DE3462923D1 - Granular detergents with a low phosphate content, and method for their preparation - Google Patents
Granular detergents with a low phosphate content, and method for their preparationInfo
- Publication number
- DE3462923D1 DE3462923D1 DE8484401588T DE3462923T DE3462923D1 DE 3462923 D1 DE3462923 D1 DE 3462923D1 DE 8484401588 T DE8484401588 T DE 8484401588T DE 3462923 T DE3462923 T DE 3462923T DE 3462923 D1 DE3462923 D1 DE 3462923D1
- Authority
- DE
- Germany
- Prior art keywords
- degrees
- weight
- surface active
- ionic surface
- sodium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title abstract 4
- 229910019142 PO4 Inorganic materials 0.000 title abstract 2
- 239000003599 detergent Substances 0.000 title abstract 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 title abstract 2
- 239000010452 phosphate Substances 0.000 title abstract 2
- 235000019832 sodium triphosphate Nutrition 0.000 abstract 3
- 239000004094 surface-active agent Substances 0.000 abstract 3
- 239000007900 aqueous suspension Substances 0.000 abstract 2
- 239000000470 constituent Substances 0.000 abstract 2
- 238000005054 agglomeration Methods 0.000 abstract 1
- 230000002776 aggregation Effects 0.000 abstract 1
- 238000000889 atomisation Methods 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 239000008187 granular material Substances 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 238000010298 pulverizing process Methods 0.000 abstract 1
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 abstract 1
- 229940048086 sodium pyrophosphate Drugs 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 239000000725 suspension Substances 0.000 abstract 1
- 235000019818 tetrasodium diphosphate Nutrition 0.000 abstract 1
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 abstract 1
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0039—Coated compositions or coated components in the compositions, (micro)capsules
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/02—Preparation in the form of powder by spray drying
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
1. A method of preparing granular detergents with a low phosphate content, that is with a content of between 10% and 25% of sodium tripolyphosphate and a combined content of sodium orthophosphate and of sodium pyrophosphate of less than about 2% by weight and preferably less than about 1% by weight, and containing non-ionic surface active agents amounting to about 10% by weight of the whole composition, the method comprising forming an essentially hot aqueous suspension with thermostable constituents, drying the suspension in an atomising tower, mixing the atomised base with sodium tripolyphosphate and the other thermosensitive constituents, and then agglomerating the solid components by pulverisation with the assistance of a non-ionic surface active agent until there are obtained essentially homogeneous granules with little tendency to glutination, and the method being characterised in that the whole of the sodium tripolyphosphate is not subjected to the phases of hot aqueous suspension or atomisation, and in that, during the agglomeration phase, the temperature of the non-ionic surface active agent is between 25 degrees C and 80 degrees C, and preferably between 50 degrees C and 70 degrees C.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR8315306A FR2552446B1 (en) | 1983-09-27 | 1983-09-27 | GRANULAR DETERGENTS WITH LOW PHOSPHATE CONTENT, AND PROCESS FOR PRODUCING THE SAME |
Publications (1)
Publication Number | Publication Date |
---|---|
DE3462923D1 true DE3462923D1 (en) | 1987-05-07 |
Family
ID=9292560
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE8484401588T Expired DE3462923D1 (en) | 1983-09-27 | 1984-07-27 | Granular detergents with a low phosphate content, and method for their preparation |
DE198484401588T Pending DE139547T1 (en) | 1983-09-27 | 1984-07-27 | GRANULATED CLEANING AGENTS WITH LOW PHOSPHATE CONTENT AND METHOD FOR THE PRODUCTION THEREOF. |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE198484401588T Pending DE139547T1 (en) | 1983-09-27 | 1984-07-27 | GRANULATED CLEANING AGENTS WITH LOW PHOSPHATE CONTENT AND METHOD FOR THE PRODUCTION THEREOF. |
Country Status (5)
Country | Link |
---|---|
EP (1) | EP0139547B1 (en) |
AT (1) | ATE26300T1 (en) |
DE (2) | DE3462923D1 (en) |
ES (1) | ES534997A0 (en) |
FR (1) | FR2552446B1 (en) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2617183B2 (en) * | 1983-09-27 | 1990-01-05 | Camp Sa | IMPROVEMENTS IN THE PROCESS FOR OBTAINING GRANULAR DETERGENTS WITH A LOW PHOSPHATE CONTENT |
CA1297376C (en) * | 1985-11-01 | 1992-03-17 | David Philip Jones | Detergent compositions, components therefor, and processes for theirpreparation |
US4762636A (en) * | 1986-02-28 | 1988-08-09 | Ciba-Geigy Corporation | Process for the preparation of granules containing an active substance and to the use thereof as speckles for treating substrates |
US5565422A (en) * | 1995-06-23 | 1996-10-15 | The Procter & Gamble Company | Process for preparing a free-flowing particulate detergent composition having improved solubility |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1107870B (en) * | 1959-01-22 | 1961-05-31 | Budenheim Rud A Oetker Chemie | Process for the production of non-dusting washing, cleaning, rinsing and degreasing agents |
US3849327A (en) * | 1971-11-30 | 1974-11-19 | Colgate Palmolive Co | Manufacture of free-flowing particulate heavy duty synthetic detergent composition containing nonionic detergent and anti-redeposition agent |
US4006110A (en) * | 1971-11-30 | 1977-02-01 | Colgate-Palmolive Company | Manufacture of free-flowing particulate heavy duty synthetic detergent composition |
US4136051A (en) * | 1974-02-25 | 1979-01-23 | Henkel Kommanditgesellschaft Auf Aktien (Henkel Kgaa) | Pourable washing compositions containing a luminosilicates and non-ionics and method for their preparation |
ATE3056T1 (en) * | 1978-10-03 | 1983-04-15 | Unilever Nv | DETERGENT COMPOSITIONS. |
NZ191691A (en) * | 1978-10-03 | 1982-02-23 | Unilever Ltd | Preparation of particulate alkaline detergent compositions by spray drying |
-
1983
- 1983-09-27 FR FR8315306A patent/FR2552446B1/en not_active Expired
-
1984
- 1984-07-27 EP EP84401588A patent/EP0139547B1/en not_active Expired
- 1984-07-27 AT AT84401588T patent/ATE26300T1/en not_active IP Right Cessation
- 1984-07-27 DE DE8484401588T patent/DE3462923D1/en not_active Expired
- 1984-07-27 DE DE198484401588T patent/DE139547T1/en active Pending
- 1984-08-09 ES ES534997A patent/ES534997A0/en active Granted
Also Published As
Publication number | Publication date |
---|---|
ES8504921A1 (en) | 1985-04-16 |
EP0139547A1 (en) | 1985-05-02 |
ATE26300T1 (en) | 1987-04-15 |
FR2552446A1 (en) | 1985-03-29 |
DE139547T1 (en) | 1985-08-29 |
FR2552446B1 (en) | 1985-12-20 |
EP0139547B1 (en) | 1987-04-01 |
ES534997A0 (en) | 1985-04-16 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8363 | Opposition against the patent | ||
8331 | Complete revocation |