EA201650118A1 - METHOD OF MEASUREMENT OF HEAT CAPACITY IN QUASI-DIABATIC CONDITIONS - Google Patents
METHOD OF MEASUREMENT OF HEAT CAPACITY IN QUASI-DIABATIC CONDITIONSInfo
- Publication number
- EA201650118A1 EA201650118A1 EA201650118A EA201650118A EA201650118A1 EA 201650118 A1 EA201650118 A1 EA 201650118A1 EA 201650118 A EA201650118 A EA 201650118A EA 201650118 A EA201650118 A EA 201650118A EA 201650118 A1 EA201650118 A1 EA 201650118A1
- Authority
- EA
- Eurasian Patent Office
- Prior art keywords
- temperature
- heat capacity
- measurements
- sample
- preceded
- Prior art date
Links
- 238000005259 measurement Methods 0.000 title abstract 7
- 238000000034 method Methods 0.000 title abstract 7
- 238000010438 heat treatment Methods 0.000 abstract 2
- 238000009529 body temperature measurement Methods 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 230000000737 periodic effect Effects 0.000 abstract 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
- G01N25/20—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analyzing Materials Using Thermal Means (AREA)
Abstract
Способ относится к области исследования или анализа материалов с помощью тепловых средств при помощи калориметрических измерений путем измерения теплоемкости или теплопроводности. Способ измерения теплоемкости материалов по схеме адиабатического калориметра заключается в том, что выбор стартовой точки для определения температуры нагрева образца в калориметре при периодических колебаниях температуры образца производится таким образом, чтобы скорость изменения температуры на данном отрезке времени была минимальна, а точке измерения температуры предшествовал участок роста или спада температуры образца. Данный способ может быть также реализован таким образом, что измерения теплоёмкости производятся дважды: когда стартовой точке предшествует участок роста температуры образца и когда стартовой точке предшествует участок её спада, затем вычисляется среднее значение для теплоёмкости материала при заданной температуре. Данный способ может быть выполнен в форме серии измерений. Использование данного способа позволяет сократить время, затрачиваемое на исследование, а также снизить погрешность измерений. При этом предлагаемый способ не ограничивает возможные режимы измерений - измерения могут проводиться как при нагревании, так и при охлаждении с различными шагами по температуре.The method relates to the field of research or analysis of materials using thermal means using calorimetric measurements by measuring the heat capacity or thermal conductivity. The method for measuring the heat capacity of materials according to the adiabatic calorimeter scheme is that the choice of the starting point for determining the sample heating temperature in the calorimeter with periodic fluctuations in the sample temperature is such that the rate of temperature change at a given time interval is minimal and the temperature measurement point is preceded by a growth site or the temperature of the sample. This method can also be implemented in such a way that measurements of heat capacity are made twice: when the starting point is preceded by a portion of the temperature rise of the sample and when the starting point is preceded by a portion of its fall, then the average value for the heat capacity of the material at a given temperature is calculated. This method can be performed in the form of a series of measurements. Using this method allows you to reduce the time spent on research, as well as reduce the measurement error. In this case, the proposed method does not limit the possible measurement modes — measurements can be carried out both during heating and during cooling with different temperature steps.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
RU2016143770A RU2649250C1 (en) | 2016-11-09 | 2016-11-09 | Method of heat capacity measuring under quasi-adiabatic conditions |
Publications (2)
Publication Number | Publication Date |
---|---|
EA201650118A1 true EA201650118A1 (en) | 2018-05-31 |
EA032329B1 EA032329B1 (en) | 2019-05-31 |
Family
ID=61867063
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EA201650118A EA032329B1 (en) | 2016-11-09 | 2016-11-25 | Method of heat capacity measuring under quasi-adiabatic conditions |
Country Status (2)
Country | Link |
---|---|
EA (1) | EA032329B1 (en) |
RU (1) | RU2649250C1 (en) |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
SU1023231A1 (en) * | 1981-01-14 | 1983-06-15 | Предприятие П/Я Р-6209 | Material heat capacity measuring method |
SU1057831A1 (en) * | 1982-02-08 | 1983-11-30 | Ленинградский технологический институт холодильной промышленности | Method of complex measuring of liquid and gas thermal physical properties |
SU1057832A1 (en) * | 1982-06-01 | 1983-11-30 | Государственное Специальное Конструкторское Бюро Теплофизического Приборостроения | Device for measuring material specific heat |
SU1516926A1 (en) * | 1987-07-28 | 1989-10-23 | Государственное Специальное Конструкторское Бюро Теплофизического Приборостроения | Method of measuring heat capacity |
FR3012880B1 (en) * | 2013-11-07 | 2023-01-13 | Centre Nat Rech Scient | CALORIMETER AT STABILIZED TEMPERATURE. |
-
2016
- 2016-11-09 RU RU2016143770A patent/RU2649250C1/en active IP Right Revival
- 2016-11-25 EA EA201650118A patent/EA032329B1/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
RU2649250C1 (en) | 2018-03-30 |
EA032329B1 (en) | 2019-05-31 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
MM4A | Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s) |
Designated state(s): AM AZ BY KZ KG TJ TM |