EP0600872A1 - Method of and apparatus for producing labels. - Google Patents

Method of and apparatus for producing labels.

Info

Publication number
EP0600872A1
EP0600872A1 EP91911485A EP91911485A EP0600872A1 EP 0600872 A1 EP0600872 A1 EP 0600872A1 EP 91911485 A EP91911485 A EP 91911485A EP 91911485 A EP91911485 A EP 91911485A EP 0600872 A1 EP0600872 A1 EP 0600872A1
Authority
EP
European Patent Office
Prior art keywords
adhesive
sheets
succession
backing
release material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP91911485A
Other languages
German (de)
French (fr)
Other versions
EP0600872B1 (en
Inventor
David John Instance
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of EP0600872A1 publication Critical patent/EP0600872A1/en
Application granted granted Critical
Publication of EP0600872B1 publication Critical patent/EP0600872B1/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B31MAKING ARTICLES OF PAPER, CARDBOARD OR MATERIAL WORKED IN A MANNER ANALOGOUS TO PAPER; WORKING PAPER, CARDBOARD OR MATERIAL WORKED IN A MANNER ANALOGOUS TO PAPER
    • B31DMAKING ARTICLES OF PAPER, CARDBOARD OR MATERIAL WORKED IN A MANNER ANALOGOUS TO PAPER, NOT PROVIDED FOR IN SUBCLASSES B31B OR B31C
    • B31D1/00Multiple-step processes for making flat articles ; Making flat articles
    • B31D1/02Multiple-step processes for making flat articles ; Making flat articles the articles being labels or tags
    • B31D1/021Making adhesive labels having a multilayered structure, e.g. provided on carrier webs
    • GPHYSICS
    • G09EDUCATION; CRYPTOGRAPHY; DISPLAY; ADVERTISING; SEALS
    • G09FDISPLAYING; ADVERTISING; SIGNS; LABELS OR NAME-PLATES; SEALS
    • G09F3/00Labels, tag tickets, or similar identification or indication means; Seals; Postage or like stamps
    • G09F3/08Fastening or securing by means not forming part of the material of the label itself
    • G09F3/10Fastening or securing by means not forming part of the material of the label itself by an adhesive layer
    • GPHYSICS
    • G09EDUCATION; CRYPTOGRAPHY; DISPLAY; ADVERTISING; SEALS
    • G09FDISPLAYING; ADVERTISING; SIGNS; LABELS OR NAME-PLATES; SEALS
    • G09F3/00Labels, tag tickets, or similar identification or indication means; Seals; Postage or like stamps
    • G09F3/02Forms or constructions
    • G09F2003/0225Carrier web
    • GPHYSICS
    • G09EDUCATION; CRYPTOGRAPHY; DISPLAY; ADVERTISING; SEALS
    • G09FDISPLAYING; ADVERTISING; SIGNS; LABELS OR NAME-PLATES; SEALS
    • G09F3/00Labels, tag tickets, or similar identification or indication means; Seals; Postage or like stamps
    • G09F3/02Forms or constructions
    • G09F2003/0225Carrier web
    • G09F2003/0226Carrier sheet
    • GPHYSICS
    • G09EDUCATION; CRYPTOGRAPHY; DISPLAY; ADVERTISING; SEALS
    • G09FDISPLAYING; ADVERTISING; SIGNS; LABELS OR NAME-PLATES; SEALS
    • G09F3/00Labels, tag tickets, or similar identification or indication means; Seals; Postage or like stamps
    • G09F3/02Forms or constructions
    • G09F2003/023Adhesive
    • GPHYSICS
    • G09EDUCATION; CRYPTOGRAPHY; DISPLAY; ADVERTISING; SEALS
    • G09FDISPLAYING; ADVERTISING; SIGNS; LABELS OR NAME-PLATES; SEALS
    • G09F3/00Labels, tag tickets, or similar identification or indication means; Seals; Postage or like stamps
    • G09F3/02Forms or constructions
    • G09F2003/0257Multilayer

Definitions

  • the present invention relates to a method of and an apparatus for producing a succession of self-adhesive labels carried on a backing of release material.
  • the present invention aims to provide an improved method of and apparatus for producing labels.
  • the present invention provides a method of producing a succession of self-adhesive labels carried on a backing of release material, the method comprising the steps of:-
  • the present invention also provides an apparatus for producing a succession of self-adhesive labels carried on a backing of release material, the apparatus comprsising an adhesive spraying station comprising a spray nozzle for spraying adhesive, means for feeding a succession of printed sheets through the adhesive spraying station so that an exposed surface of each sheet is coated with adhesive and means for adhering the adhesive-coated surface of the sheets to a backing of release material.
  • Figure 1 is a diagrammatic elevation of an apparatus for producing labels in accordance with a first embodiment of the present invention
  • Figure 2 is a diagrammatic plan view of the apparatus of Figure 1 along line A-A;
  • Figure 3 shows a modification of the endless belt of the apparatus of Figures 1 and 2;
  • Figure 4 is a diagrammatic elevation of an apparatus for producing labels in accordance with a second embodiment of the present invention.
  • the sheets 6 may be single layer or multi-layer sheets and are printed by any suitable printing method, such as lithographic, screen or laser printing.
  • a sheet feeding mechanism 8 is located above the stack of sheets 6 and is adapted to feed from the magazine 4 a succession of sheets 6 from the top of the stack.
  • the sheet feeding mechanism 8 is represented as a rotatable drive cylinder but may alternatively comprise any suitable known sheet feeding mechanism.
  • the sheets are fed in succession past an electrostatic charging device 10 which is adapted to apply an electrostatic charge of a given polarity across the upper surface of the sheets 6.
  • the electrostatic charging device 10 may be omitted when the sheet feeding mechanism 8 is adapted to feed sheets from the stack in such a way that the fed sheets have an electrostatic charge.
  • the sheets are fed by the sheet feeding mechanism 8 onto a vacuum drive means incorporating a vacuum conveyor 12 which comprises an endless belt 14 mounted between a pair of drive rollers 16.
  • the surface of the endless belt 14 is provided with a series of holes 18 and the space 20 between the opposed inner surfaces of the endless belt 14 is connected to a source of suction.
  • the bottom surface 22 of each sheet is sucked through the holes 18 against the upper surface 24 of the endless belt 14. This ensures that each sheet 6 is firmly located on the vacuum conveyor 12.
  • the vacuum conveyor 12 conveys the succession of sheets 6 through an adhesive spraying station 26 comprising a spray nozzle 28 for spraying a coating of adhesive 30 onto the exposed upper surface 32 of each sheet 6 passing through the adhesive spraying station 26.
  • the spray nozzle 28 is adapted to spray electrostatically charged droplets of adhesive onto the exposed surfaces 32. This may be effected by feeding electrostatic charge from a source of electric power to the spray nozzle 28, the charge being of opposite polarity to that which is applied by the electrostatic charging device 10.
  • the adhesive may be a water-or solvent-based pressure-sensitive adhesive or
  • the succession of sheets 6 coated with adhesive 30 is then fed by the vacuum conveyor 12 to a laminating station 34 comprising a pair of opposed rollers 36, 38 between which the succession of sheets 6 is laminated to a backing 40 of release material, the laminating being achieved by adhering the adhesive-coated surface 32 of each sheet 6 to the backing 40 of release material.
  • the backing 40 of release material is fed out from a reel 42 thereof and typically comprises a wax or silicone-coated paper.
  • the adhesive coating 30 is urged against the backing 40 of release material and then the
  • the sheets 6 are conveyed through the adhesive spraying station 26 in spaced relation.
  • the spraying nozzle 28 may be operated either continuously or intermittently in synchronism with the disposition thereunder of a sheet 6 to be sprayed with adhesive.
  • a washing and cleaning mechanism 48 is disposed in contact with the endless belt 14 for cleaning excess adhesive 30 off the outer surface of the endless belt 14.
  • the apparatus may also comprise a slitting mechanism at, or downstream of, the laminating station 34 at which the backing 40 of release material and the succession of sheets 6 adhered thereto are longitudinally slit so as to provide two adjacent reels 46 of the self-adhesive labels carried on the backing of release material.
  • each printed sheet 6 would have a pair of
  • the endless belt 14 may be modified by the provision thereon of a succession of raised pads 58.
  • the sheet feeding mechanism 8 feeds the sheets 6 so that each sheet lies on a respective pad 58 above the surface 60 of the endless belt 14. This assists the application of adhesive to the sheets 6 and ensures that those parts of the endless belt 14 which receive extraneous adhesive do not actually contact the edges of the sheets 6.
  • FIG 4. A second embodiment of an apparatus for producing labels in accordance with the present invention is shown in Figure 4. This embodiment is a modification of that shown in Figures 1 and 2 and like parts are identified by like reference numerals.
  • the vacuum conveyor 50
  • each sheet 6 engages the upper surface of the printing cylinder 52 which is rotatably driven and conveys the sheet 6 through the adhesive spraying station 26 to the laminating station 34.
  • adhesive spraying station 26 is additionally provided with a pair of shields 54, 56 which are located on ups.tream and downstream sides, in relation to the direction of feeding of the sheets 6, of the spray nozzle 28.
  • the shields 54, 56 are arranged so as to control the application of the spray of adhesive 30 to within defined boundaries. If desired, the operation of the spray nozzle 28 is controlled so as to be intermittently synchronized with the location of a sheet 6 between the shields 54, 56.
  • the apparatus may be modifed by the addition thereto of a slitter for longitunally slitting the assembly of self-adhesive labels carried on the release material.
  • the apparatus may be modifed by the addition thereto of a slitter for longitunally slitting the assembly of self-adhesive labels carried on the release material.
  • electrostatic charge initially on the sheets as they enter the adhesive spraying station is either neutralised by the

Landscapes

  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • Theoretical Computer Science (AREA)
  • Labeling Devices (AREA)
  • Making Paper Articles (AREA)
  • Laminated Bodies (AREA)
  • Adhesives Or Adhesive Processes (AREA)

Abstract

In producing a succession of self-adhesive labels carried on a backing of release material, the apparatus comprising an adhesive spraying station (26) comprising a spray nozzle (28) for spraying adhesive (30), means (8, 12) for feeding a succession of printed sheets through the adhesive spraying station (26) so that an exposed surface of each sheet is coated with adhesive (30) and means (34, 36, 38) for adhering the adhesive-coated surface of the sheets to a backing (40) of release material. <IMAGE>

Description

"METHOD OF AND APPARATUS FOR PRODUCING LABELS"
The present invention relates to a method of and an apparatus for producing a succession of self-adhesive labels carried on a backing of release material.
It is known, for example from EP-A-0275670, to produce a succession of self-adhesive labels which are carried directly on a backing of release material.
The present invention aims to provide an improved method of and apparatus for producing labels.
Accordingly, the present invention provides a method of producing a succession of self-adhesive labels carried on a backing of release material, the method comprising the steps of:-
(a) providing a plurality of printed sheets;
(b) feeding the sheets in succession through an adhesive spraying station at which adhesive is sprayed from a spray nozzle onto an exposed surface of each sheet; and
(c) adhering the adhesive-coated exposed surface of each of the succession of sheets to a backing of release material.
The present invention also provides an apparatus for producing a succession of self-adhesive labels carried on a backing of release material, the apparatus comprsising an adhesive spraying station comprising a spray nozzle for spraying adhesive, means for feeding a succession of printed sheets through the adhesive spraying station so that an exposed surface of each sheet is coated with adhesive and means for adhering the adhesive-coated surface of the sheets to a backing of release material. Embodiments of the present invention will now be
described by way of example only with reference to the
accompanying drawings, in which:-
Figure 1 is a diagrammatic elevation of an apparatus for producing labels in accordance with a first embodiment of the present invention;
Figure 2 is a diagrammatic plan view of the apparatus of Figure 1 along line A-A;
Figure 3 shows a modification of the endless belt of the apparatus of Figures 1 and 2; and
Figure 4 is a diagrammatic elevation of an apparatus for producing labels in accordance with a second embodiment of the present invention.
Referring to Figures 1 and 2, an apparatus, designated generally as 2, for producing a succession of self-adhesive labels carried on a release backing material includes a magazine 4 for holding a stack of printed sheets 6. The sheets 6 may be single layer or multi-layer sheets and are printed by any suitable printing method, such as lithographic, screen or laser printing. A sheet feeding mechanism 8 is located above the stack of sheets 6 and is adapted to feed from the magazine 4 a succession of sheets 6 from the top of the stack. The sheet feeding mechanism 8 is represented as a rotatable drive cylinder but may alternatively comprise any suitable known sheet feeding mechanism. The sheets are fed in succession past an electrostatic charging device 10 which is adapted to apply an electrostatic charge of a given polarity across the upper surface of the sheets 6. When the sheets 6 are made of paper, this charge is retained evenly over the sheets 6. If desired, the electrostatic charging device 10 may be omitted when the sheet feeding mechanism 8 is adapted to feed sheets from the stack in such a way that the fed sheets have an electrostatic charge. The sheets are fed by the sheet feeding mechanism 8 onto a vacuum drive means incorporating a vacuum conveyor 12 which comprises an endless belt 14 mounted between a pair of drive rollers 16. The surface of the endless belt 14 is provided with a series of holes 18 and the space 20 between the opposed inner surfaces of the endless belt 14 is connected to a source of suction. As the sheets 6 are deposited onto the vacuum conveyor 12 the bottom surface 22 of each sheet is sucked through the holes 18 against the upper surface 24 of the endless belt 14. This ensures that each sheet 6 is firmly located on the vacuum conveyor 12.
The vacuum conveyor 12 conveys the succession of sheets 6 through an adhesive spraying station 26 comprising a spray nozzle 28 for spraying a coating of adhesive 30 onto the exposed upper surface 32 of each sheet 6 passing through the adhesive spraying station 26. In the preferred embodiment, the spray nozzle 28 is adapted to spray electrostatically charged droplets of adhesive onto the exposed surfaces 32. This may be effected by feeding electrostatic charge from a source of electric power to the spray nozzle 28, the charge being of opposite polarity to that which is applied by the electrostatic charging device 10. The adhesive may be a water-or solvent-based pressure-sensitive adhesive or
alternatively a heat-sealable pressure-sensitive adhesive.
The succession of sheets 6 coated with adhesive 30 is then fed by the vacuum conveyor 12 to a laminating station 34 comprising a pair of opposed rollers 36, 38 between which the succession of sheets 6 is laminated to a backing 40 of release material, the laminating being achieved by adhering the adhesive-coated surface 32 of each sheet 6 to the backing 40 of release material. The backing 40 of release material is fed out from a reel 42 thereof and typically comprises a wax or silicone-coated paper. The adhesive coating 30 is urged against the backing 40 of release material and then the
combined assembly passes over an idle roller 44 and is then wound up on a take-up reel 46 of the succession of
self-adhesive labels 6 on the backing 40 of release material.
In the illustrated arrangement, the sheets 6 are conveyed through the adhesive spraying station 26 in spaced relation. The spraying nozzle 28 may be operated either continuously or intermittently in synchronism with the disposition thereunder of a sheet 6 to be sprayed with adhesive. A washing and cleaning mechanism 48 is disposed in contact with the endless belt 14 for cleaning excess adhesive 30 off the outer surface of the endless belt 14.
If desired, the apparatus may also comprise a slitting mechanism at, or downstream of, the laminating station 34 at which the backing 40 of release material and the succession of sheets 6 adhered thereto are longitudinally slit so as to provide two adjacent reels 46 of the self-adhesive labels carried on the backing of release material. With this
arrangement, each printed sheet 6 would have a pair of
identical images printed thereof transversely adjacent to each other.
As shown in Figure 3, the endless belt 14 may be modified by the provision thereon of a succession of raised pads 58. In use the sheet feeding mechanism 8 feeds the sheets 6 so that each sheet lies on a respective pad 58 above the surface 60 of the endless belt 14. This assists the application of adhesive to the sheets 6 and ensures that those parts of the endless belt 14 which receive extraneous adhesive do not actually contact the edges of the sheets 6.
A second embodiment of an apparatus for producing labels in accordance with the present invention is shown in Figure 4. This embodiment is a modification of that shown in Figures 1 and 2 and like parts are identified by like reference numerals. In this embodiment, the vacuum conveyor 50
comprises a vacuum cylinder 52 which is hollow and the
cylindrical surface of which is provided with an array of holes (not shown). The cylindrical void in the centre of the vacuum cylinder is connected to a source of suction. The sheets 6 are fed out from the stack thereof by the sheet feeding mechanism 8. The bottom surface 22 of each sheet 6 engages the upper surface of the printing cylinder 52 which is rotatably driven and conveys the sheet 6 through the adhesive spraying station 26 to the laminating station 34. The
adhesive spraying station 26 is additionally provided with a pair of shields 54, 56 which are located on ups.tream and downstream sides, in relation to the direction of feeding of the sheets 6, of the spray nozzle 28. The shields 54, 56 are arranged so as to control the application of the spray of adhesive 30 to within defined boundaries. If desired, the operation of the spray nozzle 28 is controlled so as to be intermittently synchronized with the location of a sheet 6 between the shields 54, 56.
As with the first illustrated embodiment, the apparatus may be modifed by the addition thereto of a slitter for longitunally slitting the assembly of self-adhesive labels carried on the release material. The apparatus may
additionally be provided with a downstream inspection station at which the assembly of self-adhesive labels on the reel of release backing material can be inspected.
In each of the two illustrated embodiments, the
electrostatic charge initially on the sheets as they enter the adhesive spraying station is either neutralised by the
application of the adhesive or dissipated at, or downstream of, the adhesive spraying station as a result of contact of the sheets with other parts of the apparatus. In the
resultant reel of self-adhesive labels , there is no
substantial electrostatic charge.

Claims

1. A method of producing a succession of self-adhesive labels carried on a backing of release material, the method comprising the steps of:-
(a) providing a plurality of printed sheets (6);
(b) feeding the sheets (6) in succession through an adhesive spraying station (26) at which adhesive is sprayed from a spray nozzle (28) onto an exposed surface of each sheet (6); and
(c) adhering the adhesive-coated exposed surface (32) of each of the succession of sheets (6) to a backing (40) of release material.
2. A method according to claim 1 wherein prior to feeding step (b) the sheets (6.) are electrostatically charged thereby to enhance the coating of adhesive. (30) onto the exposed surfaces.
3. A method according to claim 2 wherein the spray nozzle (28) is adapted to spray electrostatically charged droplets of adhesive onto the exposed surfaces.
4. A method according to claim 1 wherein in adhering step (c) the succession of sheets (6) and the backing (40) of release material are laminated together between a pair of opposed rollers (36,38).
5. A method according to any foregoing claim wherein the succession of sheets (6) is fed through the adhesive applying station (26) by a vacuum drive means which employs suction to suck a surface of each sheet which is remote from the spray nozzle (28) against a vacuum conveyor (12,50).
6. A method according to claim 5 wherein the vacuum conveyor (12,50) comprises an endless belt (14) mounted between a pair of drive rollers (16).
7. A method according to claim 5 wherein the vacuum conveyor comprises a vacuum cylinder (50).
8. An apparatus for producing a succession of self-adhesive labels carried on a backing of release material, the apparatus comprising an adhesive spraying station (26) comprising a spray nozzle (28) for spraying adhesive, means (8) for feeding a succession of printed sheets through the adhesive spraying station (26) so that an exposed surface of each sheet (6) is coated with adhesive and means for adhering the
adhesive-coated surface (30) of the sheets to a backing (40) of release material.
9. An apparatus according to claim 8 further comprising means (10) for electrostatically charging the sheets (6) before the sheets (6) are fed through the adhesive spraying station (26).
10. An apparatus according to claim 9 wherein the spray nozzle (28) is adapted to spray electrostatically charged droplets of adhesive onto the exposed surfaces.
11. An apparatus according to claim 8 wherein the adhering means comprises a pair of opposed rollers (36,38) between which the succession of sheets (6) and the backing (40) of release material are laminated.
12. An apparatus according to any one of claims 8 to 11 wherein the feeding means includes a vacuum drive means which employs suction to suck a surface of each sheet (6) which is remote from the spray nozzle (28) against a vacuum conveyor (12,50) of the drive means.
13. An apparatus according to claim 12 wherein the vacuum
(12,50) conveyor comprises an endless belt (14) mounted
between a pair of drive rollers (16).
14. An apparatus according to claim 13 wherein the vacuum conveyor comprises a vacuum cylinder (50).
EP91911485A 1990-06-06 1991-06-06 Method of and apparatus for producing labels Expired - Lifetime EP0600872B1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
GB9012640 1990-06-06
GB9012640A GB2244674B (en) 1990-06-06 1990-06-06 Method of and apparatus for producing labels
PCT/GB1991/000906 WO1991018737A1 (en) 1990-06-06 1991-06-06 Method of and apparatus for producing labels

Publications (2)

Publication Number Publication Date
EP0600872A1 true EP0600872A1 (en) 1994-06-15
EP0600872B1 EP0600872B1 (en) 1995-08-30

Family

ID=10677173

Family Applications (1)

Application Number Title Priority Date Filing Date
EP91911485A Expired - Lifetime EP0600872B1 (en) 1990-06-06 1991-06-06 Method of and apparatus for producing labels

Country Status (10)

Country Link
EP (1) EP0600872B1 (en)
AT (1) ATE127075T1 (en)
CA (1) CA2084670C (en)
DE (1) DE69112646T2 (en)
DK (1) DK0600872T3 (en)
ES (1) ES2079070T3 (en)
GB (1) GB2244674B (en)
GR (1) GR3018175T3 (en)
HK (1) HK139395A (en)
WO (1) WO1991018737A1 (en)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5267899A (en) * 1992-01-23 1993-12-07 Moore Business Forms, Inc. Defective equipment window stickers
DE4338214A1 (en) * 1993-11-10 1995-05-11 Bernhard Ehret Process for making form labels
GB2288162B (en) * 1994-03-30 1997-11-26 Harrison & Sons Ltd Self-adhesive stamps
GB2344577A (en) * 1997-12-12 2000-06-14 Rue De Int Ltd Self-adhesive stamps
GB9726394D0 (en) * 1997-12-12 1998-02-11 Rue De Int Ltd Self-adhesive stamps
FR2774070B1 (en) * 1998-01-29 2000-02-25 Imprimerie Bouley METHOD AND MACHINE FOR MANUFACTURING LABELS OR THE LIKE MADE ADHESIVE AND DEPOSITED ON A COIL
ITFI20130270A1 (en) * 2013-11-12 2015-05-13 Andrea Miliardi PROCEDURE FOR THE PRODUCTION OF RESINATED LABELS SUITABLE FOR USE IN THE BOTTLING AND PACKAGING INDUSTRY OF FOOD PRODUCTS

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1420933A (en) * 1972-03-16 1976-01-14 Instance Ltd David J Self-adhesive labels
DE2219994A1 (en) * 1972-04-24 1973-11-08 Voith Gmbh J M Electrostatic spraying of paper - with spray electrode at earth potential
GB2122968B (en) * 1982-06-25 1985-09-04 Instance David John Method and apparatus for producing labels
AU6029990A (en) * 1989-08-21 1991-02-21 Osaka Sealing Printing Co., Ltd. Method for manufacturing label-continued sheet

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See references of WO9118737A1 *

Also Published As

Publication number Publication date
GR3018175T3 (en) 1996-02-29
EP0600872B1 (en) 1995-08-30
WO1991018737A1 (en) 1991-12-12
ES2079070T3 (en) 1996-01-01
DE69112646T2 (en) 1996-04-25
HK139395A (en) 1995-09-08
CA2084670A1 (en) 1991-12-07
GB2244674B (en) 1994-04-27
DK0600872T3 (en) 1996-01-22
CA2084670C (en) 2000-08-01
GB2244674A (en) 1991-12-11
DE69112646D1 (en) 1995-10-05
ATE127075T1 (en) 1995-09-15
GB9012640D0 (en) 1990-07-25

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