EA033031B1 - Способ запуска и эксплуатации реактора фишера-тропша - Google Patents

Способ запуска и эксплуатации реактора фишера-тропша

Info

Publication number
EA033031B1
EA033031B1 EA201691852A EA201691852A EA033031B1 EA 033031 B1 EA033031 B1 EA 033031B1 EA 201691852 A EA201691852 A EA 201691852A EA 201691852 A EA201691852 A EA 201691852A EA 033031 B1 EA033031 B1 EA 033031B1
Authority
EA
Eurasian Patent Office
Prior art keywords
reactor
concentration
ppbv
initial concentration
feed stream
Prior art date
Application number
EA201691852A
Other languages
English (en)
Russian (ru)
Other versions
EA201691852A1 (ru
Inventor
Абейэт Иддхаварао Авхале
Робин Джон Наш
Томас Йорис Реманс
Баренд Руланд Вермер
Original Assignee
Шелл Интернэшнл Рисерч Маатсхаппий Б.В.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Шелл Интернэшнл Рисерч Маатсхаппий Б.В. filed Critical Шелл Интернэшнл Рисерч Маатсхаппий Б.В.
Publication of EA201691852A1 publication Critical patent/EA201691852A1/ru
Publication of EA033031B1 publication Critical patent/EA033031B1/ru

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/063—Titanium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/75—Cobalt
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2/00—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon
    • C10G2/30—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2/00—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon
    • C10G2/30—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen
    • C10G2/32—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts
    • C10G2/33—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used
    • C10G2/331—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used containing group VIII-metals
    • C10G2/332—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used containing group VIII-metals of the iron-group
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2/00—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon
    • C10G2/30—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen
    • C10G2/32—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts
    • C10G2/34—Apparatus, reactors
    • C10G2/341—Apparatus, reactors with stationary catalyst bed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/16—Reducing
    • B01J37/18—Reducing with gases containing free hydrogen
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1022—Fischer-Tropsch products
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/201—Impurities
    • C10G2300/202—Heteroatoms content, i.e. S, N, O, P
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/40—Characteristics of the process deviating from typical ways of processing
    • C10G2300/4031—Start up or shut down operations

Landscapes

  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
EA201691852A 2014-03-17 2015-03-16 Способ запуска и эксплуатации реактора фишера-тропша EA033031B1 (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP14160194 2014-03-17
PCT/EP2015/055423 WO2015140100A1 (en) 2014-03-17 2015-03-16 A method for start-up and operation of a fischer-tropsch reactor

Publications (2)

Publication Number Publication Date
EA201691852A1 EA201691852A1 (ru) 2016-12-30
EA033031B1 true EA033031B1 (ru) 2019-08-30

Family

ID=50391001

Family Applications (1)

Application Number Title Priority Date Filing Date
EA201691852A EA033031B1 (ru) 2014-03-17 2015-03-16 Способ запуска и эксплуатации реактора фишера-тропша

Country Status (8)

Country Link
US (1) US10155909B2 (zh)
EP (1) EP3119857A1 (zh)
CN (1) CN106103657B (zh)
AP (1) AP2016009376A0 (zh)
BR (1) BR112016021176B1 (zh)
EA (1) EA033031B1 (zh)
MY (1) MY192321A (zh)
WO (1) WO2015140100A1 (zh)

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1992006784A1 (en) * 1990-10-15 1992-04-30 Exxon Research And Engineering Company Method for preparing cobalt-containing hydrocarbon synthesis catalyst
US6284807B1 (en) * 1995-08-08 2001-09-04 Exxon Research And Engineering Company Slurry hydrocarbon synthesis process with increased catalyst life
US20050049317A1 (en) * 2003-09-03 2005-03-03 Conocophillips Company Novel method for improved fischer-tropsch catalyst stability and higher stable syngas conversion
US20050154069A1 (en) * 2004-01-13 2005-07-14 Syntroleum Corporation Fischer-Tropsch process in the presence of nitrogen contaminants
US20070287759A1 (en) * 2005-01-11 2007-12-13 Visagie Jacobus L Producing Supported Cobalt Catalysts for the Fisher-Tropsch Synthesis
US20080262112A1 (en) * 2004-12-03 2008-10-23 Marie Claire Marion Method For Temporarily Interrupting A Fischer-Tropsch Reaction In A Three-Phase Bed Reactor
US20080275144A1 (en) * 2005-12-09 2008-11-06 Robert Martijn Van Hardeveld Method to Start a Process for Producing Hydrocarbons from Synthesis Gas
US20110160510A1 (en) * 2008-04-16 2011-06-30 Michael Christian Maximillian Claeys Process for the Production of Hydrocarbons Including Olefins from Synthesis Gas
US20120202899A1 (en) * 2009-10-13 2012-08-09 Sasol Technology (Proprietary) Limited Production of hydrocarbons

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4595703A (en) 1984-06-29 1986-06-17 Exxon Research And Engineering Co. Preparation of hydrocarbons from synthesis gas
US4626552A (en) 1986-01-06 1986-12-02 Exxon Research And Engineering Company Process for the start-up of a Fischer-Tropsch reactor
EP0833807B1 (en) 1995-06-16 2004-04-14 Shell Internationale Researchmaatschappij B.V. Catalyst and process for the preparation of hydrocarbons
JP2005506190A (ja) 2001-10-25 2005-03-03 サソール テクノロジー（プロプライエタリー）リミテッド コバルト触媒を活性化するための方法

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1992006784A1 (en) * 1990-10-15 1992-04-30 Exxon Research And Engineering Company Method for preparing cobalt-containing hydrocarbon synthesis catalyst
US6284807B1 (en) * 1995-08-08 2001-09-04 Exxon Research And Engineering Company Slurry hydrocarbon synthesis process with increased catalyst life
US20050049317A1 (en) * 2003-09-03 2005-03-03 Conocophillips Company Novel method for improved fischer-tropsch catalyst stability and higher stable syngas conversion
US20050154069A1 (en) * 2004-01-13 2005-07-14 Syntroleum Corporation Fischer-Tropsch process in the presence of nitrogen contaminants
US20080262112A1 (en) * 2004-12-03 2008-10-23 Marie Claire Marion Method For Temporarily Interrupting A Fischer-Tropsch Reaction In A Three-Phase Bed Reactor
US20070287759A1 (en) * 2005-01-11 2007-12-13 Visagie Jacobus L Producing Supported Cobalt Catalysts for the Fisher-Tropsch Synthesis
US20080275144A1 (en) * 2005-12-09 2008-11-06 Robert Martijn Van Hardeveld Method to Start a Process for Producing Hydrocarbons from Synthesis Gas
US20110160510A1 (en) * 2008-04-16 2011-06-30 Michael Christian Maximillian Claeys Process for the Production of Hydrocarbons Including Olefins from Synthesis Gas
US20120202899A1 (en) * 2009-10-13 2012-08-09 Sasol Technology (Proprietary) Limited Production of hydrocarbons

Also Published As

Publication number Publication date
MY192321A (en) 2022-08-17
US10155909B2 (en) 2018-12-18
CN106103657A (zh) 2016-11-09
CN106103657B (zh) 2018-10-23
EP3119857A1 (en) 2017-01-25
EA201691852A1 (ru) 2016-12-30
AP2016009376A0 (en) 2016-08-31
BR112016021176A2 (zh) 2017-08-15
BR112016021176B1 (pt) 2021-10-26
US20180195007A1 (en) 2018-07-12
WO2015140100A1 (en) 2015-09-24

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Legal Events

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Designated state(s): AM AZ BY KZ KG TJ