EP0918573B1 - Air classifier with centrifugal action - Google Patents

Air classifier with centrifugal action Download PDF

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Publication number
EP0918573B1
EP0918573B1 EP97918235A EP97918235A EP0918573B1 EP 0918573 B1 EP0918573 B1 EP 0918573B1 EP 97918235 A EP97918235 A EP 97918235A EP 97918235 A EP97918235 A EP 97918235A EP 0918573 B1 EP0918573 B1 EP 0918573B1
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EP
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Prior art keywords
rotor
blades
section
cross
channels
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EP97918235A
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German (de)
French (fr)
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EP0918573A1 (en
Inventor
Alain Cordonnier
Danielle Lemaire
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FCB CIMENT
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FCB Ciment
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B07SEPARATING SOLIDS FROM SOLIDS; SORTING
    • B07BSEPARATING SOLIDS FROM SOLIDS BY SIEVING, SCREENING, SIFTING OR BY USING GAS CURRENTS; SEPARATING BY OTHER DRY METHODS APPLICABLE TO BULK MATERIAL, e.g. LOOSE ARTICLES FIT TO BE HANDLED LIKE BULK MATERIAL
    • B07B7/00Selective separation of solid materials carried by, or dispersed in, gas currents
    • B07B7/08Selective separation of solid materials carried by, or dispersed in, gas currents using centrifugal force
    • B07B7/083Selective separation of solid materials carried by, or dispersed in, gas currents using centrifugal force generated by rotating vanes, discs, drums, or brushes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B07SEPARATING SOLIDS FROM SOLIDS; SORTING
    • B07BSEPARATING SOLIDS FROM SOLIDS BY SIEVING, SCREENING, SIFTING OR BY USING GAS CURRENTS; SEPARATING BY OTHER DRY METHODS APPLICABLE TO BULK MATERIAL, e.g. LOOSE ARTICLES FIT TO BE HANDLED LIKE BULK MATERIAL
    • B07B11/00Arrangement of accessories in apparatus for separating solids from solids using gas currents
    • B07B11/04Control arrangements

Definitions

  • the present invention relates to a pneumatic separator with centrifugal action intended to classify a granular material into a fine fraction and a coarse fraction and comprising a rotor with vertical axis provided with blades regularly distributed on its periphery, guide vanes arranged around the rotor, along the generatrices of a fictitious cylinder, and able to communicate with a current of air or other gas entering said fictitious cylinder a rotational movement around the axis of said cylinder, and an envelope in which are enclosed the rotor and the guide vanes and which is provided with one or more air inlets and for the material to be classified, an outlet orifice placed above or below the rotor and through which is drawn the air stream charged with the fine fraction of the material and at least one outlet for the coarse fraction, the air entering the rotor at its periphery, through the channels formed between the blades, and flowing inside the rotor towards the outlet.
  • the material to be classified and the air flow can be introduced separately inside the annular section space delimited by the blades and the rotor, or the material to be classified, can be suspended in the air stream before it is admitted into said space, through the blades; the air flow enters then in the rotor and is discharged through the outlet.
  • the air flow and the material to be classified are rotated, around the rotor axis, in the annular section space between the rotor and the blades guidelines.
  • the particles constituting the coarse fraction of the material are projected by the centrifugal force generated by this rotation against the guide vanes and fall by gravity in a collecting hopper with an outlet, while the particles constituting the fine fraction are entrained by the air flow through the rotor and the orifice central exit.
  • the separated fine fraction contains practically all the particles whose size is less than a first dimension while the coarse fraction contains practically all particles larger than a second dimension, larger than the first.
  • both fractions contain particles whose size is included between the first and second dimensions. This results in a sharing curve comprising two substantially horizontal portions connected by an inclined portion, the slope characterizes the separator.
  • the distribution of particles of intermediate size in one or other of the fractions characterizes the cutting precision of the separator.
  • the product we are looking for must have a particle size distribution different from that of the fraction, fine or coarse, obtained by means of a separator of this type. It is in particular the case of cement obtained by crushing by compression of the clinker. So far, the only solution to solve this problem was to use two separators placed in series or in parallel and adjusted for cut-off dimensions different. This solution is expensive.
  • document DE 90 17 176 describes a separator with centrifugal air, in which the air is separated into several streams.
  • the separator comprises a rotor assembly consisting of four coaxial units which have the same rotational speed. He is not possible to adjust the speed and / or the flow of the different air currents between them.
  • the separator comprises two rotors independent, which is an expensive solution, and more difficult to implement in action.
  • the purpose of the present invention is to improve the separators of the type concerned so that it is possible to adjust so simple the slope of the partition curve, i.e. to modify the distribution particle size of the size between the first and second dimensions.
  • the separator object of the invention is characterized in that it has a single rotor divided into sectors and in that the air circulating in the rotor between the inlet and the exhaust duct is divided into at least two separate currents, and in that the rotor is equipped with means for adjusting the speed and / or flow of at least one of the currents.
  • the drag forces exerted by the two currents on a particle of mass and given dimensions will be different; in the channels where the air flow travels at reduced speed, the balance between the drag forces and the forces centrifugal, which corresponds to the theoretical cutoff mesh, will occur for a smaller particle size than that for which this equilibrium is produced in other channels where the air speed is higher. Everything is will therefore pass as if we had two separators in parallel with different cutting meshes; by adjusting the velocities of the air currents, we will be able to adjust the cutoff meshes and, consequently, the distribution particle size distribution in the finished product.
  • the means for adjusting the speed and / or the flow of drafts can be formed by means for varying the inlet section of at least some of the channels formed between the blades of the rotor and / or by means for varying the cross section of the openings through which air currents escape from the rotor.
  • the rotor is divided in sectors by vertical partitions arranged radially and each sector communicates with the air outlet orifice through an opening provided with means for adjusting the passage section which may be formed, for example for example, by pivoting shutters or diaphragms; in this form of realization the radial partitions fulfill the anti-vortex function of the second set of blades of the separator object of French patent N ° 90 01673 in the name of applicant,
  • each plate being mobile, for example by rotation about an axis parallel to the axis of the rotor, between a first position where it leaves practically the entire section of the respective channel free, and a second position where it almost completely closes the canal.
  • certain blades of the rotor may be orientable around vertical axes. so that their ends can come to rest on a neighboring blade to seal the channel which they delimit.
  • Another solution is to make the blades in two parts: a fixed part and a mobile part, orientable by rotation around a vertical axis.
  • one of the faces of the blade can be fixed and the other mobile and able to pivot around a vertical axis located near the periphery of the rotor to come to rest on the neighboring blade to close the channel they form.
  • the radially outer part of the blade can be fixed and its inner part rotatable, the movable parts of two neighboring blades can be brought into abutment against each other to close the channel delimited by the two blades.
  • the separator object of the invention is of the type described in the French patent n ° 90.01673 to which one can refer for more details.
  • there comprises a rotor with vertical axis, guide vanes arranged around the rotor and a envelope in which the rotor and the guide vanes are enclosed and which is provided with a or several inlets for the product to be classified and for the air flow, one or more outlets for the coarse fraction and a central outlet for the air stream charged with the fine fraction of the product.
  • the rotor 10 is fixed to the lower end of a vertical shaft 11 mounted, by by means of rolling bearings, in a tubular support 12 fixed on the ceiling of the separator shell.
  • the shaft is coupled to a variable speed control group allowing the rotor to rotate at the desired speed.
  • the rotor has a large number of vertical blades 14 regularly spaced on its periphery and whose lower and upper ends are fixed, respectively, on a bottom 16 and on a ring 18.
  • a cylindrical shell 20 fixed on the inner edge of the ring 18 defines an outlet passage for the air charged with particles of small dimensions which have entered the rotor through the channels 15 formed between the blades 14.
  • This ferrule is connects, by a rotating joint, to the lower end of a through-pipe 22 the ceiling of the separator envelope.
  • the interior of the rotor is divided into four equal sectors by four vertical partitions 24 arranged radially. These partitions are fixed on the bottom 16, on the ring 18 and on a ferrule 26 surrounding the lower part of the tubular support 12 and itself fixed on the background 16.
  • the outlet opening delimited by the ring 18 and the ferrule 26 is partially closed by pivoting flaps 28 (two per sector in the embodiment shown).
  • Each flap is fixed on a shaft 30 mounted on bearings fixed on the ring 18 and the ferrule 26.
  • a square provided at the outer end of each shaft 30 makes it possible to adjust the orientation of the flaps and, therefore, the section of the exit opening of the respective sectors, and a system of locking keeps the shutters in the desired position after adjustment.
  • a blade 14 on two is formed by a fixed part 31 constituting the active face and a part mobile 32 orientable around a vertical axis 33 located near the leading edge of the blade (see figure 3).
  • This part 32 is movable, between a first position (represented by a line continuous in FIG. 3) where it is pressed against the fixed part 31 of the blade, so as to leave free entry of channel 15, and a second position (shown in dashed lines) where it closes completely this entry.
  • the orientation of the moving parts of the blades can be controlled individually or in groups.
  • Figure 4 shows another embodiment of the sealing means of certain rotor channels 15.
  • the two blades delimiting a channel are in two parts: an external part 31 ′ which is rigidly fixed to the structure of the rotor and a lower part 32 'which is able to pivot about a vertical axis 33'.
  • a mechanism for control not shown allows the movable part 32 ′ of each blade to be moved between two positions: a first position, shown in solid lines in FIG. 4, where the parts 31 ' and 32 'are in the extension of one another and the channel 15 is completely cleared, and a second position, shown in phantom, where the free ends of the parts 32 'of the two blades are in abutment against each other and the channel 15 is closed.
  • the means for closing the channels consist of pairs of vertical plates 40 placed inside the rotor, the two plates of a pair being articulated by their inner edge on the same vertical axis 42 disposed in the plane median of the canal.
  • a cam 44 placed between the two plates and controlled by a mechanism suitable allows to separate the two plates to bring their free end into abutment against the blades 14 and close the outlet of the channel 15, as shown in solid lines in the figure.
  • the cam is rotated to bring it into the median plane of the channel, the plates 40 are pressed against the cam by centrifugal force, as shown in dashed lines on the figure, and the outlet of channel 15 is almost completely clear.
  • certain blades 14 could be orientable being mounted so that it can pivot on the rotor around vertical axes located near their leading edge and come up against the neighboring fixed or orientable blades to close off the corresponding channels 15.
  • the separator In service, the separator is incorporated into a circuit, open or closed, where a gas stream, for example an air stream.
  • a gas stream for example an air stream.
  • the air flow divides into as many elementary currents as there are channels 15 between the blades 14.
  • these elementary currents are grouped in each sector of the rotor into four secondary currents which escape through the outlet opening delimited by the ring 18 and the ferrule 26. If all the flaps 28 are in the vertical position and if all the channels 15 are open, the flows of the four secondary currents are equal and the velocities of the currents elementary are equal; the operation of the separator is the same as that of a classic separator.
  • the speed air in the 15 open channels of the first sector will be, for these two reasons, more higher than in other sector channels. Since the drag forces which act on the particles and oppose the centrifugal force in the channels 15 depend the air speed, while the centrifugal forces depend only on the speed of rotation of the rotor, the particle size for which the centrifugal and drag forces are balanced (theoretical cutoff mesh) will be more important in the first sector than in the others.
  • FIG. 7 shows by way of example the partition curves of a conventional separator, for two cut-off links, and a separator according to the invention.
  • the sharing curve gives the weight proportion, expressed in%, of the particles of size given in the fraction coarse; we would get an inverted curve for the fine fraction.
  • the three curves are combined.
  • the dashed curve corresponds to a conventional separator whose theoretical cutoff mesh is 50 ⁇ m
  • the dotted one corresponds to a separator classic with a theoretical cutting mesh of 105 ⁇ m.
  • the solid line curve has been obtained with the separator of the invention; we see that its slope is lower than that of conventional separators, which means that in the 20-200 ⁇ m range, the particle size is more spread.
  • the invention therefore makes it possible to have a partition curve with adjustable slope and, by Therefore, to obtain a finished product having the desired particle size distribution in a particle size range given by varying both the speed of the rotor and the orientation of the guide vanes, on the one hand, and the positions of the flaps 28 and the adjustment of the section of the channels 15, on the other hand.
  • the rotor could be designed as shown in FIG. 6 and divided into two parts 46, 48, by a horizontal partition 50, located for example at mid-height, an opening 52 provided in the upper wall of the rotor communicating the upper part of the rotor with the air exhaust duct 22 of the separator and a ferrule 54 whose diameter is less than that of said opening 52 being connected to a central opening 56 of the partition and delimiting a passage 55 making communicate the lower part of the rotor with the exhaust duct 22 through the first opening.
  • the rotor is provided with means such as those illustrated in FIGS.
  • the rotor could be divided into more than two superimposed parts. We could even remove the horizontal partition (s), dividing the air in two or more currents in the rotor resulting from the arrangement of one or more dip tubes placed in the rotor axis.

Abstract

A centrifugal type pneumatic separator having a rotor and a housing. The rotor has a plurality of vanes distributed around a periphery thereof. The housing contains the rotor. The housing has an air input conduit, a material input conduit and an evacuation conduit. The air input conduit passes air through channels formed between adjacent vanes such that air and material flows toward the evacuation conduit. The rotor is divided so as to define at least two separate passages whereby air from the air input conduit flows toward the evacuation conduit as two separate and parallel streams.

Description

La présente invention a pour objet un séparateur pneumatique à action centrifuge destiné à classer un matériau granulaire en une fraction fine et une fraction grossière et comportant un rotor à axe vertical muni de pales régulièrement réparties sur sa périphérie, des aubes directrices disposées autour du rotor, suivant les génératrices d'un cylindre fictif, et aptes à communiquer à un courant d'air ou autre gaz pénétrant dans ledit cylindre fictif un mouvement de rotation autour de l'axe dudit cylindre, et une enveloppe dans laquelle sont enfermés le rotor et les aubes directrices et qui est munie d'une ou plusieurs entrées pour l'air et pour le matériau à classer, d'un orifice de sortie disposé au-dessus ou au-dessous du rotor et par où est aspiré le courant d'air chargé de la fraction fine du matériau et d'au moins une sortie pour la fraction grossière, l'air pénétrant dans le rotor à sa périphérie, par les canaux formés entre les pales, et circulant à l'intérieur du rotor vers l'orifice de sortie.The present invention relates to a pneumatic separator with centrifugal action intended to classify a granular material into a fine fraction and a coarse fraction and comprising a rotor with vertical axis provided with blades regularly distributed on its periphery, guide vanes arranged around the rotor, along the generatrices of a fictitious cylinder, and able to communicate with a current of air or other gas entering said fictitious cylinder a rotational movement around the axis of said cylinder, and an envelope in which are enclosed the rotor and the guide vanes and which is provided with one or more air inlets and for the material to be classified, an outlet orifice placed above or below the rotor and through which is drawn the air stream charged with the fine fraction of the material and at least one outlet for the coarse fraction, the air entering the rotor at its periphery, through the channels formed between the blades, and flowing inside the rotor towards the outlet.

Dans un séparateur de ce type le matériau à classer et le courant d'air peuvent être introduits séparément à l'intérieur de l'espace à section annulaire délimité par les aubes directrices et le rotor, ou le matériau à classer peut être mis en suspension dans le courant d'air avant que celui-ci ne soit admis dans ledit espace, à travers les aubes ; le courant d'air pénètre ensuite dans le rotor et est évacué par l'orifice de sortie.In a separator of this type the material to be classified and the air flow can be introduced separately inside the annular section space delimited by the blades and the rotor, or the material to be classified, can be suspended in the air stream before it is admitted into said space, through the blades; the air flow enters then in the rotor and is discharged through the outlet.

Dans les deux cas, le courant d'air et le matériau à classer sont soumis à une rotation, autour de l'axe du rotor, dans l'espace à section annulaire compris entre le rotor et les aubes directrices. Les particules constituant la fraction grossière du matériau sont projetées par la force centrifuge engendrée par cette rotation contre les aubes directrices et tombent par gravité dans une trémie collectrice munie d'un orifice d'évacuation, tandis que les particules constituant la fraction fine sont entraínées par le courant d'air à travers le rotor et l'orifice de sortie central.In both cases, the air flow and the material to be classified are rotated, around the rotor axis, in the annular section space between the rotor and the blades guidelines. The particles constituting the coarse fraction of the material are projected by the centrifugal force generated by this rotation against the guide vanes and fall by gravity in a collecting hopper with an outlet, while the particles constituting the fine fraction are entrained by the air flow through the rotor and the orifice central exit.

La fraction fine séparée contient pratiquement toutes les particules dont la taille est inférieure à une première dimension tandis que la fraction grossière contient pratiquement toutes les particules dont la taille est supérieure à une seconde dimension, plus grande que la première. En plus, les deux fractions contiennent des particules dont la taille est comprise entre les première et seconde dimensions. Cela se traduit par une courbe de partage comportant deux portions sensiblement horizontales reliées par une portion inclinée dont la pente caractérise le séparateur.The separated fine fraction contains practically all the particles whose size is less than a first dimension while the coarse fraction contains practically all particles larger than a second dimension, larger than the first. In addition, both fractions contain particles whose size is included between the first and second dimensions. This results in a sharing curve comprising two substantially horizontal portions connected by an inclined portion, the slope characterizes the separator.

La distribution des particules de taille intermédiaire dans l'une ou l'autre des fractions caractérise la précision de coupure du séparateur. En général, on cherche à obtenir, par construction, une coupure aussi nette que possible entre les deux fractions, c'est-à-dire à réduire l'écart entre les première et seconde dimensions, ce qui se traduit par une courbe de partage à pente raide.The distribution of particles of intermediate size in one or other of the fractions characterizes the cutting precision of the separator. In general, we seek to obtain, by construction, a cut as clear as possible between the two fractions, that is to say reduce the gap between the first and second dimensions, which results in a curve of steep sharing.

Dans certains cas, le produit que l'on cherche à obtenir doit avoir une distribution granulométrique différente de celle de la fraction, fine ou grossière, obtenue au moyen d'un séparateur de ce type. C'est en particulier le cas du ciment obtenu par broyage par compression du clinker. Jusqu'ici, la seule solution pour résoudre ce problème était d'utiliser deux séparateurs placés en série ou en parallèle et réglés pour des dimensions de coupure différentes. Cette solution est coûteuse.In some cases, the product we are looking for must have a particle size distribution different from that of the fraction, fine or coarse, obtained by means of a separator of this type. It is in particular the case of cement obtained by crushing by compression of the clinker. So far, the only solution to solve this problem was to use two separators placed in series or in parallel and adjusted for cut-off dimensions different. This solution is expensive.

Par exemple, le document DE 90 17 176 décrit un séparateur à air à action centrifuge, dans lequel l'air est séparé en plusieurs courants. Selon une première variante, le séparateur comprend un ensemble rotor constitué de quatre unités coaxiales qui ont la même vitesse de rotation. Il n'est pas possible de régler la vitesse et/ou le débit des différents courants d'air entre eux. Selon une autre variante, le séparateur comprend deux rotors indépendants, ce qui constitue une solution coûteuse, et plus délicate à mettre en oeuvre.For example, document DE 90 17 176 describes a separator with centrifugal air, in which the air is separated into several streams. according to a first variant, the separator comprises a rotor assembly consisting of four coaxial units which have the same rotational speed. He is not possible to adjust the speed and / or the flow of the different air currents between them. According to another variant, the separator comprises two rotors independent, which is an expensive solution, and more difficult to implement in action.

Le but de la présente invention est de perfectionner les séparateurs du type concerné de façon qu'il soit possible d'ajuster de façon simple la pente de la courbe de partage, c'est-à-dire de modifier la distribution granulométrique des particules dont la taille est comprise entre les première et seconde dimensions.The purpose of the present invention is to improve the separators of the type concerned so that it is possible to adjust so simple the slope of the partition curve, i.e. to modify the distribution particle size of the size between the first and second dimensions.

Le séparateur objet de l'invention est caractérisé en ce qu'il comporte un seul rotor divisé en secteurs et en ce que l'air circulant dans le rotor entre l'entrée et le conduit d'évacuation est divisé en au moins deux courants distincts, et en ce que le rotor est équipé de moyens de réglage de la vitesse et/ou du débit d'au moins un des courants.The separator object of the invention is characterized in that it has a single rotor divided into sectors and in that the air circulating in the rotor between the inlet and the exhaust duct is divided into at least two separate currents, and in that the rotor is equipped with means for adjusting the speed and / or flow of at least one of the currents.

Si les vitesses des deux courants d'air dans les canaux ménagés entre les pales du rotor sont réglées à des valeurs différentes, les forces de traínée exercées par les deux courants sur une particule de masse et dimensions données seront différentes; dans les canaux où le courant d'air circule à vitesse réduite, l'équilibre entre les forces de traínée et les forces centrifuges, qui correspond à la maille théorique de coupure, se produira pour une dimension des particules plus faible que celle pour laquelle cet équilibre se produit dans les autres canaux où la vitesse de l'air est plus élevée. Tout se passera donc comme si on avait deux séparateurs en parallèle ayant des mailles de coupure différentes; en réglant les vitesses des courants d'air, on pourra ajuster les mailles de coupure et, par conséquent, la distribution granulométrique des particules dans le produit fini.If the velocities of the two air streams in the channels between the rotor blades are set to different values, the drag forces exerted by the two currents on a particle of mass and given dimensions will be different; in the channels where the air flow travels at reduced speed, the balance between the drag forces and the forces centrifugal, which corresponds to the theoretical cutoff mesh, will occur for a smaller particle size than that for which this equilibrium is produced in other channels where the air speed is higher. Everything is will therefore pass as if we had two separators in parallel with different cutting meshes; by adjusting the velocities of the air currents, we will be able to adjust the cutoff meshes and, consequently, the distribution particle size distribution in the finished product.

Les moyens de réglage de la vitesse et/ou du débit des courants d'air peuvent être constitués par des moyens pour faire varier la section d'entrée d'au moins certains des canaux ménagés entre les pales du rotor et/ou par des moyens pour faire varier la section de passage des ouvertures par lesquelles les courants d'air s'échappent du rotor.The means for adjusting the speed and / or the flow of drafts can be formed by means for varying the inlet section of at least some of the channels formed between the blades of the rotor and / or by means for varying the cross section of the openings through which air currents escape from the rotor.

Suivant une forme de réalisation particulière, le rotor est divisé en secteurs par des cloisons verticales disposées radialement et chaque secteur communique avec l'orifice de sortie d'air par une ouverture munie de moyens de réglage de la section de passage qui pourront être constitués, par exemple, par des volets pivotants ou des diaphragmes; dans cette forme de réalisation les cloisons radiales remplissent la fonction anti-vortex du second jeu de pales du séparateur objet du brevet français N° 90 01673 au nom du demandeur, According to a particular embodiment, the rotor is divided in sectors by vertical partitions arranged radially and each sector communicates with the air outlet orifice through an opening provided with means for adjusting the passage section which may be formed, for example for example, by pivoting shutters or diaphragms; in this form of realization the radial partitions fulfill the anti-vortex function of the second set of blades of the separator object of French patent N ° 90 01673 in the name of applicant,

Pour faire varier la section des canaux formés entre les pales du rotor, on pourra utiliser des plaques disposées dans lesdits canaux, chaque plaque étant mobile, par exemple par rotation autour d'un axe parallèle à l'axe du rotor, entre une première position où elle laisse libre pratiquement toute la section du canal respectif, et une seconde position où elle obture pratiquement complètement le canal.To vary the section of the channels formed between the rotor blades, it is possible to using plates placed in said channels, each plate being mobile, for example by rotation about an axis parallel to the axis of the rotor, between a first position where it leaves practically the entire section of the respective channel free, and a second position where it almost completely closes the canal.

On pourra, par exemple, placer à la sortie du canal deux plaques montées pivotantes sur un axe vertical disposé dans le plan médian du canal, ces plaques pourront être amenées, par un mécanisme approprié, d'une première position où elles sont plaquées l'une contre l'autre et disposées pratiquement dans ledit plan médian dans une seconde position où leurs extrémités libres sont en butée contre l'extrémité des pales délimitant le canal.We can, for example, place at the outlet of the channel two pivotally mounted plates on a vertical axis arranged in the median plane of the channel, these plates can be brought, by an appropriate mechanism, from a first position where they are pressed against each other and arranged practically in said median plane in a second position where their free ends are in abutment against the end of the blades defining the channel.

En variante, certaines pales du rotor peuvent être orientables autour d'axe verticaux de façon que leurs extrémités puissent venir s'appuyer sur une pale voisine pour obturer le canal qu'elles délimitent.As a variant, certain blades of the rotor may be orientable around vertical axes. so that their ends can come to rest on a neighboring blade to seal the channel which they delimit.

Une autre solution consiste à réaliser les pales en deux parties : une partie fixe et une partie mobile, orientable par rotation autour d'un axe vertical. Par exemple, l'une des faces de la pale peut être fixe et l'autre mobile et apte à pivoter autour d'un axe vertical situé près de la périphérie du rotor pour venir s'appuyer sur la pale voisine pour obturer le canal qu'elles forment. Selon une autre forme de réalisation, la partie radialement extérieure de la pale peut être fixe et sa partie intérieure rotative, les parties mobiles de deux pales voisines pouvant être amenées en butée l'une contre l'autre pour fermer le canal délimité par les deux pales.Another solution is to make the blades in two parts: a fixed part and a mobile part, orientable by rotation around a vertical axis. For example, one of the faces of the blade can be fixed and the other mobile and able to pivot around a vertical axis located near the periphery of the rotor to come to rest on the neighboring blade to close the channel they form. According to another embodiment, the radially outer part of the blade can be fixed and its inner part rotatable, the movable parts of two neighboring blades can be brought into abutment against each other to close the channel delimited by the two blades.

D'autres caractéristiques de l'objet de l'invention apparaitront à la lecture de la description qui suit et se réfère aux dessins l'accompagnant qui montrent, à titre d'exemple non limitatif, plusieurs formes de réalisation de l'invention. Sur ces dessins :

  • La figure 1 est une vue en coupe diamétrale d'un rotor de séparateur conforme à l'invention ;
  • La figure 2 est une vue de dessus du rotor de la figure 1, l'anneau fermant partiellement le rotor à sa partie supérieure ayant été enlevé sur une moitié du rotor ;
  • La figure 3 est une vue à plus grande échelle d'un détail du rotor ;
  • Les figures 4 et 5 sont des vues analogues à la figure 3 illustrant des variantes de réalisation ;
  • La figure 6 est une vue en coupe diamétrale d'un autre rotor de séparateur conforme à l'invention ; et
  • La figure 7 montre les courbes de partage d'un séparateur classique et du séparateur objet de l'invention.
  • Other characteristics of the subject of the invention will appear on reading the description which follows and refers to the accompanying drawings which show, by way of nonlimiting example, several embodiments of the invention. In these drawings:
  • Figure 1 is a diametrical sectional view of a separator rotor according to the invention;
  • Figure 2 is a top view of the rotor of Figure 1, the ring partially closing the rotor at its upper part having been removed on one half of the rotor;
  • Figure 3 is an enlarged view of a detail of the rotor;
  • Figures 4 and 5 are views similar to Figure 3 illustrating alternative embodiments;
  • Figure 6 is a diametrical sectional view of another separator rotor according to the invention; and
  • Figure 7 shows the partition curves of a conventional separator and the separator object of the invention.
  • Le séparateur objet de l'invention est du type décrit dans le brevet français n° 90.01673 auquel on pourra se référer pour plus de détails. Comme décrit plus haut, il comporte un rotor à axe vertical, des aubes directrices disposées autour du rotor et une enveloppe dans laquelle sont enfermés le rotor et les aubes directrices et qui est munie d'une ou plusieurs entrées pour le produit à classer et pour le courant d'air, une ou plusieurs sorties pour la fraction grossière et un orifice de sortie central pour le courant d'air chargé de la fraction fine du produit.The separator object of the invention is of the type described in the French patent n ° 90.01673 to which one can refer for more details. As described above, there comprises a rotor with vertical axis, guide vanes arranged around the rotor and a envelope in which the rotor and the guide vanes are enclosed and which is provided with a or several inlets for the product to be classified and for the air flow, one or more outlets for the coarse fraction and a central outlet for the air stream charged with the fine fraction of the product.

    Le rotor 10 est fixé à l'extrémité inférieure d'un arbre vertical 11 monté, par l'intermédiaire de paliers à roulements, dans un support tubulaire 12 fixé sur le plafond de l'enveloppe du séparateur. L'arbre est accouplé à un groupe de commande à vitesse variable permettant de faire tourner le rotor à la vitesse voulue.The rotor 10 is fixed to the lower end of a vertical shaft 11 mounted, by by means of rolling bearings, in a tubular support 12 fixed on the ceiling of the separator shell. The shaft is coupled to a variable speed control group allowing the rotor to rotate at the desired speed.

    Le rotor comporte un grand nombre de pales verticales 14 régulièrement espacées sur sa périphérie et dont les extrémités inférieures et supérieures sont fixées, respectivement, sur un fond 16 et sur un anneau 18. Une virole cylindrique 20 fixée sur le bord intérieur de l'anneau 18 définit un passage de sortie pour l'air chargé des particules de petites dimensions qui ont pénétré dans le rotor par les canaux 15 ménagés entre les pales 14. Cette virole se raccorde, par un joint tournant, à l'extrémité inférieure d'un conduit d'évacuation 22 traversant le plafond de l'enveloppe du séparateur.The rotor has a large number of vertical blades 14 regularly spaced on its periphery and whose lower and upper ends are fixed, respectively, on a bottom 16 and on a ring 18. A cylindrical shell 20 fixed on the inner edge of the ring 18 defines an outlet passage for the air charged with particles of small dimensions which have entered the rotor through the channels 15 formed between the blades 14. This ferrule is connects, by a rotating joint, to the lower end of a through-pipe 22 the ceiling of the separator envelope.

    L'intérieur du rotor est divisé en quatre secteurs égaux par quatre cloisons verticales 24 disposées radialement. Ces cloisons sont fixées sur le fond 16, sur l'anneau 18 et sur une virole 26 entourant la partie inférieure du support tubulaire 12 et elle-même fixée sur le fond 16.The interior of the rotor is divided into four equal sectors by four vertical partitions 24 arranged radially. These partitions are fixed on the bottom 16, on the ring 18 and on a ferrule 26 surrounding the lower part of the tubular support 12 and itself fixed on the background 16.

    L'ouverture de sortie délimitée par l'anneau 18 et la virole 26 est partiellement obturée par des volets pivotants 28 (deux par secteur dans la forme de réalisation représentée). Chaque volet est fixé sur un arbre 30 monté sur des paliers fixés sur l'anneau 18 et la virole 26. Un carré prévu à l'extrémité extérieure de chaque arbre 30 permet de régler l'orientation des volets et, par conséquent, la section de l'ouverture de sortie des secteurs respectifs, et un système de verrouillage permet de maintenir les volets dans la position voulue, après réglage.The outlet opening delimited by the ring 18 and the ferrule 26 is partially closed by pivoting flaps 28 (two per sector in the embodiment shown). Each flap is fixed on a shaft 30 mounted on bearings fixed on the ring 18 and the ferrule 26. A square provided at the outer end of each shaft 30 makes it possible to adjust the orientation of the flaps and, therefore, the section of the exit opening of the respective sectors, and a system of locking keeps the shutters in the desired position after adjustment.

    Dans le secteur du rotor représenté sur la partie gauche inférieure de la figure 2, une pale 14 sur deux est formée d'une partie fixe 31 constituant la face active et une partie mobile 32 orientable autour d'un axe vertical 33 situé près du bord d'attaque de la pale (voir figure 3). Cette partie 32 est déplaçable, entre une première position (représentée par un trait continu sur la figure 3) où elle est plaquée contre la partie fixe 31 de la pale, de façon à laisser libre l'entrée du canal 15, et une seconde position (représentée en traits mixtes) où elle obture complètement cette entrée. L'orientation des parties mobiles des pales pourra être commandée individuellement ou par groupes. Ces pales en deux parties devront être réparties sur la périphérie du rotor de telle sorte que celui-ci soit équilibré. On pourra, par exemple, en équiper deux secteurs du rotor diamétralement opposés.In the rotor sector represented on the lower left part of FIG. 2, a blade 14 on two is formed by a fixed part 31 constituting the active face and a part mobile 32 orientable around a vertical axis 33 located near the leading edge of the blade (see figure 3). This part 32 is movable, between a first position (represented by a line continuous in FIG. 3) where it is pressed against the fixed part 31 of the blade, so as to leave free entry of channel 15, and a second position (shown in dashed lines) where it closes completely this entry. The orientation of the moving parts of the blades can be controlled individually or in groups. These two-part blades should be distributed over the periphery of the rotor so that it is balanced. We could, for example, equip two diametrically opposite sectors of the rotor.

    La figure 4 montre une autre forme de réalisation des moyens d'obturation de certains canaux 15 du rotor. Selon cette variante les deux pales délimitant un canal sont en deux parties : une partie extérieure 31' qui est fixée rigidement à la structure du rotor et une partie inférieure 32' qui est apte à pivoter autour d'un axe vertical 33'. Un mécanisme de commande, non représenté permet de déplacer la partie mobile 32' de chaque pale entre deux positions : une première position, représentée en trait continu sur la figure 4, où les parties 31' et 32' sont dans le prolongement l'une de l'autre et le canal 15 est complètement dégagé, et une seconde position, représentée en trait mixte, où les extrémités libres des parties 32' des deux pales sont en butée l'une contre l'autre et le canal 15 est obturé.Figure 4 shows another embodiment of the sealing means of certain rotor channels 15. According to this variant the two blades delimiting a channel are in two parts: an external part 31 ′ which is rigidly fixed to the structure of the rotor and a lower part 32 'which is able to pivot about a vertical axis 33'. A mechanism for control, not shown allows the movable part 32 ′ of each blade to be moved between two positions: a first position, shown in solid lines in FIG. 4, where the parts 31 ' and 32 'are in the extension of one another and the channel 15 is completely cleared, and a second position, shown in phantom, where the free ends of the parts 32 'of the two blades are in abutment against each other and the channel 15 is closed.

    Dans la variante de la figure 5, les moyens d'obturation des canaux sont constitués par des paires de plaques verticales 40 placées à l'intérieur du rotor, les deux plaques d'une paire étant articulées par leur bord intérieur sur un même axe vertical 42 disposé dans le plan médian du canal. Une came 44 placée entre les deux plaques et commandée par un mécanisme approprié permet d'écarter les deux plaques pour amener leur extrémité libre en butée contre les pales 14 et obturer la sortie du canal 15, comme représenté en trait continu sur la figure. Lorsqu'on fait tourner la came pour l'amener dans le plan médian du canal, les plaques 40 sont plaquées contre la came par la force centrifuge, comme représenté en traits mixtes sur la figure, et la sortie du canal 15 est presque complètement dégagée.In the variant of FIG. 5, the means for closing the channels consist of pairs of vertical plates 40 placed inside the rotor, the two plates of a pair being articulated by their inner edge on the same vertical axis 42 disposed in the plane median of the canal. A cam 44 placed between the two plates and controlled by a mechanism suitable allows to separate the two plates to bring their free end into abutment against the blades 14 and close the outlet of the channel 15, as shown in solid lines in the figure. When the cam is rotated to bring it into the median plane of the channel, the plates 40 are pressed against the cam by centrifugal force, as shown in dashed lines on the figure, and the outlet of channel 15 is almost completely clear.

    Selon une autre variante, non représentée, certaines pales 14 pourraient être orientables en étant montées de façon à pouvoir pivoter sur le rotor autour d'axes verticaux situés près de leur bord d'attaque et venir buter contre les pales voisines fixes ou orientables pour obturer les canaux 15 correspondants.According to another variant, not shown, certain blades 14 could be orientable being mounted so that it can pivot on the rotor around vertical axes located near their leading edge and come up against the neighboring fixed or orientable blades to close off the corresponding channels 15.

    En service, le séparateur est incorporé à un circuit, ouvert ou fermé, où circule un courant de gaz, par exemple un courant d'air. En pénétrant dans le rotor le courant d'air se divise en autant de courants élémentaires qu'il y a de canaux 15 entre les pales 14. A la sortie des canaux ces courants élémentaires se regroupent dans chaque secteur du rotor en quatre courants secondaires qui s'échappent à travers l'ouverture de sortie délimitée par l'anneau 18 et la virole 26. Si tous les volets 28 sont en position verticale et si tous les canaux 15 sont ouverts, les débits des quatre courants secondaires sont égaux et les vitesses des courants élémentaires sont égales ; le fonctionnement du séparateur est le même que celui d'un séparateur classique.In service, the separator is incorporated into a circuit, open or closed, where a gas stream, for example an air stream. When entering the rotor the air flow divides into as many elementary currents as there are channels 15 between the blades 14. At the outlet channels these elementary currents are grouped in each sector of the rotor into four secondary currents which escape through the outlet opening delimited by the ring 18 and the ferrule 26. If all the flaps 28 are in the vertical position and if all the channels 15 are open, the flows of the four secondary currents are equal and the velocities of the currents elementary are equal; the operation of the separator is the same as that of a classic separator.

    Si l'on obture une partie des canaux 15 dans l'un des secteurs du rotor et simultanément on ferme partiellement les volets 28 dans les autres secteurs, pour que le courant d'air se divise en deux courants différents tels que le débit traversant chacun des secteurs dont les volets 28 sont fermés soit inférieur au débit traversant le secteur dont les volets sont ouverts, la vitesse de l'air dans les canaux 15 restés ouverts du premier secteur sera, pour ces deux raisons, plus élevée que dans les canaux des autres secteurs. Etant donné que les forces de traínée qui s'exercent sur les particules et s'opposent à la force centrifuge dans les canaux 15 dépendent de la vitesse de l'air, alors que les forces centrifuges ne dépendent que de la vitesse de rotation du rotor, la dimension des particules pour laquelle les forces centrifuge et de traínée sont équilibrées (maille théorique de coupure) sera plus importante dans le premier secteur que dans les autres. Tout se passe donc comme si on avait deux séparateurs en parallèle travaillant avec des mailles de coupure différentes et dont les fractions fines seraient mélangées à la sortie du séparateur. En ajustant la section d'entrée de l'air dans un ou plusieurs secteurs du rotor et en réglant les débits d'air circulant dans les différents secteurs, on peut sélectionner deux mailles de coupure différentes, ou plus, permettant d'obtenir la distribution granulométrique voulue dans une plage donnée.If part of the channels 15 are closed in one of the sectors of the rotor and simultaneously the shutters 28 are partially closed in the other sectors, so that the air flow is divided in two different currents such as the flow through each of the sectors whose flaps 28 are closed or less than the flow through the sector with the flaps open, the speed air in the 15 open channels of the first sector will be, for these two reasons, more higher than in other sector channels. Since the drag forces which act on the particles and oppose the centrifugal force in the channels 15 depend the air speed, while the centrifugal forces depend only on the speed of rotation of the rotor, the particle size for which the centrifugal and drag forces are balanced (theoretical cutoff mesh) will be more important in the first sector than in the others. Everything happens as if we had two separators working in parallel with different cutting meshes and the fine fractions of which would be mixed with the separator outlet. By adjusting the air inlet section in one or more sectors of the rotor and by adjusting the air flows circulating in the different sectors, you can select two or more different cutoffs to obtain distribution desired size within a given range.

    La figure 7 montre à titre d'exemple les courbes de partage d'un séparateur classique, pour deux mailles de coupure, et d'un séparateur conforme à l'invention. La courbe de partage donne la proportion pondérale, exprimée en %, des particules de taille donnée dans la fraction grossière ; on obtiendrait une courbe inversée pour la fraction fine. Pour des dimensions de particules inférieures à 20 µm et supérieures à 200 µm, les trois courbes sont confondues. Dans la plage 20-200 µm, la courbe en tirets correspond à un séparateur classique dont la maille de coupure théorique est de 50 µm, celle en pointillés correspond à un séparateur classique dont la maille de coupure théorique est de 105 µm. La courbe en trait continu a été obtenue avec le séparateur de l'invention ; on voit que sa pente est plus faible que celle des séparateurs classiques, ce qui signifie que dans la plage 20-200 µm, la granulométrie est plus étalée.FIG. 7 shows by way of example the partition curves of a conventional separator, for two cut-off links, and a separator according to the invention. The sharing curve gives the weight proportion, expressed in%, of the particles of size given in the fraction coarse; we would get an inverted curve for the fine fraction. For dimensions of particles smaller than 20 µm and larger than 200 µm, the three curves are combined. In the 20-200 µm range, the dashed curve corresponds to a conventional separator whose theoretical cutoff mesh is 50 µm, the dotted one corresponds to a separator classic with a theoretical cutting mesh of 105 µm. The solid line curve has been obtained with the separator of the invention; we see that its slope is lower than that of conventional separators, which means that in the 20-200 µm range, the particle size is more spread.

    L'invention permet donc d'avoir une courbe de partage à pente réglable et, par conséquent, d'obtenir un produit fini ayant la distribution granulométrique voulue dans une plage granulométrique donnée en jouant à la fois sur la vitesse du rotor et l'orientation des aubes directrices, d'une part, et les positions des volets 28 et le réglage de la section des canaux 15, d'autre part. The invention therefore makes it possible to have a partition curve with adjustable slope and, by Therefore, to obtain a finished product having the desired particle size distribution in a particle size range given by varying both the speed of the rotor and the orientation of the guide vanes, on the one hand, and the positions of the flaps 28 and the adjustment of the section of the channels 15, on the other hand.

    Au lieu d'être divisé en secteurs par des cloisons radiales, le rotor pourrait être conçu comme montré sur la figure 6 et divisé en deux parties 46, 48, par une cloison horizontale 50, située par exemple à mi-hauteur, une ouverture 52 prévue dans la paroi supérieure du rotor faisant communiquer la partie supérieure du rotor avec le conduit d'évacuation d'air 22 du séparateur et une virole 54 dont le diamètre est inférieur à celui de ladite ouverture 52 étant raccordée à une ouverture centrale 56 de la cloison et délimitant un passage 55 faisant communiquer la partie inférieure du rotor avec le conduit d'évacuation 22 à travers la première ouverture. Le rotor est muni de moyens tels que ceux illustrés par les figures 3, 4 et 5 pour obturer certains des canaux ménagés entre ses pales, sur au moins une partie de leur hauteur, et de moyens tels que les volets 28 pour régler au moins une des ouvertures de sortie. Suivant le même principe, le rotor pourrait être divisé en plus de deux parties superposées. On pourrait même supprimer la ou les cloisons horizontales, la division de l'air en deux ou plusieurs courants dans le rotor résultant de la disposition d'un ou plusieurs tubes plongeurs placés dans l'axe du rotor.Instead of being divided into sectors by radial partitions, the rotor could be designed as shown in FIG. 6 and divided into two parts 46, 48, by a horizontal partition 50, located for example at mid-height, an opening 52 provided in the upper wall of the rotor communicating the upper part of the rotor with the air exhaust duct 22 of the separator and a ferrule 54 whose diameter is less than that of said opening 52 being connected to a central opening 56 of the partition and delimiting a passage 55 making communicate the lower part of the rotor with the exhaust duct 22 through the first opening. The rotor is provided with means such as those illustrated in FIGS. 3, 4 and 5 for close off some of the channels formed between its blades, over at least part of their height, and means such as the flaps 28 for adjusting at least one of the outlet openings. next the same principle, the rotor could be divided into more than two superimposed parts. We could even remove the horizontal partition (s), dividing the air in two or more currents in the rotor resulting from the arrangement of one or more dip tubes placed in the rotor axis.

    Des moyens autres que des volets pivotants, par exemple des diaphragmes, pourraient être utilisés pour régler la section des ouvertures de sortie du rotor. Il est bien entendu que ces modifications et toutes celles qui peuvent être apportées aux formes de réalisation décrites, par l'emploi de moyens techniques équivalents, entrent dans le cadre de l'invention.Means other than pivoting shutters, for example diaphragms, could be used to adjust the section of the rotor outlet openings. It is understood that these modifications and any that may be made to the embodiments described, by the use of equivalent technical means, fall within the scope of the invention.

    Claims (14)

    1. A centrifugal action air separator comprising a rotor (10), with vertical pin (11) fitted with blades (14) spaced regularly on its periphery, guide vanes arranged around the rotor (10) and a shroud containing the rotor (10) and the guide vanes and fitted with air inlets and for the material to be classified, with an exhaust conduit (22) for the air loaded with the fine fraction of the material and with an outlet for the rough fraction, the air penetrating the rotor (10) at its periphery, via the channels (15) formed between the blades (14), and circulating inside the rotor (10) towards the exhaust conduit (22), characterised in that the separator comprises a single rotor, in that the rotor (10) is divided into sectors, in that the air circulating between the inlet and the exhaust conduit (22) is divided into at least two distinct currents, and in that the rotor (10) is fitted with means for adjusting the speed and/or the flow rate of the different currents relative to one another.
    2. A separator according to claim 1, characterised in that said rotor is fitted with means (32, 32', 40) to vary the cross section of at least some of the channels (15) through which one of the air currents penetrates inside the rotor.
    3. A separator according to claim 1 or 2, characterised in that said rotor is fitted with means (28) to vary the cross section of the opening through which at least one of the air currents exits the rotor towards the exhaust conduit (22).
    4. A separator according to claim 1, 2 or 3, characterised in that said rotor is divided into sectors by vertical walls (24) arranged radially and each sector communicates with the outlet passageway via an aperture fitted with means (28) for adjusting the cross section of the air passageway.
    5. A separator according to claim 1, 2, or 3, characterised in that said rotor is divided into two parts (46, 48) by a horizontal wall (50), in that the portion (48) of the rotor furthermost from the exhaust conduit (22) communicates with the latter via a passageway (55) delineated by a coaxial ferrule (54) connected to a central aperture (56) of said wall, in that the other portion (46) of the rotor communicates with said exhaust conduit via an annular aperture (52) surrounding said ferrule, and in that means are provided to vary the cross section of at least some of the channels laid out between the blades (14) in at least one of the portions of the rotor and to vary the cross section of said passageway (55) and/or said annular aperture (52).
    6. A separator according to claim 4 or 5, characterised in that said means for adjusting the cross section of said aperture and/or of said passageway, consist of pivoting flaps (28).
    7. A separator according to claim 4 or 5, characterised in that said means for adjusting the cross section of said aperture and/or of said passageway, consist of diaphragms.
    8. A separator according to claim 4 or 5, characterised in that said rotor is fitted with means (32, 32', 40) to vary the cross section of at least some of the channels (15) formed between the blades (14) of one of the sectors or portions of the rotor.
    9. A separator according to claim 2 or 8, characterised in that said means to vary the cross section of the channels consist of plates arranged in said channels (15), each plate being mobile from a first position where it leaves the whole cross section of the channel practically free, and a second position where it blanks off the channel practically completely.
    10. A separator according to claim 2 or 8, characterised in that said means to vary the cross section of the channels consist, for each channel, of two plates (40) placed at the outlet of the channel (15) and mounted to pivot on a vertical axis (42) laid out on the medium plane of the channel, which plates may be brought by an appropriate mechanism (44) from a first position, where they are pressed against one another and arranged practically parallel to said medium plane, into a second position where their free ends abut against the end of the blades (14) delineating the channel.
    11. A separator according to claim 2 or 8, characterised in that some blades (14) of the rotor are orientable around verticals axes so that they may rest on a neighbouring blade to blank off the channels (15) formed with the neighbouring blades, these orientable blades forming the means to vary the cross section of said channels.
    12. A separator according to claim 2 or 8, characterised in that some blades (14) of the rotor consist of two sections, a fixed section (31, 31') and a mobile section (32, 32') orientable by rotation around a vertical axis and these mobiles sections of the blades form the means to vary the cross section of the channels (15).
    13. A separator according to claim 12, characterised in that one of the faces (31) of some blades is fixed and the other face (32) is mobile and capable of pivoting around a vertical axis (33) situated close to the periphery of the rotor to rest on the neighbouring blade and blank off the channel (15) that they form.
    14. A separator according to claim 12, characterised in that the radially external portion (31') of the blade is fixed and its radially internal portion (32') is rotary, whereas the mobile portions of two neighbouring blades may be brought to rest against one another to blank off the channel delineated by both blades.
    EP97918235A 1995-11-21 1997-04-15 Air classifier with centrifugal action Expired - Lifetime EP0918573B1 (en)

    Priority Applications (1)

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    DK97918235T DK0918573T3 (en) 1995-11-21 1997-04-15 Windscreen with centrifugal action

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    FR9513764A FR2741286B1 (en) 1995-11-21 1995-11-21 AIR SEPARATOR WITH CENTRIFUGAL ACTION
    PCT/FR1997/000678 WO1998046371A1 (en) 1995-11-21 1997-04-15 Air classifier with centrifugal action

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    EP0918573B1 true EP0918573B1 (en) 2004-06-30

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    EP (1) EP0918573B1 (en)
    JP (1) JP3999278B2 (en)
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    CA2257674A1 (en) 1998-10-22
    ATE270159T1 (en) 2004-07-15
    JP2000512550A (en) 2000-09-26
    PL186138B1 (en) 2003-10-31
    DE69729731T2 (en) 2005-08-04
    CZ292237B6 (en) 2003-08-13
    CZ392498A3 (en) 1999-04-14
    US6318559B2 (en) 2001-11-20
    AU2643597A (en) 1998-11-11
    US6273269B1 (en) 2001-08-14
    JP3999278B2 (en) 2007-10-31
    ES2224236T3 (en) 2005-03-01
    DE69729731D1 (en) 2004-08-05
    UA63905C2 (en) 2004-02-16
    WO1998046371A1 (en) 1998-10-22
    FR2741286A1 (en) 1997-05-23
    AU741249B2 (en) 2001-11-29
    PL330322A1 (en) 1999-05-10
    FR2741286B1 (en) 1998-01-23
    CA2257674C (en) 2003-01-07
    DK0918573T3 (en) 2004-10-18
    US20010020597A1 (en) 2001-09-13
    EP0918573A1 (en) 1999-06-02

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