DE59905323D1 - METHOD FOR THE PRODUCTION OF METHYLENDI (PHENYLAMINE) AND METHYLENDI (PHENYLISOCYANATE) - Google Patents
METHOD FOR THE PRODUCTION OF METHYLENDI (PHENYLAMINE) AND METHYLENDI (PHENYLISOCYANATE)Info
- Publication number
- DE59905323D1 DE59905323D1 DE59905323T DE59905323T DE59905323D1 DE 59905323 D1 DE59905323 D1 DE 59905323D1 DE 59905323 T DE59905323 T DE 59905323T DE 59905323 T DE59905323 T DE 59905323T DE 59905323 D1 DE59905323 D1 DE 59905323D1
- Authority
- DE
- Germany
- Prior art keywords
- methylendi
- phenylisocyanate
- phenylamine
- production
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/68—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton
- C07C209/78—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton from carbonyl compounds, e.g. from formaldehyde, and amines having amino groups bound to carbon atoms of six-membered aromatic rings, with formation of methylene-diarylamines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Phenolic Resins Or Amino Resins (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19804915A DE19804915A1 (en) | 1998-02-07 | 1998-02-07 | Process for the preparation of methylene di (phenylamine) and methylene di (phenyl isocyanate) |
PCT/EP1999/000472 WO1999040059A1 (en) | 1998-02-07 | 1999-01-26 | Method for the production of methylenedi(phenylamine) and methylenedi(phenyl isocyanate) |
Publications (1)
Publication Number | Publication Date |
---|---|
DE59905323D1 true DE59905323D1 (en) | 2003-06-05 |
Family
ID=7856961
Family Applications (3)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE19804915A Withdrawn DE19804915A1 (en) | 1998-02-07 | 1998-02-07 | Process for the preparation of methylene di (phenylamine) and methylene di (phenyl isocyanate) |
DE59911344T Expired - Lifetime DE59911344D1 (en) | 1998-02-07 | 1999-01-26 | Process for the preparation of methylenedi (phenylamine) and methylenedi (phenyl isocyanate) |
DE59905323T Expired - Lifetime DE59905323D1 (en) | 1998-02-07 | 1999-01-26 | METHOD FOR THE PRODUCTION OF METHYLENDI (PHENYLAMINE) AND METHYLENDI (PHENYLISOCYANATE) |
Family Applications Before (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE19804915A Withdrawn DE19804915A1 (en) | 1998-02-07 | 1998-02-07 | Process for the preparation of methylene di (phenylamine) and methylene di (phenyl isocyanate) |
DE59911344T Expired - Lifetime DE59911344D1 (en) | 1998-02-07 | 1999-01-26 | Process for the preparation of methylenedi (phenylamine) and methylenedi (phenyl isocyanate) |
Country Status (13)
Country | Link |
---|---|
US (3) | US6433219B1 (en) |
EP (2) | EP1270544B1 (en) |
JP (2) | JP4731684B2 (en) |
KR (1) | KR100555814B1 (en) |
CN (2) | CN1151119C (en) |
AU (1) | AU2621799A (en) |
BR (1) | BR9907634A (en) |
CA (1) | CA2320477A1 (en) |
DE (3) | DE19804915A1 (en) |
ES (2) | ES2234969T3 (en) |
MX (1) | MXPA00007646A (en) |
PT (2) | PT1053222E (en) |
WO (1) | WO1999040059A1 (en) |
Families Citing this family (76)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19804915A1 (en) * | 1998-02-07 | 1999-08-12 | Basf Ag | Process for the preparation of methylene di (phenylamine) and methylene di (phenyl isocyanate) |
DE10031540A1 (en) * | 2000-06-28 | 2002-01-10 | Basf Ag | Production of aromatic polyamine mixture comprising 4,4'-methylenedianiline and higher homologs involves reacting aniline with formaldehyde using split stream of formaldehyde |
DE10111337A1 (en) * | 2001-03-08 | 2002-09-12 | Basf Ag | Process for the production of MDI, in particular 2.4'-MDI |
DE10141620A1 (en) | 2001-08-24 | 2003-03-06 | Bayer Ag | Process for the preparation of polyisocyanates of the diphenylmethane series with a reduced color value |
DE10211021A1 (en) | 2002-03-13 | 2003-09-25 | Bayer Ag | Process for the preparation of polyisocyanates of the diphenylmethane series with a reduced color value |
DE10222968A1 (en) * | 2002-05-23 | 2003-12-04 | Basf Ag | Process for the preparation of isocyanates |
DE10238995A1 (en) * | 2002-08-20 | 2004-02-26 | Basf Ag | Production of aromatic di-isocyanate e.g. used in polyurethane production, comprises gas-phase reaction of phosgene with diamine under moderate pressure in reactor with low phosgene hold-up |
DE10260082A1 (en) * | 2002-12-19 | 2004-07-01 | Basf Ag | Process for the continuous production of isocyanates |
DE10260093A1 (en) * | 2002-12-19 | 2004-07-01 | Basf Ag | Process for the separation of isocyanates from a reaction mixture |
DE10331772A1 (en) | 2003-07-11 | 2005-02-03 | Basf Ag | Process for the preparation of diaminodiarylmethanes |
DE10333929A1 (en) * | 2003-07-25 | 2005-02-24 | Bayer Materialscience Ag | Preparation of mixtures of di- and polyisocyanates of the diphenylmethane series with high contents of 4,4'-methylenediphenyl diisocyanate and 2,4'-methylenediphenyl diisocyanate |
DE10347438A1 (en) * | 2003-10-13 | 2005-05-04 | Bayer Materialscience Ag | Process for the preparation of di- and polyamines of the diphenylmethane series |
DE102004005319A1 (en) * | 2004-02-04 | 2005-08-25 | Bayer Materialscience Ag | Process for the preparation of high purity 2,4'-methylene diphenyl diisocyanate |
DE102004032416A1 (en) * | 2004-07-05 | 2006-02-02 | Bayer Materialscience Ag | Process for the preparation of polyamines of the diphenylmethane series at low protonation |
DE102004052370A1 (en) * | 2004-10-28 | 2006-05-04 | Bayer Materialscience Ag | Process for the preparation of di- and polyamines of the diphenylmethane series |
DE102005014244A1 (en) | 2005-03-30 | 2006-10-05 | Bayer Materialscience Ag | Process for the preparation of di- and polyamines of the diphenylmethane series |
DE102005014846A1 (en) * | 2005-03-30 | 2006-10-05 | Basf Ag | MDI production by liquid phase and gas phase phosgenation |
JP2006312619A (en) * | 2005-04-04 | 2006-11-16 | Mitsui Chemicals Polyurethanes Inc | Installation and method for producing polyisocyanate |
JP2012233004A (en) * | 2005-04-04 | 2012-11-29 | Mitsui Chemicals Inc | Equipment and method for producing polyisocyanate |
JP4739798B2 (en) * | 2005-04-05 | 2011-08-03 | 三井化学株式会社 | Polyisocyanate continuous production equipment |
PT1890998E (en) * | 2005-05-30 | 2014-03-06 | Huntsman Int Llc | Process for the preparation of polyisocyanates of the diphenylmethane series |
DE102005055189A1 (en) * | 2005-11-19 | 2007-05-24 | Bayer Materialscience Ag | Process for the preparation of 4,4'-diphenylmethane diisocyanate |
WO2007065767A1 (en) * | 2005-12-08 | 2007-06-14 | Huntsman International Llc | Process for preparing diaminodiphenylmethanes |
DE102006004041A1 (en) * | 2006-01-28 | 2007-08-02 | Bayer Materialscience Ag | Process for the preparation of di- and polyamines of the diphenylmethane series |
DE102006004047A1 (en) * | 2006-01-28 | 2007-08-02 | Bayer Materialscience Ag | Process for the preparation of di- and polyamines of the diphenylmethane series |
MX2009004261A (en) | 2006-10-26 | 2009-05-05 | Basf Se | Process for preparing isocyanates. |
KR101436181B1 (en) * | 2006-11-07 | 2014-09-01 | 바스프 에스이 | Method for the production of isocyanates |
PT2108011E (en) * | 2007-01-08 | 2013-09-06 | Basf Se | Method for the production of diphenylmethane diamine |
KR100888733B1 (en) | 2007-03-28 | 2009-03-17 | 금호미쓰이화학 주식회사 | Manufacturing method of polymethylene polyphenyl polyamine |
CN101279923B (en) * | 2007-04-06 | 2010-08-25 | 宁波万华聚氨酯有限公司 | Preparation of polymethylene polyphenyl polyamine |
EP2014641A3 (en) * | 2007-06-06 | 2009-03-18 | Huntsman International Llc | Process for preparing mixtures of diphenylmethane diisocyanates and polyphenyl polymethylene polyisocyanates |
US8466320B2 (en) | 2007-06-12 | 2013-06-18 | Basf Se | Method for the recovery of mineral acids from saline solutions |
EP2042485A1 (en) | 2007-09-28 | 2009-04-01 | Huntsman International Llc | Process for fractionating a mixture of polyisocyanates |
DE102008012037A1 (en) * | 2008-03-01 | 2009-09-03 | Bayer Materialscience Ag | Process for the preparation of methylene diphenyl diisocyanates |
DE102008015123A1 (en) | 2008-03-20 | 2009-09-24 | Bayer Materialscience Ag | Process for the preparation of di- and polyamines of the diphenylmethane series |
KR20110010752A (en) | 2008-05-26 | 2011-02-07 | 바스프 에스이 | Method for producing diphenylmethane diamine |
JP5416830B2 (en) * | 2009-04-24 | 2014-02-12 | ビーエーエスエフ ソシエタス・ヨーロピア | Method for producing color stable MDA and MDI |
JP5373972B2 (en) * | 2009-09-02 | 2013-12-18 | ハンツマン・インターナショナル・エルエルシー | Method for removing methylene-bridged polyphenyl polyamines from aqueous streams |
BR112012007391B1 (en) | 2009-10-20 | 2018-09-25 | Basf Se | process for preparing diphenylmethane diisocyanate distillation processing |
US8835673B2 (en) | 2009-12-04 | 2014-09-16 | Basf Se | Process for preparing isocyanates |
HUE025009T2 (en) | 2009-12-18 | 2016-04-28 | Basf Se | Two-stage method for cost-effective separation of homogeneous catalysts in mda synthesis |
US20110228630A1 (en) * | 2010-03-16 | 2011-09-22 | Dow Global Technologies, Inc. | Reduced Transit Static Mixer Configuration |
US20110230679A1 (en) * | 2010-03-16 | 2011-09-22 | Dow Global Technologies, Inc. | Reactive Static Mixer |
PT2640694T (en) | 2010-11-17 | 2019-04-29 | Basf Se | Process for preparing methylene diphenyl diisocyanate |
US8907124B2 (en) | 2010-11-17 | 2014-12-09 | Basf Se | Process for preparing methylenedi(phenyl isocyanate) |
HUE026867T2 (en) * | 2010-12-29 | 2016-08-29 | Wanhua Chemical Group Co Ltd | Fast mixing reactor and use thereof |
KR20140037139A (en) | 2011-05-24 | 2014-03-26 | 바스프 에스이 | Process for preparing polyisocyanates from biomass |
US8933262B2 (en) | 2011-05-24 | 2015-01-13 | Basf Se | Process for preparing polyisocyanates from biomass |
CN102516126A (en) * | 2011-11-29 | 2012-06-27 | 广州秀珀化工股份有限公司 | Preparation method of alkyl substitution diphenylmethane diisocyanate |
US20140131275A1 (en) | 2012-11-15 | 2014-05-15 | Bayer Intellectual Property Gmbh | Process for phase separation or extraction and device suitable therefor |
CN105283438B (en) | 2013-04-11 | 2017-12-22 | 科思创德国股份有限公司 | The method for preparing the diamines and polyamines of diphenylmethane series |
PT2984069T (en) | 2013-04-11 | 2018-01-04 | Covestro Deutschland Ag | Method for the preparation of di- and polyamines of the diphenyl methane series |
WO2014173856A1 (en) | 2013-04-24 | 2014-10-30 | Bayer Materialscience Ag | Process for preparation of di- and polyamines from the diphenylmethane series |
RU2017102015A (en) | 2014-06-24 | 2018-07-24 | Ковестро Дойчланд Аг | METHOD FOR PRODUCING CHEMICAL PRODUCTS WITH OPERATIONAL SIMPLICITY |
US10125090B2 (en) | 2014-06-24 | 2018-11-13 | Covestro Deutschland Ag | Process for preparation of di- and polyamines of the diphenylmethane series |
PT3160936T (en) | 2014-06-24 | 2021-12-29 | Covestro Intellectual Property Gmbh & Co Kg | Process for preparation of di- and polyamines of the diphenylmethane series |
PT3160934T (en) * | 2014-06-24 | 2022-04-20 | Covestro Intellectual Property Gmbh & Co Kg | Process for preparation of di- and polyamines of the diphenylmethane series |
CN108291242A (en) | 2015-11-20 | 2018-07-17 | 科思创德国股份有限公司 | The method for preparing aminobenzoic acid or aminobenzoic acid derivative |
HUE048336T2 (en) | 2016-01-20 | 2020-07-28 | Basf Se | Method for producing an aromatic polyamine mixture |
BR112018077149B1 (en) | 2016-06-29 | 2022-10-18 | Covestro Deutschland Ag | PROCESS FOR PRODUCTION OF ANILINE OR OTHER PRODUCTS DERIVED FROM ANILINE |
EP3500553B1 (en) | 2016-08-17 | 2021-05-12 | Covestro Intellectual Property GmbH & Co. KG | Method and device for the production of various chemical products |
WO2018050441A1 (en) * | 2016-09-14 | 2018-03-22 | Basf Se | Method for the hydrogenation of a mixture in the presence of a colourless amine |
EP3558931B1 (en) | 2016-12-20 | 2022-04-20 | Covestro Intellectual Property GmbH & Co. KG | Process for the preparation of aminobenzoic acid or an aminobenzoic acid derivative |
EP3558926B1 (en) | 2016-12-22 | 2021-01-20 | Covestro Intellectual Property GmbH & Co. KG | Method for producing diamines and polyamines of the diphenylmethane series |
WO2018114771A1 (en) | 2016-12-22 | 2018-06-28 | Covestro Deutschland Ag | Method of producing diamines and polyamines of the diphenylmethane series |
US10626078B2 (en) | 2016-12-22 | 2020-04-21 | Covestro Deutschland Ag | Method of producing diamines and polyamines of the diphenylmethane series at different production capacities |
EP3558929B1 (en) | 2016-12-22 | 2021-01-20 | Covestro Intellectual Property GmbH & Co. KG | Process for the preparation of di- and polyamines of the diphenylmethane series for various production capacities |
US11453897B2 (en) | 2018-06-07 | 2022-09-27 | Covestro Intellectual Property Gmbh & Co. Kg | Method for producing aminobenzoic acid or an aminobenzoic acid derivative product |
WO2020020919A1 (en) | 2018-07-27 | 2020-01-30 | Covestro Deutschland Ag | Method for producing aniline or an aniline derivative |
CN110387031B (en) * | 2019-07-12 | 2021-06-29 | 万华化学集团股份有限公司 | Preparation method of light-colored isocyanate |
CN111646927A (en) * | 2020-06-12 | 2020-09-11 | 万华节能科技集团股份有限公司 | Derivative of flame-retardant diphenylmethane diisocyanate and synthetic method thereof |
EP4347553A1 (en) | 2021-06-02 | 2024-04-10 | Covestro Deutschland AG | Process for preparing aniline or an aniline derivative |
WO2023194110A1 (en) | 2022-04-06 | 2023-10-12 | Covestro Deutschland Ag | Method for producing aniline or an aniline-derived product |
CN115124431B (en) * | 2022-06-30 | 2023-08-11 | 万华化学集团股份有限公司 | Preparation method of di-and polyamines of diphenylmethane series with low N-methyl impurity content |
US11542223B1 (en) | 2022-07-21 | 2023-01-03 | Covestro Llc | Process for preparing di- and polyamines of the diphenyl methane series |
EP4345088A1 (en) | 2022-09-29 | 2024-04-03 | Covestro Deutschland AG | A process for preparing di- and polyamines of the diphenyl methane series |
Family Cites Families (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE295291C (en) | ||||
DE238042C (en) | ||||
BE755243Q (en) * | 1965-07-08 | 1971-02-01 | Upjohn Co | ISOCYANATES AND POLYISOCYANATES MANUFACTURING PROCESSES |
GB1298258A (en) * | 1970-08-07 | 1972-11-29 | Ici Ltd | Manufacture of polyamines |
BE794328A (en) * | 1972-01-28 | 1973-07-19 | Ici Ltd | PROCESS FOR THE PRODUCTION OF POLYARYLAMINES WITH METHYLENIC BRIDGE |
DE2426116B2 (en) | 1973-06-01 | 1978-05-11 | Efim Freiburg Biller (Schweiz) | Process for the preparation of polyarylamines having methylene bridges |
US4189354A (en) * | 1976-07-10 | 1980-02-19 | Bayer Aktiengesellschaft | Process for the production of diisocyanatodiphenyl methane isomers with an adjusted content of chlorine compounds |
DE2750975A1 (en) * | 1976-11-19 | 1978-05-24 | Mobay Chemical Corp | PROCESS FOR THE PRODUCTION OF POLYAMINES OF THE DIPHENYLMETHANE SERIES |
DD238042B1 (en) * | 1985-06-05 | 1987-09-30 | Schwarzheide Synthesewerk Veb | METHOD FOR THE CONTINUOUS PREPARATION OF HIGH QUALITY AROMATIC ISOCYANATES |
DD295628A5 (en) | 1986-12-15 | 1991-11-07 | Basf Schwarzheide Gmbh,De | METHOD FOR THE DISCONTINUOUS PREPARATION OF METHYLENDIANILIN / POLYAMINE MIXTURES |
JP2825604B2 (en) | 1990-04-11 | 1998-11-18 | 三井化学株式会社 | Method for producing methylene-bridged polyarylamine |
EP0451422A1 (en) | 1990-04-13 | 1991-10-16 | Merrell Dow Pharmaceuticals Inc. | Pharmaceutically active fluoromethyltyrosine compounds |
DE4021712A1 (en) * | 1990-07-07 | 1992-01-09 | Basf Ag | PROCESS FOR PREPARING MIXTURES OF DIPHENYLMETHANE DIISOCYANATES AND POLYPHENOL POLYMETHYLENE POLYISOCYANATES WITH A REDUCED IODF COLOR NUMBER |
DK0538500T3 (en) * | 1991-10-19 | 1995-04-10 | Basf Corp | Process for Preparing Polymethylene Polyphenylene Polyisocyanates with Reduced Color and Chloride Content |
US5286760A (en) * | 1992-10-09 | 1994-02-15 | Miles, Inc. | Process for reducing impurity levels in methylene diphenyamines |
KR0147558B1 (en) * | 1992-10-23 | 1998-10-15 | 윤종용 | Slider housing locking device of tape recorder |
JP3037065B2 (en) * | 1994-05-26 | 2000-04-24 | 三井化学株式会社 | Method for producing methylene-crosslinked polyphenylene polyisocyanate |
CZ287463B6 (en) * | 1994-11-17 | 2000-12-13 | Bayer Ag | Process for preparing isocyanates |
DE19523851A1 (en) * | 1995-06-30 | 1997-01-02 | Basf Ag | Process for the preparation of mixtures of diphenylmethane diisocyanates and polyphenyl polymethylene polyisocyanates with a reduced iodine color number and a reduced chlorine content |
DE19804915A1 (en) * | 1998-02-07 | 1999-08-12 | Basf Ag | Process for the preparation of methylene di (phenylamine) and methylene di (phenyl isocyanate) |
-
1998
- 1998-02-07 DE DE19804915A patent/DE19804915A1/en not_active Withdrawn
-
1999
- 1999-01-26 US US09/601,097 patent/US6433219B1/en not_active Expired - Lifetime
- 1999-01-26 JP JP2000530491A patent/JP4731684B2/en not_active Expired - Fee Related
- 1999-01-26 DE DE59911344T patent/DE59911344D1/en not_active Expired - Lifetime
- 1999-01-26 KR KR1020007008609A patent/KR100555814B1/en active IP Right Grant
- 1999-01-26 DE DE59905323T patent/DE59905323D1/en not_active Expired - Lifetime
- 1999-01-26 PT PT99906202T patent/PT1053222E/en unknown
- 1999-01-26 ES ES02022029T patent/ES2234969T3/en not_active Expired - Lifetime
- 1999-01-26 AU AU26217/99A patent/AU2621799A/en not_active Abandoned
- 1999-01-26 EP EP02022029A patent/EP1270544B1/en not_active Expired - Lifetime
- 1999-01-26 EP EP99906202A patent/EP1053222B1/en not_active Expired - Lifetime
- 1999-01-26 ES ES99906202T patent/ES2198894T3/en not_active Expired - Lifetime
- 1999-01-26 CN CNB998027669A patent/CN1151119C/en not_active Expired - Lifetime
- 1999-01-26 PT PT02022029T patent/PT1270544E/en unknown
- 1999-01-26 BR BR9907634-9A patent/BR9907634A/en not_active Application Discontinuation
- 1999-01-26 CN CNB2004100317075A patent/CN1266124C/en not_active Expired - Lifetime
- 1999-01-26 WO PCT/EP1999/000472 patent/WO1999040059A1/en active IP Right Grant
- 1999-01-26 CA CA002320477A patent/CA2320477A1/en not_active Abandoned
-
2000
- 2000-08-04 MX MXPA00007646 patent/MXPA00007646A/en unknown
-
2002
- 2002-05-21 US US10/152,489 patent/US6831192B2/en not_active Expired - Lifetime
-
2004
- 2004-05-11 US US10/843,046 patent/US7230130B2/en not_active Expired - Lifetime
-
2010
- 2010-08-04 JP JP2010175044A patent/JP5449082B2/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
JP5449082B2 (en) | 2014-03-19 |
EP1270544A1 (en) | 2003-01-02 |
JP4731684B2 (en) | 2011-07-27 |
JP2010270147A (en) | 2010-12-02 |
CN1290245A (en) | 2001-04-04 |
ES2198894T3 (en) | 2004-02-01 |
EP1270544B1 (en) | 2004-12-22 |
CN1151119C (en) | 2004-05-26 |
DE59911344D1 (en) | 2005-01-27 |
EP1053222A1 (en) | 2000-11-22 |
PT1270544E (en) | 2005-05-31 |
KR100555814B1 (en) | 2006-03-03 |
DE19804915A1 (en) | 1999-08-12 |
CA2320477A1 (en) | 1999-08-12 |
US20020132953A1 (en) | 2002-09-19 |
US6831192B2 (en) | 2004-12-14 |
EP1053222B1 (en) | 2003-05-02 |
AU2621799A (en) | 1999-08-23 |
US7230130B2 (en) | 2007-06-12 |
CN1532189A (en) | 2004-09-29 |
ES2234969T3 (en) | 2005-07-01 |
PT1053222E (en) | 2003-09-30 |
WO1999040059A1 (en) | 1999-08-12 |
JP2002502838A (en) | 2002-01-29 |
US20050014975A1 (en) | 2005-01-20 |
CN1266124C (en) | 2006-07-26 |
US6433219B1 (en) | 2002-08-13 |
MXPA00007646A (en) | 2001-04-01 |
BR9907634A (en) | 2000-11-14 |
KR20010040725A (en) | 2001-05-15 |
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