EP0694340A1 - Konzentrator für feine oder gebrochene Teilchen - Google Patents
Konzentrator für feine oder gebrochene Teilchen Download PDFInfo
- Publication number
- EP0694340A1 EP0694340A1 EP95401755A EP95401755A EP0694340A1 EP 0694340 A1 EP0694340 A1 EP 0694340A1 EP 95401755 A EP95401755 A EP 95401755A EP 95401755 A EP95401755 A EP 95401755A EP 0694340 A1 EP0694340 A1 EP 0694340A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- particles
- funnel
- deflector
- fine
- broken
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000002245 particle Substances 0.000 title claims abstract description 93
- 230000004907 flux Effects 0.000 claims abstract description 11
- 230000005484 gravity Effects 0.000 claims abstract description 11
- 239000007787 solid Substances 0.000 claims description 4
- 239000003054 catalyst Substances 0.000 claims description 3
- 238000002407 reforming Methods 0.000 claims description 2
- 238000000926 separation method Methods 0.000 abstract description 4
- 239000000203 mixture Substances 0.000 abstract 2
- 230000000694 effects Effects 0.000 description 5
- 238000009434 installation Methods 0.000 description 5
- 239000010419 fine particle Substances 0.000 description 4
- 230000000903 blocking effect Effects 0.000 description 2
- 238000012550 audit Methods 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000001833 catalytic reforming Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- JTJMJGYZQZDUJJ-UHFFFAOYSA-N phencyclidine Chemical class C1CCCCN1C1(C=2C=CC=CC=2)CCCCC1 JTJMJGYZQZDUJJ-UHFFFAOYSA-N 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
- 210000004233 talus Anatomy 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B07—SEPARATING SOLIDS FROM SOLIDS; SORTING
- B07B—SEPARATING SOLIDS FROM SOLIDS BY SIEVING, SCREENING, SIFTING OR BY USING GAS CURRENTS; SEPARATING BY OTHER DRY METHODS APPLICABLE TO BULK MATERIAL, e.g. LOOSE ARTICLES FIT TO BE HANDLED LIKE BULK MATERIAL
- B07B4/00—Separating solids from solids by subjecting their mixture to gas currents
- B07B4/02—Separating solids from solids by subjecting their mixture to gas currents while the mixtures fall
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B07—SEPARATING SOLIDS FROM SOLIDS; SORTING
- B07B—SEPARATING SOLIDS FROM SOLIDS BY SIEVING, SCREENING, SIFTING OR BY USING GAS CURRENTS; SEPARATING BY OTHER DRY METHODS APPLICABLE TO BULK MATERIAL, e.g. LOOSE ARTICLES FIT TO BE HANDLED LIKE BULK MATERIAL
- B07B13/00—Grading or sorting solid materials by dry methods, not otherwise provided for; Sorting articles otherwise than by indirectly controlled devices
- B07B13/003—Separation of articles by differences in their geometrical form or by difference in their physical properties, e.g. elasticity, compressibility, hardness
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B07—SEPARATING SOLIDS FROM SOLIDS; SORTING
- B07B—SEPARATING SOLIDS FROM SOLIDS BY SIEVING, SCREENING, SIFTING OR BY USING GAS CURRENTS; SEPARATING BY OTHER DRY METHODS APPLICABLE TO BULK MATERIAL, e.g. LOOSE ARTICLES FIT TO BE HANDLED LIKE BULK MATERIAL
- B07B1/00—Sieving, screening, sifting, or sorting solid materials using networks, gratings, grids, or the like
- B07B1/06—Cone or disc shaped screens
Definitions
- the present invention relates to a concentrator device for fine or broken particles, usable in particular in installations comprising catalytic reactors with moving bed, and in particular in catalytic reforming installations.
- fine or broken particles is a nuisance in all reactors but in particular in moving bed reactors because they cause several types of drawbacks.
- these particles cause a change in the porosity of the medium which disturbs the regularity of the gas flow and therefore directly affects the performance of the unit.
- the presence of fine particles modifies the flow conditions of solid particles within the moving bed itself, in particular in the case of annular beds (delimited by concentric grids) in contact with the grid of the central collector. since, entrained by the fluids, fine or broken particles are pushed towards the grid of the central collector where they can become blocked.
- the present invention provides a concentrator device which aims to separate a flow of particles having a concentration C0 of fine or broken particles (according to needs, particles with a smaller average diameter will be defined at a determined threshold, either absolute or relative to the average diameter of the particles) in at least two flows.
- At least one of the fluxes obtained (called flux of reduced concentration in fine or broken particles) will have a concentration C1 in fine particles substantially lower than C0, while the other (the others) flux (called flux concentrated in fine particles or conversely) will have, conversely, a concentration C2 substantially higher than the concentration C0 of the initial flow.
- the device which is the subject of the invention is, in FIG. 1, placed in a cylindrical enclosure 1 with a conical bottom (which could be just as well hemispherical or elliptical) and comprising an external wall.
- An introduction means 2 brings the flow of particles to be treated to the level of the first separator stage; under the effect of gravity. Most of this flow consists of quasi-spherical particles, that is to say particles which can roll, and of variable sizes. Without these dimensions being able to limit the invention, examples of reforming catalysts 1.5 to 2.8 mm in diameter will be given.
- the particle flow flows by gravity through the device.
- the first separator stage comprises a funnel 3 and a deflector 4 connected to the funnel.
- Figure 1 therefore comprises 2 separator stages in series.
- the means of introduction of the particles for the second separator is the orifice 5 of the first separator which preferably comprises a tube.
- the funnel 3, the deflector 4 and the introduction means have substantially the same axis, which is vertical or inclined, and preferably substantially vertical, to allow gravity flow.
- the purpose of the funnel is to collect a portion of the particles coming from the upper introduction means, before redistributing them through a reduced size orifice placed substantially vertically from the first introduction point.
- the funnel flares up. Its upper diameter is preferably a fraction, approximately between 1/4 and 2/3, of the diameter of the container and the upper part is placed so as to intercept a large fraction, between 1/3 and 3/4, of the slope of solid particles while leaving a free annular space for the flow of the rest of the particles.
- the outer edge 7 of the funnel must be located at a distance H from the lower end of the means of introduction (tubing 2 or 5) of the particles. This distance is of the order of a few centimeters. The point of the slope may therefore be free or not, depending on the value of this distance.
- the section of the outlet orifice 5 of the funnel (therefore located on the axis of the funnel) is preferably close to the section of the means for introducing the particles, it can also be smaller.
- the angle of inclination ⁇ of the funnel (or that of the planar facets) relative to the horizontal is greater than the angle of sliding of the particles on the surface of the deflector so as to allow a regular flow of the particles which s 'press on this edge of the funnel. It is usually at least 5-10 degrees higher than the slip angle.
- the base of the truncated cone, or prism, forming the funnel can possibly be extended by a short tube 6.
- the purpose of the deflector is to push the largest and roundest particles towards the wall and the periphery. It is frustoconical or prismatic, with a flaring downwards. At the upper part its diameter is connected to the diameter of the upper part of the funnel, so that the line of intersection is circular if the funnel and the deflector are real trunks of cones (conical shape), but a line broken if the funnel and / or the deflector are prismatic. The deflector and the funnel are thus connected.
- the deflector leaves a space L for passage of particles sufficient to avoid the effects of arch or blockage against the external wall of the enclosure 1, therefore a space of at least 10 times the diameter of the particles the largest, and preferably at least 20 times, but not too weak so that the slope, which collapses towards the center from this crossed deflector edge, cannot reach the outer edge of the immediately lower funnel.
- the inclination of this deflector relative to the horizontal is at least 5 to 10 degrees greater than the angle of sliding of the particles on the surface of the deflector so as to allow a regular flow of the particles which are supported on this deflector.
- the operator will define the angle ⁇ , the quantity L (distance between the lower end of the deflector and the wall) and h (vertical distance between the upper edge of the funnel and the upper surface slope) or H (vertical distance between the upper edge of the funnel and the introduction means).
- the principle of the proposed device is therefore to exploit this effect by regularly bringing back towards the center part of the slope formed in line with the supply orifices.
- This process can be repeated one or more times by superimposing several separator stages which each have the objective of separating a stream of particles in two, a stream of particles enriched in fine or broken particles which are refocused while a second stream less rich in fine and broken is pushed outward.
- the funnel, immediately below associated with a deflector
- the intersection (M in FIG. 1) between the slope created at this funnel and the free particles flowing from the upper deflector, this intersection is located outside the upper section of said funnel.
- the surface of the deflector may, as indicated above, be of frustoconical or prismatic shape, its surface may be smooth or in the form of a grid or a plate provided with slots or perforations, so as to allow the passage of the finest particles while promoting the sliding of medium or large particles towards the periphery. If this wall is not full (as shown in FIG. 1), it is advantageously proposed to place under the grid or the perforated plate a small full plate which makes it possible to collect and refocus the fine particles which have passed through. through the gate. It is quite obvious that this small plate, or flange 8 of refocusing for example, of frustoconical shape should not however obstruct the flow of the slope which descends from the preceding central orifice 5. Obviously, this plate is directed towards the lower part of the device and towards the axis of the associated funnel.
- Each of the withdrawal rates can of course be adjusted independently by means of a suitable device, such as for example a mechanical or pneumatic valve.
- a suitable device such as for example a mechanical or pneumatic valve.
- We can also advantageously provide for the distances L and the diameters of the pipes 12 and 10 so that the particles can flow freely without being sorted. In this case, we would do the sorting discontinuously.
- the withdrawal of the stream concentrated in fine or broken particles is obtained by means 9, arranged substantially along the axis of the last funnel, it being understood that this is the funnel immediately above by means of racking.
- This means 9 comprises according to Figure 1 a tube 10 advantageously connected to a funnel 11 collecting the concentrated flow over an area around the axis of the last funnel. Any other means having the function of collecting and discharging the concentrated flow is suitable.
- the flow of particles remaining, containing all the other particles not discharged by means 9, is recovered, advantageously in FIG. 1 by the preferably conical or elliptical bottom of enclosure 1 and discharged by means 12. Any other means of recovering the remaining flow is suitable, in particular the means usually placed for this purpose at the base of moving bed reactors or silos.
- the funnels and deflectors can be scalloped, in particular if they are composed of plane facets, and therefore have a non-planar connection line to allow greater variation in the flow rates of solids without compromising the principle of operation of the device.
- the substantially revolution device described above instead of the substantially revolution device described above, if geometrical or space constraints encourage it, generally semi-circular or even planar devices can also be used with profit, as long as they respect the basic principle. offers.
- the complete device corresponds to a fraction of the device described above; the description and diagram given in Figures 1 and 2 to represent the section of the proposed device remains perfectly valid, except that the word funnel no longer represents a half or a quarter of frustoconical funnel, or even a flat surface if the device is no longer of revolution, and that in the same way, the deflector is no longer of revolution, but semi circular or planar.
- separator devices can coexist "in parallel" on the same plane in the same enclosure with a means of supplying particles to be treated for each of the first separator stages.
- the advantage of the device according to the invention is that all the streams of particles are re-sorted and in particular the stream of finer particles from the first separator stage is re-sorted by each of the following stages, so that at the end of at least minus 2 separator stages, and preferably more than 2, the concentration of fine or broken particles is reduced significantly.
- This objective is achieved by means of the device according to the invention thanks to the dynamic slope effect used, that is to say that all the particles are always in motion to form the slope and to flow, the slope does not is never blocked (otherwise the catalyst particles would stick). This effect also allows the speaker to be emptied completely at the desired time, and without mixing the flows.
Landscapes
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
- Combined Means For Separation Of Solids (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR9409558 | 1994-07-29 | ||
FR9409558A FR2723008B1 (fr) | 1994-07-29 | 1994-07-29 | Dispositif concentrateur en particules fines ou cassees |
Publications (1)
Publication Number | Publication Date |
---|---|
EP0694340A1 true EP0694340A1 (de) | 1996-01-31 |
Family
ID=9465980
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP95401755A Withdrawn EP0694340A1 (de) | 1994-07-29 | 1995-07-25 | Konzentrator für feine oder gebrochene Teilchen |
Country Status (7)
Country | Link |
---|---|
US (1) | US5772044A (de) |
EP (1) | EP0694340A1 (de) |
JP (1) | JPH0857428A (de) |
KR (1) | KR960003822A (de) |
CN (1) | CN1128683A (de) |
FR (1) | FR2723008B1 (de) |
TW (1) | TW269646B (de) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1998050172A1 (en) * | 1997-05-08 | 1998-11-12 | Alexei Nikiforovich Zjulin | Separator for granular materials |
CN102962192A (zh) * | 2012-12-08 | 2013-03-13 | 张家港市金腾化工机械制造有限公司 | 化工用物料筛选机 |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7819347B2 (en) * | 2006-06-08 | 2010-10-26 | Restaurant Technology, Inc. | Metered material dispenser |
US8022756B2 (en) | 2007-05-15 | 2011-09-20 | Qualcomm, Incorporated | Output circuits with class D amplifier |
BRPI0818584B1 (pt) * | 2007-10-17 | 2019-05-28 | Basf Se | Uso de um composto catalisador latente, composição polimerizável, processo para polimerização de compostos, uso da composição polimerizável, substrato revestido, composição polimerizada ou reticulada, e, composto catalisador latente |
KR101271623B1 (ko) * | 2010-11-19 | 2013-06-11 | 삼성중공업 주식회사 | 분리 장치 |
US8827185B2 (en) | 2011-10-14 | 2014-09-09 | Restaurant Technology, Inc. | Measuring dispenser for granular seasoning material and method of seasoning |
RU167396U1 (ru) * | 2016-09-08 | 2017-01-10 | Олег Владимирович Левин | Станция для разделения катализатора на фракции |
CN108686956B (zh) * | 2018-05-16 | 2024-05-03 | 华东理工大学 | 一种粉体颗粒分选装置及分选方法 |
CN111203383A (zh) * | 2020-01-08 | 2020-05-29 | 安徽中科光电色选机械有限公司 | 一种轻飘物重力分选机 |
RU208708U1 (ru) * | 2021-06-05 | 2022-01-10 | Общество с ограниченной ответственностью "Тайпс Сортинг" | Многофункциональный калибратор для гетерогенных смесей |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4231861A (en) * | 1979-03-26 | 1980-11-04 | Parsons Manufacturing, Incorporated | Grain cleaning apparatus |
EP0482683A1 (de) * | 1990-10-23 | 1992-04-29 | METALLGESELLSCHAFT Aktiengesellschaft | Verfahren und Vorrichtung zum Trennen eines Schüttgutstromes in Fraktionen mit unterschiedlicher Korngrösse |
US5123542A (en) * | 1991-06-03 | 1992-06-23 | Hoppe Gerald W | Method and apparatus for cleaning, distributing and aerating grain |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
SU1335326A1 (ru) * | 1985-11-24 | 1987-09-07 | Украинский научно-исследовательский и проектно-конструкторский институт по обогащению и брикетированию углей | Грохот |
US4738774A (en) * | 1986-10-10 | 1988-04-19 | Patrick Charles W | Spout line buster |
-
1994
- 1994-07-29 FR FR9409558A patent/FR2723008B1/fr not_active Expired - Fee Related
-
1995
- 1995-07-25 EP EP95401755A patent/EP0694340A1/de not_active Withdrawn
- 1995-07-28 CN CN95115831A patent/CN1128683A/zh active Pending
- 1995-07-28 US US08/508,459 patent/US5772044A/en not_active Expired - Fee Related
- 1995-07-28 KR KR1019950022832A patent/KR960003822A/ko not_active Application Discontinuation
- 1995-07-31 JP JP7195056A patent/JPH0857428A/ja not_active Withdrawn
- 1995-08-10 TW TW084108326A patent/TW269646B/zh active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4231861A (en) * | 1979-03-26 | 1980-11-04 | Parsons Manufacturing, Incorporated | Grain cleaning apparatus |
EP0482683A1 (de) * | 1990-10-23 | 1992-04-29 | METALLGESELLSCHAFT Aktiengesellschaft | Verfahren und Vorrichtung zum Trennen eines Schüttgutstromes in Fraktionen mit unterschiedlicher Korngrösse |
US5123542A (en) * | 1991-06-03 | 1992-06-23 | Hoppe Gerald W | Method and apparatus for cleaning, distributing and aerating grain |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1998050172A1 (en) * | 1997-05-08 | 1998-11-12 | Alexei Nikiforovich Zjulin | Separator for granular materials |
CN102962192A (zh) * | 2012-12-08 | 2013-03-13 | 张家港市金腾化工机械制造有限公司 | 化工用物料筛选机 |
Also Published As
Publication number | Publication date |
---|---|
FR2723008A1 (fr) | 1996-02-02 |
CN1128683A (zh) | 1996-08-14 |
TW269646B (de) | 1996-02-01 |
US5772044A (en) | 1998-06-30 |
FR2723008B1 (fr) | 1996-09-20 |
KR960003822A (ko) | 1996-02-23 |
JPH0857428A (ja) | 1996-03-05 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PUAI | Public reference made under article 153(3) epc to a published international application that has entered the european phase |
Free format text: ORIGINAL CODE: 0009012 |
|
AK | Designated contracting states |
Kind code of ref document: A1 Designated state(s): BE DE ES FR GB GR IT NL |
|
17P | Request for examination filed |
Effective date: 19960731 |
|
17Q | First examination report despatched |
Effective date: 19991126 |
|
STAA | Information on the status of an ep patent application or granted ep patent |
Free format text: STATUS: THE APPLICATION IS DEEMED TO BE WITHDRAWN |
|
18D | Application deemed to be withdrawn |
Effective date: 20000407 |