EP1140007B1 - Detergent composition - Google Patents
Detergent composition Download PDFInfo
- Publication number
- EP1140007B1 EP1140007B1 EP99958172A EP99958172A EP1140007B1 EP 1140007 B1 EP1140007 B1 EP 1140007B1 EP 99958172 A EP99958172 A EP 99958172A EP 99958172 A EP99958172 A EP 99958172A EP 1140007 B1 EP1140007 B1 EP 1140007B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- composition
- composition according
- benefit agent
- cationic polymer
- cationic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0241—Containing particulates characterized by their shape and/or structure
- A61K8/0275—Containing agglomerated particulates
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/54—Polymers characterized by specific structures/properties
- A61K2800/542—Polymers characterized by specific structures/properties characterized by the charge
- A61K2800/5426—Polymers characterized by specific structures/properties characterized by the charge cationic
Definitions
- the present invention relates to detergent compositions suitable for topical application for cleansing and improving the condition of the human body, particularly for moisturising the skin, hair, nails and other epithelial tissues, including the mucosae.
- compositions which are formulated to give mild cleansing and conditioning of the skin, and improved deposition of benefit agents.
- compositions formulated to cleanse the skin are well known. It is also known to formulate products which provide both a cleansing and a moisturising benefit.
- WO 90/13283 discloses a composition comprising an acyl ester of an isethionic acid salt, a long chain fatty acid, a moisturiser component and, optionally, soap.
- WO 95/22311 discloses a composition containing a surfactant, a benefit agent and a cationic deposition polymer.
- compositions such that they can deliver effective moisturising, conditioning and/or protection of the skin, and also a way of delivering benefit agents in a more efficient manner.
- an aqueous liquid cleansing and moisturising composition comprising:-
- compositions according to the invention are preferably shear thinning.
- compositions according to the present invention are that they lead to improved deposition of benefit agents from a surfactant-containing aqueous liquid composition during use.
- compositions according to the invention that particles of the skin benefit agent form aggregates which comprise a number of individual particles.
- aggregates which characterise compositions according to the invention comprise 5-5000 individual particles of benefit agent.
- compositions which comprise these aggregated particles which aggregated particles stay in this form and do not coalesce, serve to deliver to the substrate relatively large aggregates of benefit agent, which provides an effective local high concentration of the benefit agent, thus enhancing the moisturising benefit to the substrate, and also the overall efficiency of delivery of the benefit agent.
- compositions according to the invention may typically comprise relatively high populations of relatively large, aggregated particles.
- Compositions according to the invention may therefore for example have a mean individual particle size of less than 5 ⁇ m (5 microns), typically less than 1 ⁇ m (1 micron), but contain about 50% or less by weight of the benefit agent in the composition in particles less than 3 ⁇ m (3 microns) in size.
- the composition may also comprise less than 10% by weight of the benefit agent in aggregated particles of greater than 80 ⁇ m (80 microns) in size.
- Compositions according to the invention typically have more than 3% by weight of the benefit agent in aggregated particles with sizes in the range 3-80 ⁇ m (3-80 microns).
- compositions according to the invention also characteristically retain the aggregated microstructure during dilution in use, for example when diluted by a factor of 10 with distilled water. As such, compositions which have been diluted at ratios between 1:1 and 1:100 with water have been found also to retain the microstructure.
- compositions according to the invention containing the aggregated particles described preferably contain not only relatively high levels of benefit agent, cationic polymer, and contain aggregated particles of benefit agent, but may conveniently also be made according to preferred process aspects.
- the cationic polymer used in compositions according to the invention is at least partially hydrated when it is dispersed in the aqueous vehicle. If the cationic polymer is insufficiently hydrated, this may lead to insufficient aggregation of the droplets of benefit agent in the composition, whilst if the Cationic polymer in overly hydrated, in particular during its dispersion in the composition, it may prove difficult to disperse satisfactorily.
- composition according to the invention is suitable for cleansing and "moisturising", “conditioning” or “protection” of the skin.
- the benefit agent is included in the composition to moisturise, condition and/or protect the akin.
- “benefit agent” is meant a substance that softens the skin (stratum corneum) and keeps it soft by retarding the decrease of its water content and/or protects the skin.
- the benefit agent may be incorporated in the compositions of the invention in a carrier.
- the carrier could itself be a benefit agent, such as an oil.
- Such benefit agents include lipids; alkyl lactates; sunscreens; esters such as isopropyl palmitate and isopropyl myristate; and vitamins.
- the carrier can, for example, be a silicone or hydrocarbon oil which is not solubilised/micellised by the surface active phase and in which the benefit agent is relatively soluble.
- the benefit agent is preferably present in an amount of from 1.0 to 50 wt%, most preferably from 4 to 25 wt% of the composition, more preferably 5-15%, even more preferably 5-10% by weight of the composition.
- composition according to the invention is that, during use, it deposits benefit agent onto the skin at a level which results in a perceivable benefit.
- the surface active agent can be selected from any known surfactant suitable for topical application to the human body. Mild surfactants, i.e. surfactants which do not damage the stratum corneum, the outer layer of skin, are particularly preferred. Because of their lathering properties, anionic surfactants are highly preferred components of compositions according to the invention. Where the composition contains an anionic surfactant, it is preferable that the composition also contains a co-surfactant, which can be a nonionic, cationic or zwitterionic surfactant.
- One preferred anionic detergent is fatty acyl isethionate of formula: RCO 2 CH 2 CH 2 SO 3 M where R is an alkyl or alkenyl group of 7 to 21 carbon atoms and M is a solubilising cation such as sodium, potassium, ammonium or substituted ammonium.
- RCO 2 CH 2 CH 2 SO 3 M where R is an alkyl or alkenyl group of 7 to 21 carbon atoms and M is a solubilising cation such as sodium, potassium, ammonium or substituted ammonium.
- RCO 2 CH 2 CH 2 SO 3 M is an alkyl or alkenyl group of 7 to 21 carbon atoms and M is a solubilising cation such as sodium, potassium, ammonium or substituted ammonium.
- Preferably at least three quarters of the RCO groups have 12 to 18 carbon atoms and may be derived from coconut, palm or a coconut/palm blend.
- alkyl ether sulphate of formula: RO(CH 2 CH 2 O) n SO 3 M where R is an alkyl group of 8 to 22 carbon atoms, n ranges from 0.5 to 10 especially from 1.5 to 8, and M is a solubilising cation as before.
- anionic detergents include alkyl glyceryl ether sulphate, sulphosuccinates, taurates, sarcosinates, sulphoacetates, alkyl phosphate, alkyl phosphate esters and acyl lactylate, alkyl glutamates and mixtures thereof.
- Sulphosuccinates may be monoalkyl sulphosuccinates having the formula: R 5 O 2 CCH 2 CH(SO 3 M)CO 2 M; and amido-MEA sulphosuccinates of the formula: R 5 CONHCH 2 CH 2 O 2 CCH 2 CH(SO 3 M)CO 2 M; wherein R 5 ranges from C 8 -C 20 alkyl, preferably C 12 -C 15 alkyl and M is a solubilising cation.
- compositions include opacifiers, preferably 0.2 to 2.0 wt%; preservatives, preferably 0.2 to 2.0 wt% and perfumes, preferably 0.5 to 2.0 wt%.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GBGB9827614.0A GB9827614D0 (en) | 1998-12-15 | 1998-12-15 | Detergent composition |
GB9827614 | 1998-12-15 | ||
PCT/EP1999/009588 WO2000035416A1 (en) | 1998-12-15 | 1999-12-03 | Detergent composition |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1140007A1 EP1140007A1 (en) | 2001-10-10 |
EP1140007B1 true EP1140007B1 (en) | 2002-09-04 |
Family
ID=10844269
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP99958172A Expired - Lifetime EP1140007B1 (en) | 1998-12-15 | 1999-12-03 | Detergent composition |
Country Status (19)
Country | Link |
---|---|
US (1) | US6255264B1 (es) |
EP (1) | EP1140007B1 (es) |
JP (1) | JP4531262B2 (es) |
KR (1) | KR100576658B1 (es) |
CN (1) | CN1273108C (es) |
AT (1) | ATE223198T1 (es) |
AU (1) | AU747078B2 (es) |
BR (1) | BR9916232A (es) |
CA (1) | CA2354772C (es) |
CZ (1) | CZ302598B6 (es) |
DE (1) | DE69902815T2 (es) |
ES (1) | ES2183629T3 (es) |
GB (1) | GB9827614D0 (es) |
HU (1) | HU228032B1 (es) |
ID (1) | ID30045A (es) |
PL (1) | PL197485B1 (es) |
RU (1) | RU2230548C2 (es) |
WO (1) | WO2000035416A1 (es) |
ZA (1) | ZA200104665B (es) |
Families Citing this family (40)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2002036095A2 (en) * | 2000-10-31 | 2002-05-10 | Unilever Plc | Personal cleansing composition |
GB0126280D0 (en) * | 2001-11-01 | 2002-01-02 | Unilever Plc | Liquid detergent compositions |
US7037513B1 (en) | 2005-01-31 | 2006-05-02 | Aquea Scientific Corporation | Bodywash additives |
US20060173709A1 (en) * | 2005-01-31 | 2006-08-03 | Traynor Daniel H | Bodywash additive business methods |
US6998113B1 (en) * | 2005-01-31 | 2006-02-14 | Aquea Scientific Corporation | Bodywashes containing additives |
US7025952B1 (en) | 2005-01-31 | 2006-04-11 | Aquea Scientific Corporation | Methods of preparation and use of bodywashes containing additives |
JP2004262838A (ja) * | 2003-02-28 | 2004-09-24 | Kao Corp | 皮膚洗浄剤組成物 |
US8623341B2 (en) * | 2004-07-02 | 2014-01-07 | The Procter & Gamble Company | Personal care compositions containing cationically modified starch and an anionic surfactant system |
US7326672B2 (en) * | 2004-07-29 | 2008-02-05 | Vivek Subramanian | Substantially enzyme free personal wash compositions comprising non-silicates with basal layer cationic charge |
CA2590707A1 (en) * | 2004-12-06 | 2006-06-15 | The Procter & Gamble Company | Fabric enhancing composition |
EP1838280A2 (en) * | 2005-01-10 | 2007-10-03 | Dow Global Technologies Inc. | Personal care compositions |
US7001592B1 (en) | 2005-01-31 | 2006-02-21 | Aquea Scientific Corporation | Sunscreen compositions and methods of use |
US20080112904A1 (en) * | 2005-03-08 | 2008-05-15 | Daniel Henry Traynor | Sunscreen Compositions And Methods Of Use |
CA2603299A1 (en) * | 2005-04-13 | 2006-10-26 | The Procter & Gamble Company | Structured multi-phased personal care composition comprising branched anionic surfactants |
US7820609B2 (en) | 2005-04-13 | 2010-10-26 | The Procter & Gamble Company | Mild, structured, multi-phase personal cleansing compositions comprising density modifiers |
US20120015009A9 (en) * | 2005-06-07 | 2012-01-19 | The Procter & Gamble Company | Multi-phased personal care composition comprising a blooming perfume composition |
EP1957374A2 (en) * | 2005-12-08 | 2008-08-20 | The Procter and Gamble Company | A container comprising an in-mold label positioned proximate to a surface topography |
US20070167338A1 (en) * | 2006-01-09 | 2007-07-19 | Mchugh Colin M | Multiphase personal care compositions comprising beads |
US8104616B2 (en) | 2006-02-11 | 2012-01-31 | The Procter & Gamble Company | Clamshell package for holding and displaying consumer products |
US8153144B2 (en) | 2006-02-28 | 2012-04-10 | The Proctor & Gamble Company | Stable multiphase composition comprising alkylamphoacetate |
ATE455165T1 (de) * | 2006-04-04 | 2010-01-15 | Unilever Nv | Waschmittelszusammensetzung mit verkapseltem flüssigem pflegemittel |
DE102007017307A1 (de) | 2007-04-11 | 2008-10-16 | Beiersdorf Ag | Zubereitung zur Pflege des Haares, enthaltend ein ampholytisches Copolymer |
WO2008144734A1 (en) * | 2007-05-21 | 2008-11-27 | Aquea Scientific Corporation | Highly charged microcapsules |
US20090324520A1 (en) * | 2007-07-27 | 2009-12-31 | Jonathan Robert Cetti | Personal-care article for sequentially dispensing compositions with variable concentrations of partitioned benefit or suspended benefit agents |
US20090028809A1 (en) * | 2007-07-27 | 2009-01-29 | Jonathan Robert Cetti | Personal care article for sequentially dispensing compositions with variable concentrations of hydrophobic benefit materials |
US20090028808A1 (en) * | 2007-07-27 | 2009-01-29 | The Procter & Gamble Company | Personal care article for sequentially dispensing compositions with variable concentrations of partitioned benefit or suspended benefit agents |
WO2010013203A2 (en) * | 2008-07-28 | 2010-02-04 | The Procter & Gamble Company | In-vitro deposition evaluation method for identifying personal care compositions which provide improved deposition of benefit agents |
US8840871B2 (en) * | 2008-07-28 | 2014-09-23 | The Procter & Gamble Company | Multiphase personal care composition with enhanced deposition |
EP2551337A1 (en) * | 2011-07-27 | 2013-01-30 | The Procter & Gamble Company | Process for the production of a rheology modifier containing composition |
US20130045263A1 (en) * | 2011-08-15 | 2013-02-21 | Edward Dewey Smith, III | Personal Care Compositions Having Dried Zinc Pyrithione-Polymer Aggregates |
US10322301B2 (en) | 2012-11-06 | 2019-06-18 | CoLabs International Corporation | Compositions containing a cellulose derived capsule with a sunscreen active agent |
US11690793B2 (en) | 2012-11-06 | 2023-07-04 | Colabs Int'l Corp. | Composition containing a cellulose derived capsule with a sunscreen |
US11724134B2 (en) | 2012-11-06 | 2023-08-15 | CoLabs International Corporation | Compositions containing a cellulose derived capsule with a sunscreen active agent |
US11707421B2 (en) | 2012-11-06 | 2023-07-25 | Colabs Int'l Corp. | Compositions containing a flexible derived capsule with an active agent |
JP2015536985A (ja) | 2012-11-06 | 2015-12-24 | コラブス インターナショナル コーポレーション | 日焼け止めを含むセルロース由来カプセル含有組成物 |
US11491088B2 (en) | 2012-11-06 | 2022-11-08 | CoLabs International Corporation | Compositions containing a capsule with a moisturizing agent |
RU2605426C1 (ru) | 2012-12-07 | 2016-12-20 | Колгейт-Палмолив Компани | Композиции мыльных брусков и способы их получения |
US20140303135A1 (en) * | 2013-04-04 | 2014-10-09 | The Procter & Gamble Company | Personal Care Compositions Having Dried Zinc Pyrithione-Polymer Aggregates |
CN104212659A (zh) * | 2013-05-30 | 2014-12-17 | 上海珀理玫化学科技有限公司 | 一种生态洗衣液 |
EP3813786A4 (en) | 2018-06-27 | 2022-06-29 | Colabs International Corporation | Compositions comprising silicon dioxide-based particles including one or more agents |
Family Cites Families (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DK132838A (es) * | 1967-12-11 | |||
US4364837A (en) * | 1981-09-08 | 1982-12-21 | Lever Brothers Company | Shampoo compositions comprising saccharides |
GB2147606B (en) | 1983-10-04 | 1987-06-24 | Procter & Gamble | Anti-dandruff compositions |
US5132037A (en) | 1989-05-05 | 1992-07-21 | Lever Brothers Company, Division Of Conopco, Inc. | Aqueous based personal washing cleanser |
GB8912391D0 (en) * | 1989-05-30 | 1989-07-12 | Unilever Plc | Shampoo composition |
DE69004057T3 (de) * | 1989-12-04 | 2005-05-19 | Unilever N.V. | Haarbehandlungsmittel. |
GB9016100D0 (en) * | 1990-07-23 | 1990-09-05 | Unilever Plc | Shampoo composition |
DE4127731C1 (es) * | 1991-08-22 | 1993-03-11 | Goldwell Ag, 6100 Darmstadt, De | |
JP2972039B2 (ja) * | 1991-10-28 | 1999-11-08 | 信越化学工業株式会社 | 化粧料 |
GB9208653D0 (en) * | 1992-04-22 | 1992-06-10 | Unilever Plc | Cosmetic composition and process for making it |
JPH05310540A (ja) * | 1992-05-13 | 1993-11-22 | Kao Corp | 液状洗浄剤組成物 |
US5308526A (en) * | 1992-07-07 | 1994-05-03 | The Procter & Gamble Company | Liquid personal cleanser with moisturizer |
GB9216854D0 (en) * | 1992-08-07 | 1992-09-23 | Unilever Plc | Detergent composition |
GB9216758D0 (en) * | 1992-08-07 | 1992-09-23 | Unilever Plc | Detergent composition |
GB9320556D0 (en) * | 1993-10-06 | 1993-11-24 | Unilever Plc | Hair conditioning composition |
EP0744935B2 (en) * | 1994-02-18 | 2003-09-10 | Unilever Plc | Personal washing compositions |
EP0805673A1 (en) * | 1994-10-20 | 1997-11-12 | The Procter & Gamble Company | Personal treatment compositions and/or cosmetic compositions containing enduring perfume |
CN1169112A (zh) | 1994-12-06 | 1997-12-31 | 普罗克特和甘保尔公司 | 保存稳定的,含有胶凝聚合物、脂类和脂肪酸乙二醇酯晶体的洁肤液 |
FR2736262B1 (fr) * | 1995-07-07 | 1997-09-26 | Oreal | Compositions cosmetiques detergentes a usage capillaire et utilisation de ces dernieres |
US5747435A (en) * | 1995-08-01 | 1998-05-05 | Colgate-Palmolive Company | Mild foaming and conditioning detergents |
TW446563B (en) * | 1996-01-16 | 2001-07-21 | Colgate Palmolive Co | Low static conditioning shampoo |
GB9610966D0 (en) * | 1996-05-24 | 1996-07-31 | Unilever Plc | Composition |
GB9616411D0 (en) * | 1996-08-05 | 1996-09-25 | Unilever Plc | Shampoo compositions and method |
US6026534A (en) * | 1997-09-22 | 2000-02-22 | Lever Brothers Company | Bathing ball |
-
1998
- 1998-12-15 GB GBGB9827614.0A patent/GB9827614D0/en not_active Ceased
-
1999
- 1999-12-03 ES ES99958172T patent/ES2183629T3/es not_active Expired - Lifetime
- 1999-12-03 WO PCT/EP1999/009588 patent/WO2000035416A1/en active IP Right Grant
- 1999-12-03 PL PL350090A patent/PL197485B1/pl unknown
- 1999-12-03 EP EP99958172A patent/EP1140007B1/en not_active Expired - Lifetime
- 1999-12-03 ID IDW00200101271A patent/ID30045A/id unknown
- 1999-12-03 KR KR1020017007353A patent/KR100576658B1/ko not_active IP Right Cessation
- 1999-12-03 BR BR9916232-6A patent/BR9916232A/pt not_active Application Discontinuation
- 1999-12-03 DE DE69902815T patent/DE69902815T2/de not_active Expired - Lifetime
- 1999-12-03 CA CA002354772A patent/CA2354772C/en not_active Expired - Fee Related
- 1999-12-03 JP JP2000587737A patent/JP4531262B2/ja not_active Expired - Fee Related
- 1999-12-03 CZ CZ20012194A patent/CZ302598B6/cs not_active IP Right Cessation
- 1999-12-03 CN CNB998160776A patent/CN1273108C/zh not_active Expired - Fee Related
- 1999-12-03 HU HU0104764A patent/HU228032B1/hu not_active IP Right Cessation
- 1999-12-03 RU RU2001119444/15A patent/RU2230548C2/ru not_active IP Right Cessation
- 1999-12-03 AT AT99958172T patent/ATE223198T1/de not_active IP Right Cessation
- 1999-12-03 AU AU15597/00A patent/AU747078B2/en not_active Ceased
- 1999-12-13 US US09/459,486 patent/US6255264B1/en not_active Expired - Lifetime
-
2001
- 2001-06-07 ZA ZA200104665A patent/ZA200104665B/en unknown
Also Published As
Publication number | Publication date |
---|---|
CZ302598B6 (cs) | 2011-07-27 |
ZA200104665B (en) | 2002-06-07 |
HU228032B1 (en) | 2012-08-28 |
DE69902815T2 (de) | 2003-01-09 |
ES2183629T3 (es) | 2003-03-16 |
KR20010089570A (ko) | 2001-10-06 |
CN1273108C (zh) | 2006-09-06 |
PL350090A1 (en) | 2002-11-04 |
JP4531262B2 (ja) | 2010-08-25 |
HUP0104764A2 (hu) | 2002-05-29 |
CZ20012194A3 (cs) | 2001-11-14 |
JP2002532404A (ja) | 2002-10-02 |
WO2000035416A1 (en) | 2000-06-22 |
ID30045A (id) | 2001-11-01 |
BR9916232A (pt) | 2001-09-04 |
US6255264B1 (en) | 2001-07-03 |
AU747078B2 (en) | 2002-05-09 |
DE69902815D1 (de) | 2002-10-10 |
AU1559700A (en) | 2000-07-03 |
PL197485B1 (pl) | 2008-04-30 |
ATE223198T1 (de) | 2002-09-15 |
GB9827614D0 (en) | 1999-02-10 |
CA2354772A1 (en) | 2000-06-22 |
EP1140007A1 (en) | 2001-10-10 |
RU2230548C2 (ru) | 2004-06-20 |
CN1334722A (zh) | 2002-02-06 |
CA2354772C (en) | 2009-02-10 |
KR100576658B1 (ko) | 2006-05-08 |
HUP0104764A3 (en) | 2011-04-28 |
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