DE69220829D1 - Vergasung-Kombikraftwerk - Google Patents

Vergasung-Kombikraftwerk

Info

Publication number
DE69220829D1
DE69220829D1 DE69220829T DE69220829T DE69220829D1 DE 69220829 D1 DE69220829 D1 DE 69220829D1 DE 69220829 T DE69220829 T DE 69220829T DE 69220829 T DE69220829 T DE 69220829T DE 69220829 D1 DE69220829 D1 DE 69220829D1
Authority
DE
Germany
Prior art keywords
power plant
combined cycle
cycle power
gasification combined
gasification
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69220829T
Other languages
English (en)
Other versions
DE69220829T2 (de
Inventor
Horomichi Toda
Takaaki Furuya
Shigeyasu Ishigami
Norihisa Kobayashi
Jun Izumi
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsubishi Heavy Industries Ltd
Original Assignee
Mitsubishi Heavy Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsubishi Heavy Industries Ltd filed Critical Mitsubishi Heavy Industries Ltd
Publication of DE69220829D1 publication Critical patent/DE69220829D1/de
Application granted granted Critical
Publication of DE69220829T2 publication Critical patent/DE69220829T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • B01D53/053—Pressure swing adsorption with storage or buffer vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10J—PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
    • C10J3/00—Production of combustible gases containing carbon monoxide from solid carbonaceous fuels
    • C10J3/72—Other features
    • C10J3/82—Gas withdrawal means
    • C10J3/84—Gas withdrawal means with means for removing dust or tar from the gas
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10K—PURIFYING OR MODIFYING THE CHEMICAL COMPOSITION OF COMBUSTIBLE GASES CONTAINING CARBON MONOXIDE
    • C10K1/00—Purifying combustible gases containing carbon monoxide
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10K—PURIFYING OR MODIFYING THE CHEMICAL COMPOSITION OF COMBUSTIBLE GASES CONTAINING CARBON MONOXIDE
    • C10K1/00—Purifying combustible gases containing carbon monoxide
    • C10K1/002—Removal of contaminants
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10K—PURIFYING OR MODIFYING THE CHEMICAL COMPOSITION OF COMBUSTIBLE GASES CONTAINING CARBON MONOXIDE
    • C10K1/00—Purifying combustible gases containing carbon monoxide
    • C10K1/002—Removal of contaminants
    • C10K1/003—Removal of contaminants of acid contaminants, e.g. acid gas removal
    • C10K1/004—Sulfur containing contaminants, e.g. hydrogen sulfide
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10K—PURIFYING OR MODIFYING THE CHEMICAL COMPOSITION OF COMBUSTIBLE GASES CONTAINING CARBON MONOXIDE
    • C10K1/00—Purifying combustible gases containing carbon monoxide
    • C10K1/02—Dust removal
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F01—MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
    • F01K—STEAM ENGINE PLANTS; STEAM ACCUMULATORS; ENGINE PLANTS NOT OTHERWISE PROVIDED FOR; ENGINES USING SPECIAL WORKING FLUIDS OR CYCLES
    • F01K23/00—Plants characterised by more than one engine delivering power external to the plant, the engines being driven by different fluids
    • F01K23/02—Plants characterised by more than one engine delivering power external to the plant, the engines being driven by different fluids the engine cycles being thermally coupled
    • F01K23/06—Plants characterised by more than one engine delivering power external to the plant, the engines being driven by different fluids the engine cycles being thermally coupled combustion heat from one cycle heating the fluid in another cycle
    • F01K23/067—Plants characterised by more than one engine delivering power external to the plant, the engines being driven by different fluids the engine cycles being thermally coupled combustion heat from one cycle heating the fluid in another cycle the combustion heat coming from a gasification or pyrolysis process, e.g. coal gasification
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F02—COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
    • F02C—GAS-TURBINE PLANTS; AIR INTAKES FOR JET-PROPULSION PLANTS; CONTROLLING FUEL SUPPLY IN AIR-BREATHING JET-PROPULSION PLANTS
    • F02C3/00—Gas-turbine plants characterised by the use of combustion products as the working fluid
    • F02C3/20—Gas-turbine plants characterised by the use of combustion products as the working fluid using a special fuel, oxidant, or dilution fluid to generate the combustion products
    • F02C3/26—Gas-turbine plants characterised by the use of combustion products as the working fluid using a special fuel, oxidant, or dilution fluid to generate the combustion products the fuel or oxidant being solid or pulverulent, e.g. in slurry or suspension
    • F02C3/28—Gas-turbine plants characterised by the use of combustion products as the working fluid using a special fuel, oxidant, or dilution fluid to generate the combustion products the fuel or oxidant being solid or pulverulent, e.g. in slurry or suspension using a separate gas producer for gasifying the fuel before combustion
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/30—Sulfur compounds
    • B01D2257/304—Hydrogen sulfide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/40—Nitrogen compounds
    • B01D2257/406—Ammonia
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/40—Nitrogen compounds
    • B01D2257/408—Cyanides, e.g. hydrogen cyanide (HCH)
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/50—Carbon oxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40003—Methods relating to valve switching
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/404—Further details for adsorption processes and devices using four beds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10J—PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
    • C10J2300/00—Details of gasification processes
    • C10J2300/16—Integration of gasification processes with another plant or parts within the plant
    • C10J2300/164—Integration of gasification processes with another plant or parts within the plant with conversion of synthesis gas
    • C10J2300/1643—Conversion of synthesis gas to energy
    • C10J2300/165—Conversion of synthesis gas to energy integrated with a gas turbine or gas motor
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10J—PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
    • C10J2300/00—Details of gasification processes
    • C10J2300/18—Details of the gasification process, e.g. loops, autothermal operation
    • C10J2300/1846—Partial oxidation, i.e. injection of air or oxygen only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10J—PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
    • C10J2300/00—Details of gasification processes
    • C10J2300/18—Details of the gasification process, e.g. loops, autothermal operation
    • C10J2300/1861—Heat exchange between at least two process streams
    • C10J2300/1884—Heat exchange between at least two process streams with one stream being synthesis gas
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02C—CAPTURE, STORAGE, SEQUESTRATION OR DISPOSAL OF GREENHOUSE GASES [GHG]
    • Y02C20/00—Capture or disposal of greenhouse gases
    • Y02C20/10—Capture or disposal of greenhouse gases of nitrous oxide (N2O)
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E20/00—Combustion technologies with mitigation potential
    • Y02E20/16—Combined cycle power plant [CCPP], or combined cycle gas turbine [CCGT]
    • Y02E20/18—Integrated gasification combined cycle [IGCC], e.g. combined with carbon capture and storage [CCS]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency
    • Y02P20/129—Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • General Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Industrial Gases (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Exhaust Gas Treatment By Means Of Catalyst (AREA)
DE69220829T 1991-04-02 1992-03-26 Vergasung-Kombikraftwerk Expired - Fee Related DE69220829T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP3096396A JPH0593519A (ja) 1991-04-02 1991-04-02 ガス化複合発電プラント

Publications (2)

Publication Number Publication Date
DE69220829D1 true DE69220829D1 (de) 1997-08-21
DE69220829T2 DE69220829T2 (de) 1997-12-18

Family

ID=14163803

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69220829T Expired - Fee Related DE69220829T2 (de) 1991-04-02 1992-03-26 Vergasung-Kombikraftwerk

Country Status (6)

Country Link
US (2) US5313781A (de)
EP (1) EP0507422B1 (de)
JP (1) JPH0593519A (de)
CA (1) CA2063978C (de)
DE (1) DE69220829T2 (de)
ES (1) ES2104816T3 (de)

Families Citing this family (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0593519A (ja) * 1991-04-02 1993-04-16 Mitsubishi Heavy Ind Ltd ガス化複合発電プラント
US5451249A (en) * 1994-06-14 1995-09-19 International Fuel Cells Landfill gas treatment system
US6432368B1 (en) * 1994-06-30 2002-08-13 General Electric Company Staged catalytic ammonia decomposition in integrated gasification combined cycle systems
US5666801A (en) * 1995-09-01 1997-09-16 Rohrer; John W. Combined cycle power plant with integrated CFB devolatilizer and CFB boiler
JP3773302B2 (ja) * 1995-10-03 2006-05-10 株式会社荏原製作所 熱回収システム及び発電システム
US5798250A (en) * 1996-04-15 1998-08-25 Icn Pharmaceuticals, Inc. Facilitating hepatitus virus infection in cell culture using a membrane stressor
US5753198A (en) * 1996-12-30 1998-05-19 General Electric Company Hot coal gas desulfurization
GB9703989D0 (en) * 1997-02-26 1997-04-16 Boc Group Plc Gas separation
GB9703959D0 (en) * 1997-02-26 1997-04-16 Boc Group Plc Air separation
EP0880992B1 (de) * 1997-05-26 2004-12-15 Kabushiki Kaisha Toshiba Entschwefelungsvorrichtung
GB2334094B (en) * 1998-02-05 2002-08-14 Howden Aircontrol Ltd Air environment control systems
CA2274318A1 (en) * 1999-06-10 2000-12-10 Questor Industries Inc. Pressure swing adsorption with axial or centrifugal compression machinery
WO2001034732A2 (en) * 1999-11-12 2001-05-17 Lee Andrew O Refuse derived briquette gasification process and briquetting press
DE10155936A1 (de) * 2001-09-25 2003-05-08 Alstom Switzerland Ltd Verfahren zum Betrieb einer Kraftwerksanlage
EP2252108A3 (de) * 2005-03-28 2016-03-23 Sony Corporation Mobiles Kommunikationssystem, Handover-Steuerungsverfahren, Basisstationskontrollgerät und mobiles Endgerät
US7507276B1 (en) * 2006-02-15 2009-03-24 Wilburn Daniel L Gas treatment system
US7805923B2 (en) * 2006-12-12 2010-10-05 Mitsubishi Heavy Industries, Ltd. Integrated coal gasification combined cycle plant
US7814742B2 (en) * 2006-12-13 2010-10-19 Mitsubishi Heavy Industries, Ltd. Integrated coal gasification combined cycle plant
US7810310B2 (en) * 2006-12-14 2010-10-12 Mitsubishi Heavy Industries, Ltd. Integrated coal gasification combined cycle plant
US20080302106A1 (en) * 2007-06-07 2008-12-11 Econo-Power International Corporation Integration of coal fired steam plants with integrated gasification combined cycle power plants
US20110146282A1 (en) * 2009-12-18 2011-06-23 General Electric Company System and method for reducing sulfur compounds within fuel stream for turbomachine
US8268044B2 (en) * 2010-07-13 2012-09-18 Air Products And Chemicals, Inc. Separation of a sour syngas stream
DE102011002320B3 (de) 2011-04-28 2012-06-21 Knauf Gips Kg Verfahren und Vorrichtung zur Erzeugung von Strom aus schwefelwasserstoffhaltigen Abgasen
JP2020007979A (ja) * 2018-07-09 2020-01-16 一般財団法人電力中央研究所 発電設備
CN108865269A (zh) * 2018-08-06 2018-11-23 许荣根 以生物质为燃料的移动式发电装置
US11549432B2 (en) 2018-09-21 2023-01-10 King Fahd University Of Petroleum And Minerals Integrated chemical looping combustion system and method for power generation and carbon dioxide capture
CN110252111A (zh) * 2019-06-05 2019-09-20 成都易态科技有限公司 烟气净化处理方法
CN115430222A (zh) * 2022-09-05 2022-12-06 徐州燃烧控制研究院有限公司 一种环形仓干式固定床烟气脱硫脱硝装置

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US3974256A (en) * 1974-05-07 1976-08-10 Exxon Research And Engineering Company Sulfide removal process
DE2429993C3 (de) * 1974-06-22 1984-01-05 Krupp-Koppers Gmbh, 4300 Essen Verfahren zum Erzeugen elektrischer Energie
US3986349A (en) * 1975-09-15 1976-10-19 Chevron Research Company Method of power generation via coal gasification and liquid hydrocarbon synthesis
US4238923A (en) * 1979-06-22 1980-12-16 Combustion Engineering, Inc. Method of low temperature heat utilization for atmospheric pressure coal gasification
DE3029187C2 (de) * 1980-08-01 1986-04-17 Bergwerksverband Gmbh, 4300 Essen Verfahren zur Entfernung von Schwefelwasserstoff aus sauerstofffreien oder sauerstoffhaltigen Gasgemischen
DE3414140A1 (de) * 1984-04-14 1985-10-24 M.A.N. Maschinenfabrik Augsburg-Nürnberg AG, 8000 München Verfahren und vorrichtung zum betreiben eines vergasungsreaktors
US4696680A (en) * 1985-10-03 1987-09-29 The United States Of America As Represented By The United States Department Of Energy Method and apparatus for the selective separation of gaseous coal gasification products by pressure swing adsorption
DE3629817A1 (de) * 1986-09-02 1988-03-03 Bergwerksverband Gmbh Verfahren zur verringerung der schadstoffemisionen von kraftwerken mit kombinierten gas-/dampfturbinenprozessen mit vorgeschalteter kohlevergasung
DE3636024A1 (de) * 1986-10-23 1988-05-05 Rheinische Braunkohlenw Ag Kraftwerksprozess mit einer gasturbine
JPH0776348B2 (ja) * 1987-05-26 1995-08-16 財団法人電力中央研究所 高温還元性ガスの精製方法
JPH0593519A (ja) * 1991-04-02 1993-04-16 Mitsubishi Heavy Ind Ltd ガス化複合発電プラント

Also Published As

Publication number Publication date
JPH0593519A (ja) 1993-04-16
EP0507422B1 (de) 1997-07-16
CA2063978A1 (en) 1992-10-03
EP0507422A1 (de) 1992-10-07
US5440873A (en) 1995-08-15
ES2104816T3 (es) 1997-10-16
CA2063978C (en) 1997-03-11
DE69220829T2 (de) 1997-12-18
US5313781A (en) 1994-05-24

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