DE602004002755D1 - Einrichtung zur automatisierten kopplung zwischen einem mikrochromatograph und einem massenspektrometer mit temperatureinstellung - Google Patents

Einrichtung zur automatisierten kopplung zwischen einem mikrochromatograph und einem massenspektrometer mit temperatureinstellung

Info

Publication number
DE602004002755D1
DE602004002755D1 DE602004002755T DE602004002755T DE602004002755D1 DE 602004002755 D1 DE602004002755 D1 DE 602004002755D1 DE 602004002755 T DE602004002755 T DE 602004002755T DE 602004002755 T DE602004002755 T DE 602004002755T DE 602004002755 D1 DE602004002755 D1 DE 602004002755D1
Authority
DE
Germany
Prior art keywords
mass spectrometer
microchromatograph
temperature adjustment
automated coupling
coupling
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE602004002755T
Other languages
English (en)
Other versions
DE602004002755T2 (de
Inventor
Ronan Cozic
Jean-Louis Gass
Jean Bourliaud
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Centre National de la Recherche Scientifique CNRS
Commissariat a lEnergie Atomique et aux Energies Alternatives CEA
Original Assignee
Centre National de la Recherche Scientifique CNRS
Commissariat a lEnergie Atomique CEA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Centre National de la Recherche Scientifique CNRS, Commissariat a lEnergie Atomique CEA filed Critical Centre National de la Recherche Scientifique CNRS
Publication of DE602004002755D1 publication Critical patent/DE602004002755D1/de
Application granted granted Critical
Publication of DE602004002755T2 publication Critical patent/DE602004002755T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/62Detectors specially adapted therefor
    • G01N30/72Mass spectrometers
    • G01N30/7206Mass spectrometers interfaced to gas chromatograph
    • G01N30/7213Mass spectrometers interfaced to gas chromatograph splitting of the gaseous effluent
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/84Preparation of the fraction to be distributed
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J49/00Particle spectrometers or separator tubes
    • H01J49/02Details
    • H01J49/04Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N2030/0075Separation due to differential desorption
    • G01N2030/008Thermal desorption
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/26Conditioning of the fluid carrier; Flow patterns
    • G01N30/28Control of physical parameters of the fluid carrier
    • G01N30/30Control of physical parameters of the fluid carrier of temperature
    • G01N2030/3038Control of physical parameters of the fluid carrier of temperature temperature control of column exit, e.g. of restrictors
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/26Conditioning of the fluid carrier; Flow patterns
    • G01N30/28Control of physical parameters of the fluid carrier
    • G01N30/32Control of physical parameters of the fluid carrier of pressure or speed
    • G01N2030/324Control of physical parameters of the fluid carrier of pressure or speed speed, flow rate

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
  • Investigating Or Analyzing Materials Using Thermal Means (AREA)
DE602004002755T 2003-01-14 2004-01-09 Einrichtung zur automatisierten kopplung zwischen einem mikrochromatograph und einem massenspektrometer mit temperatureinstellung Expired - Lifetime DE602004002755T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR0300343A FR2849924B1 (fr) 2003-01-14 2003-01-14 Dispositif de couplage automatise entre un micro-chromatographe et un spectrometre de masse comprenant un ajustement de temperature
FR0300343 2003-01-14
PCT/FR2004/050010 WO2004065956A1 (fr) 2003-01-14 2004-01-09 Dispositif de couplage automatise entre un micro-chromatographe et un spectrometre de masse comprenant un ajustement de temperature

Publications (2)

Publication Number Publication Date
DE602004002755D1 true DE602004002755D1 (de) 2006-11-23
DE602004002755T2 DE602004002755T2 (de) 2007-08-16

Family

ID=32524891

Family Applications (1)

Application Number Title Priority Date Filing Date
DE602004002755T Expired - Lifetime DE602004002755T2 (de) 2003-01-14 2004-01-09 Einrichtung zur automatisierten kopplung zwischen einem mikrochromatograph und einem massenspektrometer mit temperatureinstellung

Country Status (10)

Country Link
US (1) US7148475B2 (de)
EP (1) EP1583960B1 (de)
JP (1) JP4440252B2 (de)
KR (1) KR20050096933A (de)
AT (1) ATE342503T1 (de)
CA (1) CA2513011A1 (de)
DE (1) DE602004002755T2 (de)
FR (1) FR2849924B1 (de)
IL (1) IL169179A (de)
WO (1) WO2004065956A1 (de)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10319130B3 (de) * 2003-04-28 2004-09-09 Siemens Ag Gaschromatograph mit nachgeordnetem Massenspektrometer und Verfahren zur gaschromatographisch-massenspektrometrischen Analyse eines Stoffgemischs
DE102006015535A1 (de) * 2006-03-31 2007-10-04 Thermo Electron (Bremen) Gmbh Verfahren und Vorrichtung zur Analyse von Isotopenverhältnissen
US7928369B2 (en) 2006-03-31 2011-04-19 Thermo Fisher Scientific (Bremen) Gmbh Device for the analysis of isotope ratios
US7633753B2 (en) * 2007-09-27 2009-12-15 Intel Corporation Piezoelectric air jet augmented cooling for electronic devices
WO2011046875A1 (en) 2009-10-12 2011-04-21 Nadia Pervez Photonic crystal spectrometer
US9360462B2 (en) * 2012-10-26 2016-06-07 Shimadzu Corporation Gas chromatograph mass spectrometer
US20190227039A1 (en) * 2018-01-22 2019-07-25 Waters Technologies Corporation Systems and methods for compressible fluid chromatography

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4501817A (en) * 1981-09-30 1985-02-26 The Ohio State University Method for the analysis of materials by chromatography and mass spectrometry
US4662914A (en) * 1985-03-18 1987-05-05 Hewlett-Packard Company Flow-limited direct GC/MS interface
US4970905A (en) * 1989-05-25 1990-11-20 University Of Utah Apparatus and method for sampling
US4988870A (en) * 1989-10-10 1991-01-29 Und-Sem Foundation Open-split interface for mass spectrometers
US5281397A (en) * 1991-03-14 1994-01-25 General Electric Company Adjustable open-split interface for a gas chromatograph and a mass spectrometer
US5424539A (en) * 1992-12-18 1995-06-13 Finnegan Mat Gmbh Process for the analysis of gaseous components by mass spectrometry
FR2817347B1 (fr) * 2000-11-29 2003-01-03 Commissariat Energie Atomique Dispositif de couplage d'un microchromatographe avec un spectrometre de masse et dispositif d'analyse

Also Published As

Publication number Publication date
FR2849924A1 (fr) 2004-07-16
JP4440252B2 (ja) 2010-03-24
ATE342503T1 (de) 2006-11-15
WO2004065956A1 (fr) 2004-08-05
DE602004002755T2 (de) 2007-08-16
IL169179A (en) 2010-06-30
EP1583960A1 (de) 2005-10-12
US20060097148A1 (en) 2006-05-11
IL169179A0 (en) 2007-07-04
KR20050096933A (ko) 2005-10-06
EP1583960B1 (de) 2006-10-11
US7148475B2 (en) 2006-12-12
JP2006515069A (ja) 2006-05-18
CA2513011A1 (en) 2004-08-05
FR2849924B1 (fr) 2005-02-11

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