DE69107526D1 - Chromatographische Trennung von Zirconium-Isotopen mit wasserfreien leicht-recyclierbaren Eluierungsmitteln. - Google Patents

Chromatographische Trennung von Zirconium-Isotopen mit wasserfreien leicht-recyclierbaren Eluierungsmitteln.

Info

Publication number
DE69107526D1
DE69107526D1 DE69107526T DE69107526T DE69107526D1 DE 69107526 D1 DE69107526 D1 DE 69107526D1 DE 69107526 T DE69107526 T DE 69107526T DE 69107526 T DE69107526 T DE 69107526T DE 69107526 D1 DE69107526 D1 DE 69107526D1
Authority
DE
Germany
Prior art keywords
eluents
anhydrous
chromatographic separation
easily recyclable
zirconium isotopes
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69107526T
Other languages
English (en)
Other versions
DE69107526T2 (de
Inventor
Thomas Stephen Snyder
Ernest Dewitt Lee
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Westinghouse Electric Co LLC
Original Assignee
Westinghouse Electric Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Westinghouse Electric Corp filed Critical Westinghouse Electric Corp
Publication of DE69107526D1 publication Critical patent/DE69107526D1/de
Application granted granted Critical
Publication of DE69107526T2 publication Critical patent/DE69107526T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/08—Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/12—Compounds containing phosphorus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1892—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns the sorbent material moving as a whole, e.g. continuous annular chromatography, true moving beds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D59/00—Separation of different isotopes of the same chemical element
    • B01D59/28—Separation by chemical exchange
    • B01D59/30—Separation by chemical exchange by ion exchange
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00—Compounds of zirconium
    • C01G25/003—Preparation involving a liquid-liquid extraction, an adsorption or an ion-exchange
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/50—Conditioning of the sorbent material or stationary liquid
    • G01N30/58—Conditioning of the sorbent material or stationary liquid the sorbent moving as a whole
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/60—Construction of the column
    • G01N30/6052—Construction of the column body
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction
    • B01D15/361—Ion-exchange
    • B01D15/362—Cation-exchange
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/28—Control of physical parameters of the fluid carrier
    • G01N30/34—Control of physical parameters of the fluid carrier of fluid composition, e.g. gradient
    • G01N2030/342—Control of physical parameters of the fluid carrier of fluid composition, e.g. gradient fluid composition fixed during analysis
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/50—Conditioning of the sorbent material or stationary liquid
    • G01N30/58—Conditioning of the sorbent material or stationary liquid the sorbent moving as a whole
    • G01N2030/587—Continuous annular chromatography
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
    • G01N2030/8809—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
    • G01N2030/8809—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample
    • G01N2030/8859—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample inorganic compounds
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/28—Control of physical parameters of the fluid carrier
    • G01N30/34—Control of physical parameters of the fluid carrier of fluid composition, e.g. gradient
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/38—Flow patterns
    • G01N30/44—Flow patterns using recycling of the fraction to be distributed
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/60—Construction of the column
    • G01N30/6004—Construction of the column end pieces
    • G01N30/6017—Fluid distributors
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/60—Construction of the column
    • G01N30/6047—Construction of the column with supporting means; Holders

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Pathology (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Inorganic Chemistry (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Treatment Of Water By Ion Exchange (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
DE69107526T 1990-07-02 1991-06-21 Chromatographische Trennung von Zirconium-Isotopen mit wasserfreien leicht-recyclierbaren Eluierungsmitteln. Expired - Fee Related DE69107526T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US07/546,982 US5023061A (en) 1990-07-02 1990-07-02 Chromatographic separation of zirconium isotopes with anhydrous readily recyclable eluents

Publications (2)

Publication Number Publication Date
DE69107526D1 true DE69107526D1 (de) 1995-03-30
DE69107526T2 DE69107526T2 (de) 1995-12-21

Family

ID=24182848

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69107526T Expired - Fee Related DE69107526T2 (de) 1990-07-02 1991-06-21 Chromatographische Trennung von Zirconium-Isotopen mit wasserfreien leicht-recyclierbaren Eluierungsmitteln.

Country Status (7)

Country Link
US (1) US5023061A (de)
EP (1) EP0464513B1 (de)
JP (1) JP2887333B2 (de)
KR (1) KR100196040B1 (de)
CA (1) CA2045893A1 (de)
DE (1) DE69107526T2 (de)
ES (1) ES2069124T3 (de)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5110474A (en) * 1990-04-09 1992-05-05 Arch Development Corporation Method for liquid chromatographic extraction of strontium from acid solutions
US5174971A (en) * 1990-10-10 1992-12-29 Westinghouse Electric Corp. Continuous anion exchange chromatography for the separation of zirconium isotopes
US5130001A (en) * 1990-12-03 1992-07-14 Westinghouse Electric Corp. Uranium isotope separation by continuous anion exchange chromatography
US5112493A (en) * 1990-12-10 1992-05-12 Westinghouse Electric Corp. Zirconium-hafnium production in a zero liquid discharge process
JP2808065B2 (ja) * 1993-03-29 1998-10-08 三井造船株式会社 円環状クロマトグラフィ装置
US5368736A (en) * 1993-07-26 1994-11-29 The United States Of America As Represented By The United States Department Of Energy Process for the separation and purification of yttrium-90 for medical applications
US5618502A (en) * 1995-07-17 1997-04-08 Westinghouse Electric Corporation Zirconium and hafnium separation in sulfate solutions using continuous ion exchange chromatography
AU713167B2 (en) * 1995-07-17 1999-11-25 Westinghouse Electric Company Llc Zirconium and hafnium separation in chloride solutions using continuous ion exchange chromatography
EP1134581B1 (de) * 2000-03-07 2006-06-07 A.L.P. Technology AG Autoklavierbarer Annularchromatograph
JP4994340B2 (ja) * 2008-09-26 2012-08-08 第一稀元素化学工業株式会社 ジルコニウムとハフニウムの分離方法
CN104368301B (zh) * 2013-08-14 2016-08-17 中国石油化工股份有限公司 一种超重力反应器及反应方法
CN107427741B (zh) * 2015-03-12 2020-04-10 陶氏环球技术有限责任公司 使用聚合大孔亚烷基桥接的树脂对糖进行色谱分离
CN108751544A (zh) * 2018-06-28 2018-11-06 深圳市玖品空气净化科技有限公司 一种具有消毒功能的水处理设备

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2546953A (en) * 1949-11-25 1951-03-27 Jr Kenneth Street Zirconium-hafnium separation process
US2571237A (en) * 1950-10-04 1951-10-16 Robert S Hansen Adsorption separation of zirconium and hafnium
US2759793A (en) * 1951-02-21 1956-08-21 Lister Bryan Alfred Jack Separating hafnium from zirconium
US2753250A (en) * 1953-08-18 1956-07-03 Harley A Wilhelm Solvent extraction of zirconium values
GB800426A (en) * 1954-03-17 1958-08-27 Commissariat Energie Atomique Improvements in methods for separating and purifying zirconium and hafnium
US3960762A (en) * 1971-12-18 1976-06-01 Bayer Aktiengesellschaft Production of absorbents
US3891413A (en) * 1974-06-04 1975-06-24 Robert E Sievers Separation of compounds differing in isotopic composition
US3971842A (en) * 1974-08-08 1976-07-27 Atlantic Richfield Company Continuous displacement chromatographic separation
US4276267A (en) * 1979-10-17 1981-06-30 The United States Of America As Represented By The United States Department Of Energy Hot cell purification of strontium-82, 85 and other isotopes from proton irradiated molybdenum
US4584183A (en) * 1983-12-21 1986-04-22 Westinghouse Electric Corp. Process for separating zirconium isotopes
US4711768A (en) * 1984-08-06 1987-12-08 Westinghouse Electric Corp. Process for the separation of gadolinium isotopes
EP0173484B1 (de) * 1984-08-06 1990-11-28 Westinghouse Electric Corporation Verfahren zur Trennung von Gadoliniumisotopen
US4767513A (en) * 1987-03-10 1988-08-30 Westinghouse Electric Corp. Zirconium isotope separation process

Also Published As

Publication number Publication date
KR920002469A (ko) 1992-02-28
ES2069124T3 (es) 1995-05-01
DE69107526T2 (de) 1995-12-21
KR100196040B1 (ko) 1999-06-15
JPH04227027A (ja) 1992-08-17
JP2887333B2 (ja) 1999-04-26
US5023061A (en) 1991-06-11
EP0464513B1 (de) 1995-02-22
CA2045893A1 (en) 1992-01-03
EP0464513A1 (de) 1992-01-08

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Legal Events

Date Code Title Description
8332 No legal effect for de
8370 Indication related to discontinuation of the patent is to be deleted
8364 No opposition during term of opposition
8327 Change in the person/name/address of the patent owner

Owner name: WESTINGHOUSE ELECTRIC COMPANY LLC, MONROEVILLE, PA

8339 Ceased/non-payment of the annual fee