DE69707551T2 - Tintenzusammensetzungen - Google Patents
TintenzusammensetzungenInfo
- Publication number
- DE69707551T2 DE69707551T2 DE69707551T DE69707551T DE69707551T2 DE 69707551 T2 DE69707551 T2 DE 69707551T2 DE 69707551 T DE69707551 T DE 69707551T DE 69707551 T DE69707551 T DE 69707551T DE 69707551 T2 DE69707551 T2 DE 69707551T2
- Authority
- DE
- Germany
- Prior art keywords
- ink
- printing
- inks
- acoustic
- pigment
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
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- 239000012943 hotmelt Substances 0.000 claims description 43
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- 239000000049 pigment Substances 0.000 claims description 38
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- -1 Poly(ethylene glycol) Polymers 0.000 claims description 33
- 239000007788 liquid Substances 0.000 claims description 31
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- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 4
- 229910052739 hydrogen Inorganic materials 0.000 claims description 2
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- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims 1
- 239000000976 ink Substances 0.000 description 205
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- WTFAGPBUAGFMQX-UHFFFAOYSA-N 1-[2-[2-(2-aminopropoxy)propoxy]propoxy]propan-2-amine Chemical compound CC(N)COCC(C)OCC(C)OCC(C)N WTFAGPBUAGFMQX-UHFFFAOYSA-N 0.000 description 21
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- XCJYREBRNVKWGJ-UHFFFAOYSA-N copper(II) phthalocyanine Chemical compound [Cu+2].C12=CC=CC=C2C(N=C2[N-]C(C3=CC=CC=C32)=N2)=NC1=NC([C]1C=CC=CC1=1)=NC=1N=C1[C]3C=CC=CC3=C2[N-]1 XCJYREBRNVKWGJ-UHFFFAOYSA-N 0.000 description 7
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- FIXBBOOKVFTUMJ-UHFFFAOYSA-N 1-(2-aminopropoxy)propan-2-amine Chemical compound CC(N)COCC(C)N FIXBBOOKVFTUMJ-UHFFFAOYSA-N 0.000 description 4
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- CGLVZFOCZLHKOH-UHFFFAOYSA-N 8,18-dichloro-5,15-diethyl-5,15-dihydrodiindolo(3,2-b:3',2'-m)triphenodioxazine Chemical compound CCN1C2=CC=CC=C2C2=C1C=C1OC3=C(Cl)C4=NC(C=C5C6=CC=CC=C6N(C5=C5)CC)=C5OC4=C(Cl)C3=NC1=C2 CGLVZFOCZLHKOH-UHFFFAOYSA-N 0.000 description 2
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- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical class OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 description 2
- FHNINJWBTRXEBC-UHFFFAOYSA-N Sudan III Chemical compound OC1=CC=C2C=CC=CC2=C1N=NC(C=C1)=CC=C1N=NC1=CC=CC=C1 FHNINJWBTRXEBC-UHFFFAOYSA-N 0.000 description 2
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
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- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 235000019239 indanthrene blue RS Nutrition 0.000 description 2
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- VKWNTWQXVLKCSG-UHFFFAOYSA-N n-ethyl-1-[(4-phenyldiazenylphenyl)diazenyl]naphthalen-2-amine Chemical compound CCNC1=CC=C2C=CC=CC2=C1N=NC(C=C1)=CC=C1N=NC1=CC=CC=C1 VKWNTWQXVLKCSG-UHFFFAOYSA-N 0.000 description 2
- 230000006911 nucleation Effects 0.000 description 2
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- 230000003287 optical effect Effects 0.000 description 2
- 150000002989 phenols Chemical class 0.000 description 2
- 229920006295 polythiol Polymers 0.000 description 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 2
- DNIAPMSPPWPWGF-UHFFFAOYSA-N propylene glycol Substances CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 2
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 2
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- QPAPQRFSPBUJAU-CPNJWEJPSA-N (4e)-5-methyl-4-[(3-methyl-5-oxo-1-phenyl-4h-pyrazol-4-yl)methylidene]-2-phenylpyrazol-3-one Chemical compound CC1=NN(C=2C=CC=CC=2)C(=O)C1\C=C(C1=O)/C(C)=NN1C1=CC=CC=C1 QPAPQRFSPBUJAU-CPNJWEJPSA-N 0.000 description 1
- AVQQQNCBBIEMEU-UHFFFAOYSA-N 1,1,3,3-tetramethylurea Chemical compound CN(C)C(=O)N(C)C AVQQQNCBBIEMEU-UHFFFAOYSA-N 0.000 description 1
- CYSGHNMQYZDMIA-UHFFFAOYSA-N 1,3-Dimethyl-2-imidazolidinon Chemical compound CN1CCN(C)C1=O CYSGHNMQYZDMIA-UHFFFAOYSA-N 0.000 description 1
- YHMYGUUIMTVXNW-UHFFFAOYSA-N 1,3-dihydrobenzimidazole-2-thione Chemical class C1=CC=C2NC(S)=NC2=C1 YHMYGUUIMTVXNW-UHFFFAOYSA-N 0.000 description 1
- 150000005208 1,4-dihydroxybenzenes Chemical class 0.000 description 1
- TXWSZJSDZKWQAU-UHFFFAOYSA-N 2,9-dimethyl-5,12-dihydroquinolino[2,3-b]acridine-7,14-dione Chemical compound N1C2=CC=C(C)C=C2C(=O)C2=C1C=C(C(=O)C=1C(=CC=C(C=1)C)N1)C1=C2 TXWSZJSDZKWQAU-UHFFFAOYSA-N 0.000 description 1
- HXIQYSLFEXIOAV-UHFFFAOYSA-N 2-tert-butyl-4-(5-tert-butyl-4-hydroxy-2-methylphenyl)sulfanyl-5-methylphenol Chemical compound CC1=CC(O)=C(C(C)(C)C)C=C1SC1=CC(C(C)(C)C)=C(O)C=C1C HXIQYSLFEXIOAV-UHFFFAOYSA-N 0.000 description 1
- AIBRSVLEQRWAEG-UHFFFAOYSA-N 3,9-bis(2,4-ditert-butylphenoxy)-2,4,8,10-tetraoxa-3,9-diphosphaspiro[5.5]undecane Chemical compound CC(C)(C)C1=CC(C(C)(C)C)=CC=C1OP1OCC2(COP(OC=3C(=CC(=CC=3)C(C)(C)C)C(C)(C)C)OC2)CO1 AIBRSVLEQRWAEG-UHFFFAOYSA-N 0.000 description 1
- CMJLMPKFQPJDKP-UHFFFAOYSA-N 3-methylthiolane 1,1-dioxide Chemical compound CC1CCS(=O)(=O)C1 CMJLMPKFQPJDKP-UHFFFAOYSA-N 0.000 description 1
- BPTKLSBRRJFNHJ-UHFFFAOYSA-N 4-phenyldiazenylbenzene-1,3-diol Chemical compound OC1=CC(O)=CC=C1N=NC1=CC=CC=C1 BPTKLSBRRJFNHJ-UHFFFAOYSA-N 0.000 description 1
- XCKGFJPFEHHHQA-UHFFFAOYSA-N 5-methyl-2-phenyl-4-phenyldiazenyl-4h-pyrazol-3-one Chemical compound CC1=NN(C=2C=CC=CC=2)C(=O)C1N=NC1=CC=CC=C1 XCKGFJPFEHHHQA-UHFFFAOYSA-N 0.000 description 1
- KHBQMWCZKVMBLN-UHFFFAOYSA-N Benzenesulfonamide Chemical compound NS(=O)(=O)C1=CC=CC=C1 KHBQMWCZKVMBLN-UHFFFAOYSA-N 0.000 description 1
- ZLFVRXUOSPRRKQ-VHEBQXMUSA-N CI Pigment Red 3 Chemical compound [O-][N+](=O)C1=CC(C)=CC=C1\N=N\C1=C(O)C=CC2=CC=CC=C12 ZLFVRXUOSPRRKQ-VHEBQXMUSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 238000005033 Fourier transform infrared spectroscopy Methods 0.000 description 1
- VPWFPZBFBFHIIL-UHFFFAOYSA-L Lithol Rubine Chemical compound OC=1C(=CC2=CC=CC=C2C1N=NC1=C(C=C(C=C1)C)S(=O)(=O)[O-])C(=O)[O-].[Na+].[Na+] VPWFPZBFBFHIIL-UHFFFAOYSA-L 0.000 description 1
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- NRCMAYZCPIVABH-UHFFFAOYSA-N Quinacridone Chemical class N1C2=CC=CC=C2C(=O)C2=C1C=C1C(=O)C3=CC=CC=C3NC1=C2 NRCMAYZCPIVABH-UHFFFAOYSA-N 0.000 description 1
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- GBTNCRZBGFMBGM-UHFFFAOYSA-N copper 2-ethyl-N-(2-ethylhexyl)hexan-1-amine (10Z,29Z)-2,11,20,29,38,40-hexaza-37,39-diazanidanonacyclo[28.6.1.13,10.112,19.121,28.04,9.013,18.022,27.031,36]tetraconta-1,3(40),4(9),5,7,10,12,14,16,19,21(38),22,24,26,29,31,33,35-octadecaene-6,15-disulfonic acid Chemical compound [Cu++].CCCCC(CC)CNCC(CC)CCCC.CCCCC(CC)CNCC(CC)CCCC.OS(=O)(=O)C1=CC2=C3N=C(\N=C4/[N-]C([N-]C5=N\C(=N/C6=N/C(=N\3)/c3ccc(cc63)S(O)(=O)=O)c3ccccc53)c3ccccc43)C2C=C1 GBTNCRZBGFMBGM-UHFFFAOYSA-N 0.000 description 1
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- WNWZKKBGFYKSGA-UHFFFAOYSA-N n-(4-chloro-2,5-dimethoxyphenyl)-2-[[2,5-dimethoxy-4-(phenylsulfamoyl)phenyl]diazenyl]-3-oxobutanamide Chemical compound C1=C(Cl)C(OC)=CC(NC(=O)C(N=NC=2C(=CC(=C(OC)C=2)S(=O)(=O)NC=2C=CC=CC=2)OC)C(C)=O)=C1OC WNWZKKBGFYKSGA-UHFFFAOYSA-N 0.000 description 1
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- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- TVRGPOFMYCMNRB-UHFFFAOYSA-N quinizarine green ss Chemical compound C1=CC(C)=CC=C1NC(C=1C(=O)C2=CC=CC=C2C(=O)C=11)=CC=C1NC1=CC=C(C)C=C1 TVRGPOFMYCMNRB-UHFFFAOYSA-N 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- WPPDXAHGCGPUPK-UHFFFAOYSA-N red 2 Chemical compound C1=CC=CC=C1C(C1=CC=CC=C11)=C(C=2C=3C4=CC=C5C6=CC=C7C8=C(C=9C=CC=CC=9)C9=CC=CC=C9C(C=9C=CC=CC=9)=C8C8=CC=C(C6=C87)C(C=35)=CC=2)C4=C1C1=CC=CC=C1 WPPDXAHGCGPUPK-UHFFFAOYSA-N 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 1
- 229960001755 resorcinol Drugs 0.000 description 1
- 230000002441 reversible effect Effects 0.000 description 1
- RCTGMCJBQGBLKT-PAMTUDGESA-N scarlet red Chemical compound CC1=CC=CC=C1\N=N\C(C=C1C)=CC=C1\N=N\C1=C(O)C=CC2=CC=CC=C12 RCTGMCJBQGBLKT-PAMTUDGESA-N 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000008247 solid mixture Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- YCUVUDODLRLVIC-VPHDGDOJSA-N sudan black b Chemical compound C1=CC(=C23)NC(C)(C)NC2=CC=CC3=C1\N=N\C(C1=CC=CC=C11)=CC=C1\N=N\C1=CC=CC=C1 YCUVUDODLRLVIC-VPHDGDOJSA-N 0.000 description 1
- 229940099373 sudan iii Drugs 0.000 description 1
- NVBFHJWHLNUMCV-UHFFFAOYSA-N sulfamide Chemical class NS(N)(=O)=O NVBFHJWHLNUMCV-UHFFFAOYSA-N 0.000 description 1
- HXJUTPCZVOIRIF-UHFFFAOYSA-N sulfolane Chemical compound O=S1(=O)CCCC1 HXJUTPCZVOIRIF-UHFFFAOYSA-N 0.000 description 1
- 229940124530 sulfonamide Drugs 0.000 description 1
- 150000003456 sulfonamides Chemical class 0.000 description 1
- 150000003457 sulfones Chemical class 0.000 description 1
- 150000003460 sulfonic acids Chemical class 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 150000003672 ureas Chemical class 0.000 description 1
- 150000003673 urethanes Chemical class 0.000 description 1
- JEVGKYBUANQAKG-UHFFFAOYSA-N victoria blue R Chemical compound [Cl-].C12=CC=CC=C2C(=[NH+]CC)C=CC1=C(C=1C=CC(=CC=1)N(C)C)C1=CC=C(N(C)C)C=C1 JEVGKYBUANQAKG-UHFFFAOYSA-N 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 239000001052 yellow pigment Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/34—Hot-melt inks
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
- Ink Jet (AREA)
- Ink Jet Recording Methods And Recording Media Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/641,866 US5932630A (en) | 1996-05-02 | 1996-05-02 | Ink compositions |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE69707551D1 DE69707551D1 (de) | 2001-11-29 |
| DE69707551T2 true DE69707551T2 (de) | 2002-05-16 |
Family
ID=24574191
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE69707551T Expired - Fee Related DE69707551T2 (de) | 1996-05-02 | 1997-05-01 | Tintenzusammensetzungen |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US5932630A (enExample) |
| EP (1) | EP0805192B1 (enExample) |
| JP (1) | JPH1036742A (enExample) |
| DE (1) | DE69707551T2 (enExample) |
Families Citing this family (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62102241A (ja) * | 1985-10-30 | 1987-05-12 | Tokyo Ohka Kogyo Co Ltd | 感光性組成物 |
| US6439709B1 (en) * | 1998-09-04 | 2002-08-27 | Trident International, Inc. | Method for reducing cavitation in impulse ink jet printing device |
| US7030173B2 (en) | 1998-09-04 | 2006-04-18 | Illinois Tool Works, Inc. | High resolution pigment ink for impulse ink jet printing |
| US6688738B2 (en) | 1998-09-04 | 2004-02-10 | Illinois Tool Works Inc | Method for reducing cavitation in impulse ink jet printing devices |
| US6319310B1 (en) | 1999-03-30 | 2001-11-20 | Xerox Corporation | Phase change ink compositions |
| US6789194B1 (en) * | 1999-05-25 | 2004-09-07 | Silverbrook Research Pty Ltd | Network publishing authorization protocol |
| US6221137B1 (en) * | 1999-06-18 | 2001-04-24 | Xerox Corporation | Metal phthalocyanine colorants for phase change inks |
| US6350889B1 (en) | 1999-06-24 | 2002-02-26 | Arizona Chemical Company | Ink jet printing compositions containing ester-terminated dimer acid-based oligo (ester/amide) |
| US6414051B1 (en) * | 2000-02-01 | 2002-07-02 | Xerox Corporation | Acoustic printing inks containing bis(carbamates) |
| US6328792B1 (en) | 2000-02-22 | 2001-12-11 | Xerox Corporation | Ink compositions |
| US6322619B1 (en) | 2000-02-22 | 2001-11-27 | Xerox Corporation | Ink compositions |
| US6492458B1 (en) | 2000-05-16 | 2002-12-10 | Arizona Chemical Company | Polyalkyleneoxydiamine polyamides useful for formulating inks for phase-change jet printing |
| US20020064809A1 (en) * | 2000-11-29 | 2002-05-30 | Mutz Mitchell W. | Focused acoustic ejection cell sorting system and method |
| US6399713B1 (en) | 2001-01-24 | 2002-06-04 | Arizona Chemical Company | Hydrocarbon-terminated polyether-polyamide block copolymers and uses thereof |
| US6870011B2 (en) * | 2001-01-24 | 2005-03-22 | Arizona Chemical Company | Hydrocarbon-terminated polyether-polyamide block copolymers and uses thereof |
| TWI238068B (en) * | 2001-03-06 | 2005-08-21 | Kao Corp | Composition for external application |
| US20030203988A1 (en) * | 2001-03-30 | 2003-10-30 | Eastman Kodak Company | Ink jet printing method |
| US6552160B2 (en) | 2001-05-14 | 2003-04-22 | Arizona Chemical Company | Ester-terminated poly(ester-amides) useful for formulating transparent gels in low polarity fluids |
| US6713529B2 (en) * | 2001-08-10 | 2004-03-30 | Illinois Tool Works, Inc. | Phase-change ink composition |
| US20030050361A1 (en) * | 2001-09-05 | 2003-03-13 | Eastman Kodak Company | Ink jet ink composition |
| US6585816B1 (en) | 2001-11-09 | 2003-07-01 | Xerox Corporation | Phase change inks containing borate esters |
| US6702884B2 (en) | 2001-12-31 | 2004-03-09 | Markem Corporation | Pigmented hot melt inks |
| WO2003102092A1 (en) * | 2002-05-31 | 2003-12-11 | Dainichiseika Color & Chemicals Mfg. Co., Ltd. | Water-based pigment inks, image recording method, and image recording system |
| DE10323178A1 (de) * | 2003-05-22 | 2004-12-09 | Basf Ag | Mischung, umfassend ein Tensid und ein Cotensid |
| DE602006008117D1 (de) * | 2006-05-19 | 2009-09-10 | Agfa Graphics Nv | Stabile, nicht wässrige Tintenstrahldruckfarben |
| DE602006008116D1 (de) * | 2006-05-19 | 2009-09-10 | Agfa Graphics Nv | Stabile nicht-wässrige Tintenstrahldrucktinten |
| US8101231B2 (en) | 2007-12-07 | 2012-01-24 | Cabot Corporation | Processes for forming photovoltaic conductive features from multiple inks |
| KR101318708B1 (ko) * | 2010-12-15 | 2013-10-16 | 에스케이이노베이션 주식회사 | 폴리프로필렌카보네이트를 이용한 로토그라비아 핫멜트 잉크 조성물 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4490731A (en) * | 1982-11-22 | 1984-12-25 | Hewlett-Packard Company | Ink dispenser with "frozen" solid ink |
| US4791439A (en) * | 1986-07-15 | 1988-12-13 | Dataproducts Corporation | Ink jet apparatus with improved reservoir system for handling hot melt ink |
| JPS63246281A (ja) * | 1986-11-01 | 1988-10-13 | Ricoh Co Ltd | 転写記録媒体 |
| US4822674A (en) * | 1987-04-27 | 1989-04-18 | Xerox Corporation | Ink donor films |
| US5041161A (en) * | 1988-02-24 | 1991-08-20 | Dataproducts Corporation | Semi-solid ink jet and method of using same |
| US5122187A (en) * | 1989-06-22 | 1992-06-16 | Xerox Corporation | Hot melt ink compositions |
| US5006170A (en) * | 1989-06-22 | 1991-04-09 | Xerox Corporation | Hot melt ink compositions |
| US5085698A (en) * | 1990-04-11 | 1992-02-04 | E. I. Du Pont De Nemours And Company | Aqueous pigmented inks for ink jet printers |
| US5160369A (en) * | 1991-02-21 | 1992-11-03 | Sri Inc. | Mechanically erasable ballpoint ink |
| EP0556649B1 (en) * | 1992-02-20 | 1999-06-23 | E.I. Du Pont De Nemours & Company Incorporated | Aqueous dispersions containing ABC triblock polymer dispersants |
| US5455326A (en) * | 1994-09-28 | 1995-10-03 | Union Camp Corporation | Ink-jet printing compositions |
-
1996
- 1996-05-02 US US08/641,866 patent/US5932630A/en not_active Expired - Fee Related
-
1997
- 1997-04-24 JP JP9106924A patent/JPH1036742A/ja active Pending
- 1997-05-01 EP EP97302984A patent/EP0805192B1/en not_active Expired - Lifetime
- 1997-05-01 DE DE69707551T patent/DE69707551T2/de not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| EP0805192A3 (en) | 1998-03-18 |
| US5932630A (en) | 1999-08-03 |
| JPH1036742A (ja) | 1998-02-10 |
| EP0805192A2 (en) | 1997-11-05 |
| EP0805192B1 (en) | 2001-10-24 |
| DE69707551D1 (de) | 2001-11-29 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |