shows in perspective a ultrasound chamber 1 for homogenisation as emulsification of liquid(s) I as II, with guiding plates 2 and working or driven of ultrasound transducers 4 which self each and together work in displaced order.
  • the figure shows an example of an embodiment with vertical placed chamber 1 or boiler 1, which self also in the same time make a pressure safe chamber of mixing 1.
  • the liquids I as II which in the example of embodiment have been supplied from above in the chamber of mixing 1, will immediately after this be influenced of an arrangement of wheel of scoop 3. Where the just now partly mixed liquid I as II via the wheels of scoops 3 will be thrown against the guiding plates 2, and in the same time, because of the liquids I as II continuous have been supplied from above via supply lines,- then will the partly homogenised liquid be led against the bottom of the chamber 1 to the exhauster pipe 8, and to continued treatment via the ultrasound transducers 4.
  • the ultrasound arrangement 4 can as shown on the figure ideal as an example consist of four ultrasound transducers 4. Which as an example could work in the field from 18-120 kHz, but still as here ideal as an example in the field from 20 -50 kHz.
  • An ideal cycle of mutual working operation for the transducers 4 will be by a continuous mutual changing 5 as "rif 5 between these. So that some of the transducers 4 drive, and other transducers 4 do not drive.
  • one drive or work with three transducers 4 at a time and so successive working or driving of the common system of the transducers 4.
  • driving three transducers 4 at a time Where for that matter the one transducer 4 continuous in its "rif 5 or changing will be new.
  • Fig.2 shows a ring of lamellas -or guiding plates 2, which rotate 9 together or joint around/in the centre axle of the ultrasound chamber 1.
  • the system 2 could consist of as an alternative several rotating 9 ring systems or rims 9' with vertical sitting plates of lamellas-or guiding plates 2. Where these 2 or the rims 9' then perhaps alternative ideal could drive or work opposite each other 2, as 9', or perhaps with different speed or both working operations in combination.
  • Fig.3 shows in perspective and seen from the side a single vertical lamella-or guiding plate 2, which rotate around itself.
  • the arrangement 2 could of cause also be combined with the system, which is shown in Fig.2.
  • the system will especially has an extra effect, if the system turn opposite of, what the arrangement of middle rings system 3 do.
  • Fig.4 shows a picture of a pulsing 7 ultrasound signal 10, which drive or work as a whole. And which drive as a part of the "rif- driving of the ultrasound transducers 4, namely in a displace succession 5, with one transducer 4 in rest, by which there, by this summing up driving, has been obtained a specially effect namely a "synergi" -effect, in the effectiveness of the total effect of homogenising. And which effect therefore is larger than one logical could think, with or by every one of the single section-operations or working forms 5 as 7, "looked” driven for itself and without the other working form as supplement .

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mixers With Rotating Receptacles And Mixers With Vibration Mechanisms (AREA)
EP00907456A 1999-03-05 2000-03-02 Verfahren und vorrichtung für einen optimal integrierten homogenisierungsproze Withdrawn EP1220714A2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DK199900296A DK173810B1 (da) 1999-03-05 1999-03-05 Fremgangsmåde og apparatur for en optimal integreret homogeniseringsproces
DK29699 1999-03-05

Publications (1)

Publication Number Publication Date
EP1220714A2 true EP1220714A2 (de) 2002-07-10

Family

ID=59053835

Family Applications (1)

Application Number Title Priority Date Filing Date
EP00907456A Withdrawn EP1220714A2 (de) 1999-03-05 2000-03-02 Verfahren und vorrichtung für einen optimal integrierten homogenisierungsproze

Country Status (6)

Country Link
EP (1) EP1220714A2 (de)
KR (1) KR20010103767A (de)
CN (1) CN1141173C (de)
AU (1) AU2903400A (de)
DK (1) DK173810B1 (de)
WO (1) WO2000054095A2 (de)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108607374A (zh) * 2014-12-22 2018-10-02 江山显进机电科技服务有限公司 悬挂式溶解乳化装置

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20040022637A (ko) * 2002-09-09 2004-03-16 주식회사 효성 동시 유화법을 이용한 아크릴 미립자 제조방법
GB0222421D0 (en) * 2002-09-27 2002-11-06 Ratcliff Henry K Advanced ultrasonic processor
CN1311896C (zh) * 2005-03-08 2007-04-25 杭州电子科技大学 循环式多级超声波分散机
KR100737120B1 (ko) 2006-08-31 2007-07-06 박병인 재료의 혼합 및 균질화장치
US8215822B2 (en) * 2007-12-28 2012-07-10 Kimberly-Clark Worldwide, Inc. Ultrasonic treatment chamber for preparing antimicrobial formulations
CN102847479B (zh) * 2012-10-11 2014-06-18 北京化工大学 一种大容量超声破碎分散装置
CN102974248A (zh) * 2012-11-30 2013-03-20 大连隆星新材料有限公司 一种化工原料搅拌装置
CN107626244A (zh) * 2016-07-18 2018-01-26 林荣良 一种真空搅拌式超声波分散破碎处理罐
CN111111486A (zh) * 2020-01-10 2020-05-08 杭小洁 一种涂料乳化均质装置

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SE412702B (sv) * 1979-03-06 1980-03-17 Reson System Aps Forfarande och apparat for kontinuerlig homogenisering av vetskor

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See references of WO0054095A2 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108607374A (zh) * 2014-12-22 2018-10-02 江山显进机电科技服务有限公司 悬挂式溶解乳化装置

Also Published As

Publication number Publication date
WO2000054095A3 (en) 2001-01-04
CN1362893A (zh) 2002-08-07
DK173810B1 (da) 2001-11-12
CN1141173C (zh) 2004-03-10
KR20010103767A (ko) 2001-11-23
WO2000054095A2 (en) 2000-09-14
AU2903400A (en) 2000-09-28

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