DE69505190D1 - Verfahren zur Herstellung von hochreiner Essigsäure - Google Patents

Verfahren zur Herstellung von hochreiner Essigsäure

Info

Publication number
DE69505190D1
DE69505190D1 DE69505190T DE69505190T DE69505190D1 DE 69505190 D1 DE69505190 D1 DE 69505190D1 DE 69505190 T DE69505190 T DE 69505190T DE 69505190 T DE69505190 T DE 69505190T DE 69505190 D1 DE69505190 D1 DE 69505190D1
Authority
DE
Germany
Prior art keywords
production
acetic acid
high purity
purity acetic
acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69505190T
Other languages
English (en)
Other versions
DE69505190T3 (de
DE69505190T2 (de
Inventor
Hiroyuki Miura
Masahiko Shimizu
Takashi Sato
Yoshiaki Morimoto
Masahiro Kagotani
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Daicel Corp
Original Assignee
Daicel Chemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=27527318&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=DE69505190(D1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Priority claimed from JP14965294A external-priority patent/JP3581725B2/ja
Priority claimed from JP15440194A external-priority patent/JP3306227B2/ja
Priority claimed from JP19652494A external-priority patent/JP3244385B2/ja
Application filed by Daicel Chemical Industries Ltd filed Critical Daicel Chemical Industries Ltd
Publication of DE69505190D1 publication Critical patent/DE69505190D1/de
Application granted granted Critical
Publication of DE69505190T2 publication Critical patent/DE69505190T2/de
Publication of DE69505190T3 publication Critical patent/DE69505190T3/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C53/00—Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
    • C07C53/08—Acetic acid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/10—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
    • C07C51/12—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE69505190T 1994-06-15 1995-06-13 Verfahren zur Herstellung von hochreiner Essigsäure Expired - Fee Related DE69505190T3 (de)

Applications Claiming Priority (10)

Application Number Priority Date Filing Date Title
JP13272494 1994-06-15
JP132724/94 1994-06-15
JP137213/94 1994-06-20
JP13721394 1994-06-20
JP14965294A JP3581725B2 (ja) 1994-06-30 1994-06-30 アセトアルデヒドとヨウ化メチルの分離方法
JP149652/94 1994-06-30
JP154401/94 1994-07-06
JP15440194A JP3306227B2 (ja) 1994-07-06 1994-07-06 酢酸および／または無水酢酸の製造法
JP196524/94 1994-08-22
JP19652494A JP3244385B2 (ja) 1994-06-15 1994-08-22 高純度酢酸の製造方法

Publications (3)

Publication Number Publication Date
DE69505190D1 true DE69505190D1 (de) 1998-11-12
DE69505190T2 DE69505190T2 (de) 1999-03-04
DE69505190T3 DE69505190T3 (de) 2007-10-31

Family

ID=27527318

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69505190T Expired - Fee Related DE69505190T3 (de) 1994-06-15 1995-06-13 Verfahren zur Herstellung von hochreiner Essigsäure

Country Status (9)

Country Link
US (1) US5625095A (de)
EP (1) EP0687662B2 (de)
KR (1) KR0169844B1 (de)
CN (1) CN1150155C (de)
AU (1) AU684005B2 (de)
BR (1) BR9502786A (de)
DE (1) DE69505190T3 (de)
MY (1) MY112912A (de)
SG (1) SG44317A1 (de)

Families Citing this family (74)

* Cited by examiner, † Cited by third party
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JP3927237B2 (ja) * 1995-04-27 2007-06-06 ダイセル化学工業株式会社 酢酸の製造法
US6339171B1 (en) 1996-10-18 2002-01-15 Celanese International Corporation Removal or reduction of permanganate reducing compounds and alkyl iodides from a carbonylation process stream
IN192600B (de) * 1996-10-18 2004-05-08 Hoechst Celanese Corp
GB9819079D0 (en) * 1998-09-03 1998-10-28 Bp Chem Int Ltd Carbonylation process
US6552221B1 (en) * 1998-12-18 2003-04-22 Millenium Petrochemicals, Inc. Process control for acetic acid manufacture
US6251256B1 (en) 1999-02-04 2001-06-26 Celanese International Corporation Process for electrochemical oxidation of an aldehyde to an ester
US6303813B1 (en) 1999-08-31 2001-10-16 Celanese International Corporation Rhodium/inorganic iodide catalyst system for methanol carbonylation process with improved impurity profile
US6346645B1 (en) 2000-04-18 2002-02-12 Uop Llc Adsorptive removal of carbonyl impurities from oxygenated organic liquids
US6627770B1 (en) * 2000-08-24 2003-09-30 Celanese International Corporation Method and apparatus for sequesting entrained and volatile catalyst species in a carbonylation process
US6657078B2 (en) 2001-02-07 2003-12-02 Celanese International Corporation Low energy carbonylation process
US6667418B2 (en) 2002-04-16 2003-12-23 Celanese International Corporation Oxidation treatment of a recycle stream in production of acetic acid by methanol carbonylation
US7208624B2 (en) * 2004-03-02 2007-04-24 Celanese International Corporation Process for producing acetic acid
US7271293B2 (en) * 2004-03-02 2007-09-18 Celanese International Corporation Control method for process of removing permanganate reducing compounds from methanol carbonylation process
US7223886B2 (en) 2004-03-02 2007-05-29 Celanese International Corporation Removal of permanganate reducing compounds from methanol carbonylation process stream
US7223883B2 (en) * 2004-03-02 2007-05-29 Celanese International Corporation Removal of permanganate reducing compounds from methanol carbonylation process stream
JP4526381B2 (ja) * 2004-12-27 2010-08-18 ダイセル化学工業株式会社 酢酸の製造方法
US7855306B2 (en) * 2005-04-28 2010-12-21 Celanese International Corporation Process for the production of acetic acid
US20070292486A1 (en) * 2006-06-15 2007-12-20 The Penn State Research Foundation Novel polymer-nano/microparticle composites
US7524988B2 (en) * 2006-08-01 2009-04-28 Lyondell Chemical Technology, L.P. Preparation of acetic acid
US7208625B1 (en) 2006-08-04 2007-04-24 Lyondell Chemical Technology, L.P. Removing permanganate-reducing impurities from acetic acid
US7485749B2 (en) * 2006-08-22 2009-02-03 Lyondell Chemical Technology, L.P. Preparation of acetic acid
JP4995522B2 (ja) * 2006-09-25 2012-08-08 千代田化工建設株式会社 有機酸からのヨウ素化合物除去方法
US8062482B2 (en) * 2007-10-30 2011-11-22 Celanese International Corporation Acetaldehyde removal from methyl acetate by distillation at elevated pressure
CN102177127B (zh) * 2008-08-13 2014-04-09 Amt国际有限公司 从含有相应酯的原料流回收醋酸的方法和装置
WO2011146446A1 (en) 2010-05-18 2011-11-24 Celanese International Corporation Process for purifying acetic acid streams by removing permanganate reducing compounds
EP2628720B1 (de) * 2010-10-06 2018-11-07 Daicel Corporation Verfahren zur herstellung von essigsäure
JP5995853B2 (ja) * 2010-10-13 2016-09-21 セラニーズ・インターナショナル・コーポレーション ハロゲン促進剤を回収し、且つ過マンガン酸塩還元性化合物を除去するためのプロセス
WO2012081418A1 (ja) 2010-12-15 2012-06-21 株式会社ダイセル 酢酸の製造方法
CN104024206A (zh) 2011-12-21 2014-09-03 伊奎斯塔化学有限公司 用于制备乙酸的方法
US9090554B2 (en) 2011-12-21 2015-07-28 Lyondellbasell Acetyls, Llc Process for the manufacture of acetic acid
US9051258B2 (en) 2011-12-21 2015-06-09 Lyondellbasell Acetyls, Llc Process for the manufacture of acetic acid
TWI547477B (zh) 2012-03-14 2016-09-01 大賽璐股份有限公司 醋酸之製造方法
US8969613B2 (en) 2012-10-31 2015-03-03 Lyondellbasell Acetyls, Llc Removal of aldehydes in acetic acid production
MX356188B (es) 2012-12-21 2018-05-16 Daicel Corp Procedimiento para producir acido acetico.
CN104028178B (zh) * 2013-03-06 2016-03-02 中石化上海工程有限公司 强化水力学反应器混合效果的方法
MX363829B (es) 2013-03-15 2019-04-03 Celanese Int Corp Proceso para separar gas de producto usando proceso de carbonilación.
RS59574B1 (sr) 2014-10-02 2019-12-31 Celanese Int Corp Proces za proizvodnju sirćetne kiseline
KR102467611B1 (ko) 2014-11-14 2022-11-16 셀라니즈 인터내셔날 코포레이션 낮은 요오드화에틸 함량을 갖는 반응 매질로부터 아세트산을 제조하기 위한 방법
US9260369B1 (en) * 2014-11-14 2016-02-16 Celanese International Corporation Processes for producing acetic acid product having low butyl acetate content
MY181654A (en) * 2014-11-14 2020-12-31 Celanese Int Corp Processes for improving acetic acid yield by removing iron
US9340481B1 (en) 2014-11-14 2016-05-17 Celanese International Corporation Process for flashing a reaction medium comprising lithium acetate
SG11201703442TA (en) * 2014-11-14 2017-05-30 Celanese Int Corp Process for producing acetic acid by introducing a lithium compound
US9302975B1 (en) 2015-07-01 2016-04-05 Celanese International Corporation Process for flashing a reaction medium
MX2017006295A (es) 2014-11-14 2017-08-21 Celanese Int Corp Procesos para producir acido acetico con control de decantador.
US9540304B2 (en) * 2014-11-14 2017-01-10 Celanese International Corporation Processes for producing an acetic acid product having low butyl acetate content
US9487464B2 (en) 2015-01-30 2016-11-08 Celanese International Corporation Processes for producing acetic acid
US9561994B2 (en) 2015-01-30 2017-02-07 Celanese International Corporation Processes for producing acetic acid
US9540302B2 (en) 2015-04-01 2017-01-10 Celanese International Corporation Processes for producing acetic acid
US9505696B2 (en) 2015-02-04 2016-11-29 Celanese International Corporation Process to control HI concentration in residuum stream
US10413840B2 (en) 2015-02-04 2019-09-17 Celanese International Coporation Process to control HI concentration in residuum stream
US9512056B2 (en) * 2015-02-04 2016-12-06 Celanese International Corporation Process to control HI concentration in residuum stream
US9540303B2 (en) 2015-04-01 2017-01-10 Celanese International Corporation Processes for producing acetic acid
BR112017020974B1 (pt) * 2015-06-01 2020-11-24 Daicel Corporation Processos para separar ou remover um composto redutor de permanganato e para produzir acido acetico
US10428006B2 (en) 2015-09-30 2019-10-01 Daicel Corporation Method and apparatus for producing acetic acid
US9416088B1 (en) 2015-10-02 2016-08-16 Celanese International Corporation Process to produce acetic acid with recycle of water
US9957216B2 (en) 2015-11-13 2018-05-01 Celanese International Corporation Processes for producing acetic acid
US9908835B2 (en) 2015-11-13 2018-03-06 Celanese International Corporation Processes for purifying acetic and hydrating anhydride
US10265639B2 (en) * 2016-07-07 2019-04-23 Daicel Corporation Process for producing acetic acid
US10428003B2 (en) 2017-01-18 2019-10-01 Daicel Corporation Method for producing acetic acid
JP6481040B2 (ja) * 2017-01-18 2019-03-13 株式会社ダイセル 酢酸の製造方法
JP6529592B2 (ja) * 2017-03-08 2019-06-12 株式会社ダイセル 酢酸の製造方法
US10550058B2 (en) 2017-03-08 2020-02-04 Daicel Corporation Method for producing acetic acid
US10428005B2 (en) 2017-03-22 2019-10-01 Daicel Corporation Method for producing acetic acid
MX2019011612A (es) * 2017-03-28 2019-11-18 Daicel Corp Metodo para producir acido acetico.
US10308581B2 (en) 2017-03-28 2019-06-04 Daicel Corporation Method for producing acetic acid
CN107141213A (zh) * 2017-05-24 2017-09-08 北京三聚环保新材料股份有限公司 一种甲醇羰基化合成醋酸的方法
JP6588658B1 (ja) 2018-05-29 2019-10-09 株式会社ダイセル 酢酸の製造方法
EP3594197B1 (de) 2018-05-29 2021-09-29 Daicel Corporation Verfahren zur herstellung von essigsäure
JP6626987B1 (ja) 2018-05-29 2019-12-25 株式会社ダイセル 酢酸の製造方法
WO2019229857A1 (ja) * 2018-05-29 2019-12-05 株式会社ダイセル 酢酸の製造方法
US10807935B2 (en) 2018-11-02 2020-10-20 Celanese International Corporation Process for continuous acetic acid production
US20220185760A1 (en) * 2019-04-01 2022-06-16 Celanese International Corporation Aldehyde removal process for methanol carbonylation
WO2021202270A1 (en) 2020-04-01 2021-10-07 Celanese International Corporation Processes for removing and/or reducing permanganate reducing compounds and alkyl iodides
US20230375478A1 (en) 2022-05-19 2023-11-23 Lyondellbasell Acetyls, Llc Methods for improved control of glacial acetic acid processes

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DE1202778B (de) * 1963-07-13 1965-10-14 Basf Ag Verfahren zur kontinuierlichen Aufarbeitung von Essigsaeure enthaltenden Gemischen
US4102922A (en) † 1974-12-30 1978-07-25 Monsanto Company Purification of carbonylation products
US4008131A (en) * 1975-12-11 1977-02-15 Monsanto Company Purification of acetic acid
US5214203A (en) * 1983-09-02 1993-05-25 Daicel Chemical Industries, Ltd. Process for producing carboxylic acids
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US4615806B1 (en) * 1985-03-07 1994-05-03 Hoechst Co American Removal of iodide compounds from non-aqueous organic media
US4894477A (en) * 1986-10-14 1990-01-16 Hoechst Celanese Corporation Process for regenerating a carbonylation catalyst solution to remove corrosion metals and carbonylation of methanol to acetic acid
US5155265A (en) * 1987-12-23 1992-10-13 Hoechst Celanese Corporation Purification of acetic acid with ozone followed by treatment with activated carbon and/or an ion-exchange resin
AU8790391A (en) * 1990-11-19 1992-05-21 Hoechst Celanese Corporation Removal of carbonyl impurities from a carbonylation process stream
AU639630B2 (en) * 1991-01-28 1993-07-29 Celanese International Corporation Removal of carbonyl impurities from carbonylation process stream
DE4327011A1 (de) * 1993-08-12 1995-02-16 Hoechst Ag Verfahren zur Entfernung von Aldehyden und Acetalen aus technisch hergestellter Essigsäure

Also Published As

Publication number Publication date
EP0687662A3 (de) 1996-03-06
KR960000841A (ko) 1996-01-25
MY112912A (en) 2001-10-31
EP0687662B1 (de) 1998-10-07
CN1126195A (zh) 1996-07-10
SG44317A1 (en) 1997-12-19
AU2051495A (en) 1995-12-21
AU684005B2 (en) 1997-11-27
EP0687662A2 (de) 1995-12-20
BR9502786A (pt) 1996-03-12
EP0687662B2 (de) 2007-02-14
DE69505190T3 (de) 2007-10-31
KR0169844B1 (ko) 1999-03-20
DE69505190T2 (de) 1999-03-04
CN1150155C (zh) 2004-05-19
US5625095A (en) 1997-04-29

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Legal Events

Date Code Title Description
8363 Opposition against the patent
8366 Restricted maintained after opposition proceedings
8339 Ceased/non-payment of the annual fee