EP0567360B2 - Verfahren und Apparat zum Überführen einer Flüssigkeit - Google Patents

Verfahren und Apparat zum Überführen einer Flüssigkeit Download PDF

Info

Publication number
EP0567360B2
EP0567360B2 EP19930400745 EP93400745A EP0567360B2 EP 0567360 B2 EP0567360 B2 EP 0567360B2 EP 19930400745 EP19930400745 EP 19930400745 EP 93400745 A EP93400745 A EP 93400745A EP 0567360 B2 EP0567360 B2 EP 0567360B2
Authority
EP
European Patent Office
Prior art keywords
column
pressure
liquid
point
expansion valve
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP19930400745
Other languages
English (en)
French (fr)
Other versions
EP0567360A1 (de
EP0567360B1 (de
Inventor
Bernard Darredeau
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Original Assignee
Air Liquide SA
LAir Liquide SA a Directoire et Conseil de Surveillance pour lEtude et lExploitation des Procedes Georges Claude
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=9427993&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=EP0567360(B2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Air Liquide SA, LAir Liquide SA a Directoire et Conseil de Surveillance pour lEtude et lExploitation des Procedes Georges Claude filed Critical Air Liquide SA
Publication of EP0567360A1 publication Critical patent/EP0567360A1/de
Application granted granted Critical
Publication of EP0567360B1 publication Critical patent/EP0567360B1/de
Publication of EP0567360B2 publication Critical patent/EP0567360B2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04642Recovering noble gases from air
    • F25J3/04648Recovering noble gases from air argon
    • F25J3/04654Producing crude argon in a crude argon column
    • F25J3/04666Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system
    • F25J3/04672Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system having a top condenser
    • F25J3/04678Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system having a top condenser cooled by oxygen enriched liquid from high pressure column bottoms
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C6/00Methods and apparatus for filling vessels not under pressure with liquefied or solidified gases
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C9/00Methods or apparatus for discharging liquefied or solidified gases from vessels not under pressure
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04151Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
    • F25J3/04187Cooling of the purified feed air by recuperative heat-exchange; Heat-exchange with product streams
    • F25J3/0423Subcooling of liquid process streams
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04406Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system
    • F25J3/04412Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system in a classical double column flowsheet, i.e. with thermal coupling by a main reboiler-condenser in the bottom of low pressure respectively top of high pressure column
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04763Start-up or control of the process; Details of the apparatus used
    • F25J3/04769Operation, control and regulation of the process; Instrumentation within the process
    • F25J3/04793Rectification, e.g. columns; Reboiler-condenser
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2270/00Applications
    • F17C2270/05Applications for industrial use
    • F17C2270/0509"Dewar" vessels
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2235/00Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams
    • F25J2235/06Lifting of liquids by gas lift, e.g. "Mammutpumpe"
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2245/00Processes or apparatus involving steps for recycling of process streams
    • F25J2245/40Processes or apparatus involving steps for recycling of process streams the recycled stream being air
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2245/00Processes or apparatus involving steps for recycling of process streams
    • F25J2245/42Processes or apparatus involving steps for recycling of process streams the recycled stream being nitrogen
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S62/00Refrigeration
    • Y10S62/912External refrigeration system
    • Y10S62/913Liquified gas

Definitions

  • the present invention relates to a method of transfer of a liquid, via a riser fitted an expansion valve, a first column of distillation operating at a first press, typically relatively high, to equipment, especially to a second distillation column, operating at a second press, typically relatively low, less than the first press.
  • Apparatuses for the separation of gases from air by distillation cryogenic most often use the scheme classic double column. Liquids produced in tank (liquid rich in oxygen), in the middle (lean liquid) and at the top (liquid nitrogen) of the column medium pressure (or MP column), are sent at an intermediate point or at the top of the column low pressure (or BP column). Most of the time, for economic reasons, the low pressure column is placed above the medium pressure column. It is therefore necessary to send liquids to a point located higher than the point where they are taken. Conventionally, the pressure difference between the average column pressure and the low pressure column is higher at hydrostatic pressure of the liquid column between the sampling point in the column MP and the end point of the BP column.
  • the invention aims to allow, in a simple way and efficient, safe transfer of liquids, without use of a pump.
  • the method according to the invention is characterized by injecting it into the riser, downstream of the expansion valve, a lightening gas available at a pressure higher than the pressure created by a column of said liquid between the injection point of the gas and the point of introduction of the liquid into said equipment.
  • the invention relates to a process for transferring a liquid, via a pipe rising fitted with an expansion valve, a first distillation column operating at a first pressure on equipment, especially one second distillation column, operating at a second pressure, less than first pressure, characterized in that the liquid is sub-cooled before its expansion, at except for a minority fraction of this liquid, so as to produce a controlled amount of gas from flash, this flash gas is injected downstream of the expansion valve and serves as a lightening gas for the liquid.
  • this installation also relates to an installation distillation intended for the implementation of such a process.
  • this installation of type comprising a first distillation column operating at first pressure, equipment, in particular a second distillation column, operating at a second press, less than the first pressure, and a riser fitted with a expansion valve and connecting a liquid withdrawal point from the first column to an introduction point of liquid in said equipment, is characterized in that that it includes means of injection into the pipe rising, downstream of the expansion valve, by a lightening gas available at higher pressure at the pressure created by a column of said liquid between the gas injection point and the point of introduction of the liquid in said equipment.
  • the invention relates to an installation according to claim 10.
  • the air distillation installation shown in the figure 1 essentially comprises a double column distillation 1.
  • This includes a medium column pressure 2 surmounted by a low pressure column 3.
  • a vaporizer-condenser 4 puts in exchange relation thermal steam at the top of column 2, consisting practically pure nitrogen, and the tank liquid column 3, consisting of oxygen at a determined purity.
  • Porture liquid (impure nitrogen) is drawn off in one intermediate point of column 2 via line 11 equipped with an expansion valve (not shown) and, after sub-cooling and expansion, is introduced in an intermediate point in column 3. Liquid nitrogen practically pure is withdrawn at the head of column 3 via a pipe 12 fitted with an expansion valve 13, sub-cooled in a sub-cooler 14 upstream of this expansion valve, relaxed in the latter and introduced at the top of column 3.
  • an air line 19 is tapped into supply line 5 and splits into two branches 20, 21.
  • Each of these branches is equipped with an expansion valve 22, 23 and joined respectively lines 6 and 9 just downstream of their expansion valves 7 and 10.
  • a pipe 24 gas equipped with a relief valve 25 starts from the top from column 2 and joins line 12 just by downstream of the expansion valve 13.
  • Another line for gas 26, fitted with an expansion valve (not shown), starts from a location in column 2 next to the point of withdrawal of the poor liquid (line 11) and joined this pipe 11 just downstream of the expansion valve of it.
  • a low flow of conveyed air at the supply pressure of column 2, through the pipe 19, 20, is expanded in the expansion valve 22 and injected into the newly expanded rich liquid in the expansion valve 7.
  • the air bubbles lighten the rich liquid and reduce the pressure required for bring up to column 2.
  • a low air flow conveyed by line 19, 21 is relaxed in the expansion valve 23 and injected into the rich liquid which has just been expanded in the expansion valve 10.
  • the total diverted air flow via line 19 is weak, typically less than 1 % of the air flow entering the installation.
  • the lightening gas corresponding in line 24 must be nitrogen practically pure.
  • the compositions of the liquid rich and poor liquid are not critical, so that the corresponding lightening gases can have somewhat different compositions from these liquids, provided that they do not pollute them, all the more more than the flow of these gases is very low.
  • the main expansion valves 7, 10 and 13 are placed as low as possible to guarantee feeding them with frank liquid, and we introduce gas bubbles just downstream of these valves trigger to assist the upward propulsion of liquids in question. More specifically, the pressure of lightening gas must be sufficient to overcome the height of liquid above the injection point of the gas, and this pressure is obtained, in the example shown, thanks to the fact that every gas, which is available at the pressure of column 3, is injected above the point of withdrawal of the associated liquid.
  • FIGS 2 and 3 illustrate, in the case of the ascent liquid nitrogen via line 12, two variants obtaining lightening gas. In these two variants, the pipe 24 and the expansion valve 25 are eliminated.
  • a minority flow control of liquid nitrogen conveyed by line 12 bypass the sub-cooler 14 via a bypass pipe 24A fitted, preferably at its lowest point, an expansion valve 25A and ending downstream of the expansion valve 13.
  • the expansion valve 25A is deleted, and there is provision, in line 12, a three-way valve 27 having an input connected to the line 12 upstream of the sub-cooler 14, an outlet connected to the input of this subcooler and another output connected to the 24A bypass line.
  • this pipe 24A ends upstream of the expansion valve 13.

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Separation By Low-Temperature Treatments (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Gas Separation By Absorption (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Claims (10)

  1. Verfahren zum Überführen einer Flüssigkeit über eine mit einem Druckminderventil (7, 10, 13) ausgestattete Steigleitung (6, 9, 11, 12) von einer ersten Destillationskolonne (2), die bei einem ersten Druck arbeitet, zu einer Einrichtung (3), insbesondere einer zweiten Destillationskolonne, die bei einem tieferen Druck als dem ersten Druck arbeitet, dadurch gekennzeichnet, dass man in die Steigleitung stromab von dem Druckminderventil ein Verdünnungsgas einleitet, das bei einem Druck vorliegt, der höher ist als der von einer Flüssigkeitskolonne zwischen dem Einleitungspunkt des Gases und dem Einführungspunkt der Flüssigkeit in die Einrichtung (3) erzeugte Druck.
  2. Verfahren nach Anspruch 1, dadurch gekennzeichnet, dass das Verdichtungsgas bei dem Druck der ersten Destillationskolonne (2) vorliegt und in die Flüssigkeit in der Steigleitung oberhalb des Entnahmepunktes der Flüssigkeit eingeleitet wird.
  3. Verfahren nach Anspruch 2, dadurch gekennzeichnet, dass man als Verdünnungsgas ein an einem Punkt der ersten Kolonne entnommenes Gas verwendet, das derart ausgewählt wird, dass die Zusammensetzung der überführten Flüssigkeit nicht wesentlich verändert wird.
  4. Verfahren nach Anspruch 2 zum Überführen der Wannenflüssigkeit von einer Mitteldruck-Kolonne (2) einer doppelten Luftdestillationskolonne (1) zu einem Zwischenpunkt einer Niederdruck-Kolonne (3), welche über die Mitteldruck-Kolonne hinausragt, und/oder zu dem Kopfkondensator einer mit der Niederdruck-Kolonne (3) verbundenen Sauerstoff/Argon-Trennkolonne, dadurch gekennzeichnet, dass man als Verdünnungsgas einen geringen Durchfluss an Zufuhrluft der doppelten Kolonne (1) verwendet.
  5. Verfahren zum Überführen einer Flüssigkeit über eine mit einem Druckminderventil (7, 10, 13) ausgestattete Steigleitung (6, 9, 11, 12) von einer ersten Destillationskolonne (2), die bei einem ersten Druck arbeitet, zu einer Einrichtung (3), insbesondere einer zweiten Destillationskolonne, die bei einem zweiten tieferen Druck als dem ersten Druck arbeitet, dadurch gekennzeichnet, dass man die Flüssigkeit vor ihrer Entspannung mit Ausnahme eines kleinen Bruchteils der Flüssigkeit derart unterkühlt, dass eine kontrollierte Menge an Flash-Gas erzeugt wird, wobei das Flash-Gas stromab von dem Druckminderventil (7, 10, 13) eingeleitet wird und als Verdünnungsgas der Flüssigkeit dient.
  6. Destillationsanlage mit einer ersten Destillationskolonne (2), die bei einem ersten Druck arbeitet, einer Einrichtung (3), insbesondere einer zweiten Destillationskolonne, die bei einem zweiten tieferen als dem ersten Druck arbeitet, und einer mit einem Druckminderventil (7, 10, 13) ausgestatteten Steigleitung (6, 9, 11, 12), die einen Entnahmepunkt der Flüssigkeit der ersten Kolonne (2) mit einem Einführungspunkt der Flüssigkeit in die Einrichtung (3) verbindet, der sich oberhalb des Entnahmepunktes befindet, dadurch gekennzeichnet, dass sie stromab von dem Druckminderventil in der Steigleitung eine Einrichtung (19 bis 26) zum Einleiten eines Verdünnungsgases aufweist, das bei einem Druck vorliegt, der höher ist als der von einer Flüssigkeitskolonne zwischen dem Einleitungspunkt des Gases und dem Einführungspunkt der Flüssigkeit in die Einrichtung (3) erzeugte Druck.
  7. Anlage nach Anspruch 6, dadurch gekennzeichnet, dass das Verdünnungsgas in der ersten Kolonne (2) oder an deren Eingang abgezweigt wird und dass die Einleit-Einrichtung (19 bis 26) in die Steigleitung (6, 9, 11, 12) in einer Höhe oberhalb des Ausgangspunktes der Leitung mündet.
  8. Anlage nach Anspruch 7, dadurch gekennzeichnet, dass die Einleit-Einrichtung eine mit einem Druckminderventil (25) ausgestattete Gasleitung (11, 24) aufweist, die von einem zu dem Entnahmepunkt der Flüssigkeit benachbarten Punkt der ersten Kolonne (2) aus verläuft.
  9. Anlage nach Anspruch 7, bei welcher die erste Kolonne (2) die Mitteldruck-Kolonne (2) einer doppelten Luftdestillationskolonne (1) ist und die Einrichtung (3) die Niederdruck-Kolonne (3) ist, die über die Mitteldruck-Kolonne der doppelten Kolonne und/oder den Kopfkondensator einer mit der Niederdruck-Kolonne (3) verbundenen Sauerstoff/Argon-Trennkolonne hinausragt, dadurch gekennzeichnet, dass die Einleit-Einrichtung eine mit einem Druckminderventil (22, 23) ausgestattete Leitung (19 bis 21) aufweist, die von der Ankunftsleitung (5) der zu destillierenden Luft oder von der Wanne der Mitteldruck-Kolonne (2) aus verläuft.
  10. Destillationsanlage mit einer ersten Destillationskolonne (2), die bei einem relativ hohen Druck arbeitet, einer Einrichtung (3), insbesondere einer zweiten Destillationskolonne, die bei einem relativ tiefen Druck arbeitet, und einer mit einem Druckminderventil (7, 10, 13) ausgestatteten Steigleitung (6, 9, 11, 12), die einen Entnahmepunkt der Flüssigkeit der ersten Kolonne (2) mit einem Einführungspunkt der Flüssigkeit in die Einrichtung (3) verbindet, dadurch gekennzeichnet, dass die Steigleitung (6, 12) eine Unterkühl-Einrichtung (8, 14) stromauf von dem Druckminderventil (7, 13) durchläuft und mit einer Umgehungsleitung (24A) für die Unterkühl-Einrichtung und das Ventil (13) versehen ist, wobei diese Umgehungsleitung mit einem Druckminderventil (25A) ausgerüstet ist.
EP19930400745 1992-03-24 1993-03-23 Verfahren und Apparat zum Überführen einer Flüssigkeit Expired - Lifetime EP0567360B2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR9203500A FR2689223B1 (fr) 1992-03-24 1992-03-24 Procede et installation de transfert de fluide en provenance d'une colonne de distillation, notamment d'air.
FR9203500 1992-03-24

Publications (3)

Publication Number Publication Date
EP0567360A1 EP0567360A1 (de) 1993-10-27
EP0567360B1 EP0567360B1 (de) 1996-05-15
EP0567360B2 true EP0567360B2 (de) 2002-06-12

Family

ID=9427993

Family Applications (1)

Application Number Title Priority Date Filing Date
EP19930400745 Expired - Lifetime EP0567360B2 (de) 1992-03-24 1993-03-23 Verfahren und Apparat zum Überführen einer Flüssigkeit

Country Status (8)

Country Link
US (1) US5337569A (de)
EP (1) EP0567360B2 (de)
JP (1) JPH0618162A (de)
CN (1) CN1078946C (de)
CA (1) CA2092139C (de)
DE (1) DE69302619T2 (de)
ES (1) ES2086895T5 (de)
FR (1) FR2689223B1 (de)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2753638B1 (fr) * 1996-09-25 1998-10-30 Procede pour l'alimentation d'une unite consommatrice d'un gaz
GB9705889D0 (en) * 1997-03-21 1997-05-07 Boc Group Plc Heat exchange method and apparatus
CN1073883C (zh) * 1998-05-15 2001-10-31 中国石油化工总公司 一种采用管壁补气与排气实现循环流化床多段化操作的方法及其装置
DE19921949A1 (de) * 1999-05-12 2000-11-16 Linde Ag Verfahren und Vorrichtung zur Tieftemperaturzerlegung von Luft
DE19933558C5 (de) * 1999-07-16 2010-04-15 Linde Ag Dreisäulenverfahren und -vorrichtung zur Tieftemperaturzerlegung von Luft
EP1338856A3 (de) * 2002-01-31 2003-09-10 L'AIR LIQUIDE, Société Anonyme à Directoire et Conseil de Surveillance pour l'Etude et l'Exploitation des Verfahren und Vorrichtung zur Zerlegung von Luft durch Tieftemperaturdestillation
US6568208B1 (en) * 2002-05-03 2003-05-27 Air Products And Chemicals, Inc. System and method for introducing low pressure reflux to a high pressure column without a pump
FR2853405A1 (fr) * 2003-04-01 2004-10-08 Air Liquide Procede et installation de separation d'air par distillation cryogenique
FR2853406A1 (fr) * 2003-04-01 2004-10-08 Air Liquide Procede et appareil de separation d'air par distillation cryogenique
DE102010011803A1 (de) * 2010-03-18 2011-09-22 Linde Aktiengesellschaft Verfahren zum Betreiben einer 2-Phasen-Steigleitung im Teillastbetrieb
CN102734591B (zh) * 2012-07-12 2015-08-19 杭州杭氧股份有限公司 一种低温液体节流阀输送液体的自动提升装置
US20140165648A1 (en) * 2012-12-18 2014-06-19 Air Liquide Process & Construction, Inc. Purification of inert gases to remove trace impurities
US20140165649A1 (en) * 2012-12-18 2014-06-19 Air Liquide Process & Construction, Inc. Purification of inert gases to remove trace impurities
CN107998681A (zh) * 2017-12-29 2018-05-08 上海联风能源科技有限公司 一种低压差下将液体输送到高位的方法及其装置

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2633272A1 (de) 1976-07-23 1978-01-26 Linde Ag Rektifiziereinrichtung
GB1593253A (en) 1976-08-24 1981-07-15 Boc Ltd Biological treatment of aqueous waste material with oxygen
EP0321163A2 (de) 1987-12-14 1989-06-21 Air Products And Chemicals, Inc. Argon-Sauerstoffgemischtrennung
EP0410832A1 (de) 1989-07-28 1991-01-30 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Verdampfer-Kondensator für eine Zweisäulenanlage zur Luftzerlegung

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3059440A (en) * 1960-01-19 1962-10-23 John J Loporto Fluid transfer arrangement
DE1229561B (de) * 1962-12-21 1966-12-01 Linde Ag Verfahren und Vorrichtung zum Zerlegen von Luft durch Verfluessigung und Rektifikation mit Hilfe eines Inertgaskreislaufes
US3217502A (en) * 1963-04-22 1965-11-16 Hydrocarbon Research Inc Liquefaction of air
US4137056A (en) * 1974-04-26 1979-01-30 Golovko Georgy A Process for low-temperature separation of air
DE2535489C3 (de) * 1975-08-08 1978-05-24 Linde Ag, 6200 Wiesbaden Verfahren und Vorrichtung zur Zerlegung eines tiefsiedenden Gasgemisches
GB8820582D0 (en) * 1988-08-31 1988-09-28 Boc Group Plc Air separation
JPH0672740B2 (ja) * 1989-01-20 1994-09-14 ル・エール・リクイツド・ソシエテ・アノニム・プール・ル・エチユド・エ・ル・エクスプルワテション・デ・プロセデ・ジエオルジエ・クロード 空気分離及び超高純度酸素製造方法並びに装置
GB9008752D0 (en) * 1990-04-18 1990-06-13 Boc Group Plc Air separation

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2633272A1 (de) 1976-07-23 1978-01-26 Linde Ag Rektifiziereinrichtung
GB1593253A (en) 1976-08-24 1981-07-15 Boc Ltd Biological treatment of aqueous waste material with oxygen
EP0321163A2 (de) 1987-12-14 1989-06-21 Air Products And Chemicals, Inc. Argon-Sauerstoffgemischtrennung
EP0410832A1 (de) 1989-07-28 1991-01-30 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Verdampfer-Kondensator für eine Zweisäulenanlage zur Luftzerlegung

Non-Patent Citations (6)

* Cited by examiner, † Cited by third party
Title
Chambers Science and Technology Dictionary, Chambers-Cambridge, 1988, p. 380
Din, F. et al., Low-Temperature Techniques, Georges Newnes Ltd, London, 1960, pp. 16-18 et 158-161
Hausen, H. et al., Tieftemperaturtechnik, Erzeugung sehr tiefer Temperaturen, Gasverflüssigung und Zerlegung von Gasgemischen, Springer-Verlag 1985,pp. 317-334
Perry's Chemical Engineers' Handbook, McGraw-Hill Book Company, 1984, pp. 5-42 et 5-43
Ullmanns Encyclopädie der technischen Chemie, vol. 3, Verfahrenstechnik II und Reaktionsapparate, 4e édition, Verlag Chemie, Weinheim (sans date), pp. 172-173
v.d.Ster, J., The Production of Liquid Nitrogen from Atmospheric Air Using a Gas Refrigerating Machine, Thesis, Technische Hogeschool Delft, 1960, pp. 1-3, 29, 33-35 et 60-70

Also Published As

Publication number Publication date
EP0567360A1 (de) 1993-10-27
DE69302619D1 (de) 1996-06-20
US5337569A (en) 1994-08-16
FR2689223A1 (fr) 1993-10-01
CN1076775A (zh) 1993-09-29
CN1078946C (zh) 2002-02-06
FR2689223B1 (fr) 1994-05-06
DE69302619T2 (de) 1996-09-26
ES2086895T5 (es) 2002-12-16
CA2092139A1 (fr) 1993-09-25
CA2092139C (fr) 2004-05-04
JPH0618162A (ja) 1994-01-25
ES2086895T3 (es) 1996-07-01
EP0567360B1 (de) 1996-05-15

Similar Documents

Publication Publication Date Title
EP0567360B2 (de) Verfahren und Apparat zum Überführen einer Flüssigkeit
EP0848220B1 (de) Verfahren und Anlage zur Lieferung eines Luftgases in variablen Mengen
EP0628778B1 (de) Verfahren und Hochdruckgasversorgungseinheit für eine ein Luftbestandteil verbrauchende Anlage
EP0531182B2 (de) Verfahren und Einrichtung zur Luftdestillation und die Verwendung bei der Zuführung von Gas in Stahlwerken
EP0622595B1 (de) Lufttrennungsverfahren und Anlage dafür
EP0229803B1 (de) Verfahren und vorrichtung für luftdestillation
EP1223395B2 (de) Integriertes Verfahren zur Luftzerlegung und Energieerzeugung
EP0789208B1 (de) Verfahren und Einrichtung zur Herstellung von gasförmigem Sauerstoff unter hohem Druck
EP0178207A1 (de) Verfahren und Anlage zur kryogenischen Fraktionierung gasförmiger Massen
WO2007068858A2 (fr) Procédé de séparation d'air par distillation cryogénique
FR2774752A1 (fr) Installation de distillation d'air et boite froide correspondante
FR2716816A1 (fr) Procédé de redémarrage d'une colonne auxiliaire de séparation argon/oxygène par distillation, et installation correspondante.
FR2805339A1 (fr) Procede de production d'oxygene par rectification cryogenique
EP0430803B1 (de) Verfahren und Einrichtung zur Luftdestillierung mit Argongewinnung
FR2670278A1 (fr) Procede et installation de distillation d'air en regime variable de production d'oxygene gazeux.
EP2140216B1 (de) Verfahren und vorrichtung zur trennung einer mischung mit mindestens einem wasserstoff, stickstoff und kohlenmonoxid durch kryogene destillation
EP0914584B1 (de) Verfahren und einrichtung zur herstellung eines luftgases mit variablen mengen
EP2440871A2 (de) Vorrichtung und verfahren zur lufttrennung durch kryogene destillation
WO1999054673A1 (fr) Procede et installation de distillation d'air avec production d'argon
FR2710370A1 (fr) Procédé et ensemble de compression d'un gaz.
FR2686405A1 (fr) Procede et application de separation d'air, et application d'une telle installation.
EP1409937B1 (de) Verfahren zur dampferzeugung und luftzerlegung
WO2005047790A2 (fr) Procede et installation d'enrichissement d'un flux gazeux en l'un de ses constituants
EP1651915B1 (de) Verfahren und system zur versorgung einer lufttrenneinheit mittels einer gasturbine
FR2853406A1 (fr) Procede et appareil de separation d'air par distillation cryogenique

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

17P Request for examination filed

Effective date: 19930326

AK Designated contracting states

Kind code of ref document: A1

Designated state(s): DE ES FR GB IT NL SE

17Q First examination report despatched

Effective date: 19950727

GRAH Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOS IGRA

GRAA (expected) grant

Free format text: ORIGINAL CODE: 0009210

AK Designated contracting states

Kind code of ref document: B1

Designated state(s): DE ES FR GB IT NL SE

ITF It: translation for a ep patent filed
REF Corresponds to:

Ref document number: 69302619

Country of ref document: DE

Date of ref document: 19960620

REG Reference to a national code

Ref country code: ES

Ref legal event code: FG2A

Ref document number: 2086895

Country of ref document: ES

Kind code of ref document: T3

GBT Gb: translation of ep patent filed (gb section 77(6)(a)/1977)

Effective date: 19960618

PLBQ Unpublished change to opponent data

Free format text: ORIGINAL CODE: EPIDOS OPPO

PLBI Opposition filed

Free format text: ORIGINAL CODE: 0009260

PLBF Reply of patent proprietor to notice(s) of opposition

Free format text: ORIGINAL CODE: EPIDOS OBSO

26 Opposition filed

Opponent name: LINDE AKTIENGESELLSCHAFT

Effective date: 19970217

Opponent name: THE BOC GROUP PLC

Effective date: 19970213

NLR1 Nl: opposition has been filed with the epo

Opponent name: LINDE AKTIENGESELLSCHAFT

Opponent name: THE BOC GROUP PLC

PLBF Reply of patent proprietor to notice(s) of opposition

Free format text: ORIGINAL CODE: EPIDOS OBSO

PLAW Interlocutory decision in opposition

Free format text: ORIGINAL CODE: EPIDOS IDOP

APAC Appeal dossier modified

Free format text: ORIGINAL CODE: EPIDOS NOAPO

APAE Appeal reference modified

Free format text: ORIGINAL CODE: EPIDOS REFNO

APAC Appeal dossier modified

Free format text: ORIGINAL CODE: EPIDOS NOAPO

REG Reference to a national code

Ref country code: GB

Ref legal event code: IF02

APAC Appeal dossier modified

Free format text: ORIGINAL CODE: EPIDOS NOAPO

PLAW Interlocutory decision in opposition

Free format text: ORIGINAL CODE: EPIDOS IDOP

RAP2 Party data changed (patent owner data changed or rights of a patent transferred)

Owner name: L'AIR LIQUIDE, S.A. A DIRECTOIRE ET CONSEIL DE SUR

PUAH Patent maintained in amended form

Free format text: ORIGINAL CODE: 0009272

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: PATENT MAINTAINED AS AMENDED

27A Patent maintained in amended form

Effective date: 20020612

AK Designated contracting states

Kind code of ref document: B2

Designated state(s): DE ES FR GB IT NL SE

NLT2 Nl: modifications (of names), taken from the european patent patent bulletin

Owner name: L'AIR LIQUIDE, S.A. A DIRECTOIRE ET CONSEIL DE SUR

NLR2 Nl: decision of opposition
GBTA Gb: translation of amended ep patent filed (gb section 77(6)(b)/1977)
NLR3 Nl: receipt of modified translations in the netherlands language after an opposition procedure
NLT1 Nl: modifications of names registered in virtue of documents presented to the patent office pursuant to art. 16 a, paragraph 1

Owner name: L'AIR LIQUIDE, S.A. A DIRECTOIR ET CONSEIL DE SURV

REG Reference to a national code

Ref country code: ES

Ref legal event code: DC2A

Date of ref document: 20020906

Kind code of ref document: T5

REG Reference to a national code

Ref country code: DE

Ref legal event code: 8570

APAH Appeal reference modified

Free format text: ORIGINAL CODE: EPIDOSCREFNO

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: GB

Payment date: 20070214

Year of fee payment: 15

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: SE

Payment date: 20070219

Year of fee payment: 15

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: ES

Payment date: 20070307

Year of fee payment: 15

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: IT

Payment date: 20070606

Year of fee payment: 15

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: FR

Payment date: 20070212

Year of fee payment: 15

EUG Se: european patent has lapsed
GBPC Gb: european patent ceased through non-payment of renewal fee

Effective date: 20080323

REG Reference to a national code

Ref country code: FR

Ref legal event code: ST

Effective date: 20081125

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20080324

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: FR

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20080331

REG Reference to a national code

Ref country code: ES

Ref legal event code: FD2A

Effective date: 20080324

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: GB

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20080323

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: ES

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20080324

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IT

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20080323

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: DE

Payment date: 20120323

Year of fee payment: 20

REG Reference to a national code

Ref country code: DE

Ref legal event code: R082

Ref document number: 69302619

Country of ref document: DE

Representative=s name: PATENTANWAELTE HENKEL, BREUER & PARTNER, DE

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: NL

Payment date: 20120327

Year of fee payment: 20

REG Reference to a national code

Ref country code: DE

Ref legal event code: R071

Ref document number: 69302619

Country of ref document: DE

REG Reference to a national code

Ref country code: DE

Ref legal event code: R071

Ref document number: 69302619

Country of ref document: DE

REG Reference to a national code

Ref country code: NL

Ref legal event code: V4

Effective date: 20130323

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: DE

Free format text: LAPSE BECAUSE OF EXPIRATION OF PROTECTION

Effective date: 20130326