EA200600954A1 - Способ приготовления гранул мочевины - Google Patents

Способ приготовления гранул мочевины

Info

Publication number
EA200600954A1
EA200600954A1 EA200600954A EA200600954A EA200600954A1 EA 200600954 A1 EA200600954 A1 EA 200600954A1 EA 200600954 A EA200600954 A EA 200600954A EA 200600954 A EA200600954 A EA 200600954A EA 200600954 A1 EA200600954 A1 EA 200600954A1
Authority
EA
Eurasian Patent Office
Prior art keywords
urea
melt
granules
preparation
urea granules
Prior art date
Application number
EA200600954A
Other languages
English (en)
Other versions
EA009533B1 (ru
Inventor
Станислаус Мартинус Петрус Мютсерс
Original Assignee
ДСМ Ай Пи ЭССЕТС Б.В.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ДСМ Ай Пи ЭССЕТС Б.В. filed Critical ДСМ Ай Пи ЭССЕТС Б.В.
Publication of EA200600954A1 publication Critical patent/EA200600954A1/ru
Publication of EA009533B1 publication Critical patent/EA009533B1/ru

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/16Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by suspending the powder material in a gas, e.g. in fluidised beds or as a falling curtain
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Fertilizers (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Glanulating (AREA)
  • Medicinal Preparation (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

Способ приготовления гранул мочевины в грануляторе с псевдоожиженным слоем посредством использования по меньшей мере одного подающего устройства для подачи расплава мочевины в виде пленки в псевдоожиженный слой твердых зародышей мочевины, после чего зародыши растут благодаря затвердеванию расплава мочевины на зародышах, в котором количества биурета и воды в расплаве мочевины и в гранулах мочевины подчиняется следующему соотношению (1): b·b/W(W-W)=0,1-20, где b= мас.% биурета в расплаве мочевины; b= мас.% биурета в гранулах мочевины; W= мас.% воды в расплаве мочевины; W= мас.% воды в гранулах мочевины.
EA200600954A 2003-11-10 2004-10-15 Способ приготовления гранул мочевины EA009533B1 (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP03078522 2003-11-10
PCT/EP2004/011678 WO2005049193A1 (en) 2003-11-10 2004-10-15 Process for the preparation of urea granules

Publications (2)

Publication Number Publication Date
EA200600954A1 true EA200600954A1 (ru) 2006-08-25
EA009533B1 EA009533B1 (ru) 2008-02-28

Family

ID=34610068

Family Applications (1)

Application Number Title Priority Date Filing Date
EA200600954A EA009533B1 (ru) 2003-11-10 2004-10-15 Способ приготовления гранул мочевины

Country Status (13)

Country Link
US (1) US7498055B2 (ru)
EP (1) EP1682255B1 (ru)
CN (1) CN100434152C (ru)
AR (1) AR047118A1 (ru)
AU (1) AU2004291238B2 (ru)
BR (1) BRPI0416384B1 (ru)
CA (1) CA2545073C (ru)
EA (1) EA009533B1 (ru)
EG (1) EG24323A (ru)
MY (1) MY141017A (ru)
PL (1) PL1682255T3 (ru)
UA (1) UA86207C2 (ru)
WO (1) WO2005049193A1 (ru)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1868963B1 (en) * 2005-04-18 2017-05-10 Stamicarbon B.V. Process for the production of urea-comprising particles
JP4852270B2 (ja) * 2005-07-13 2012-01-11 東洋エンジニアリング株式会社 顆粒尿素製品の製造方法
EP2077147A1 (en) 2008-01-04 2009-07-08 Urea Casale S.A. Fluid bed granulation process and apparatus
EP2489429A1 (en) * 2011-02-21 2012-08-22 Urea Casale S.A. Fluid bed granulation of urea and related apparatus
EP3112332A1 (en) * 2015-07-03 2017-01-04 Casale SA Method for producing solid urea by granulation
DE102017108842A1 (de) * 2017-04-25 2018-10-25 Thyssenkrupp Ag Verfahren und Vorrichtung zur Herstellung von Harnstoff
DE102019118702A1 (de) * 2019-07-10 2021-01-14 Thyssenkrupp Ag Reduzierung der biuretgeneration in der harnstoffproduktion
EP3995488A1 (en) * 2020-11-06 2022-05-11 Casale Sa Process for producing feed-grade urea

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB767716A (en) * 1952-10-25 1957-02-06 Chemical Construction Corp Improvements in a method for granulating urea
US3117020A (en) * 1957-11-29 1964-01-07 Montedison Spa Process for the spherical granulation of water-soluble nitrogenous material
CH411834A (de) * 1961-10-10 1966-04-30 Stamicarbon Biuretarme Harnstoffprills
GB1581761A (en) * 1977-06-09 1980-12-17 Azote Sa Cie Neerlandaise Urea granulation
JPS6034517B2 (ja) * 1978-03-03 1985-08-09 宇部興産株式会社 流動層で尿素を造粒する方法
JPS5855807B2 (ja) * 1979-10-08 1983-12-12 三井東圧化学株式会社 造粒方法
US4345099A (en) * 1981-08-10 1982-08-17 Union Oil Company Of California Method of selectively removing biuret from urea and compositions for use therein
NL8302999A (nl) * 1983-08-27 1985-03-18 Unie Van Kunstmestfab Bv Werkwijze voor het bereiden van granules.
NL8700913A (nl) * 1987-04-16 1988-11-16 Nl Stikstof Werkwijze voor het vervaardigen van kunstmestgranules.
GEP19981292B (en) * 1992-08-07 1998-05-01 Hydro Agri Sluiskil Bv Process for the Production of Urea Granules
US6217630B1 (en) * 1999-05-03 2001-04-17 Cargill, Incorporated Conditioned fertilizer product, method for conditioning fertilizer, and method for using conditioned fertilizer product
EP1205455B1 (en) * 2000-11-14 2012-05-30 Urea Casale S.A. Method and apparatus for obtaining urea prills
CN1288129C (zh) * 2002-04-16 2006-12-06 李思斌 一种改进的大颗粒尿素组合转鼓造粒方法及设备

Also Published As

Publication number Publication date
WO2005049193A1 (en) 2005-06-02
PL1682255T3 (pl) 2017-02-28
EP1682255B1 (en) 2016-07-27
CN100434152C (zh) 2008-11-19
AR047118A1 (es) 2006-01-11
CA2545073C (en) 2013-02-19
AU2004291238A1 (en) 2005-06-02
EA009533B1 (ru) 2008-02-28
US20070059446A1 (en) 2007-03-15
MY141017A (en) 2010-02-25
BRPI0416384A (pt) 2007-02-21
US7498055B2 (en) 2009-03-03
CN1878608A (zh) 2006-12-13
CA2545073A1 (en) 2005-06-02
AU2004291238B2 (en) 2009-09-17
UA86207C2 (ru) 2009-04-10
EP1682255A1 (en) 2006-07-26
BRPI0416384B1 (pt) 2014-07-08
EG24323A (en) 2009-01-25

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Legal Events

Date Code Title Description
MM4A Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s)

Designated state(s): AM KG MD TJ

PC4A Registration of transfer of a eurasian patent by assignment
QB4A Registration of a licence in a contracting state
QB4A Registration of a licence in a contracting state