DE59503295D1 - Production of high-purity metal powder from metal alkoxides - Google Patents

Production of high-purity metal powder from metal alkoxides

Info

Publication number
DE59503295D1
DE59503295D1 DE59503295T DE59503295T DE59503295D1 DE 59503295 D1 DE59503295 D1 DE 59503295D1 DE 59503295 T DE59503295 T DE 59503295T DE 59503295 T DE59503295 T DE 59503295T DE 59503295 D1 DE59503295 D1 DE 59503295D1
Authority
DE
Germany
Prior art keywords
pref
alkoxide
methoxide
ethoxide
production
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE59503295T
Other languages
German (de)
Inventor
D- Koeln Dr Schloh
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HC Starck GmbH
Original Assignee
HC Starck GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by HC Starck GmbH filed Critical HC Starck GmbH
Application granted granted Critical
Publication of DE59503295D1 publication Critical patent/DE59503295D1/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00—Obtaining refractory metals
    • C22B34/20—Obtaining niobium, tantalum or vanadium
    • C22B34/24—Obtaining niobium or tantalum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/16—Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
    • B22F9/28—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from gaseous metal compounds
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00—Obtaining refractory metals
    • C22B34/30—Obtaining chromium, molybdenum or tungsten
    • C22B34/36—Obtaining tungsten
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B5/00—General methods of reducing to metals
    • C22B5/02—Dry methods smelting of sulfides or formation of mattes
    • C22B5/12—Dry methods smelting of sulfides or formation of mattes by gases
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2201/00—Treatment under specific atmosphere
    • B22F2201/01—Reducing atmosphere
    • B22F2201/013—Hydrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2203/00—Controlling
    • B22F2203/11—Controlling temperature, temperature profile

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Manufacturing & Machinery (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Prodn. of high purity metal powder is effected by reaction of volatile alkoxide cpd(s). with a redn. gas, pref. H2 opt. diluted with an inert carrier gas selected from the noble gases, pref. Ar. Pref. the metal alkoxide is an alkoxide of a gp. 3-14 element (IUPAC 1985) and reaction is carried out at 400-1400 (pref. 600-1200) degrees C. The alkoxide is pref. selected from chromium tert.-butoxide, niobium methoxide, niobium ethoxide, tantalum methoxide, tantalum ethoxide, tungsten methoxide and tungsten ethoxide.
DE59503295T 1994-02-15 1995-02-02 Production of high-purity metal powder from metal alkoxides Expired - Fee Related DE59503295D1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE4404747A DE4404747C2 (en) 1994-02-15 1994-02-15 Production of pure metal powder from metal alkoxides

Publications (1)

Publication Number Publication Date
DE59503295D1 true DE59503295D1 (en) 1998-10-01

Family

ID=6510268

Family Applications (2)

Application Number Title Priority Date Filing Date
DE4404747A Expired - Fee Related DE4404747C2 (en) 1994-02-15 1994-02-15 Production of pure metal powder from metal alkoxides
DE59503295T Expired - Fee Related DE59503295D1 (en) 1994-02-15 1995-02-02 Production of high-purity metal powder from metal alkoxides

Family Applications Before (1)

Application Number Title Priority Date Filing Date
DE4404747A Expired - Fee Related DE4404747C2 (en) 1994-02-15 1994-02-15 Production of pure metal powder from metal alkoxides

Country Status (11)

Country Link
US (1) US5711783A (en)
EP (1) EP0667200B1 (en)
JP (1) JPH07252511A (en)
KR (1) KR950031331A (en)
CN (1) CN1112467A (en)
AT (1) ATE170116T1 (en)
CA (1) CA2142254A1 (en)
DE (2) DE4404747C2 (en)
IL (1) IL112620A (en)
RU (1) RU2126735C1 (en)
TW (1) TW257706B (en)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6100415A (en) * 1998-03-16 2000-08-08 Japan Pionics Co., Ltd. Purified alkoxide and process for purifying crude alkoxide
WO2000067936A1 (en) * 1998-05-06 2000-11-16 H.C. Starck, Inc. Metal powders produced by the reduction of the oxides with gaseous magnesium
US5997612A (en) * 1998-07-24 1999-12-07 The Boc Group, Inc. Pressure swing adsorption process and apparatus
US6375704B1 (en) * 1999-05-12 2002-04-23 Cabot Corporation High capacitance niobium powders and electrolytic capacitor anodes
DE10231777A1 (en) * 2002-07-13 2004-02-05 Diehl Munitionssysteme Gmbh & Co. Kg Production of a tungsten base material for hollow charges, fragments and/or penetrators comprises removing interstitial impurities from the base material
US7187396B2 (en) 2003-11-07 2007-03-06 Engelhard Corporation Low visibility laser marking additive
KR20070083557A (en) 2004-09-23 2007-08-24 엘리먼트 씩스 (프티) 리미티드 Polycrystalline abrasive materials and method of manufacture
US7399335B2 (en) * 2005-03-22 2008-07-15 H.C. Starck Inc. Method of preparing primary refractory metal
US7758668B1 (en) 2006-04-18 2010-07-20 Chemnano, Inc. Process of manufacturing metallic nano-scale powders
WO2014008410A1 (en) * 2012-07-03 2014-01-09 Ceramatec, Inc. Apparatus and method of producing metal in a nasicon electrolytic cell
CN109396456B (en) * 2018-12-28 2024-02-13 西安赛隆金属材料有限责任公司 Preparation device and method of spherical tungsten powder

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3117833A (en) * 1958-09-25 1964-01-14 Fansteel Metallurgical Corp Process of purifying and separating columbium and tantalum values from each other
US3640093A (en) * 1969-03-10 1972-02-08 Owens Illinois Inc Process of converting metalorganic compounds and high purity products obtained therefrom
GB1307581A (en) * 1970-05-05 1973-02-21 Monsanto Chemicals Production of alkoxides
EP0197271B1 (en) * 1985-03-04 1989-04-19 Kabushiki Kaisha Toshiba Methods for preparing high-purity molybdenum or tungsten powder and high-purity oxides powder of the same
US4582696A (en) * 1985-04-15 1986-04-15 Ford Motor Company Method of making a special purity silicon nitride powder
US4615736A (en) * 1985-05-01 1986-10-07 Allied Corporation Preparation of metal powders
US4755369A (en) * 1985-05-22 1988-07-05 Research Development Corporation Of Japan Production of ultrafine particles
JPS61275108A (en) * 1985-05-30 1986-12-05 Mitsubishi Mining & Cement Co Ltd Preparation of powder of dielectric substance
JPS63184306A (en) * 1986-09-22 1988-07-29 Mitsui Toatsu Chem Inc Stabilization of ferromagnetic metal powder
JPH0230706A (en) * 1988-07-19 1990-02-01 Central Glass Co Ltd Manufacture of beta-tungsten powder

Also Published As

Publication number Publication date
EP0667200A1 (en) 1995-08-16
IL112620A0 (en) 1995-05-26
CN1112467A (en) 1995-11-29
IL112620A (en) 1997-09-30
RU2126735C1 (en) 1999-02-27
EP0667200B1 (en) 1998-08-26
ATE170116T1 (en) 1998-09-15
CA2142254A1 (en) 1995-08-16
KR950031331A (en) 1995-12-18
RU95101844A (en) 1997-03-10
JPH07252511A (en) 1995-10-03
US5711783A (en) 1998-01-27
TW257706B (en) 1995-09-21
DE4404747C2 (en) 1995-12-14
DE4404747A1 (en) 1995-08-17

Similar Documents

Publication Publication Date Title
DE59503295D1 (en) Production of high-purity metal powder from metal alkoxides
MXPA03005998A (en) Epoxidation catalyst and process.
DK0411153T3 (en)
GR3026433T3 (en) Semi-synthesis of taxane derivatives using metal alkoxides and oxazinones
MY104627A (en) A 1-pyridylimidazole derivative and its production and use.
CA2074533A1 (en) 2-nitroimidazole derivative, production thereof, and radiosensitizer containing the same as active ingredient
HU905850D0 (en) Insecticide preparatives containing n-phenyl-pyrazole derivatives as active substance and process for producing the active substance
ZA93267B (en) Novel arylcyloakyl derivatives their production and their use
DK1225175T3 (en) Intermediate for the synthesis of D-chiro-3-inosose and (+) - D-chiro-inositol
SE0102214D0 (en) Process for making a single-phase composition comprising metal
AU559132B2 (en) Heterocyclic substituted sulphonyl ureas
DE69000819D1 (en) REDUCTION OF NITROSAMINE FORMATION.
AU3922097A (en) Azabicyclo (3.2.0) heptane derivatives
WO1993018166A3 (en) PRODUCTION OF $i(ASPERGILLUS NIGER CATALASE-R)
AU600054B2 (en) 2,5,6,7-tetranor-18,18,19,19-tetradehydro-4,8-inter-m- phenylene pgi2 derivatives
DK0924968T3 (en) Gas mixture for plasma spraying and use of this mixture for plasma spraying of refractory materials
ATE211582T1 (en) MAGNETRON
AU3287493A (en) Use of a chemically-stabilised chlorite matrix for the parenteral treatment of HIV infections
CA2141209A1 (en) Novel pyridyl- and pyrimidylpiperazine derivatives
AU3814800A (en) Enantiomers of mercapto lactones and processes for their synthesis
NO921097D0 (en) 4-SUBSTITUTED AZETIDINONES, AND PROCEDURES FOR PREPARING THEM
DK0444280T3 (en) Process for producing physiologically compatible oxide layers on bone implants
ES451752A1 (en) 4-Hydroxymethyl-2-pyrrolidinones
AU8295591A (en) Synthesis of carminic acid and principal intermediates
JPS6419069A (en) Production of polyhalogenoquinoline derivative

Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8327 Change in the person/name/address of the patent owner

Owner name: H.C. STARCK GMBH, 38642 GOSLAR, DE

8339 Ceased/non-payment of the annual fee