EP0423461B1 - Solid bowl decanter centrifuge - Google Patents

Solid bowl decanter centrifuge Download PDF

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Publication number
EP0423461B1
EP0423461B1 EP90116037A EP90116037A EP0423461B1 EP 0423461 B1 EP0423461 B1 EP 0423461B1 EP 90116037 A EP90116037 A EP 90116037A EP 90116037 A EP90116037 A EP 90116037A EP 0423461 B1 EP0423461 B1 EP 0423461B1
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EP
European Patent Office
Prior art keywords
centrifuge
solid
screw
drum
guide elements
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EP90116037A
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German (de)
French (fr)
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EP0423461A3 (en
EP0423461A2 (en
Inventor
Reinhold Dr. Schilp
Wolfgang Epper
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Deutz AG
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Deutz AG
Kloeckner Humboldt Deutz AG
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Application filed by Deutz AG, Kloeckner Humboldt Deutz AG filed Critical Deutz AG
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Publication of EP0423461A3 publication Critical patent/EP0423461A3/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04BCENTRIFUGES
    • B04B1/00Centrifuges with rotary bowls provided with solid jackets for separating predominantly liquid mixtures with or without solid particles
    • B04B1/20Centrifuges with rotary bowls provided with solid jackets for separating predominantly liquid mixtures with or without solid particles discharging solid particles from the bowl by a conveying screw coaxial with the bowl axis and rotating relatively to the bowl
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04BCENTRIFUGES
    • B04B1/00Centrifuges with rotary bowls provided with solid jackets for separating predominantly liquid mixtures with or without solid particles
    • B04B1/20Centrifuges with rotary bowls provided with solid jackets for separating predominantly liquid mixtures with or without solid particles discharging solid particles from the bowl by a conveying screw coaxial with the bowl axis and rotating relatively to the bowl
    • B04B2001/2033Centrifuges with rotary bowls provided with solid jackets for separating predominantly liquid mixtures with or without solid particles discharging solid particles from the bowl by a conveying screw coaxial with the bowl axis and rotating relatively to the bowl with feed accelerator inside the conveying screw

Definitions

  • the invention relates to a solid-bowl screw centrifuge for the continuous separation of a solid-liquid mixture, consisting of an elongated centrifuge drum which is rotatably mounted about its longitudinal axis and which surrounds a coaxially arranged screw conveyor rotating at a different speed, the screw spirals of which are attached to a screw drum , Means for feeding material to be separated into the drum along its axis and openings for the discharge of the separated light and heavy materials are provided.
  • a screw centrifuge is known in which, by arranging the discharge openings for the light phase in the vicinity of the drum shaft axis, the centrifuge drum can be filled with light phase to such an extent that the screw conveyor, which is hollow and of particularly low weight, can be filled is floating self-centering in the light phase. This enables high speeds and high throughputs, but means that the centrifuge must always be completely filled, which requires a particularly high monitoring effort.
  • a cylindrical solid-bowl screw centrifuge of the above type for separating suspensions which has a cutting disc with an annular gap between the cutting disc and centrifuge drum at the end of the separation space.
  • Clear phase channels are arranged radially on the screw body at a distance in front of the cutting disc and open into an axially arranged clear phase discharge line.
  • a radially extending sediment channel Immediately behind the cutting disc is a radially extending sediment channel, which opens into a sediment discharge line arranged coaxially with the clear phase discharge line.
  • a disadvantage of this known solid-bowl screw centrifuge is that, owing to the risk of clogging of the discharge channels, it can only be used to separate thin media, and that these media must not only be supplied to the centrifuge under excess pressure, but also that the centrifuge only under excess pressure can be operated.
  • the centrifuge must be provided with special seals, in particular mechanical seals, both in the feed area and in the discharge area of the separated media, which not only have to be replaced frequently due to the rapid wear and tear, but which also have a relatively complicated design and are therefore very expensive to buy.
  • the liquid discharge through the centrifuge hollow shaft is required a special hollow shaft gear for the worm drive, which is also relatively expensive and associated with correspondingly higher acquisition costs.
  • the same disadvantages also apply to the solid-bowl screw centrifuge known from US Pat. No. 4,566,873, which is basically of the same design.
  • the object of the invention is to provide a solid-bowl screw centrifuge which, while avoiding the disadvantages mentioned above, is not only distinguished by its simple structural design, but which, even with high separation performance and very low energy consumption, continuously separates solid-liquid mixtures, in particular the drainage of thick sludge.
  • the design of the centrifuge according to the invention not only enables a pressure-free feeding of the solid-liquid mixture into the separating space of the centrifuge and the discharge of the separated substances from the centrifuge without special mechanical seals, but also a radial deflection of the Liquid separated from the solid reached laterally to the liquid discharge and thereby recovered a large part of the kinetic energy, which is in the suspension in the separation chamber of the centrifuge.
  • the centrifuge according to the invention is therefore distinguished from known centrifuges of a similar design by its relatively simple construction and by its significantly lower energy consumption with high separation performance.
  • the arrangement of the pump-like guide elements in the inlet area very advantageously results in a particularly uniform distribution of the solid-liquid mixture in the separation space of the centrifuge, while the arrangement of the turbine-like ones Guiding elements in the discharge area for the lighter substances enable a particularly energy-saving discharge of the lighter substances from the separation area of the centrifuge.
  • a further considerable saving in kinetic energy is also very advantageously achieved in that the turbine or pump-like guide elements or their flow channels are arranged or formed radially or at an oblique angle as well as straight or curved.
  • the solid bowl screw centrifuge consists of a cylindrical solid shell part (1), which is followed by a conical solid shell part (2) tapering in the direction of the discharge of the heavy substances.
  • the cylindrical-conical drum casing (1, 2) is mounted in a housing (3) so that it can rotate.
  • a screw conveyor (4) with a screw drum (4 ') and a screw helix (5) arranged thereon are rotatably mounted coaxially in this cylindrical-conical solid jacket.
  • a feed tube (7) axially leading into the centrifuge drum (1, 2) is also arranged on the right side.
  • the material inlet pipe (7) opens into a distributor chamber (8) arranged on the screw drum (4 '), to which a plurality of pump-like guide elements, which are arranged in the between the The screw drum (4 ') and the centrifuge drum (1, 2) separating space (10) open.
  • Turbine-like guide elements in the form of flow channels (11) are provided on the conveyor screw (4) on the left-hand side Divert liquid (arrow 13) separated from the solid matter (12) radially inwards laterally towards the liquid discharge opening (15 ').
  • discharge openings (15 ') are provided for the light substances, which on the one hand have a smaller radial distance (r1) from the centrifuge drum axis (a) than the largest radial distance (r2) of the outer circumference the worm drum (4 ') from the centrifuge drum axis (a), and which on the other hand have a greater radial distance (r1) from the centrifuge drum axis (a) than the outer circumference (r3) of the centrifuge drum shaft (16'), that is are arranged outside the centrifuge drum shaft.
  • This embodiment of the solid-bowl screw centrifuge according to the invention not only very advantageously enables a completely pressure-free supply of the solid-liquid mixture into the separation space of the centrifuge and the discharge of the separated substances from the centrifuge without special mechanical seals, but it also makes a particularly large proportion of the kinetic Energy that is in the suspension in the centrifuge separation area can be recovered with high separation performance. It is also of not insignificant advantage that the radial distance (r4) of the discharge openings (15) for the heavy substances from the centrifuge drum axis (a) is smaller than the greatest radial distance (r2) of the outer casing of the screw drum (4 ') .
  • the screw conveyor (4) is driven at different speeds in relation to the centrifuge drum consisting of the solid bowl parts (1) and (2) and the solid-liquid mixture to be separated from the centrifuge is fed via the feed pipe (7). supplied from outside without pressure. Under the action of the centrifugal forces, the solids or thick matter is separated from the liquid in the separating space (10) of the centrifuge, the discharge for the heavy substances at the end of the centrifuge drum opposite the discharge for the light substances or the liquid (arrow 13) (1, 2) takes place.
  • the liquid separated from the solid (12) is diverted to the liquid discharge opening (15 ') via the flow channels, which first run parallel to the worm shaft and then radially inwards, and are discharged from the centrifuge drum, while the solids (12) felt by the screw helix (5) and transported inwards via the conical drum shell part (2) and discharged from the centrifuge drum via lateral openings (15).
  • the guide elements (9) designed as flow channels deflect the solid-liquid mixture radially emerging from the feed pipe (7) into an axial flow in the separating space (10) of the centrifuge, the solid discharged from the feed pipe (7) is Liquid mixture formed by the flow channels which also rotate with the screw conveyor (4) Turbine or pump-like guide elements (9) are detected and accelerated by them with a high degree of efficiency and very low frictional losses to the high peripheral speed of the rotating separation space required in the direction of rotation.
  • the predominantly radial direction of flow of the solid-liquid mixture is diverted without loss of energy into the axial direction of flow, where it moves in spiral and / or axially oriented paths over a large radius towards the discharge end of the centrifuge drum and under the influence of the Centrifugal force separates the heavy components (solids) from the lighter components (liquid).
  • the liquid separated from the solid is guided by the turbine or pump-like radial, oblique, straight or curved guide elements (11) practically without loss of energy to the smallest possible radius and passes next to the drive shaft (16) of the screw conveyor (4) through the openings (15 ') from the centrifuge drum without pressure.
  • the solid (12) separated from the liquid is also conveyed to the smallest possible radius by means of the screw conveyor (4) via the conical jacket part (2) and discharged from the centrifuge drum with very little kinetic energy through the side openings (15).
  • the radial distance (r4) of the discharge openings (15) for the heavy substances from the centrifuge drum axis (a) is advantageously less than the largest radial distance (r2) of the outer shell of the screw drum (4 ').
  • additional other transport aids such as, for example, can also be used very advantageously.
  • the pressure effect of the clear phase in connection with a baffle plate and negative pond height can be used.
  • the bearings (17) and (18) of the screw conveyor (4) are very advantageously arranged with a smaller radial distance from the drum axis (a) than the outlet openings (15, 15 ') for the solids (12) and the liquid ( 13), whereby the bearings (17, 18) are safely protected against splashing water and dirt.
  • the solid bowl screw centrifuge according to the invention can, as shown in FIG. 2, possibly also be carried out very advantageously as a direct current centrifuge.
  • guide elements (20, 22) are arranged on the outside of the hollow screw shaft (19), through which the liquid, which is conducted in the separating space (21) in cocurrent and separated from the solid, directs an inward radial deflection via the guide elements (20, 22) formed Flow channels reach the liquid discharge openings (23 ') arranged outside the centrifuge drum shaft and are discharged from there to the outside.
  • turbine or pump-like guide elements (24) according to the invention are very advantageously arranged on the hollow screw shaft (19) in the feed inlet area, which guide elements contain the solid-liquid mixture radially emerging from the feed pipe (25) deflected into an axial flow in the centrifuge separation space (21) without loss of energy.
  • the solid bowl screw centrifuge according to the invention can also be very advantageously designed as a cocurrent and countercurrent centrifuge.
  • the centrifuge drum (26) and screw conveyor (27) are cylindrical, and the solids discharge (28) is very advantageously carried out in the center of the centrifuge drum (26).
  • turbine or pump-like guide elements (31, 32, 33) according to the invention are arranged on the screw conveyor (27), which direct the solid-liquid mixture emerging radially from the feed pipe into a flow in the centrifuge separation chamber, which runs axially parallel to the screw conveyor and deflect the liquid separated from the solid in the discharge area radially inwards laterally towards the liquid discharge opening (34), which are arranged outside the centrifuge drum shaft (35).
  • the arrangement according to the invention of turbine or pump-like guide elements on the screw conveyor achieves the same advantages as in the solid bowl screw centrifuges shown in FIGS. 1 and 2.
  • the turbine or pump-like guide elements can very advantageously run radially or at an oblique angle, straight or also curved, in particular also spiral running, arranged or designed so that they act like a pump or turbine impeller during operation of the centrifuge.
  • the cross section of the flow channels formed by the guide elements can, depending on the need and depending on the solid / liquid mixture to be separated in each case, also be very advantageously round or angular in order to thereby ensure operation that is as smooth as possible.
  • the guide elements acting like a pump wheel can be arranged on the centrifuge drum with the same advantages instead of on the screw conveyor. In case of need, it is also very easy to provide separate discharges for more than two substances separated from one another in the centrifuge on the centrifuge drum.
  • the centrifuge according to the invention is not only characterized by its simple and reliable machine construction and the very low product damage or flake and cell destruction, but also due to their insensitivity to coarse substances or individual heavy particles in the feed material.
  • the centrifuge designed according to the invention eliminates both mechanical seals for the screw bearings and hollow shaft gears for the screw drive, as a result of which a particularly strong reduction in investment and operating costs is achieved.
  • the noise level, ie the noise level of the centrifuge according to the invention is also considerably lower compared to known centrifuges and the throughput and separation performance are significantly higher.

Description

Die Erfindung bezieht sich auf eine Vollmantel-Schneckenzentrifuge zum kontinuierlichen Trennen eines Feststoff-Flüssigkeitsgemisches, bestehend aus einer langgestreckten Zentrifugentrommel, die um ihre Längsachse drehbar gelagert ist und die eine koaxial angeordnete, mit abweichender Drehzahl umlaufende Förderschnecke umschließt, deren Schneckenwendel auf einer Schnekkentrommel befestigt sind, wobei Einrichtungen zum Zuführen von zu trennendem Gut in die Trommel längs deren Achse sowie Öffnungen für den Austrag der getrennten leichten und schweren Stoffe vorgesehen sind.The invention relates to a solid-bowl screw centrifuge for the continuous separation of a solid-liquid mixture, consisting of an elongated centrifuge drum which is rotatably mounted about its longitudinal axis and which surrounds a coaxially arranged screw conveyor rotating at a different speed, the screw spirals of which are attached to a screw drum , Means for feeding material to be separated into the drum along its axis and openings for the discharge of the separated light and heavy materials are provided.

Aus der WO 87/06856 ist eine Schneckenzentrifuge bekannt, in der durch die Anordnung der Austragsöffnungen für die leichte Phase in der Nähe der Trommelwellenachse die Zentrifugentrommel so weitgehend mit leichter Phase gefüllt werden kann, daß die Förderschnecke, die hohl konstruiert und von besonders geringem Geweicht ist, sich selbst zentrierend in der leichten Phase schwimmt. Dies ermöglicht hohe Umdrehungs- und hohe Durchsatzzahlen, bedeutet aber, daß die Zentrifuge stets vollständig gefüllt sein muß, was einen besonders hohen Überwachungsaufwand erfordert.From WO 87/06856 a screw centrifuge is known in which, by arranging the discharge openings for the light phase in the vicinity of the drum shaft axis, the centrifuge drum can be filled with light phase to such an extent that the screw conveyor, which is hollow and of particularly low weight, can be filled is floating self-centering in the light phase. This enables high speeds and high throughputs, but means that the centrifuge must always be completely filled, which requires a particularly high monitoring effort.

Aus der deutschen Offenlegungsschrift 33 17 047 ist eine zylinderförmige Vollmantel-Schneckenzentrifuge obiger Bauart zur Trennung von Suspensionen bekannt, die am Ende des Trennraumes eine Trennscheibe mit einem Ringspalt zwischen Trennscheibe und Zentrifugentrommel aufweist. Mit Abstand vor der Trennscheibe sind hierbei am Schneckenkörper Klarphasenkanäle radial angeordnet, die in eine axial angeordnete Klarphasenaustragsleitung münden. Unmittelbar hinter der Trennscheibe ist ein ebenfalls radial verlaufender Sedimentkanal angeordnet, der in eine koaxial zur Klarphasenaustragsleitung angeordnete Sedimentaustragsleitung mündet. Nachteilig bei dieser bekannten Vollmantel-Schneckenzentrifuge ist jedoch, daß sie aufgrund der Verstopfungsgefahr der Austragskanäle nur zur Trennung von dünnflüssigen Medien eingesetzt werden kann, und daß darüberhinaus diese Medien nicht nur der Zentrifuge unter Überdruck zugeführt werden müssen, sondern daß auch die Zentrifuge nur unter Überdruck betrieben werden kann. Um dies zu bewerkstelligen, muß die Zentrifuge sowohl im Gutzulaufbereich als auch im Austragsbereich der voneinander getrennten Medien mit besonderen Dichtungen, insbesondere Gleitringdichtungen, versehen werden, die nicht nur aufgrund des raschen Verschleisses häufig ausgewechselt werden müssen, sondern die auch in ihrem konstruktiven Aufbau verhältnismäßig kompliziert und daher auch sehr teuer in der Anschaffung sind. Darüberhinaus erfordert hierbei der Flüssigkeitsaustrag durch die Zentrifugenhohlwelle ein besonderes Hohlwellengetriebe für den Schneckenantrieb, das ebenfalls verhältnismäßig aufwendig und mit entsprechend erhöhten Anschaffungskosten verbunden ist. Mit ebendenselben Nachteilen ist auch die aus der US-PS 4,566,873 bekannte, im Prinzip gleich ausgebildete Vollmantel-Schneckenzentrifuge behaftet.From German Offenlegungsschrift 33 17 047, a cylindrical solid-bowl screw centrifuge of the above type for separating suspensions is known, which has a cutting disc with an annular gap between the cutting disc and centrifuge drum at the end of the separation space. Clear phase channels are arranged radially on the screw body at a distance in front of the cutting disc and open into an axially arranged clear phase discharge line. Immediately behind the cutting disc is a radially extending sediment channel, which opens into a sediment discharge line arranged coaxially with the clear phase discharge line. A disadvantage of this known solid-bowl screw centrifuge, however, is that, owing to the risk of clogging of the discharge channels, it can only be used to separate thin media, and that these media must not only be supplied to the centrifuge under excess pressure, but also that the centrifuge only under excess pressure can be operated. In order to accomplish this, the centrifuge must be provided with special seals, in particular mechanical seals, both in the feed area and in the discharge area of the separated media, which not only have to be replaced frequently due to the rapid wear and tear, but which also have a relatively complicated design and are therefore very expensive to buy. In addition, the liquid discharge through the centrifuge hollow shaft is required a special hollow shaft gear for the worm drive, which is also relatively expensive and associated with correspondingly higher acquisition costs. The same disadvantages also apply to the solid-bowl screw centrifuge known from US Pat. No. 4,566,873, which is basically of the same design.

Die Aufgabe der Erfindung besteht darin, eine Vollmantel-Schnekkenzentrifuge zu schaffen, die sich unter Vermeidung der oben angeführten Nachteile nicht nur durch ihren einfachen konstruktiven Aufbau auszeichnet, sondern die auch bei hoher Trennleistung und sehr geringem Energieverbrauch eine kontinuierliche Trennung von Feststoff-Flüssigkeitsgemischen, insbesondere die Entwässerung von Dickschlamm, ermöglicht.The object of the invention is to provide a solid-bowl screw centrifuge which, while avoiding the disadvantages mentioned above, is not only distinguished by its simple structural design, but which, even with high separation performance and very low energy consumption, continuously separates solid-liquid mixtures, in particular the drainage of thick sludge.

Diese Aufgabe wird durch die Merkmale des Kennzeichnungsteils des Anspruchs 1 gelöst. Vorteilhafte Ausgestaltungen der Erfindung sind in den Unteransprüchen angegeben.This object is achieved by the features of the characterizing part of claim 1. Advantageous embodiments of the invention are specified in the subclaims.

Durch die Ausgestaltung der Zentrifuge gemäß der Erfindung wird nicht nur eine drucklose Zuführung des Feststoff-Flüssigkeitsgemisches in den Trennraum der Zentrifuge und der Austrag der voneinander getrennten Stoffe aus der Zentrifuge ohne besondere Gleitringdichtungen in einfacher Weise ermöglicht, sondern es wird hierbei auch eine radiale Umlenkung der vom Feststoff abgetrennten Flüssigkeit nach innen seitlich zum Flüssigkeitsaustrag erreicht und dadurch ein großer Teil der kinetischen Energie, die in der Suspension im Trennraum der Zentrifuge steckt, wieder zurückgewonnen. Die Zentrifuge gemäß der Erfindung zeichnet sich daher im Vergleich zu bekannten Zentrifugen ähnlicher Bauart durch ihren verhältnismäßig einfachen konstruktiven Aufbau und durch ihren wesentlich niedrigeren Energieverbrauch bei hoher Trennleistung aus.The design of the centrifuge according to the invention not only enables a pressure-free feeding of the solid-liquid mixture into the separating space of the centrifuge and the discharge of the separated substances from the centrifuge without special mechanical seals, but also a radial deflection of the Liquid separated from the solid reached laterally to the liquid discharge and thereby recovered a large part of the kinetic energy, which is in the suspension in the separation chamber of the centrifuge. The centrifuge according to the invention is therefore distinguished from known centrifuges of a similar design by its relatively simple construction and by its significantly lower energy consumption with high separation performance.

Durch die Anordnung der pumpenartigen Leitelemente im Einlaufbereich wird sehr vorteilhaft eine besonders gleichmäßige Verteilung des Feststoff-Flüssigkeitsgemisches im Trennraum der Zentrifuge erreicht, während die Anordnung der turbinenartigen Leitelemente im Austragsbereich für die leichteren Stoffe einen besonders energiesparenden Austrag der leichteren Stoffe aus dem Trennraum der Zentrifuge ermöglicht.The arrangement of the pump-like guide elements in the inlet area very advantageously results in a particularly uniform distribution of the solid-liquid mixture in the separation space of the centrifuge, while the arrangement of the turbine-like ones Guiding elements in the discharge area for the lighter substances enable a particularly energy-saving discharge of the lighter substances from the separation area of the centrifuge.

In weiterer Ausgestaltung der Erfindung wird sehr vorteilhaft eine weitergehende erhebliche Einsparung an kinetischer Energie auch dadurch erreicht, daß die turbinen- oder pumpenartigen Leitelemente bzw. deren Strömungskanäle radial oder schiefwinkelig sowie gerade oder gekrümmt angeordnet oder ausgebildet sind.In a further embodiment of the invention, a further considerable saving in kinetic energy is also very advantageously achieved in that the turbine or pump-like guide elements or their flow channels are arranged or formed radially or at an oblique angle as well as straight or curved.

Weitere Einzelheiten, Merkmale und Vorteile der Erfindung ergeben sich aus der nachfolgenden Erläuterung von in Zeichnungsfiguren schematisch dargestellten Vollmantel-Schneckenzentrifugen.Further details, features and advantages of the invention result from the following explanation of solid bowl screw centrifuges schematically shown in the drawing figures.

Es zeigt:

Fig. 1:
eine Gegenstrom-Vollmantel-Schneckenzentrifuge mit an der Förderschnecke angeordneten Leitelementen gemäß der Erfindung im Längsschnitt;
Fig. 2:
eine Gleichstrom-Vollmantel-Schneckenzentrifuge mit an der Förderschnecke angeordneten Leitelementen gemäß der Erfindung im Teillängsschnit;
Fig. 3:
eine Gleichstrom-Gegenstrom-Vollmantel-Schneckenzentrifuge mit an der Förderschnecke angeordneten Leitelementen und mittigem Feststoffaustrag gemäß der Erfindung im Teillängsschnitt.
It shows:
Fig. 1:
a countercurrent solid bowl screw centrifuge with guide elements arranged on the screw conveyor according to the invention in longitudinal section;
Fig. 2:
a direct current solid bowl screw centrifuge with guide elements arranged on the screw conveyor according to the invention in partial longitudinal section;
Fig. 3:
a cocurrent-countercurrent solid-bowl screw centrifuge with arranged on the screw conveyor Guide elements and central solids discharge according to the invention in partial longitudinal section.

Wie Fig. 1 zeigt, besteht die Vollmantel-Schneckenzentrifuge aus einem zylindrischen Vollmantelteil (1), an den sich ein in Richtung auf den Austrag der schweren Stoffe verjüngender konischer Vollmantelteil (2) anschließt. Der zylindrisch-konisch ausgebildete Trommelmantel (1, 2) ist in einem Gehäuse (3) rotationsbeweglich gelagert. In diesem zylindrisch-konischen Vollmantel ist koaxial eine Förderschnecke (4) mit Schneckentrommel (4') und darauf angeordneter Schneckenwendel (5) drehbeweglich gelagert. Auf der linken Seite außen befindet sich ein Antrieb (6) für die Förderschnecke (4) und auf der rechten Seite außen ein Antrieb (6') für die Zentrifugentrommel (1, 2). Ferner ist auf der rechten Seite ein axial in die Zentrifugentrommel (1, 2) hineinführendes Gutzulaufrohr (7) angeordnet. Das Gutzulaufrohr (7) mündet in eine an der Schneckentrommel (4') angeordnete Verteilerkammer (8), an die mehrere, gleichmäßig über den Umfang verteilt angeordnete, als Strömungskanäle (9) ausgebildete, pumpenartig wirkende Leitelemente angeschlossen sind, die in den zwischen der Schneckentrommel (4') und der Zentrifugentrommel (1, 2) befindlichen Trennraum (10) münden. Auf der linken Seite sind an der Förderschnecke (4) turbinenartige Leitelemente in Form von Strömungskanälen (11) vorgesehen, die die vom Feststoff (12) abgetrennte Flüssigkeit (Pfeil 13) radial nach innen seitlich zur Flüssigkeitsaustragsöffnung (15') hin umlenken.As shown in Fig. 1, the solid bowl screw centrifuge consists of a cylindrical solid shell part (1), which is followed by a conical solid shell part (2) tapering in the direction of the discharge of the heavy substances. The cylindrical-conical drum casing (1, 2) is mounted in a housing (3) so that it can rotate. A screw conveyor (4) with a screw drum (4 ') and a screw helix (5) arranged thereon are rotatably mounted coaxially in this cylindrical-conical solid jacket. On the left outside there is a drive (6) for the screw conveyor (4) and on the right outside there is a drive (6 ') for the centrifuge drum (1, 2). A feed tube (7) axially leading into the centrifuge drum (1, 2) is also arranged on the right side. The material inlet pipe (7) opens into a distributor chamber (8) arranged on the screw drum (4 '), to which a plurality of pump-like guide elements, which are arranged in the between the The screw drum (4 ') and the centrifuge drum (1, 2) separating space (10) open. Turbine-like guide elements in the form of flow channels (11) are provided on the conveyor screw (4) on the left-hand side Divert liquid (arrow 13) separated from the solid matter (12) radially inwards laterally towards the liquid discharge opening (15 ').

Im Flüssigkeitsaustragsbereich sind in der Stirnwandung der Zentrifugentrommel (1) Austragsöffnungen (15') für die leichten Stoffe vorgesehen, die einerseits einen geringeren radialen Abstand (r₁) von der Zentrifugen-Trommelachse (a) aufweisen als der größte radiale Abstand (r₂) des Außenumfangs der Schneckentrommel (4') von der Zentrifugen-Trommelachse (a), und die andererseits einen größeren radialen Abstand (r₁) von der Zentrifugen-Trommelachse (a) aufweisen als der Außenumfang (r₃) der Zentrifugen-Trommelwelle (16'), also außehalb der Zentrifugen-Trommelwelle angeordnet sind. Diese erfindungsgemäße Ausgestaltung der Vollmantel-Schneckenzentrifuge ermöglicht nicht nur sehr vorteilhaft eine völlig drucklose Zuführung des Feststoff-Flüssigkeitsgemisches in den Trennraum der Zentrifuge und den Austrag der voneinander getrennten Stoffe aus der Zentrifuge ohne besondere Gleitringdichtungen, sondern es wird hierdurch auch ein besonders großer Anteil der kinetischen Energie, die in der Suspension im Trennraum der Zentrifuge steckt, bei hoher Trennleistung wieder zurückgewonnen. Von nicht unwesentlichem Vorteil ist hierbei auch, daß der radiale Abstand (r₄) der Austragsöffnungen (15) für die schweren Stoffe von der Zentrifugen-Trommelachse (a) geringer ist als der größte radiale Abstand (r₂) des Außenmantels der Schneckentrommel (4').In the liquid discharge area in the end wall of the centrifuge drum (1) discharge openings (15 ') are provided for the light substances, which on the one hand have a smaller radial distance (r₁) from the centrifuge drum axis (a) than the largest radial distance (r₂) of the outer circumference the worm drum (4 ') from the centrifuge drum axis (a), and which on the other hand have a greater radial distance (r₁) from the centrifuge drum axis (a) than the outer circumference (r₃) of the centrifuge drum shaft (16'), that is are arranged outside the centrifuge drum shaft. This embodiment of the solid-bowl screw centrifuge according to the invention not only very advantageously enables a completely pressure-free supply of the solid-liquid mixture into the separation space of the centrifuge and the discharge of the separated substances from the centrifuge without special mechanical seals, but it also makes a particularly large proportion of the kinetic Energy that is in the suspension in the centrifuge separation area can be recovered with high separation performance. It is also of not insignificant advantage that the radial distance (r₄) of the discharge openings (15) for the heavy substances from the centrifuge drum axis (a) is smaller than the greatest radial distance (r₂) of the outer casing of the screw drum (4 ') .

Im Betrieb der in Fig. 1 dargestellten Vollmantel-Schneckenzentrifuge wird die Förderschnecke (4) gegenüber der aus den Vollmantelteilen (1) und (2) bestehenden Zentrifugentrommel mit unterschiedlichen Drehzahlen angetrieben und das zu trennende Feststoff-Flüssigkeitsgemisch der Zentrifuge über das Gutzulaufrohr (7) von außen drucklos zugeführt. Unter Einwirkung der Zentrifugalkräfte erfolgt im Trennraum (10) der Zentrifuge eine Trennung der Feststoffe bzw. Dickstoffe von der Flüssigkeit, wobei der Austrag für die schweren Stoffe an dem dem Austrag für die leichten Stoffe bzw. der Flüssigkeit (Pfeil 13) entgegengesetzten Ende der Zentrifugentrommel (1, 2) erfolgt. Die vom Feststoff (12) abgetrennte Flüssigkeit wird über die zuerst parallel zur Schneckenwelle und anschließend radial nach innen verlaufenden, aus den Leitelementen (11) gebildeten Strömungskanäle zur Flüssigkeitsaustragsöffnung (15') hin umgelenkt und aus der Zentrifugentrommel abgeführt, während die Feststoffe (12) von der Schneckenwendel (5) ertaßt und über den konischen Trommelmantelteil (2) nach innen transportiert und über seitliche Öffnungen (15) aus der Zentrifugentrommel ausgetragen werden. Dadurch, daß die als Strömungskanäle ausgebildeten Leitelemente (9) gemäß der Erfindung das aus dem Gutzulaufrohr (7) radial austretende Feststoff-Flüssigkeitsgemisch in eine im Trennraum (10) der Zentrifuge axiale Strömung umlenken, wird das aus dem Gutzulaufrohr (7) austretende Feststoff-Flüssigkeitsgemisch von den mit der Förderschnecke (4) mitrotierenden als Strömungskanäle ausgebildeten turbinen- oder pumpenartig wirkenden Leitelemente (9) erfaßt und von diesen mit einem hohen Wirkungsgrad und sehr geringen Reibungsverlusten auf die jeweils erforderliche hohe Umfangsgeschwindigkeit des rotierenden Trennraumes in Drehrichtung beschleunigt. Im Trennraum (10) wird hierbei sehr vorteilhaft die vorwiegend radiale Strömungsrichtung des Feststoff-Flüssigkeitsgemisches energieverlustfrei in die axiale Strömungsrichtung umgelenkt, wo sie sich in spiral- und/oder axialförmig gerichteten Bahnen auf großem Radius zum Austragsende der Zentrifugentrommel hin bewegt und dabei unter Einwirkung der Fliehkraft die schweren Komponenten (Feststoffe) von den leichteren Komponenten (Flüssigkeit) getrennt werden. Die vom Feststoff abgetrennte Flüssigkeit wird hierbei von den turbinen- oder pumpenartigen radial, schiefwinkelig, gerade oder gekrümmt ausgebildeten Leitelementen (11) praktisch ohne Energieverlust auf kleinstmöglichen Radius geführt und tritt neben der Antriebswelle (16) der Förderschnecke (4) durch die Öffnungen (15') drucklos aus der Zentrifugentrommel aus. Der von der Flüssigkeit getrennte Feststoff (12) wird mit Hilfe der Förderschnecke (4) über den konischen Mantelteil (2) ebenfalls auf einen möglichst kleinen Radius gefördert und durch die seitlichen Öffnungen (15) mit sehr geringer kinetischer Energie aus der Zentrifugentrommel ausgetragen. Hierbei ist der radiale Abstand (r₄) der Austragsöffnungen (15) für die schweren Stoffe von der Zentrifugen-Trommelachse (a) vorteilhaft geringer als der größte radiale Abstand (r₂) des Außenmantels der Schneckentrommel (4'). Zur Unterstützung des Feststofftransportes im konischen Trommelmantelteil (2) können gegebenenfalls auch sehr vorteilhaft noch zusätzliche andere Transporthilfen, wie z. B. die Druckwirkung der Klarphase in Verbindung mit einer Stauscheibe und negativer Teichhöhe, eingesetzt werden. Ferner sind hierbei die Lager (17) und (18) der Förderschnecke (4) sehr vorteilhaft mit einem geringeren radial Abstand von der Trommelachse (a) angeordnet als die Austrittsöffnungen (15, 15') für die Feststoffe (12) und die Flüssigkeit (13), wodurch die Lager (17, 18) sicher vor Spritzwasser und Verschmutzung geschützt sind.In operation of the solid bowl screw centrifuge shown in FIG. 1, the screw conveyor (4) is driven at different speeds in relation to the centrifuge drum consisting of the solid bowl parts (1) and (2) and the solid-liquid mixture to be separated from the centrifuge is fed via the feed pipe (7). supplied from outside without pressure. Under the action of the centrifugal forces, the solids or thick matter is separated from the liquid in the separating space (10) of the centrifuge, the discharge for the heavy substances at the end of the centrifuge drum opposite the discharge for the light substances or the liquid (arrow 13) (1, 2) takes place. The liquid separated from the solid (12) is diverted to the liquid discharge opening (15 ') via the flow channels, which first run parallel to the worm shaft and then radially inwards, and are discharged from the centrifuge drum, while the solids (12) felt by the screw helix (5) and transported inwards via the conical drum shell part (2) and discharged from the centrifuge drum via lateral openings (15). As a result of the fact that the guide elements (9) designed as flow channels, according to the invention, deflect the solid-liquid mixture radially emerging from the feed pipe (7) into an axial flow in the separating space (10) of the centrifuge, the solid discharged from the feed pipe (7) is Liquid mixture formed by the flow channels which also rotate with the screw conveyor (4) Turbine or pump-like guide elements (9) are detected and accelerated by them with a high degree of efficiency and very low frictional losses to the high peripheral speed of the rotating separation space required in the direction of rotation. In the separating chamber (10), the predominantly radial direction of flow of the solid-liquid mixture is diverted without loss of energy into the axial direction of flow, where it moves in spiral and / or axially oriented paths over a large radius towards the discharge end of the centrifuge drum and under the influence of the Centrifugal force separates the heavy components (solids) from the lighter components (liquid). The liquid separated from the solid is guided by the turbine or pump-like radial, oblique, straight or curved guide elements (11) practically without loss of energy to the smallest possible radius and passes next to the drive shaft (16) of the screw conveyor (4) through the openings (15 ') from the centrifuge drum without pressure. The solid (12) separated from the liquid is also conveyed to the smallest possible radius by means of the screw conveyor (4) via the conical jacket part (2) and discharged from the centrifuge drum with very little kinetic energy through the side openings (15). The radial distance (r₄) of the discharge openings (15) for the heavy substances from the centrifuge drum axis (a) is advantageously less than the largest radial distance (r₂) of the outer shell of the screw drum (4 '). To support the transport of solids in the conical drum casing part (2), additional other transport aids, such as, for example, can also be used very advantageously. B. the pressure effect of the clear phase in connection with a baffle plate and negative pond height can be used. Furthermore, the bearings (17) and (18) of the screw conveyor (4) are very advantageously arranged with a smaller radial distance from the drum axis (a) than the outlet openings (15, 15 ') for the solids (12) and the liquid ( 13), whereby the bearings (17, 18) are safely protected against splashing water and dirt.

Die Vollmantel-Schneckenzentrifuge gemäß der Erfindung kann, wie Fig. 2 zeigt, gegebenenfalls auch sehr vorteilhaft als Gleichstrom-Zentrifuge ausgeführt werden. Hierbei sind außen an der Schneckenhohlwelle (19) Leitelemente (20, 22) angeordnet, durch die die im Trennraum (21) im Gleichstrom geführte und vom Feststoff abgetrennte Flüssigkeit nach innen gerichteter, radialer Umlenkung über die aus den Leitelementen (20, 22) gebildeten Strömungskanäle in die außerhalb der Zentrifugen-Trommelwelle angeordneten Flüssigkeitsaustragsöffnungen (23') gelangt und von dort nach außen abgeführt wird. Auch hierbei sind an der Förderschneckenhohlwelle (19) im Gutzulaufbereich sehr vorteilhaft turbinen- oder pumpenartige Leitelemente (24) gemäß der Erfindung angeordnet, welche das aus dem Gutzulaufrohr (25) radial austretende Feststoff-Flüssigkeitsgemisch in eine im Trennraum (21) der Zentrifuge axiale Strömung ohne Energieverlust umlenkt.The solid bowl screw centrifuge according to the invention can, as shown in FIG. 2, possibly also be carried out very advantageously as a direct current centrifuge. In this case, guide elements (20, 22) are arranged on the outside of the hollow screw shaft (19), through which the liquid, which is conducted in the separating space (21) in cocurrent and separated from the solid, directs an inward radial deflection via the guide elements (20, 22) formed Flow channels reach the liquid discharge openings (23 ') arranged outside the centrifuge drum shaft and are discharged from there to the outside. Here, too, turbine or pump-like guide elements (24) according to the invention are very advantageously arranged on the hollow screw shaft (19) in the feed inlet area, which guide elements contain the solid-liquid mixture radially emerging from the feed pipe (25) deflected into an axial flow in the centrifuge separation space (21) without loss of energy.

Schließlich kann, wie Fig. 3 zeigt, die Vollmantel-Schneckenzentrifuge gemäß der Erfindung auch sehr vorteilhaft als Gleich- und Gegenstrom-Zentrifuge ausgeführt werden. Hierbei sind Zentrifugentrommel (26) und Förderschnecke (27) zylinderförmig ausgebildet, und der Feststoffaustrag (28) erfolgt sehr vorteilhaft in der Mitte der Zentrifugentrommel (26). Auch hierbei sind an der Förderschnecke (27) turbinen- oder pumpenartig ausgebildete Leitelemente (31, 32, 33) gemäß der Erfindung angeordnet, welche das aus dem Gutzulaufrohr radial austretende Feststoff-Flüssigkeitsgemisch in eine im Trennraum der Zentrifuge axiale parallel zur Förderschnecke verlaufende Strömung und die im Austragsbereich vom Feststoff abgetrennte Flüssigkeit radial nach innen seitlich zur Flüssigkeitsaustragsöffnung (34) hin umlenken, die außerhalb der Zentrifugen-Trommelwelle (35) angeordnet sind. Auch bei dieser in Fig. 3 dargestellten Gleich- und Gegenstrom-Vollmantel-Schneckenzentrifuge werden durch die erfindungsgemäße Anordnung von turbinen- oder pumpenartig ausgebildeten Leitelementen an der Förderschnecke dieselben Vorteile erreicht, wie bei den in den Fig. 1 und 2 dargestellten Vollmantel-Schneckenzentrifugen.Finally, as shown in FIG. 3, the solid bowl screw centrifuge according to the invention can also be very advantageously designed as a cocurrent and countercurrent centrifuge. The centrifuge drum (26) and screw conveyor (27) are cylindrical, and the solids discharge (28) is very advantageously carried out in the center of the centrifuge drum (26). Here too, turbine or pump-like guide elements (31, 32, 33) according to the invention are arranged on the screw conveyor (27), which direct the solid-liquid mixture emerging radially from the feed pipe into a flow in the centrifuge separation chamber, which runs axially parallel to the screw conveyor and deflect the liquid separated from the solid in the discharge area radially inwards laterally towards the liquid discharge opening (34), which are arranged outside the centrifuge drum shaft (35). Also in this co-current and countercurrent solid bowl screw centrifuge shown in FIG. 3, the arrangement according to the invention of turbine or pump-like guide elements on the screw conveyor achieves the same advantages as in the solid bowl screw centrifuges shown in FIGS. 1 and 2.

Die turbinen- oder pumpenartigen Leitelemente können sehr vorteilhaft radial oder schiefwinkelig, gerade oder auch gekrümmt verlaufend, insbesondere auch spiralförmig verlaufend, angeordnet bzw. ausgebildet sein, so daß sie im Betrieb der Zentrifuge wie ein Pumpen- oder Turbinenlaufrad wirken. Auch der Querschnitt der durch die Leitelemente gebildeten Strömungskanäle kann je nach Bedarf und in Abhängigkeit des jeweils zu trennenden Feststoff-Flüssigkeitsgemisches sehr vorteilhaft rund oder auch eckig ausgebildet sein, um dadurch einen möglichst stoßfreien Betrieb zu gewährleisten. Gegebenenfalls können die wie ein Pumpenrad wirkenden Leitelemente mit ebendenselben Vorteilen anstatt an der Förderschnecke auch an der Zentrifugentrommel angeordnet werden. Auch können im Bedarsfalle an der Zentrifugentrommel sehr leicht getrennte Austräge für mehr als zwei in der Zentrifuge voneinander getrennte Stoffe vorgesehen werden. Wesentlich ist hierbei, daß die in der Zentrifuge abgetrennte, mengenmäßig größere Komponente möglichst weit nach innen geführt und von dort drucklos nach außen ausgetragen wird, um die Zentrifuge gemäß der Erfindung gegenüber bisher bekannten Zentrifugen mit bedeutend geringerem Energie- und Kostenaufwand betreiben zu können.The turbine or pump-like guide elements can very advantageously run radially or at an oblique angle, straight or also curved, in particular also spiral running, arranged or designed so that they act like a pump or turbine impeller during operation of the centrifuge. The cross section of the flow channels formed by the guide elements can, depending on the need and depending on the solid / liquid mixture to be separated in each case, also be very advantageously round or angular in order to thereby ensure operation that is as smooth as possible. If necessary, the guide elements acting like a pump wheel can be arranged on the centrifuge drum with the same advantages instead of on the screw conveyor. In case of need, it is also very easy to provide separate discharges for more than two substances separated from one another in the centrifuge on the centrifuge drum. It is essential here that the component in the centrifuge which is separated in terms of quantity and is guided as far as possible inwards and discharged from there without pressure in order to be able to operate the centrifuge according to the invention with significantly less energy and cost compared to previously known centrifuges.

Die Energieeinsparung, die durch die erfindungsgemäß ausgebildete Vollmantel-Schneckenzentrifuge im Vergleich zu den bisher bekannten Zentrifugen erreicht wird, ergibt sich aus nachfolgender Berechnung:The energy saving achieved by the solid-bowl screw centrifuge designed according to the invention in comparison with the centrifuges known hitherto results from the following calculation:

Um die Suspension auf die im Trennraum der Zentrifuge erforderliche Umfangsgeschwindigkeit zu bringen, kann die Beschleunigungsleistung nach folgender Erfahrungsformel berechnet werden:

P B =3,81 x 10⁻⁷ x 1 η x m x D² x n² (kW)

Figure imgb0001


Hierbei bedeutet:

m
die Durchsatzleistung (t/h).
D
den Durchmesser der Zentrifugentrommel (m).
n
die Trommelumdrehung pro Minute (U/min.)
η
den Wirkungsgrad der Zentrifuge.
In order to bring the suspension up to the peripheral speed required in the separation area of the centrifuge, the acceleration power can be calculated using the following empirical formula:

P B = 3.81 x 10⁻⁷ x 1 η xmx D² x n² (kW)
Figure imgb0001


Here means:
m
the throughput (t / h).
D
the diameter of the centrifuge drum (m).
n
the drum revolution per minute (rpm)
η
the efficiency of the centrifuge.

Der Wirkungsgrad η liegt bei bekannten Zentrifugen im allgemeinen bei ca. 50 %. Durch die erfindungsgemäße Ausbildung der Vollmantel-Schneckenzentrifuge, und zwar durch die Anordnung der turbinen- oder pumpenartigen Leitelemente bzw. Strömungskanäle, verringert sich der Energieaufwand bei sonst gleicher Trennwirkung der Zentrifuge sehr drastisch auf etwa 1/6 der bisher benötigten Energie auf:

P B = 0,7 x 10⁻⁷ x m x D² x n² (kW)

Figure imgb0002


Dieser Berechnung liegt ein Wirkungsgrad η von 0,80 und reduzierte Zulauf- und Absprifzradien von etwa 1/3 x Trommelinnendurchmesser D zugrunde.The efficiency η in known centrifuges is generally around 50%. Due to the inventive design of the solid bowl screw centrifuge, namely by the arrangement of the turbine or pump-like guide elements or flow channels, the energy expenditure is reduced drastically to about 1/6 of the previously required energy with otherwise the same separating effect of the centrifuge:

P B = 0.7 x 10⁻⁷ xmx D² x n² (kW)
Figure imgb0002


This calculation is based on an efficiency η of 0.80 and reduced inflow and spray radii of around 1/3 x inner drum diameter D.

Neben diesem sehr geringen Energieverbrauch für den Zentrifugenantrieb zeichnet sich die Zentrifuge gemäß der Erfindung nicht nur durch ihren einfachen und betriebssicheren Maschinenaufbau und der sehr geringen Produktschädigung bzw. Flocken- und Zellzerstörung aus, sondern auch durch ihre Unempfindlichkeit gegen Grobstoffe oder einzelne schwere Partikeln im Aufgabegut. Darüber hinaus entfallen bei der erfindungsgemäß ausgebildeten Zentrifuge sowohl Gleitringdichtungen für die Schneckenlager als auch Hohlwellengetriebe für den Schneckenantrieb, wodurch eine besonders starke Reduzierung der Investitions- und Betriebskosten erreicht wird. Auch die Lärmentwicklung, d. h. der Geräuschpegel der Zentrifuge gemäß der Erfindung ist im Vergleich zu bekannten Zentrifugen ganz erheblich geringer und die Durchsatz- und Trennleistung wesentlich höher.In addition to this very low energy consumption for the centrifuge drive, the centrifuge according to the invention is not only characterized by its simple and reliable machine construction and the very low product damage or flake and cell destruction, but also due to their insensitivity to coarse substances or individual heavy particles in the feed material. In addition, the centrifuge designed according to the invention eliminates both mechanical seals for the screw bearings and hollow shaft gears for the screw drive, as a result of which a particularly strong reduction in investment and operating costs is achieved. The noise level, ie the noise level of the centrifuge according to the invention, is also considerably lower compared to known centrifuges and the throughput and separation performance are significantly higher.

Claims (4)

  1. A solid-bowl screw centrifuge for continuously separating a solid-liquid mixture, comprising an elongate centrifuge drum mounted for rotation around its longitudinal axis and surrounding a coaxially-disposed conveying screw which rotates at a different speed, the screw turns being secured to a drum, there being devices for supplying material for separation to the drum along the axis thereof as well as openings for discharging the separated light and heavy substances, characterised by a number of turbine or pump-like guide elements (9, 11, 20, 22, 24, 31, 32) in the form of flow ducts uniformly distributed around the periphery and disposed on the outside of the conveyor screw (4, 19, 27), wherein
    (a) the guide elements (9, 24, 31) serve to convert the gas-liquid mixture emerging radially and without pressure from the material feed pipe (7, 25, 29) into an axial flow,
    (b) the guide elements (11, 20, 22, 23) serve for the transport of the liquid (light phase) separated from solid parallel to the conveying screw (4, 19, 27) in the direction of the outlet opening (15', 23', 34) for the light phase, and
    (c) the guide elements (11, 20, 32) serve for deflection of the light phase radially inwards towards the discharge opening for the light phase (15', 23', 34), and
    (d) the flow ducts formed by the guide elements as per (a), (b) and (c) are interconnected,
    and by outlet openings (15', 23', 34) for the light phase disposed outside the centrifuge-drum shaft (16', 35, 56) on an end wall of the centrifuge and at a smaller radial distance from the centrifuge axis a than the greatest radial distance between the centrifuge axis a and the outer jacket of the screw drum.
  2. A solid-bowl screw centrifuge according to claim 1, characterised in that the turbine or pump-like guide elements (9, 11, 20, 22, 24, 31, 32) are disposed or formed radially, or at an oblique angle, or are straight or curved.
  3. A solid-bowl screw centrifuge according to claim 1 or 2, characterised in that the outlet for heavy substances is disposed at the end opposite the outlet for light substances or in the middle of the centrifuge drum (1, 2, 26).
  4. A solid-bowl screw centrifuge according to any one of the preceding claims, characterised in that separate outlets are provided for more than two substances separated from one another in the centrifuge.
EP90116037A 1989-10-17 1990-08-22 Solid bowl decanter centrifuge Expired - Lifetime EP0423461B1 (en)

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DE3934612 1989-10-17
DE3934612 1989-10-17
DE4005755 1990-02-23
DE4005755A DE4005755A1 (en) 1989-10-17 1990-02-23 FULL-COVERED SNAIL CENTRIFUGE

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DE4005755A1 (en) 1991-04-18
EP0423461A3 (en) 1991-07-24
DE59006496D1 (en) 1994-08-25
US5545119A (en) 1996-08-13
EP0423461A2 (en) 1991-04-24
DK0423461T3 (en) 1994-08-22

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