EA201650118A1 - METHOD OF MEASUREMENT OF HEAT CAPACITY IN QUASI-DIABATIC CONDITIONS - Google Patents

METHOD OF MEASUREMENT OF HEAT CAPACITY IN QUASI-DIABATIC CONDITIONS

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Publication number
EA201650118A1
EA201650118A1 EA201650118A EA201650118A EA201650118A1 EA 201650118 A1 EA201650118 A1 EA 201650118A1 EA 201650118 A EA201650118 A EA 201650118A EA 201650118 A EA201650118 A EA 201650118A EA 201650118 A1 EA201650118 A1 EA 201650118A1
Authority
EA
Eurasian Patent Office
Prior art keywords
temperature
heat capacity
measurements
sample
preceded
Prior art date
Application number
EA201650118A
Other languages
Russian (ru)
Other versions
EA032329B1 (en
Inventor
Радель Радикович Гимаев
Юрий Иванович Спичкин
Мира Леонардовна Пляшкевич
Original Assignee
Общество с ограниченной ответственностью "Перспективные магнитные технологии и консультации"
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Общество с ограниченной ответственностью "Перспективные магнитные технологии и консультации" filed Critical Общество с ограниченной ответственностью "Перспективные магнитные технологии и консультации"
Publication of EA201650118A1 publication Critical patent/EA201650118A1/en
Publication of EA032329B1 publication Critical patent/EA032329B1/en

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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00Investigating or analyzing materials by the use of thermal means
    • G01N25/20Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Or Analyzing Materials Using Thermal Means (AREA)

Abstract

Способ относится к области исследования или анализа материалов с помощью тепловых средств при помощи калориметрических измерений путем измерения теплоемкости или теплопроводности. Способ измерения теплоемкости материалов по схеме адиабатического калориметра заключается в том, что выбор стартовой точки для определения температуры нагрева образца в калориметре при периодических колебаниях температуры образца производится таким образом, чтобы скорость изменения температуры на данном отрезке времени была минимальна, а точке измерения температуры предшествовал участок роста или спада температуры образца. Данный способ может быть также реализован таким образом, что измерения теплоёмкости производятся дважды: когда стартовой точке предшествует участок роста температуры образца и когда стартовой точке предшествует участок её спада, затем вычисляется среднее значение для теплоёмкости материала при заданной температуре. Данный способ может быть выполнен в форме серии измерений. Использование данного способа позволяет сократить время, затрачиваемое на исследование, а также снизить погрешность измерений. При этом предлагаемый способ не ограничивает возможные режимы измерений - измерения могут проводиться как при нагревании, так и при охлаждении с различными шагами по температуре.The method relates to the field of research or analysis of materials using thermal means using calorimetric measurements by measuring the heat capacity or thermal conductivity. The method for measuring the heat capacity of materials according to the adiabatic calorimeter scheme is that the choice of the starting point for determining the sample heating temperature in the calorimeter with periodic fluctuations in the sample temperature is such that the rate of temperature change at a given time interval is minimal and the temperature measurement point is preceded by a growth site or the temperature of the sample. This method can also be implemented in such a way that measurements of heat capacity are made twice: when the starting point is preceded by a portion of the temperature rise of the sample and when the starting point is preceded by a portion of its fall, then the average value for the heat capacity of the material at a given temperature is calculated. This method can be performed in the form of a series of measurements. Using this method allows you to reduce the time spent on research, as well as reduce the measurement error. In this case, the proposed method does not limit the possible measurement modes — measurements can be carried out both during heating and during cooling with different temperature steps.

EA201650118A 2016-11-09 2016-11-25 Method of heat capacity measuring under quasi-adiabatic conditions EA032329B1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RU2016143770A RU2649250C1 (en) 2016-11-09 2016-11-09 Method of heat capacity measuring under quasi-adiabatic conditions

Publications (2)

Publication Number Publication Date
EA201650118A1 true EA201650118A1 (en) 2018-05-31
EA032329B1 EA032329B1 (en) 2019-05-31

Family

ID=61867063

Family Applications (1)

Application Number Title Priority Date Filing Date
EA201650118A EA032329B1 (en) 2016-11-09 2016-11-25 Method of heat capacity measuring under quasi-adiabatic conditions

Country Status (2)

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EA (1) EA032329B1 (en)
RU (1) RU2649250C1 (en)

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1023231A1 (en) * 1981-01-14 1983-06-15 Предприятие П/Я Р-6209 Material heat capacity measuring method
SU1057831A1 (en) * 1982-02-08 1983-11-30 Ленинградский технологический институт холодильной промышленности Method of complex measuring of liquid and gas thermal physical properties
SU1057832A1 (en) * 1982-06-01 1983-11-30 Государственное Специальное Конструкторское Бюро Теплофизического Приборостроения Device for measuring material specific heat
SU1516926A1 (en) * 1987-07-28 1989-10-23 Государственное Специальное Конструкторское Бюро Теплофизического Приборостроения Method of measuring heat capacity
FR3012880B1 (en) * 2013-11-07 2023-01-13 Centre Nat Rech Scient CALORIMETER AT STABILIZED TEMPERATURE.

Also Published As

Publication number Publication date
RU2649250C1 (en) 2018-03-30
EA032329B1 (en) 2019-05-31

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