DE69804638D1 - Trennung von methanol und propylenoxid aus einem reaktiosgemisch - Google Patents
Trennung von methanol und propylenoxid aus einem reaktiosgemischInfo
- Publication number
- DE69804638D1 DE69804638D1 DE69804638T DE69804638T DE69804638D1 DE 69804638 D1 DE69804638 D1 DE 69804638D1 DE 69804638 T DE69804638 T DE 69804638T DE 69804638 T DE69804638 T DE 69804638T DE 69804638 D1 DE69804638 D1 DE 69804638D1
- Authority
- DE
- Germany
- Prior art keywords
- reactious
- methanol
- separation
- mixture
- propylene oxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Revoked
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/32—Separation; Purification
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
- B01D3/40—Extractive distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Epoxy Compounds (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/926,420 US5849938A (en) | 1997-09-02 | 1997-09-02 | Separation of methanol and propylene oxide from a reaction mixture |
PCT/EP1998/005470 WO1999011639A1 (en) | 1997-09-02 | 1998-08-28 | Separation of methanol and propylene oxide from a reaction mixture |
Publications (2)
Publication Number | Publication Date |
---|---|
DE69804638D1 true DE69804638D1 (de) | 2002-05-08 |
DE69804638T2 DE69804638T2 (de) | 2002-10-17 |
Family
ID=25453174
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69804638T Revoked DE69804638T2 (de) | 1997-09-02 | 1998-08-28 | Trennung von methanol und propylenoxid aus einem reaktiosgemisch |
Country Status (11)
Country | Link |
---|---|
US (1) | US5849938A (de) |
EP (1) | EP1009746B1 (de) |
JP (1) | JP2001514258A (de) |
KR (1) | KR20010023443A (de) |
CN (1) | CN1268946A (de) |
AU (1) | AU9739798A (de) |
BR (1) | BR9811423A (de) |
CA (1) | CA2301060A1 (de) |
DE (1) | DE69804638T2 (de) |
ES (1) | ES2175803T3 (de) |
WO (1) | WO1999011639A1 (de) |
Families Citing this family (36)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1122248A1 (de) * | 2000-02-07 | 2001-08-08 | Degussa AG | Verfahren zur Epoxidierung von Olefinen |
EP1122247A1 (de) | 2000-02-07 | 2001-08-08 | Degussa AG | Verfahren zur Epoxidierung von Olefinen |
EP1122246A1 (de) | 2000-02-07 | 2001-08-08 | Degussa AG | Verfahren zur Epoxidierung von Olefinen |
EP1221442B1 (de) | 2001-01-08 | 2010-07-28 | Evonik Degussa GmbH | Verfahren zur Epoxidierung von Olefinen |
JP2002322167A (ja) * | 2001-04-27 | 2002-11-08 | Sumitomo Chem Co Ltd | プロピレンオキサイドの製造方法 |
US6596881B2 (en) | 2001-06-13 | 2003-07-22 | Degussa Ag | Process for the epoxidation of olefins |
US6600055B2 (en) | 2001-06-13 | 2003-07-29 | Degussa Ag | Process for the epoxidation of olefins |
US6608219B2 (en) | 2001-06-13 | 2003-08-19 | Degussa Ag | Process for the epoxidation of olefins |
US6749668B2 (en) * | 2001-06-18 | 2004-06-15 | Degussa Ag | Process for the recovery of combustible components of a gas stream |
US6610865B2 (en) | 2001-08-15 | 2003-08-26 | Degussa Ag | Process for the epoxidation of olefins |
US6596883B2 (en) | 2001-08-23 | 2003-07-22 | Degussa Ag | Process for the epoxidation of olefins |
US6500311B1 (en) * | 2001-09-21 | 2002-12-31 | Arco Chemical Technology, L.P. | Propylene oxide purification |
JP4078482B2 (ja) * | 2002-02-15 | 2008-04-23 | 住友化学株式会社 | プロピレンオキサイドの精製方法 |
US6720436B2 (en) | 2002-03-18 | 2004-04-13 | Degussa Ag | Process for the epoxidation of olefins |
US7141683B2 (en) * | 2002-05-02 | 2006-11-28 | Degussa Ag | Process for the epoxidation of olefins |
US20040000473A1 (en) * | 2002-06-20 | 2004-01-01 | Willi Hofen | Process of separating 1-methoxy-2-propanol and 2-methoxy-1-propanol from aqueous compositions |
US7722847B2 (en) * | 2002-09-30 | 2010-05-25 | Evonik Degussa Gmbh | Aqueous hydrogen peroxide solutions and method of making same |
US6838572B2 (en) * | 2002-09-30 | 2005-01-04 | Degussa Ag | Process for the epoxidation of olefins |
EP1424332A1 (de) * | 2002-11-26 | 2004-06-02 | Degussa AG | Verfahren zur Reinigung rohen Propenoxids |
US7169945B2 (en) * | 2002-11-26 | 2007-01-30 | Degussa Ag | Process for the epoxidation of olefins |
US7594979B2 (en) * | 2003-03-18 | 2009-09-29 | Dow Global Technologies, Inc. | Purification of propylene oxide resulting from epoxidation of propylene with hydrogen peroxide |
US20060006054A1 (en) * | 2004-07-07 | 2006-01-12 | Basf Aktiengesellshaft | Separation of propylene oxide from a mixture comprising propylene oxide and methanol |
US7323579B2 (en) * | 2004-07-07 | 2008-01-29 | Basf Aktiengesellschaft | Separation of propylene oxide from a mixture comprising propylene oxide and methanol |
US7105687B1 (en) * | 2005-12-22 | 2006-09-12 | Lyondell Chemical Technology, L.P. | Propylene oxide purification and recovery |
KR100846435B1 (ko) * | 2006-12-22 | 2008-07-16 | 한화석유화학 주식회사 | 옥시란 화합물의 제조 방법 |
US7741498B2 (en) * | 2008-08-29 | 2010-06-22 | Lyondell Chemical Technology, L.P. | Propylene oxide process |
RU2573849C2 (ru) | 2010-05-18 | 2016-01-27 | Текнолоджикал Ресорсиз Пти. Лимитед | Способ прямой плавки |
RU2013106290A (ru) | 2010-07-14 | 2014-08-20 | ДАУ ГЛОБАЛ ТЕКНОЛОДЖИЗ, ЭлЭлСи | Способ и комплекс оборудования для производства алкиленоксидов и гликолевых простых эфиров |
US8389750B2 (en) * | 2010-09-28 | 2013-03-05 | Lyondell Chemical Technology, L.P. | Purification of propylene oxide |
US8981133B2 (en) | 2011-06-07 | 2015-03-17 | Lyondell Chemical Technology, L.P. | Alkylene oxide separation systems, methods, and apparatuses |
CN103172596B (zh) * | 2011-12-22 | 2015-02-25 | 中国石油化工股份有限公司 | 一种环氧丙烷精制方法 |
CN103172595B (zh) * | 2011-12-22 | 2015-03-18 | 中国石油化工股份有限公司 | 一种从直接环氧化反应产物中提纯环氧丙烷的方法 |
BR112016012516B1 (pt) | 2013-12-06 | 2021-03-09 | Shell Internationale Research Maatschappij B.V. | métodos para separar impurezas de óxido de propileno impuro e para produzir óxido de propileno |
CN106467503A (zh) * | 2015-08-20 | 2017-03-01 | 陕西煤业化工集团(上海)胜帮化工技术有限公司 | 环氧丙烷分离方法 |
CN105712953A (zh) * | 2016-01-26 | 2016-06-29 | 江苏怡达化学股份有限公司 | 一种预纯化环氧丙烷的方法 |
CN113801076A (zh) * | 2020-06-16 | 2021-12-17 | 江苏怡达化学股份有限公司 | 环氧丙烷精馏工艺 |
Family Cites Families (27)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3578568A (en) * | 1968-11-29 | 1971-05-11 | Atlantic Richfield Co | Purification of low molecular weight epoxides by extractive distillation with a glycol or glycol ether |
US3881996A (en) * | 1973-11-21 | 1975-05-06 | Oxirane Corp | Recovery of propylene oxide by plural stage distillation |
US4140588A (en) * | 1977-08-05 | 1979-02-20 | Halcon Research And Development Corporation | Purification of propylene oxide by extractive distillation |
US4584063A (en) * | 1982-06-28 | 1986-04-22 | Lloyd Berg | Separation of acetone from methanol by extractive distillation |
IT1152299B (it) * | 1982-07-28 | 1986-12-31 | Anic Spa | Procedimento per l'espossidazione di composti olefinici |
US4597834A (en) * | 1983-04-14 | 1986-07-01 | Lloyd Berg | Separation of methyl acetate from methanol by extractive distillation |
US4620901A (en) * | 1985-11-04 | 1986-11-04 | Lloyd Berg | Separation of acetone from methanol by extractive distillation |
ES2033693T3 (es) * | 1986-01-28 | 1993-04-01 | Eniricerche S.P.A. | Un procedimiento para la exposidacion de compuestos olefinicos. |
US5000825A (en) * | 1989-03-23 | 1991-03-19 | Arco Chemical Technology, Inc. | Monoepoxide purification |
JPH02268174A (ja) | 1989-03-23 | 1990-11-01 | Arco Chem Technol Inc | モノエポキシドの精製 |
US4971661A (en) * | 1989-10-20 | 1990-11-20 | Texaco Chemical Company | Purification of propylene oxide using an aqueous acetone extractive distillatin agent |
US5139622A (en) * | 1991-10-03 | 1992-08-18 | Texaco Chemical Company | Purification of propylene oxide by extractive distillation |
US5160587A (en) * | 1991-11-01 | 1992-11-03 | Texaco Chemical Company | Extractive distillation of propylene oxide |
US5116465A (en) * | 1991-11-01 | 1992-05-26 | Texaco Chemical Company | Removal of water, methanol and acetone from propylene oxide by extractive distillation |
US5154803A (en) * | 1991-11-01 | 1992-10-13 | Texaco Chemical Company | Purification of contaminated propylene oxide by extractive distillation |
US5154804A (en) * | 1991-11-01 | 1992-10-13 | Texaco Chemical Company | Removal of water, acetone and methanol from propylene oxide by extractive distillation |
US5145563A (en) * | 1991-11-01 | 1992-09-08 | Texaco Chemical Company | Dehydration of propylene oxide by extracting distillation |
US5262550A (en) | 1992-04-30 | 1993-11-16 | Arco Chemical Technology, L.P. | Epoxidation process using titanium-rich silicalite catalysts |
US5340446A (en) * | 1992-10-23 | 1994-08-23 | Texaco Chemical Company | Purification of propylene oxide by cosolvent extractive distillation |
US5453511A (en) * | 1993-12-23 | 1995-09-26 | Arco Chemical Technology, L.P. | Bis-piperidinium compounds |
US5464505A (en) * | 1994-05-31 | 1995-11-07 | Texaco Chemical Inc. | Use of propylene oxide adducts in the purification of propylene oxide by extractive distillation |
US5453160A (en) * | 1994-05-31 | 1995-09-26 | Texaco Chemical Inc. | Use of mixed polyoxypropylene glycols in the extractive distillation of propylene oxide |
US5646314A (en) * | 1994-11-16 | 1997-07-08 | Arco Chemical Technology, L.P. | Process for titanium silicalite-catalyzed epoxidation |
US5523426A (en) * | 1995-01-04 | 1996-06-04 | Arco Chemical Technology, L.P. | Integrated process for epoxidation |
US5693834A (en) * | 1995-03-15 | 1997-12-02 | Arco Chemical Technology, L.P. | Integrated process for epoxidation |
US5591875A (en) * | 1995-08-02 | 1997-01-07 | Chang; Te | Epoxidation Process |
US5620568A (en) * | 1996-06-03 | 1997-04-15 | Texaco Chemical, Inc. | Extractive distillation of propylene oxide using propanol |
-
1997
- 1997-09-02 US US08/926,420 patent/US5849938A/en not_active Expired - Lifetime
-
1998
- 1998-08-28 KR KR1020007002086A patent/KR20010023443A/ko not_active Application Discontinuation
- 1998-08-28 AU AU97397/98A patent/AU9739798A/en not_active Abandoned
- 1998-08-28 CN CN98808688A patent/CN1268946A/zh active Pending
- 1998-08-28 JP JP2000508678A patent/JP2001514258A/ja active Pending
- 1998-08-28 WO PCT/EP1998/005470 patent/WO1999011639A1/en not_active Application Discontinuation
- 1998-08-28 CA CA002301060A patent/CA2301060A1/en not_active Abandoned
- 1998-08-28 BR BR9811423-9A patent/BR9811423A/pt not_active IP Right Cessation
- 1998-08-28 ES ES98951325T patent/ES2175803T3/es not_active Expired - Lifetime
- 1998-08-28 DE DE69804638T patent/DE69804638T2/de not_active Revoked
- 1998-08-28 EP EP98951325A patent/EP1009746B1/de not_active Revoked
Also Published As
Publication number | Publication date |
---|---|
EP1009746A1 (de) | 2000-06-21 |
WO1999011639A1 (en) | 1999-03-11 |
DE69804638T2 (de) | 2002-10-17 |
KR20010023443A (ko) | 2001-03-26 |
BR9811423A (pt) | 2000-08-22 |
ES2175803T3 (es) | 2002-11-16 |
US5849938A (en) | 1998-12-15 |
EP1009746B1 (de) | 2002-04-03 |
JP2001514258A (ja) | 2001-09-11 |
CA2301060A1 (en) | 1999-03-11 |
CN1268946A (zh) | 2000-10-04 |
AU9739798A (en) | 1999-03-22 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8363 | Opposition against the patent | ||
8331 | Complete revocation |