EP0223609B1

EP0223609B1 - Contact for terminating an optical fiber

Info

Publication number: EP0223609B1
Application number: EP86309060A
Authority: EP
Inventors: Frank H. Levinson; Pravin Soni; Adam C. Tanous; Richard J. Mccrae; Mark Ostasiuk
Original assignee: Raychem Corp
Current assignee: Raychem Corp
Priority date: 1985-11-20
Filing date: 1986-11-19
Publication date: 1994-02-16
Anticipated expiration: 2006-11-19
Also published as: CA1295501C; EP0223609A3; EP0223609A2; US4790622A; JPS62129803A; DE3689647D1; ES2051263T3; ATE101727T1; DE3689647T2

Abstract

An optical fiber contact for terminating an optical fiber (73) includes a solid multi-part thermoset mixture (55) in a cavity (54) in a front portion of the contact, an optical fiber being terminated by heating the thermoset so as to cause it to soften and liquify and subsequently inserting an optical fiber through the contact. The thermoset when liquified chemically reacts so as to form an epoxy adhesive which secures the optical fiber within the contact and keeps the optical fiber in place even when subjected to extremely wide temperature variations.

Description

The present invention relates to a method of terminating optical fibres.
Numerous methods have been proposed in the prior art for terminating optical fibres to fibre contacts and interconnecting such contacts. In severe environments where a relatively wide temperature range can be expected, such as in aerospace, geophysical, industrial, and marine applications, it has been common to mix two liquids together in the field to form a liquid epoxy which is then used to terminate an optical fibre to a fibre contact, the contact then being mechanically assembled with additional hardware to form a connector. This termination method is disadvantageous since it is messy, very craft sensitive, and time consuming. In addition, such fibre contacts tend to be intricate in design in that they include the connector hardware and therefore are unduly large which makes them hard to use since they are substantially larger in cross-section than the fibre cable.
Prior art contacts suffer from a further disadvantage in that they are oftentimes required to be formed to be precise longitudinal lengths to insure that an optical fibre terminated therewith will be disposed a pre-controlled distance from an optical source when connected thereto. A further disadvantage of prior art optical fibre contacts is that oftentimes the user is required to cleave an end of the optical fibre at a position flush with an end of the contact, and then subsequently polish the cleaved optical fibre end, which operations are very craft sensitive and time consuming. Finally, prior art contacts have relatively short shelf lives.
GB 2068142 describes a termination for a clad optical fibre in which a length of the cladding is removed from the end of the optical fibre and replaced by a fluorinated hydrocarbon polymer material. A clamping ferrule and the silica core of the fibre are bonded to this material by melting it or heat shrinking it into position.
GB 1567636 describes a termination for optical fibre cables which comprises a composite ferrule consisting of an outer ferrule, a driving ferrule and a fusible glass bead, the driving ferrule and glass bead being dimensioned to fit into the outer ferrule.
GB 2052790 describes a method for the formation of a ferrule termination on an optical fibre, which comprises inserting the fibre through the ferrule and severing the fibre at its point of emergence from the ferrule tip.
Accordingly, it is an object of the invention to eliminate the above-noted drawbacks of prior art optical fibre contacts and termination methods, and to provide an optical fibre contact which is relatively simple in design, small in size, and easy to install.
Thus, the present invention provides a method of terminating an optical fibre, which includes inserting the fibre though a contact aperture of a contact body, characterized in that:
a solid body of uncured thermosetting adhesive (referred to herein as a thermoset) is provided within a cavity of the contact body in a substantially unreacted form, the adhesive comprising a multi-component room-temperature stable solid mixture which when heated softens, liquefies, mixes and then cures to form an adhesive capable of adhering to the optical fibre and the contact body,
then the optical fibre is inserted through the adhesive; and
the adhesive is heated thereby softening, liquefying, mixing and curing it.
Use of a thermoset (for example a multipart epoxy) makes termination of an optical fibre easy, and since the thermoset is in a solid multipart unreacted form, it is inherently stable and has a relatively long shelf life. A preferred curing mechanism is chemical crosslinking.
According to one preferred embodiment of the invention, the thermoset is provided to completely fill the cavity, and the optical fibre is terminated by first heating the contact body so as to liquefy the thermoset, and thereafter an end of the optical fibre is inserted through the liquefied thermoset. Preferably the thermoset is formulated so as to be optically transparent and so as to have an index of refraction substantially the same as that of a core of the optical fibre, and accordingly a portion of the thermoset which adheres to an end of the optical fibre and cures thereon thus forms a relatively hard resiliently deformable index matching material on the end of the terminated optical fibre which can then be pressed against a similar index matching material disposed on a similarly terminated optical fibre to eliminate an air gap therebetween.
According to another preferred embodiment, the thermoset is provided in the form of a cylinder having a bore therein through which the optical fibre being terminated is inserted, and in this embodiment it is advantageous to dispose an index matching material on an end of the optical fibre being terminated subsequent to inserting it through the contact body.
A further feature of the invention is that of forming a reservoir adjacent the front end of the contact body aperture which allows the relatively hard resiliently deformable index matching material disposed on the terminated end of the optical fibre to flatten out when it is pressed against another similarly terminated optical fibre so as to eliminate any air gap therebetween and associated optical losses.
According to a further feature of the invention, the contact body comprises a ring and first and second tubes, the ring preferably being press fitted onto the second tube adjacent a flange thereof, the first and second tubes being telescopically press fitted together such that a back end of the first tube is separated from a front end of the ring so as to form a gap therebetween, a length of the gap being controlled so as to precisely control a distance l between a front end of the first tube and the front end of the ring, this assembly procedure eliminating any need for precisely machining and controlling a longitudinal length of the first tube and yet allows a means for accurately positioning an end of the terminated optical fiber relative to a reference point, e.g. the front of the ring, which enables the terminated optical fiber end to be positioned at an optimum focusing point.
Preferably, the contact further includes a plurality of flanges at a back end of the contact body which extend from an outer circumferential surface of the contact body, the flanges forming at least one annular reservoir on the surface of the contact body between the flanges, the contact further including a second solid adhesive disposed in the reservoir and secured to the contact body, the adhesive being capable of tightly adhering to braids of an optical fiber cable when the braids are forced into the second adhesive preferably by hoop stresses generated by a sleeve disposed around the braids when recovered using heat.
The invention further includes improved methods of terminating an optical fiber, one method being first cleaving the optical fiber and then inserting the cleaved optical fiber end through the contact body so as to be precisely positioned flush with a front end of the contact body. According to an alternative preferred termination method, the optical fiber is first inserted through the contact body so as to extend a substantial distance in front of the front face of the contact body and cleaved thereat, and subsequently the cleaved optical fiber end is retracted so as to be flush against the front face of the contact body.
The invention will be further described by reference to the accompanying figures, of which:

Figure 1 is a cross-sectional view of a preferred embodiment of an optical fiber contact 11 for terminating an optical fiber 73; and
Figure 2 is an enlarged more detailed cross-sectional view of a front end 52 of the optical fiber contact 11 of the invention which lacks a preformed adhesive bore 53 shown in Figure 1 but which is otherwise identical in construction with the contact of Figure 1.

Referring to Figures 1 and 2, the optical fiber contact 11 comprises a ring 59 and first and second tubes 50, 58. Preferably, the ring 59 and a flange 60 of the second tube 58 are formed so that an outside diameter of the flange 60 and an inside diameter of the ring 59 are closely sized such that a press fit therebetween is created. Extending forward of the flange 60 is a reduced diameter section 86 which has an outside diameter which closely corresponds to an inside diameter of the first tube 50 such that the first and second tubes 50, 58 telescopically mate in a press fitting manner.
In many applications, it is advantageous if a distance l (Figure 2) between a fixed reference point, in this case a front face 85 of the ring 59, and a front face 61 of the contact is precisely controlled so that an end 87 of the optical fiber, which is flush with the front face 61 of the contact 11, can be precisely axially positioned relative to a light source so as to be optimally situated with respect thereto so as to receive an optimum amount of light from the light source. To this end, prior art contacts have generally been precisely machined so as to precisely control a longitudinal length thereof relative to a fixed reference point such as ring or seating flange so that the front end 87 of the optical fiber 73 could be precisely positioned longitudinally relative to another element such as a light source.
However, with the invention, since the first and second tubes 50, 58 are press fit together in a variable manner, a longitudinal length of the first tube 50 is not required to be precisely controlled since when the first and second tubes 50, 58 are telescopically assembled, the first tube 50 is slideably engaged over the section 86 only a distance sufficient such that the distance l equals a predetermined value. In other words, a gap 63 between the front face 85 of the ring 59 and a back end of the tube 50 compensates for variations in length of the tube 50 such that a length of the gap 63 plus a length of the tube 50 always equals the value l. In practice, it is a relatively expedient matter to assemble the tubes 50, 58 so to achieve the value l between the front face 61 and the front face 85, whereas it is much more difficult to precisely fabricate elements so as to have a precise longitudinal length as is done with prior art contacts.
Figure 2 further illustrates a cavity 54 within the first tube 50, the cavity being formed by the assembly of parts 50, 58 and 59. A thermoset 55 is disposed within the cavity 54, the thermoset comprising a multipart solid material mixture, one example being an epoxy mixture. The thermoset 55 is disposed in the cavity 54 in a substantially unreacted form, and includes chemicals which when liquified mix and chemically react so as to form an adhesive, the chemical reaction preferably including crosslinking curing. Subsequent to curing and cooling, the mixture 55 provides a strong bond capable of adhering over a wide temperature range. Specifically, the thermoset 55 when heated softens, liquefies, mixes and cures to form an adhesive capable of adhering to the optical fibre 73 and the inside of the tube 50. The use of a solid multipart thermoset pre-installed within the tube 50 is advantageous since the user is not required to mix multiple shelf-life sensitive materials in the field so as to form an adhesive for terminating an optical fibre.
The cavity 54 may be completely filled with the thermoset 55, or alternatively the thermoset 55 may be formed so as to have a preformed bore 53 (Figure 1) in a central regional thereof which aligns with aperture 51 of the front end 52 of the contact tube 50. If the bore 53 is so preformed, to terminate an optical fiber, the user simply inserts the optical fiber through the bore 53 and the aperture 51 for termination, accurately positions the front end 87 of the fiber relative to the contact face 61, and then heats the tube 50 so as to liquify the thermoset and secure the fiber within the contact. When liquified, a portion of the thermoset will wick into the aperture 51.
For the embodiment where the thermoset completely fills a traverse cross-sectional area and volume of the cavity 54, the user must heat the contact tube 50 so as to soften and liquify the thermoset 55 after which the optical fiber 73 can be inserted through the hot thermoset and through the contact aperture 51. With this embodiment, since the optical fiber is inserted through the liquified thermoset 55, the insertion of the optical fiber through the thermost 55 will cause a portion of the thermoset to be disposed within the aperture 51 and enhance the wicking effect so as to better secure the optical fiber in place, with a portion of the thermoset 55 further adhering to an end of the optical fiber. In this case it is advantageous to formulate the thermoset 55 so as to be substantially optically transparent and so as to have an index of refraction preferably close to that of a core of the optical fiber being terminated in which case the portion of the thermoset 55 on a front end of the optical fiber can function as an index matching medium when the terminated optical fiber is abutted against another similarly terminated optical fiber. Preferably, when the thermoset 55 hardens, it forms a relatively hard but resiliently deformable material which will conform to a similar relatively hard resiliently deformable material on an end of the other contact to be optically connected with the terminated optical fiber 73. This allows the contact 11 to be resiliently urged towards its mating contact and eliminates any air gap between the optically coupled fibers.
A further advantageous feature of the contact 11 is the provision of a reservoir 62 adjacent the front end 61 in a vicinity of the aperture or passageway 51 of the contact body 50, the embodiment illustrated in Figure 2 being conical in shape. The function of the reservoir 62 becomes apparent when it is realized that any relatively hard solid resiliently deformable index matching material disposed on an end of the optical fiber 73 will tend to be displaced when urged against a similar index matching material when the terminated optical fiber is optically connected to another terminated optical fiber. The reservoir 62 provides an area for the compressed index matching material to expand into which allows an excellent continuous interface to be formed between the optical fibers being interconnected so as to eliminate any air gap and associated optical losses which an air gap may otherwise create.
A further feature of the invention, illustrated in Figure 1, is the provision of annular flanges 66 formed on a back portion of the contact 11, and a solid adhesive 72 disposed on the exterior surface of the contact 11 and in adherence therewith. Adjacent flanges 66 form annular reservoirs for containing the adhesive 72. The adhesive 72 and the flanges 66 provide an efficient and convenient means for clamping onto braids 67 of an optical fiber cable containing the optical fiber 73 being terminated.
As illustrated in Figure 1, by disposing the braids 67 longitudinally along the contact 11 so as to confront the adhesive 72 and the flanges 66, and by disposing a force means 68 around the braids which is capable of generating inwardly directed radial forces onto the braids 67, the braids 67 can be urged into the adhesive 72 and furthermore pinned between the force means 68 and the flanges 66. With this structure, axial pull out forces exerted on the cable are transferred to the exterior surface of the contact 11 via the braids 67, flanges 66, and adhesive 72 thus isolating the optical fiber itself from these axial pull out forces. A preferred adhesive is KYNAR™, with polypropylene or nylon being possible as well.
According to one preferred embodiment, the force means 68 comprises a dimensionally recoverable member, preferably a heat recoverable sleeve, which has the property of shrinking and generating radially inwardly directed forces when heated. Hoops stresses generated by recovery of the sleeve 68 thus urge the braids 67 into the adhesive 72 and pin the braids 67 against the flanges 66 upon recovery of the sleeve 68. In addition, the sleeve 68 can further provide an environmental barrier around a joint between the optical fiber cable and the contact 11.
The contact 11 further includes a flange 88, which in conjunction with the ring 59, provide an area for retaining a compression spring 90. The spring 90 provides a means for urging the contact 11 in an axial direction when the contact 11 is assembled within a connector for connecting the contact 11 with a similar additional contact 11.
The invention further includes several means of terminating an optical fiber. Prior art optical fiber termination techniques generally require that the optical fiber be inserted into a contact so that a front end of the fiber extends beyond a front face of the optical fiber contact, with the optical fiber then being cleaved at a position flush with the front face of the optical fiber contact and then being polished thereat.
On the other hand, according to the methods of terminating an optical fiber according to the invention, according to a first embodiment, the optical fiber is first cleaved prior to inserting it within the optical fiber contact 11. Thereafter, the cleaved optical fiber end is inserted through the contact 11. A hard resiliently deformable index matching material 87 is then disposed on the end of the fiber, or alternatively the material 87 can comprise part of the liquid thermoset 55 in the embodiment where the thermoset is liquified using heat prior to inserting the fiber through the passageway 51. Thereafter, the end of the fiber is precisely positioned so as to be flush with a plane of the front face 61 of the contact 11.
According to an alternative preferred method of the invention, the optical fiber is not first cleaved, and is simply inserted through the contact 11 so as to extend beyond a front face 61 of the contact to a vicinity of a point such as that illustrated by the X identified by reference number 91 in Figure 2. Thereafter, the optical fiber is cleaved at the point 91, retracted so as to be flush with the front face 61, and thereafter an index matching material is disposed on an end of the optical fiber. Such a termination procedure does not require that the optical fiber be polished as do prior art techniques. In addition, if a relatively hard resiliently deformable index matching material is disposed on the end of the optical fiber subsequent to cleaving, an efficient means of optically connecting the optical fiber 73 is provided since substantially no air gap will exist across an optical joint when the resiliently deformable index matching material is pressed against another similar type of index matching material. As explained previously, the reservoir 62 provides a means for allowing the index matching material to deform when pressed using compression forces of the spring 90 so as to insure that no air gap exists across the optical joint.
Finally, if desired, a back end of the contact 11 can contain some type of potting material, such as a potting adhesive in a vicinity of reference numberal 80, though this is not required.
According to a preferred embodiment, the thermoset 55 includes an epoxy resin, a curing agent and an accelerator, all disposed in the cavity 54 in solid form such that they substantially do not react over time until heated above a predetermined temperature. One preferred embodiment is a mixture of 100 parts novolac epoxy available from Ciba-Geigy as product ECN1299, 2-10 parts dicyandiamide available from Aldrich Chemical Co. as product dicyandiamide, a preferred amount being 8 parts, and 0.3-2 parts imidazole available form Shikokou Chemical Co. as product 2P4MHZ a preferred amount being 0.5 parts. The latter two chemicals comprise a curing agent and an accelerator, respectively.
Another thermoset example found useful but less preferred than the aforementioned mixture is 100 parts of the novolac epoxy as described above, 2-10 parts, preferably 8 parts, substituted dicyandiamide available from Ciba-Geigy as product Hardener HT2833 and 0.3-2 parts, preferably 0.5 parts, imidazole as described above. Another alternative sealant composition comprises 100 parts of novolac epoxy, 20-40 parts, preferably 30 parts, of Sumicure S available from Sumitomo Chemical Co. and 0.3-2 parts, preferably 0.5 parts imidazole as described above. It should readily be understood that other alternative thermoset compositions can be used in accordance with the invention, the above three being preferred compositions only.

EXAMPLE

A thermoset mixture comprising 100, 8, and 0.5 parts of novolac, dicyandiamide and imidazole, respectively, was used to secure an optical fiber within a stainless steel capillary tube, and after curing was heated to a temperature of 150°C whereat a pull-out strength test was conducted by pulling on the optical fiber longitudinally relative to the stainless steel capillary tube, and during this test the optical fiber fractured prior to the adhesive. A glass transition temperature Tg of this thermoset composition was measured and found to be 170°C - 180°C. The thermoset was further used to secure two stainless steel plates together, and at 150°C a lap sheer strength test was conducted whereat the thermoset was found to fail at approximately 950 psi. No weight loss for the cured thermoset composition was found to occur until approximately 300°C as measured by a thermogravimetric analysis test (TGA).
Although the invention has been described with reference to particular embodiments thereof, it should be understood that various modifications thereto can be made within the scope of the invention, and accordingly the invention is to be limited only by the appended claims.

Claims

A method of terminating an optical fibre (73) which includes inserting the fibre though a contact aperture (53) of a contact body (11), characterized in that:
a solid body of uncured thermosetting adhesive (66) is provided within a cavity (54) of the contact body (11) the adhesive comprising a multi-component room-temperature stable solid mixture which when heated softens, liquefies, mixes and then cures to form an adhesive capable of adhering to the optical fibre (73) and contact body (11),
then the optical fibre (73) is inserted through the adhesive (55); and
the adhesive (55) is heated thereby softening, liquefying, mixing and curing it.
The method of claim 1, the adhesive being heated after the optical fibre has been inserted through it.
The method of claim 1 or 2, the substantially unreacted adhesive having a preformed bore (53) preferably in a central region thereof through which the optical fibre is inserted.
The method of any one of claims 1-3, further comprising the step of providing an index matching material on an end of the fibre subsequent to inserting it through the contact body.
The method of claim 1, the adhesive being heated prior to inserting the optical fibre through it.
The method of claim 5, the substantially unreacted adhesive completely filling the cavity.
The method of any one of claims 1-6, the adhesive comprising a solid mixture of novolac epoxy resin, either dicyandiamide or substituted dicyandiamide, and imidazole.
The method of any of claims 1-7, the contact body (11) having a front face (61) adjacent a front end thereof whereat an end of the optical fibre being terminated can be optically connected to another optical fibre, a back end of the contact body having a plurality of flanges (66) extending from an outer surface thereof, the flanges forming at least one annular reservoir on the surface of the contact body between the flanges, the method further comprising the step of providing a second solid adhesive (72) in the reservoir.
The method of claim 8, further comprising the step of urging a braid (67) of an optical fibre cable into the second adhesive (66).
The method of claim 9, the braid being urged by a dimensionally recoverable member (68) which when heated recovers radially inward and attempts to conform to a shape of the outer surface of the contact body and the second adhesive.
The method of any one of claims 1-10 in which the contact body includes first and second tubes (50, 58) and a ring (50), the method further comprising the steps of press fitting the ring (59) onto the second tube (58) adjacent a flange (60) thereof, and telescopically press fitting the first tube (50) onto the second tube (58) so as to form a gap (63) between a back end of the first tube (50) and a front end of the ring (59).