DE69719831D1 - Fluor-Desoxy-Glucose-Synthesizer unter Verwendung von Kolonnen - Google Patents

Fluor-Desoxy-Glucose-Synthesizer unter Verwendung von Kolonnen

Info

Publication number
DE69719831D1
DE69719831D1 DE69719831T DE69719831T DE69719831D1 DE 69719831 D1 DE69719831 D1 DE 69719831D1 DE 69719831 T DE69719831 T DE 69719831T DE 69719831 T DE69719831 T DE 69719831T DE 69719831 D1 DE69719831 D1 DE 69719831D1
Authority
DE
Germany
Prior art keywords
deoxy
fluorine
columns
synthesizer
glucose
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69719831T
Other languages
English (en)
Other versions
DE69719831T2 (de
Inventor
Shigeki Yamazaki
Katsuhiko Ohsaki
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NKK Plant Engineering Corp
Original Assignee
NKK Plant Engineering Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from JP08075536A external-priority patent/JP3133253B2/ja
Priority claimed from JP07553296A external-priority patent/JP3279914B2/ja
Priority claimed from JP08075535A external-priority patent/JP3133252B2/ja
Priority claimed from JP08075533A external-priority patent/JP3133250B2/ja
Priority claimed from JP08075534A external-priority patent/JP3133251B2/ja
Application filed by NKK Plant Engineering Corp filed Critical NKK Plant Engineering Corp
Application granted granted Critical
Publication of DE69719831D1 publication Critical patent/DE69719831D1/de
Publication of DE69719831T2 publication Critical patent/DE69719831T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
    • B01J31/0235—Nitrogen containing compounds
    • B01J31/0239—Quaternary ammonium compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0046—Sequential or parallel reactions, e.g. for the synthesis of polypeptides or polynucleotides; Apparatus and devices for combinatorial chemistry or for making molecular arrays
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
    • B01J31/0255—Phosphorus containing compounds
    • B01J31/0267—Phosphines or phosphonium compounds, i.e. phosphorus bonded to at least one carbon atom, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, the other atoms bonded to phosphorus being either carbon or hydrogen
    • B01J31/0268—Phosphonium compounds, i.e. phosphine with an additional hydrogen or carbon atom bonded to phosphorous so as to result in a formal positive charge on phosphorous
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/06—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing polymers
    • B01J31/08—Ion-exchange resins
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H5/00—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
    • C07H5/02—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00279—Features relating to reactor vessels
    • B01J2219/00281—Individual reactor vessels
    • B01J2219/00286—Reactor vessels with top and bottom openings
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00279—Features relating to reactor vessels
    • B01J2219/00281—Individual reactor vessels
    • B01J2219/00286—Reactor vessels with top and bottom openings
    • B01J2219/00288—Reactor vessels with top and bottom openings in the shape of syringes
    • B01J2219/0029—Reactor vessels with top and bottom openings in the shape of syringes with pistons or plungers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00279—Features relating to reactor vessels
    • B01J2219/00306—Reactor vessels in a multiple arrangement
    • B01J2219/00308—Reactor vessels in a multiple arrangement interchangeably mounted in racks or blocks
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583—Features relative to the processes being carried out
    • B01J2219/00585—Parallel processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583—Features relative to the processes being carried out
    • B01J2219/0059—Sequential processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583—Features relative to the processes being carried out
    • B01J2219/00596—Solid-phase processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718—Type of compounds synthesised
    • B01J2219/0072—Organic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/90—Catalytic systems characterized by the solvent or solvent system used
    • B01J2531/98—Phase-transfer catalysis in a mixed solvent system containing at least 2 immiscible solvents or solvent phases
    • C—CHEMISTRY; METALLURGY
    • C40—COMBINATORIAL TECHNOLOGY
    • C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
    • C40B60/00—Apparatus specially adapted for use in combinatorial chemistry or with libraries
    • C40B60/14—Apparatus specially adapted for use in combinatorial chemistry or with libraries for creating libraries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Saccharide Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE69719831T 1996-03-29 1997-03-27 Fluor-Desoxy-Glucose-Synthesizer unter Verwendung von Kolonnen Expired - Fee Related DE69719831T2 (de)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
JP08075536A JP3133253B2 (ja) 1996-03-29 1996-03-29 標識反応および加水分解反応をカラムで行うｆｄｇ合成装置
JP07553296A JP3279914B2 (ja) 1996-03-29 1996-03-29 オンカラムｆｄｇ合成装置
JP08075535A JP3133252B2 (ja) 1996-03-29 1996-03-29 三方切り替え活栓を組み込んだｆｄｇ合成装置
JP08075533A JP3133250B2 (ja) 1996-03-29 1996-03-29 使い捨てカートリッジを使用するｆｄｇ合成装置
JP08075534A JP3133251B2 (ja) 1996-03-29 1996-03-29 陽イオン交換樹脂カラム上で、溶媒除去と加水分解反応を同時に行うｆｄｇ合成装置

Publications (2)

Publication Number Publication Date
DE69719831D1 true DE69719831D1 (de) 2003-04-24
DE69719831T2 DE69719831T2 (de) 2003-11-06

Family

ID=27524572

Family Applications (2)

Application Number Title Priority Date Filing Date
DE69719831T Expired - Fee Related DE69719831T2 (de) 1996-03-29 1997-03-27 Fluor-Desoxy-Glucose-Synthesizer unter Verwendung von Kolonnen
DE69719576T Expired - Fee Related DE69719576T2 (de) 1996-03-29 1997-03-27 Fluor-desoxy-glucose-Synthetisierer unter Verwendung von Kolonnen

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE69719576T Expired - Fee Related DE69719576T2 (de) 1996-03-29 1997-03-27 Fluor-desoxy-glucose-Synthetisierer unter Verwendung von Kolonnen

Country Status (3)

Country Link
US (1) US5932178A (de)
EP (2) EP1134228B1 (de)
DE (2) DE69719831T2 (de)

Families Citing this family (38)

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BE1010280A3 (fr) * 1996-05-02 1998-05-05 Coincidence S A Procede et dispositif de synthese de 2-[18f] fluoro-2-deoxy-d-glucose.
JPH11295494A (ja) * 1998-04-08 1999-10-29 Nippon Meji Physics Kk ［ｆ−１８］−フッ化物イオンの製造方法
US6599484B1 (en) * 2000-05-12 2003-07-29 Cti, Inc. Apparatus for processing radionuclides
US6567492B2 (en) 2001-06-11 2003-05-20 Eastern Isotopes, Inc. Process and apparatus for production of F-18 fluoride
US6902704B2 (en) * 2002-02-28 2005-06-07 Equistar Chemicals, L.P Injection pump assembly for a combinatorial reactor and related method
US7018614B2 (en) * 2002-11-05 2006-03-28 Eastern Isotopes, Inc. Stabilization of radiopharmaceuticals labeled with 18-F
JP2006505610A (ja) * 2002-11-05 2006-02-16 イヨン ベアム アプリカスィヨン エッス．アー． １８−ｆ標識放射性製剤の安定化
PL1620373T3 (pl) * 2003-05-07 2008-09-30 Bayer Schering Pharma Ag Urządzenie i sposób fluorowania nukleofilowego
EP1660519B1 (de) * 2003-07-29 2014-05-14 Immunomedics, Inc. Konjugate von 2-[18F]Fluor-2-desoxy-D-glucose und einem Peptid-Molekül
EP1670519B1 (de) 2003-09-11 2016-07-13 Mayo Foundation For Medical Education And Research Festphasenextraktionsreinigungsverfahren für radioaktiv markiertes thymidin
WO2005030677A1 (ja) * 2003-09-30 2005-04-07 Nihon Medi-Physics Co., Ltd. 放射性フッ素化合物の製造方法
US20070071671A1 (en) * 2003-11-11 2007-03-29 Keiichi Hirano Process for producing radioactive-fluorine-labeled compound
US7734331B2 (en) * 2004-03-02 2010-06-08 General Electric Company Systems, methods and apparatus for preparation, delivery and monitoring of radioisotopes in positron emission tomography
US20060062342A1 (en) * 2004-09-17 2006-03-23 Cyclotron Partners, L.P. Method and apparatus for the production of radioisotopes
GB201420094D0 (en) 2014-11-12 2014-12-24 Ge Healthcare Ltd Flouride trapping arrangement
GB0428020D0 (en) * 2004-12-22 2005-01-26 Amersham Health As Stabilisation of radiopharmaceutical precursors
US7235216B2 (en) * 2005-05-01 2007-06-26 Iba Molecular North America, Inc. Apparatus and method for producing radiopharmaceuticals
WO2006119622A1 (en) * 2005-05-09 2006-11-16 Saxonia Biotec Gmbh. Apparatus for providing media to cell culture modules
DE102005028897A1 (de) * 2005-06-17 2006-12-28 Eckert & Ziegler Eurotope Gmbh Anordnung und Verfahren zur Verarbeitung von chemischen Stoffen, Computerprogramm zur Steuerung einer solchen Anordnung sowie ein entsprechendes computerlesbares Speichermedium
CN100374453C (zh) * 2005-11-18 2008-03-12 南方医科大学南方医院 2－18f－2－脱氧－d－葡萄糖的合成工艺
US8206571B2 (en) 2006-06-27 2012-06-26 Ge Healthcare Limited Formation of [18F] fluoride complexes suitable for [18F] fluorinations
US7556780B1 (en) * 2006-09-11 2009-07-07 Atomic Energy Council-Institute Of Nuclear Energy Research Device for 123I-ADAM and automatic manufacturing device thereof
WO2008055652A2 (en) * 2006-11-07 2008-05-15 Saxonia Biotec Gmbh Supply system for cell culture module
CN101657552B (zh) * 2007-02-21 2012-12-12 特拉西斯股份有限公司 作为不需要任何蒸发步骤的适用于有效放射性标记的形式的捕集在阴离子交换相上的18f氟化物的洗脱方法
EP2017359A3 (de) * 2007-06-11 2009-08-05 Trasis S.A. Verfahren zur Eluierung eines auf einem Anionenaustauschharz gefangenen 18F-Fluorids in einer für effiziente radioaktive Markierung geeigneten Form ohne Verdampfungsschritt
EP1990310A1 (de) * 2007-04-23 2008-11-12 Trasis S.A. Verfahren zur Herstellung von reaktivem 18F-Fluorid und zur Etikettierung von Radiotracern unter Verwendung eines modifizierten nicht-ionischen festen Trägers und ohne Evaporationsschritt
US8435454B2 (en) * 2009-07-09 2013-05-07 Siemens Medical Solutions Usa, Inc. Modular system for radiosynthesis with multi-run capabilities and reduced risk of radiation exposure
US8273300B2 (en) * 2009-07-09 2012-09-25 Siemens Medical Solutions Usa, Inc. Modular system for radiosynthesis with multi-run capabilities and reduced risk of radiation exposure
EP2556372A1 (de) 2010-04-08 2013-02-13 Siemens Medical Solutions USA, Inc. Synthese von 18f-markierten tracern in wasserhaltigen organischen lösungsmitteln
US9139316B2 (en) 2010-12-29 2015-09-22 Cardinal Health 414, Llc Closed vial fill system for aseptic dispensing
KR101221483B1 (ko) * 2011-05-13 2013-01-16 서강대학교산학협력단 Ｆ-18 표지 방사성의약품 합성 장치 및 방법
US20130020727A1 (en) 2011-07-15 2013-01-24 Cardinal Health 414, Llc. Modular cassette synthesis unit
US9417332B2 (en) 2011-07-15 2016-08-16 Cardinal Health 414, Llc Radiopharmaceutical CZT sensor and apparatus
WO2013012822A1 (en) 2011-07-15 2013-01-24 Cardinal Health 414, Llc Systems, methods, and devices for producing, manufacturing, and control of radiopharmaceuticals
WO2015143019A2 (en) 2014-03-18 2015-09-24 Mayo Foundation For Medical Education And Research Gaseous f-18 technologies
GB201405591D0 (en) * 2014-03-28 2014-05-14 Ge Healthcare Ltd Heatseal
CN105646601A (zh) * 2016-01-21 2016-06-08 甘肃圣普诺生物技术有限公司 一种制备18f-fdg的水解纯化方法
CN107474082B (zh) * 2017-08-11 2020-07-17 深圳市保健委员会办公室 双批次pet显像剂18f-fdg药物合成设备及方法

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USH74H (en) * 1983-02-24 1986-06-03 The United States Of America As Represented By The United States Department Of Energy Process for the production of 18F-2-deoxy-2-fluoro-D-glucose
US4617386A (en) * 1983-04-25 1986-10-14 The United States Of America As Represented By The United States Department Of Energy Process for the production of 18 F-2-deoxy-2-fluoro-D-glucose
US5264570A (en) * 1992-08-05 1993-11-23 General Electric Company Method for making 2-[18 F]fluoro-2-deoxy-D-glucose
WO1994021653A1 (en) * 1993-03-22 1994-09-29 General Electric Company Method for making 2-fluoro-2-deoxyglucose
JP3008329B2 (ja) * 1995-01-26 2000-02-14 信彦 中澤 ラジオアイソトープ標識試薬調整用プレフィルドキット
JPH08325169A (ja) * 1995-03-29 1996-12-10 Nkk Corp フッ素放射性同位元素標識有機化合物の製造方法
BE1010280A3 (fr) * 1996-05-02 1998-05-05 Coincidence S A Procede et dispositif de synthese de 2-[18f] fluoro-2-deoxy-d-glucose.
US5808020A (en) * 1996-08-12 1998-09-15 Associated Universities, Inc. Optical reaction cell and light source for 18F! fluoride radiotracer synthesis

Also Published As

Publication number Publication date
EP0798307B1 (de) 2003-03-19
DE69719576D1 (de) 2003-04-10
DE69719831T2 (de) 2003-11-06
DE69719576T2 (de) 2003-11-20
EP1134228B1 (de) 2003-03-05
EP1134228A1 (de) 2001-09-19
US5932178A (en) 1999-08-03
EP0798307A1 (de) 1997-10-01

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